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Effect of red mud on mechanical and thermal properties of agave sisalana/glass fiber–reinforced hybrid composites 赤泥对龙舌兰/玻璃纤维增强混杂复合材料力学和热性能的影响
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-10-04 DOI: 10.1515/mt-2023-0118
Karthick Rasu, Anbumalar Veerabathiran
Abstract The mechanical, thermal, and morphological analysis of red mud filled sisal/glass fiber–reinforced polyester composites have been investigated. In this study, four composite specimens were prepared through hand layup technique by changing the weight percentage of sisal fiber and red mud. Weight percentage of glass fiber and polyester resin are kept constant. The fabricated composite specimens were subjected to mechanical properties such as hardness, impact and tensile behavior, thermal, and morphological analysis. From the results, it is observed that, maximum tensile strength of 45.6 MPa was obtained for C1 specimen. Maximum hardness and impact strength of 85.67 and 391.5 J m −1 was achieved for C2 specimen. In TGA study, C1 and C2 specimen exhibited 85 % of weight loss with the temperature ranges from 300 °C to 400 °C. From SEM analysis, good bonding between fiber and matrix, voids, fiber breakages, fiber pullout, delamination, rich matrix area, poor adhesion between fiber and matrix, poor arrangement of fibers, interlinked fibers, and crack propagation were observed. Based on the results, C2 specimen which contains 30 wt% of sisal fiber and 5 wt% of red mud is performed well than other composites and it is suitable for various applications such as marine, automobile, and aeronautical.
摘要研究了赤泥填充剑麻/玻璃纤维增强聚酯复合材料的力学、热学和形态分析。本研究通过改变剑麻纤维和赤泥的重量百分比,采用手铺技术制备了4种复合材料试样。玻璃纤维和聚酯树脂的重量百分比保持不变。对制备的复合材料试样进行了硬度、冲击和拉伸性能、热性能和形态分析等力学性能测试。结果表明,C1试件的最大抗拉强度为45.6 MPa。C2试样的最大硬度为85.67,冲击强度为391.5 J m−1。在TGA研究中,C1和C2试样在300 ~ 400℃温度范围内失重85%。通过SEM分析,观察到纤维与基体结合良好,存在空洞、纤维断裂、纤维拔出、分层、基体面积大、纤维与基体粘结性差、纤维排列不整齐、纤维相互连通、裂纹扩展等现象。结果表明,剑麻纤维含量为30%,赤泥含量为5%的C2试样性能优于其他复合材料,适用于船舶、汽车、航空等多种用途。
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引用次数: 0
Frontmatter 头版头条
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-10-01 DOI: 10.1515/mt-2023-frontmatter10
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引用次数: 0
Lateral compression behavior of expanded polypropylene foam–filled carbon and glass fiber composite tubes 膨胀聚丙烯泡沫填充碳/玻璃纤维复合管的侧向压缩性能
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-29 DOI: 10.1515/mt-2023-0120
Mehmet İskender Özsoy, Muhammet Muaz Yalçın
Abstract The crashworthiness and deformation behavior of circular composite tubes that were internally supported with expanded polypropylene (EPP) foams were investigated under lateral compression tests. Carbon woven (CFRP) and glass woven fiber/epoxy (GFRP) composites and EPP foam with densities of 30, 60, and 75 kg·m −3 were used. According to results, empty CFRP and GFRP tubes absorbed almost the same amount of energy; however, the GFRP tube had a higher specific energy absorption value due to its lower weight compared to the CFRP tube. EPP foam filling has a more significant effect on the crashworthiness of CFRP tubes compared to GFRP tubes. The best results in CFRP tubes, in terms of specific energy absorption, were obtained as 2.67 J g −1 at 75 kg·m −3 EPP foam-filled sample; however, 60 kg·m −3 EPP foam–filled sample exhibited the best configuration in terms of force efficiency. For the GFRP tubes, the best configuration was obtained at 60 kg·m −3 EPP foam–filled sample for all of the crashworthiness parameters. It is seen that the crushable length of composite tubes was shortened with the increase of EPP foam density. Lastly, the deformation behaviors of composite tubes showed that the CFRP tubes were more brittle than the GFRP tubes.
摘要通过侧压试验研究了内支聚丙烯(EPP)泡沫圆复合材料管的耐撞性和变形特性。使用密度分别为30、60和75 kg·m−3的碳纤维(CFRP)和玻璃纤维/环氧树脂(GFRP)复合材料和EPP泡沫。结果表明,CFRP空管与GFRP空管吸收的能量基本相同;然而,由于GFRP管的重量较轻,与CFRP管相比,GFRP管具有更高的比能吸收值。EPP泡沫填充对CFRP管耐撞性的影响比GFRP管更显著。在75 kg·m−3 EPP泡沫填充时,CFRP管的比能吸收效果最佳,为2.67 J g−1;然而,60 kg·m−3 EPP泡沫填充样品在力效率方面表现出最好的结构。对于GFRP管,在60 kg·m−3 EPP泡沫填充样品时获得了所有耐撞性参数的最佳配置。结果表明,随着EPP泡沫密度的增大,复合管材的可破碎长度缩短。最后,复合材料管的变形行为表明CFRP管比GFRP管更脆。
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引用次数: 0
Wear and residual stress in high-feed milling of AISI H13 tool steel AISI H13工具钢大进给铣削的磨损与残余应力
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-28 DOI: 10.1515/mt-2023-0144
Altug Bakirci, Selim Koca, Ozlem Erdogan, Mustafa Cemal Cakir
Abstract With the new manufacturing technologies, it has been possible to machine hard metals efficiently. During high-speed machining (HSM) of high-strength steel, the poor surface integrity of the workpiece affects the performance of the process. Surface roughness, microstructure, microhardness and residual stress are key performance indices for surface integrity directly controlled by tool wear and cutting parameters. In this study, high-feed milling (HFM) of a pocket on test samples made of DIN 1.2344 ESR mould steel with 55 HRc hardness was carried out on the CNC vertical milling machine. Three different cutting speeds and five different feed rates were used. At the end of the machining, tool wear was measured using a microscope. Subsequently, X-ray diffraction and hole drilling procedures were used to quantify residual stresses on machined test specimens. The results showed that under cutting conditions, the highest tensile residual stress was attained at f z = 0.78 mm·tooth −1 , v = 127.58 m·min −1 , and the highest compressive residual stress at f z = 0.5 mm·tooth −1 , v = 127.58 m·min −1 , on the workpiece surface. The most suitable cutting parameters were reported as f z = 0.63 mm·tooth −1 and v = 70 m·min −1 cutting speed when tool wear and residual stresses are considered together.
随着新的制造技术的发展,高效加工硬质金属已成为可能。在高强度钢的高速加工过程中,工件表面完整性差会影响加工性能。表面粗糙度、显微组织、显微硬度和残余应力是刀具磨损和切削参数直接控制的表面完整性的关键性能指标。本研究在数控立式铣床上对硬度为55 HRc的DIN 1.2344 ESR模型钢试样进行了口袋的高进给铣削(HFM)。采用了三种不同的切削速度和五种不同的进给速度。在加工结束时,使用显微镜测量刀具磨损。随后,使用x射线衍射和钻孔程序来量化加工试样的残余应力。结果表明:在切削条件下,工件表面在f z = 0.78 mm·齿−1,v = 127.58 m·min−1处的残余拉伸应力最大;在f z = 0.5 mm·齿−1,v = 127.58 m·min−1处的残余压应力最大;在综合考虑刀具磨损和残余应力的情况下,最适宜的切削参数为fz = 0.63 mm·齿−1和v = 70 m·min−1。
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引用次数: 0
Preparation, characterization, and antimicrobial activity of novel chitosan blended almond gum–nanosilica bionanocomposite film for food packaging applications 新型壳聚糖混合杏仁胶-纳米二氧化硅生物纳米复合食品包装膜的制备、表征及抗菌性能研究
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-27 DOI: 10.1515/mt-2023-0092
Ruby Thomas, Vinaya Thattil Vincent, Umapathy Manickam Janarthanam, Lakshmanan Rajagopal, Skandha Jay
Abstract Almond gum and varied concentrations of nanosilica (0.2, 0.4, 0.6, 0.8, and 1.0 wt%) were introduced into the chitosan polymer matrix by solution cast method to enrich the characteristics of the bionanocomposite film. The surface topography, thermal stability, crystalline nature, and functional moieties of the synthesized bionanocomposite films were characterized by SEM, TGA, XRD, and FT-IR. The UV–Vis spectrophotometer showed a maximum absorption wavelength for the film containing the highest concentration of nanosilica. Change in properties such as increased tensile strength, elongation and reduced water solubility, and swelling properties were observed for the bionanocomposite film containing 1.0 wt% nanosilica. In addition, the films exhibited excellent inhibition effect against Escherichia coli bacteria and Candida albicans fungus, which were proven by well diffusion assay method. The carrot slices packed in the bionanocomposite film containing the highest amount of nanosilica retained their freshness for a longer period of time, suggesting the film to be an effective and excellent food packaging material.
摘要:采用溶液浇铸法将杏仁胶和不同浓度的纳米二氧化硅(0.2、0.4、0.6、0.8和1.0 wt%)加入壳聚糖聚合物基体中,以丰富生物纳米复合膜的特性。采用SEM、TGA、XRD和FT-IR等手段对合成的生物纳米复合膜的表面形貌、热稳定性、晶体性质和功能组分进行了表征。紫外可见分光光度计测定了含纳米二氧化硅浓度最高的薄膜的最大吸收波长。对于含有1.0 wt%纳米二氧化硅的生物纳米复合膜,观察到其抗拉强度、伸长率和水溶性降低以及膨胀性能的变化。此外,该膜对大肠杆菌和白色念珠菌具有良好的抑菌效果,经孔扩散试验证实。用纳米二氧化硅含量最高的生物复合薄膜包装的胡萝卜片保鲜时间较长,是一种有效的、优良的食品包装材料。
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引用次数: 0
Effect of welding processes on ferrite content, microstructure and mechanical properties of super duplex stainless steel 2507 welds 焊接工艺对超级双相不锈钢2507焊缝铁素体含量、组织和力学性能的影响
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-27 DOI: 10.1515/mt-2023-0002
Chandragiri Baskar Sekar, Sajja Rama Koteswara Rao, Sundaravel Vijayan, Sadayan Rajendra Boopathy
Abstract Super duplex stainless steel (SDSS) plates of 6 mm thickness have been welded using tungsten inert gas, activated tungsten inert gas, electron beam welding and friction stir welding processes. Among these, in the first two, melting and solidification of material occurs slowly whereas, it is faster in electron beam welding process and no melting occurs in friction stir welding. Macro and microstructural studies, hardness surveys, tensile tests and percentage of ferrite content were compared for all the welds. The ferrite–austenite phase balance is 50 % each, with electron beam weld metal at about 65 % ferrite. This showed the hardness of the weld metal and heat affected zones to be higher than base metal. The weldment joint efficiencies are more than 90 %. The fracture location is found to be in the weld metal for tungsten inert gas and activated tungsten inert gas weld, in the nugget for friction stir welds and in the base metal for electron beam welds. The ductility of electron beam weld joints is 32 % while it is around 20 % for the others. The preferred order while choosing the welding process should be activated tungsten inert gas welding, tungsten inert gas welding, electron beam welding, and friction stir welding.
摘要采用钨惰性气体、活化钨惰性气体、电子束焊和搅拌摩擦焊等工艺对6mm厚的超级双相不锈钢(SDSS)板进行了焊接。其中,在前两种焊接工艺中,材料的熔化和凝固速度较慢,而电子束焊接工艺的熔化和凝固速度较快,搅拌摩擦焊接工艺则不发生熔化。对所有焊缝进行了宏观和微观组织研究、硬度调查、拉伸试验和铁素体含量百分比的比较。铁素体-奥氏体相平衡各为50%,电子束焊接金属的铁素体含量约为65%。这表明焊接金属的硬度和热影响区高于母材。焊件接头效率达90%以上。钨惰性气体和活化钨惰性气体焊的断口在焊缝金属中,搅拌摩擦焊的断口在熔核中,电子束焊的断口在母材中。电子束焊接接头的延展性为32%,而其他焊接接头的延展性在20%左右。在选择焊接工艺时,应优先考虑活化钨惰性气体焊、钨惰性气体焊、电子束焊、搅拌摩擦焊。
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引用次数: 0
Analyzing the effect of notch geometry on the impact strength of 3D-printed specimens 分析缺口几何形状对3d打印试样冲击强度的影响
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-26 DOI: 10.1515/mt-2023-0088
Ali Solouki, Mohammad Reza Mohammad Aliha, Ahmad Makui, Naghdali Choupani
Abstract Additive manufacturing (AM) using 3D printing techniques such as fused deposition modeling (FDM) has now found much attention, not only in prototyping but also in industrial production. Indeed, the 3D-printed components are now widely used as structural elements in many applications such as biomechanical engineering (dentistry, orthopedics, bio implants, etc.) and therefore, full understanding of their strength, load carrying capacity, improving the mechanical behaviors, and manufacturing process is an important issue. Charpy impact experiments offer information on the strength of a material to sudden failure where a sharp stress raiser or notch is present. In addition to providing information not available from any other simple mechanical experiments, the impact resistance tests are quick and inexpensive, so they are often used. In this research, impact strength experiments were conducted at room temperatures on rectangular samples containing three different notches including V-notch, U-notch, and Keyhole-notch to determine impact resistance of the 3D-printed polylactic acid (PLA) components. The capability of multiple comparison tests for analysis of variance like ANOVA, Tukey, and Fisher methods for prediction of impact resistance in the tested specimens were also investigated. The samples containing Keyhole notch showed highest Charpy impact resistance. In contrary, V-notched sample provided the lowest impact energy. All the employed statistical analyses reveal that the notch type has meaningful influence on the impact energy of 3D-printed parts.
利用3D打印技术(如熔融沉积建模(FDM))进行增材制造(AM)现在不仅在原型制作中而且在工业生产中受到了广泛关注。事实上,3d打印部件现在广泛用作生物力学工程(牙科,骨科,生物植入物等)等许多应用中的结构元件,因此,充分了解其强度,承载能力,改善机械行为和制造过程是一个重要问题。夏比冲击实验提供了材料在突然失效时的强度信息,其中存在尖锐的应力凸起或缺口。除了提供从任何其他简单的机械实验中无法获得的信息外,抗冲击性测试快速且廉价,因此经常使用。本研究在室温下对含有v形缺口、u形缺口和keyhole -缺口三种不同缺口的矩形样品进行冲击强度实验,以确定3d打印聚乳酸(PLA)部件的抗冲击性。对方差分析的多重比较检验如ANOVA、Tukey和Fisher方法预测试件抗冲击性的能力也进行了研究。含有锁眼缺口的样品具有最高的抗夏比冲击性能。相反,v形缺口试样的冲击能最低。统计分析表明,缺口类型对3d打印零件的冲击能有显著影响。
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引用次数: 0
Optimum design of a composite drone component using slime mold algorithm 基于黏菌算法的复合无人机部件优化设计
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-25 DOI: 10.1515/mt-2023-0245
Mehmet Kopar, Ali Rıza Yıldız, Betül Sultan Yıldız
Abstract Composite materials have a wide range of applications in many industries due to their manufacturability, high strength values, and light filling. The sector where composite materials are mostly used is the aviation industry. Today, as a result of the development of aviation systems, drones have started to be actively used, and many studies have started to be carried out to mitigate them. In this study, the subcarrier part, which is part of the drone, was designed using glass and carbon fiber–reinforced composite materials. Using the data obtained at the end of the analysis, the stacking angle with the optimal displacement and stress value was determined by using the genetic algorithm (GA), gray wolf algorithm (GWO), and slime mold optimization (SMO) techniques in order to develop a carrier with a minimum displacement and stress value of more than 60 MPa. As a result of the optimization, it was determined that artificial intelligence algorithms could be used effectively in determining the stacking angle of composite materials, and the optimum values were determined in the slime mold algorithm.
摘要复合材料具有易制造、强度值高、填充量小等优点,在许多行业有着广泛的应用。航空工业是复合材料应用最多的领域。今天,由于航空系统的发展,无人机已经开始被积极使用,并且已经开始进行许多研究来减轻它们。在本研究中,副载体部分是无人机的一部分,使用玻璃和碳纤维增强复合材料进行设计。利用分析结束后获得的数据,采用遗传算法(GA)、灰狼算法(GWO)和黏菌优化(SMO)技术确定最优位移和应力值的堆垛角度,以开发最小位移和应力值大于60 MPa的载体。优化结果表明,人工智能算法可以有效地用于复合材料堆积角的确定,并在泥霉菌算法中确定了最优值。
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引用次数: 0
Influence of heat input on temperature and stress field of X80 steel pipeline cirumferential weld using type-B sleeve repairing 热输入对X80钢管道环焊缝b型套管修复温度和应力场的影响
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-25 DOI: 10.1515/mt-2023-0274
Lei Guo, Mingchang Wu, Yan Xu, Leilei Wang, Fengping Yang, Qiang Bai, Zhenjun Feng, Xiaoyong Zhang, Yongxin Lu
Abstract The multi-pass fillet welds of casing pipe were welded onto the in-service pipeline, which is widely used in pipeline repairs. However, the influence of welding heat input of B-type sleeve circumferential fillet weld on the temperature and stress field at the pipe circumferential weld is still unclear. In this paper, a double ellipsoid heat source model is developed to investigate the weld temperature field, residual stress field, and deformation field of the repair welding in service. The results show that the increase of weld heat input can effectively increase the size of the weld pool and the size of the high-temperature zone of the B-type sleeve circumferential fillet weld. And the peak temperature of the inner wall of the pipe girth weld increases with the increase of welding heat input of the sleeve circumferential fillet weld. The axial stress peak of the inner wall of the pipe girth weld reduces with the increase of welding heat input of sleeve circumferential fillet weld, and the axial deformation peak of the inner wall of the pipe girth weld increases first and then decreases with the increase of welding heat input of sleeve circumferential fillet weld.
摘要将套管多道角焊缝焊接到在役管道上,广泛应用于管道维修。然而,b型套管周向角焊缝的焊接热输入对管道周焊缝温度场和应力场的影响尚不清楚。本文建立了双椭球热源模型,研究了在役补焊的焊缝温度场、残余应力场和变形场。结果表明:焊缝热输入的增加可以有效地增大b型套管周向角焊缝的熔池尺寸和高温区尺寸;随着套管周向角焊缝焊接热输入量的增加,管道环焊缝内壁峰值温度升高。管道环焊缝内壁轴向应力峰值随套管周向角焊缝焊接热输入的增加而减小,管道环焊缝内壁轴向变形峰值随套管周向角焊缝焊接热输入的增加先增大后减小。
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引用次数: 0
Comparison between laser and TIG welding of electron beam melted Ti6Al4V parts 电子束熔化Ti6Al4V零件激光与TIG焊接的比较
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-20 DOI: 10.1515/mt-2023-0149
Murat Sen, Mustafa Kurt
Abstract A large number of metal parts specific to the aviation, energy, and biomedical industries are produced by the electron beam melting (EBM) method, which is one of the powder bed additive manufacturing techniques. The limited build volume of EBM machines does not allow the production of parts in the desired dimensions. One way to overcome this limitation is to weld small size additive manufactured parts. In this study, EBMed Ti6Al4V tensile specimens were joined by laser (LBW) and tungsten inert gas (TIG) welding. Welding morphologies, microstructures, and mechanical properties of joints were investigated. The main defects in the samples are pore formation and insufficient penetration. The weld zones of TIG samples contain a higher amount of pores than laser samples, and these pores are distributed over the entire area of the weld. The pores are less than 200 µm in diameter. TIG welded samples exhibited higher mechanical properties than laser welded samples. The highest microhardness was measured in the weld zone. Microhardness of laser welded samples are higher than TIG welded samples. While the welding regions of TIG welded samples consist of coarse and acicular α and α + β structures, laser welded samples consist of thin and acicular α′ structure.
电子束熔化(EBM)是粉末床增材制造技术的一种,用于航空、能源和生物医药等行业的大量金属零件的生产。EBM机器有限的制造体积不允许生产所需尺寸的零件。克服这一限制的一种方法是焊接小尺寸的增材制造零件。本研究采用激光(LBW)和钨惰性气体(TIG)焊接方法连接EBMed Ti6Al4V拉伸试样。研究了接头的焊接形貌、显微组织和力学性能。样品的主要缺陷是孔隙形成和渗透不足。TIG试样的焊缝区比激光试样含有更多的气孔,并且这些气孔分布在整个焊缝区域。孔隙直径小于200µm。TIG焊接样品的力学性能优于激光焊接样品。焊缝区显微硬度最高。激光焊接试样的显微硬度高于TIG焊接试样。TIG焊接试样的焊接区为粗晶针状α和α + β组织,而激光焊接试样的焊接区为细晶针状α '组织。
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引用次数: 0
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Materials Testing
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