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Optimization and control of gaseous nitriding of a 33CrMoV12-9 steel 33CrMoV12-9 钢气体氮化的优化与控制
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-04-01 DOI: 10.1515/mt-2023-0275
M. Aggoune, L. Torchane
This work propose a new experimental methodology to optimize the gaseous nitriding process of 33CrMoV12-9 steel grade, widely used in the mechanical industry for the fabrication of gears, pinions, and bearings. Several nitriding experiments were conducted at a temperature of 520 °C in the interval between 4 and 55 h using both constant and variable nitriding potential K N . The obtained results allowed us to determine the optimal conditions and to propose a sequenced cycle consisting of three steps. Multiple characterizations using X-ray diffraction (XRD), optical microscopy (OM), Vickers microhardness testing (HV), and electron probe microanalysis (EPMA) indicate a surface hardness of 810 HV0.5, nitrogen diffusion depth of approximately 0.7 mm. finally, a metallurgical structure devoid of complex networks of nitrides and carbonitrides. The validation results confirmed the effectiveness of the proposed methodology, thereby paving the way for improving the nitriding process in the mechanical industry. This work represents a significant contribution to the optimization of thermochemical treatments for materials used in demanding environments.
33CrMoV12-9 钢种广泛应用于机械行业的齿轮、小齿轮和轴承制造,本研究提出了一种优化 33CrMoV12-9 钢种气体渗氮工艺的新实验方法。在温度为 520 °C 的条件下,使用恒定和可变氮化电位 K N 在 4 至 55 小时之间进行了多次氮化实验。根据实验结果,我们确定了最佳条件,并提出了由三个步骤组成的有序循环。使用 X 射线衍射 (XRD)、光学显微镜 (OM)、维氏显微硬度测试 (HV) 和电子探针显微分析 (EPMA) 进行的多种表征表明,表面硬度为 810 HV0.5,氮扩散深度约为 0.7 毫米,最后,冶金结构中没有复杂的氮化物和碳氮化物网络。验证结果证实了所提方法的有效性,从而为改进机械行业的氮化工艺铺平了道路。这项工作为优化在苛刻环境中使用的材料的热化学处理做出了重大贡献。
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引用次数: 0
Experimental Investigation on Mechanical properties of CF15PET and GF30PP materials produced with different raster angles 不同光栅角度生产的 CF15PET 和 GF30PP 材料机械性能的实验研究
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-22 DOI: 10.1515/mt-2023-0226
Mehmet Kopar, Mehmet Umut Erdaş, Ali Rıza Yıldız
In recent years, additive manufacturing (AM) technologies have been used in many industries, such as automotive, defense, space, and aviation. Depending on the development of this technology, the effect of the relationship between many parameters, such as raster angles, production speed, and melting temperature used during the production of materials, has been an important issue in the mechanical properties of materials. In this study, the effects of ±45° and 0–90° raster angles used during the production of 15 % short carbon fiber reinforced polyethylenetereflatate (CF15PET) and 30 % short glass fiber reinforced polypropylene (GF30PP) materials on the mechanical properties of the materials were investigated. As a result of the study, it was determined that different raster angles affect the mechanical properties of both materials.
近年来,增材制造(AM)技术已在汽车、国防、航天和航空等许多行业得到应用。随着该技术的发展,材料生产过程中使用的光栅角度、生产速度和熔化温度等许多参数之间的关系对材料力学性能的影响已成为一个重要问题。在本研究中,研究了在生产 15% 短碳纤维增强聚对苯二甲酸乙二酯(CF15PET)和 30% 短玻璃纤维增强聚丙烯(GF30PP)材料过程中使用的 ±45° 和 0-90° 光栅角对材料机械性能的影响。研究结果表明,不同的光栅角度会影响两种材料的机械性能。
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引用次数: 0
Hybrid effect on tensile, flexural, and quasi-static punch shear behavior of jute/ramie and jute/flax reinforced hybrid composites 混合效应对黄麻/拉米和黄麻/亚麻增强混合复合材料的拉伸、弯曲和准静态冲剪行为的影响
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.1515/mt-2023-0383
Özlem Keleş, Serkan Bati, Y. H. Çelik
The high specific properties and environmental durability of synthetic fibers make them a popular choice for reinforcing lightweight composites. Unfortunately, they are often limited by their poor biodegradability and high cost. Nevertheless, natural fibers are critical in industrial applications due to their environmental and economic benefits. This study investigated the tensile and flexural behavior of natural hybrid jute/ramie and jute/flax composites with different stacking sequences. A quasi-static punch shear test was also performed to understand their deformation behavior. Jute, ramie, and flax composites have also been fabricated for comparison. Tensile and flexural tests showed a positive hybrid effect in some samples, whereas flax–jute hybrid composites in two different stacking sequences exhibited a synergistic effect. While a maximum improvement of 37.99 % was achieved in the tensile test, this rate was 64.81 % in the flexural test with these hybrid composites. According to punch shear experiments, punch geometry and stacking sequence considerably impact punch shear strength, energy absorption capacity, and deformation.
合成纤维具有较高的特定性能和环境耐久性,因此成为增强轻质复合材料的热门选择。遗憾的是,它们往往受到生物降解性差和成本高昂的限制。尽管如此,天然纤维因其环境和经济效益,在工业应用中仍然至关重要。本研究调查了不同堆叠顺序的天然混合黄麻/拉米和黄麻/亚麻复合材料的拉伸和弯曲行为。为了了解它们的变形行为,还进行了准静态冲剪试验。此外,还制作了黄麻、苎麻和亚麻复合材料进行比较。拉伸和弯曲测试表明,一些样品具有积极的混合效应,而采用两种不同堆叠顺序的亚麻-黄麻混合复合材料则表现出协同效应。这些混合复合材料在拉伸试验中的最大改进率为 37.99%,而在弯曲试验中的改进率为 64.81%。根据冲压剪切实验,冲压几何形状和堆叠顺序对冲压剪切强度、能量吸收能力和变形有很大影响。
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引用次数: 0
Design optimization of bellow joints used in liquid propellant rocket engines 液体推进剂火箭发动机所用波纹管接头的优化设计
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-19 DOI: 10.1515/mt-2023-0377
E. Acar, Oğulcan Öztürkler
Bellow joints are frequently used in hydraulic lines, constructions, and various areas such as nuclear stations to absorb the energy caused by flow and external forces, provide flexibility to the lines, and prevent damages such as cracking and deterioration in the flow lines. There exist various types of bellow joints (e.g., axial type, gimbal type, and hinge type) that allow axial, lateral, and angular movements. Bellow joints that assist thrust vector control in liquid propellant rocket engines prevent the hydraulic lines from being damaged during the orientation movements of the missile. While providing this flexibility to the lines in rocket engines, they create additional force against the linear actuators that move the liquid motor nozzle. This additional force causes the need for larger actuators, resulting in more weight and volume. In this study, design optimization of the bellow joint used in liquid propellant rocket engines is conducted to minimize the force transferred to the actuators by minimizing the bending moment developed in the bellow joint. It is found that the bending moment developed in the bellow joint could be reduced by a significant rate of 75 % without compromising the structural integrity of the bellow joint.
波纹管接头经常用于液压管路、建筑和核电站等各种领域,以吸收流动和外力造成的能量,使管路具有柔韧性,并防止管路开裂和老化等损坏。波纹管接头有多种类型(如轴向型、万向节型和铰链型),允许轴向、横向和角度运动。用于辅助液体推进剂火箭发动机推力矢量控制的波纹管接头可防止液压管路在导弹定向运动过程中受损。在为火箭发动机中的管路提供这种灵活性的同时,它们也对移动液体发动机喷嘴的线性执行器产生了额外的力。这种额外的力导致需要更大的执行器,从而增加了重量和体积。在这项研究中,对液体推进剂火箭发动机中使用的波纹管接头进行了设计优化,以通过最大限度地减小波纹管接头中产生的弯矩来最小化传递给致动器的力。研究发现,在不影响波纹管接头结构完整性的情况下,波纹管接头中产生的弯矩可显著减少 75%。
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引用次数: 0
A novel experimental method for measuring the direct tensile strength of concrete 测量混凝土直接抗拉强度的新型实验方法
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-18 DOI: 10.1515/mt-2023-0288
Oussama Merabet, Mohamed Bentchikou, Nasreddine Amoura, Ahmed Elshafie
This study deals with the development of a load-converting device designed for measuring the direct tensile strength of the concrete. In this regard, a new testing technique based on a novel testing device and modified cylindrical (Ø 100 × 200) molds for the preparation of concrete samples is explained. The embedded rod method was adopted to transmit the uniaxial tensile load to the specimens using the universal compression machine and the current converting device. In order to examine the reliability of the suggested test method, a comparison with indirect tensile methods (splitting and three-point loading flexural tests) was made. The results show that the tensile strength of the tested specimens is lower for the direct tensile test obtained by the proposed test setup than for the flexural test and closer to the strength results obtained from the splitting test. As expected, all the specimens tested using the introduced test method demonstrated a sudden and unique fracture in the middle portion. Additionally, no slippage of embedded bars was noticed during the test.
本研究涉及一种用于测量混凝土直接抗拉强度的荷载转换装置的开发。在这方面,解释了一种基于新型测试装置和用于制备混凝土试样的改进型圆柱(直径 100 × 200)模具的新测试技术。采用预埋杆法,利用万能压缩机和电流转换装置向试样传递单轴拉伸载荷。为了检验建议试验方法的可靠性,与间接拉伸方法(劈裂试验和三点加载弯曲试验)进行了比较。结果表明,用建议的试验装置进行直接拉伸试验获得的试样拉伸强度低于弯曲试验,更接近劈裂试验获得的强度结果。正如预期的那样,所有使用所引入的测试方法进行测试的试样都在中间部分出现了突然和独特的断裂。此外,在测试过程中没有发现预埋钢筋滑动。
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引用次数: 0
Exfoliation behavior of EN AW 7020 with T6, step aging and ultrasonic impact peening processes 采用 T6、阶跃时效和超声冲击强化工艺的 EN AW 7020 的剥落行为
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-18 DOI: 10.1515/mt-2023-0373
Halil Ibrahim Yurdgülü, Recep Sadeler, Barış Koç
In this study the effect of T6 heat treatment, two-step aging treatment and ultrasonic impact peening on the exfoliation corrosion behavior of welded EN AW 7020 was investigated. Exfoliation tests were performed according to the ASTM G34-01 standard. As expected, as a result of the tests, the base material region of all three samples were showed better corrosion resistance than the heat-affected region. Ultrasonic impact peening and two-step aging treatment was observed that improved EXCO sensitivity in the weld area. When sorting was made by considering the resistance to corrosion of the heat affected zone of the samples, it was observed that the best resistance was shown by the sample with two-step aging treatment, and the worst resistance was shown by the sample with T6 heat treatment.
本研究探讨了 T6 热处理、两步时效处理和超声波冲击强化对焊接 EN AW 7020 的剥落腐蚀行为的影响。剥落试验是根据 ASTM G34-01 标准进行的。不出所料,试验结果表明,所有三个样品的母材区域都比热影响区域表现出更好的耐腐蚀性。据观察,超声波冲击强化和两步时效处理提高了焊接区域的 EXCO 灵敏度。根据样品热影响区的耐腐蚀性能进行分类,发现经过两步老化处理的样品耐腐蚀性能最好,而经过 T6 热处理的样品耐腐蚀性能最差。
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引用次数: 0
Operational wear behaviour of 3D-printed lightweight metal gears: EDS and oil analysis comparison 3D 打印轻质金属齿轮的运行磨损特性:EDS 和油分析比较
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-18 DOI: 10.1515/mt-2023-0222
Tuğçe Tezel, Ulrich Schultheiss, Helga Hornberger, V. Kovan
Additive manufacturing (AM) has come to the fore in recent years among manufacturing techniques. This technique, which has different advantages than traditional ones such as casting, forging and machining, is expected to be widely used in producing machine parts like gears in the coming years. Therefore, experimental data on AM parameters for lightweight metal gears are important for industrial production. In this study, a wear test was applied to AlSi10Mg and Ti6Al4V gears under operational conditions, and the wear behaviour of conventionally and additively manufactured gears was compared. The amount of abrasion elements was determined by analysing the oil in the gearbox. In addition, gear surfaces were analysed using scanning electron microscopy and an energy-dispersive spectrometer before and after wear. Thus, the wear behaviour of gears produced by conventional and AM under service conditions was demonstrated comparatively.
近年来,快速成型制造(AM)技术在各种制造技术中脱颖而出。与铸造、锻造和机械加工等传统技术相比,这种技术具有不同的优势,预计未来几年将广泛应用于生产齿轮等机械零件。因此,有关轻质金属齿轮 AM 参数的实验数据对于工业生产非常重要。本研究对工作条件下的 AlSi10Mg 和 Ti6Al4V 齿轮进行了磨损测试,并比较了传统齿轮和增材制造齿轮的磨损行为。磨损元素的数量是通过分析齿轮箱中的油来确定的。此外,还使用扫描电子显微镜和能量色散光谱仪对磨损前后的齿轮表面进行了分析。因此,传统齿轮和 AM 生产的齿轮在使用条件下的磨损行为得到了比较证明。
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引用次数: 0
Electrochemical corrosion behaviour of UNS S32205 duplex stainless steel dependent on sigma phase precipitation UNS S32205 双相不锈钢的电化学腐蚀行为取决于西格玛相析出
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-18 DOI: 10.1515/mt-2023-0325
Burçin Özbay Kısasöz, İbrahim Tütük, S. Acar, Alptekin Kısasöz
In this study, the microstructure and electrochemical corrosion behavior of the UNS S32205 alloy were investigated. Firstly, the phase diagram of the studied samples was determined by Thermo-Calc 2022 software, and the solution treatment temperature was designated. The studied samples were cooled by various cooling rates following the solution treatment at 1050 °C for 30 min. The samples were characterized by optical microscope, scanning electron microscope, and XRD analysis. Also, electrochemical corrosion behavior was investigated by potentiodynamic polarization, cyclic potentiodynamic polarization and electrochemical impedance spectroscopy analyses. Microstructural examinations revealed that decreasing cooling rate causes the precipitation of the sigma phase, and the ratio of the sigma phase was increased up to 29 % by the decreasing cooling rate. Furthermore, it was determined that precipitation of the sigma phase reduces the E pit values, and the sample with the highest amount of sigma exhibits the lowest corrosion resistance. On the other hand, presence of the sigma changed the electrochemical impedance spectroscopy behavior of the UNS S32205 and double-layered model fit the results.
本研究对 UNS S32205 合金的微观结构和电化学腐蚀行为进行了研究。首先,利用 Thermo-Calc 2022 软件确定了研究样品的相图,并指定了固溶处理温度。研究样品在 1050 °C 溶液处理 30 分钟后,以不同的冷却速率进行冷却。通过光学显微镜、扫描电子显微镜和 XRD 分析对样品进行了表征。此外,还通过电位极化、循环电位极化和电化学阻抗谱分析研究了电化学腐蚀行为。微观结构分析表明,降低冷却速度会导致σ相析出,并且σ相的比例会随着冷却速度的降低而增加,最高可达 29%。此外,σ相的析出还降低了 E pit 值,σ含量最高的样品耐腐蚀性能最低。另一方面,σ相的存在改变了 UNS S32205 的电化学阻抗谱行为,双层模型与结果相吻合。
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引用次数: 0
Optimum design of additively manufactured aerospace components with different lattice structures 具有不同晶格结构的快速成型航空航天组件的优化设计
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-14 DOI: 10.1515/mt-2023-0364
Mert Taşçı, Mehmet Umut Erdaş, Mehmet Kopar, B. Yildiz, Ali Rıza Yıldız
Nowadays, the need for new technologies is increasing, especially to find solutions to the inadequacies in the production of complex structures. The additive manufacturing methods developed facilitate the production of complex parts and move the technology forward with factors such as cost and efficiency. With the optimization of new parts designed by additive manufacturing methods, it is possible to obtain the optimum product even in the most complex structures. At the end of the production process, the final product with the desired properties is obtained as a result of part size tolerance precision and optimizations. In this study, lattice optimization is applied to a passenger aircraft bracket. It is aimed to reduce the weight and, at the same time, increase the efficiency of the part by optimizing it with lattice structures. For this purpose, the Altair Inspire program was used, and the variation of mass, displacement, safety coefficient, and stress values of the part according to different lattice structures were investigated.
如今,人们对新技术的需求与日俱增,尤其是为了解决复杂结构生产中的不足。所开发的增材制造方法促进了复杂部件的生产,并在成本和效率等因素上推动了技术的发展。通过对增材制造方法设计的新零件进行优化,即使是最复杂的结构也能获得最佳产品。在生产流程结束时,通过零件尺寸公差精度和优化,最终可获得具有所需性能的产品。在本研究中,晶格优化被应用于客机支架。其目的是通过优化晶格结构减轻零件重量,同时提高效率。为此,研究人员使用 Altair Inspire 程序,根据不同的晶格结构研究了零件质量、位移、安全系数和应力值的变化。
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引用次数: 0
Effect of temperature on oxidation during boriding of Ni-Hard 4 温度对硼化镍硬质合金 4 过程中氧化作用的影响
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-03-14 DOI: 10.1515/mt-2023-0385
Tuna Aydogmus
Ni-Hard 4, also known as white cast iron, is widely used in many applications that demand high mechanical strength. This material is recognized for its ability to withstand challenging conditions. In this study, surface modification processes, particularly boriding, were carried out on the material. Boriding is considered an effective process for enhancing the mechanical strength of a surface. While there are various methods for performing boriding, the pack-boriding method was chosen for this study. This method was applied in a typical heat treatment furnace. Ni-Hard 4 specimens were subjected to different combinations of temperature (1000–1200 °C) and 4 h duration, resulting in a total of three distinct samples. Subsequently, the microstructure, hardness, and chemical composition of the boride layers formed on the material’s surface were meticulously examined. As a result of the detailed analysis, it was determined that if the boriding process was carried out in a furnace without controlled atmosphere, high temperature oxidation started on the surface of Ni-Hard 4, and in this case it increased in parallel with the increase in temperature.
Ni-Hard 4 又称白口铸铁,广泛应用于许多需要高机械强度的场合。这种材料因其能够经受挑战性条件的考验而得到认可。在本研究中,对这种材料进行了表面改性处理,特别是硼化处理。硼化被认为是提高表面机械强度的有效工艺。虽然进行硼化的方法多种多样,但本研究选择了包硼法。该方法在典型的热处理炉中进行。对 Ni-Hard 4 试样进行了不同的温度组合(1000-1200 °C)和 4 小时的持续时间处理,总共产生了三种不同的试样。随后,对材料表面形成的硼化物层的微观结构、硬度和化学成分进行了细致的检测。详细分析的结果表明,如果在没有控制气氛的熔炉中进行硼化过程,Ni-Hard 4 的表面就会开始高温氧化,在这种情况下,氧化程度会随着温度的升高而增加。
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引用次数: 0
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Materials Testing
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