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Fe2B layer growth kinetics on ASTM A307 steel evaluated by two diffusion models 用两种扩散模型评估 ASTM A307 钢上的 Fe2B 层生长动力学
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-23 DOI: 10.1515/mt-2023-0306
M. Ortiz-Domínguez, M. Keddam
In this study, we implemented two simple models to simulate the growth of the Fe2B layer on ASTM A307 steel through boriding. The first model considered steady-state boron diffusion, while the second model incorporated transient regime effects. In the steady-state model, the boron concentration profile within the Fe2B layer exhibited linearity. By correlating the boron chemical potential with the inward mass flux at the (Fe2B/substrate) interface, we confirmed the parabolic nature of layer growth. Both models were employed to determine the boron activation energies, yielding the same value of approximately 164 kJ mol−1. Experimental validation of the two models was conducted under two additional boriding conditions (1323 K for 1.5 and 2 h). Finally, the simulated layer thicknesses matched with the experimental values.
在这项研究中,我们采用了两个简单的模型来模拟 ASTM A307 钢上通过渗硼形成的 Fe2B 层。第一个模型考虑了稳态硼扩散,而第二个模型则考虑了瞬态效应。在稳态模型中,Fe2B 层内的硼浓度曲线呈现线性。通过将硼化学势与(Fe2B/基底)界面的内向质量通量相关联,我们证实了硼层生长的抛物线性质。这两个模型都被用来确定硼活化能,得出的数值相同,都是约 164 kJ mol-1。我们在另外两种硼化条件下(1323 K,1.5 小时和 2 小时)对两个模型进行了实验验证。最后,模拟层厚度与实验值相吻合。
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引用次数: 0
Multi-pass friction hardening treatment of Ti6Al4V alloy toward improved tribological properties 对 Ti6Al4V 合金进行多道摩擦硬化处理以改善其摩擦学特性
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-23 DOI: 10.1515/mt-2023-0298
Atiyeh Shafaghatian, R. Taghiabadi, Reza Ahmadi, F. Shahriyari, Mohammad Emami
Multi-pass surface friction hardening was employed to modify the microstructure and enhance the tribology characteristics of the Ti6Al4V alloy. The process was performed by reciprocated sliding a flat-head WC-Co cylindrical pin tool on the alloy surface under different applied loads of 350, 700, 1050, and 1400 N. The sliding was conducted at different speeds of 45, 90, 180, 360, 720, and 900 mm min−1 for 30, 60, 90, 120, and 150 passes, respectively. Based on the hardness test and microstructural characterization results, the applied load of 1050 N, the sliding speed of 900 mm min−1, and the pass number of 60 (900-60 sample) were chosen as the optimum economic process parameters for the subsequent experiments. Performing surface friction hardening under the optimized conditions increased the surface hardness of the annealed sample from 350 HV1 to 564 HV1 showing an increase of about 60 %. Surface friction hardening was also found to substantially improve the tribology characteristics of the Ti6Al4V alloy. According to the obtained results, under the applied loads of 1 and 6 N, the wear rate and the average friction coefficient of the 900-60 sample were lower than those of the annealed one by 58 and 83 %, and 33 and 50 %, respectively.
为了改变 Ti6Al4V 合金的微观结构并提高其摩擦学特性,采用了多道表面摩擦硬化工艺。该过程是在 350、700、1050 和 1400 牛顿的不同外加载荷下,通过在合金表面往复滑动平头 WC-Co 圆柱销工具来完成的。滑动速度分别为 45、90、180、360、720 和 900 mm/min-1,滑动次数分别为 30、60、90、120 和 150 次。根据硬度测试和微观结构表征结果,为后续实验选择了 1050 N 的施加载荷、900 mm min-1 的滑动速度和 60 次的滑动次数(900-60 样品)作为最佳经济工艺参数。在优化条件下进行表面摩擦硬化,退火样品的表面硬度从 350 HV1 提高到 564 HV1,提高了约 60%。研究还发现,表面摩擦硬化还大大改善了 Ti6Al4V 合金的摩擦学特性。根据所得结果,在施加 1 N 和 6 N 负载的情况下,900-60 样品的磨损率和平均摩擦系数分别比退火样品低 58% 和 83%,以及 33% 和 50%。
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引用次数: 0
Effect of tool rotational speed on friction stir spot welds of AZ31B Mg alloy to AISI 304 stainless steel 工具转速对 AISI 304 不锈钢 AZ31B Mg 合金搅拌摩擦点焊的影响
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-23 DOI: 10.1515/mt-2023-0372
Omer Ekinci
AZ31B Mg alloy were welded to AISI 304 stainless steel (which is a very challenging task because of their huge different chemical and physical features) by friction stir spot welding (FSSW) at different tool rotation speeds (700, 1000, and 1300 rpm) while keeping other conditions the same. Welds were evaluated and compared by examining their cross-sectional geometry, XRD pattern, tensile shear strength, fracture way and area. From cross-sections of welds, it was obtained that joining area expanded when speed was enhanced and the weld made through 1300 rpm had the largest one. Therefore, weld fabricated with the highest speed of 1300 rpm displayed the biggest tensile shear load of 3741 N while that manufactured with the lowest speed of 700 rpm possessed the lowest of 2430 N. All welds showed tensile shear type fracture and fracture occurred from the hooking regions where joining took place. From the fracture joint region, the weld of 700 rpm had the smallest joined area, whereas that of 1300 rpm showed the biggest. Higher speed produced a stronger joint, which agreed with a bigger bonding area and broken joint region. Also, joint became more ductile with increasing speed. Some phases were detected in joints.
在保持其他条件不变的情况下,以不同的工具转速(700、1000 和 1300 rpm)通过搅拌摩擦点焊 (FSSW) 将 AZ31B 镁合金焊接到 AISI 304 不锈钢上(这是一项非常具有挑战性的任务,因为它们的化学和物理特性存在巨大差异)。通过检查焊缝的横截面几何形状、XRD 图谱、拉伸剪切强度、断裂方式和面积,对焊缝进行评估和比较。从焊缝的横截面可以看出,当转速提高时,接合面积会扩大,而 1300 转/分钟时的焊缝接合面积最大。因此,以 1300 转/分的最高转速制造的焊缝显示出最大的拉伸剪切载荷,为 3741 牛顿,而以 700 转/分的最低转速制造的焊缝载荷最小,为 2430 牛顿。从断裂接头区域来看,700 转/分的焊缝接合面积最小,而 1300 转/分的焊缝接合面积最大。转速越高,接合强度越大,这与接合区域和断裂接合区域越大有关。此外,接头的韧性也随着转速的增加而增加。在接头中发现了一些相位。
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引用次数: 0
Pull-out strength of screws in long bones at different insertion angles: finite element analysis and experimental investigations 长骨中不同插入角度螺钉的拔出强度:有限元分析和实验研究
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-23 DOI: 10.1515/mt-2023-0239
Osman İyibilgin, Engin Gepek, Levent Bayam, Efstathios Drampalos, Amer Shoaib
Different types of plates are available to allow insertion of screws for internal fixation of long bone fractures. The aim of the study was to determine the effect of the insertion of screws at different angles on a long bone to the pull-out strength. Using 3D printed bone models, we tested the pull-out strength of screws in long bones at insertion angles between 0 and 40° with both finite element analysis and on printed models experimentally and compared the results. Test samples and cortical screws used were modeled with SolidWorks software and analyzed with Ansys software. As the screw insertion angle increases, the pull-out forces on the test specimens increase from 61.14 ± 3.5 N at 0° to 273 ± 6.8 N at 40° with an exception of a small drop between 15 and 20° from 235.4 ± 6.2 to 233 ± 6.9 N. Both methods showed an increase in the pull-out strength of screws as the insertion angle increases. This might be applicable in the clinical practice of bone fixation. Further studies on plate and screw fixation are needed to complement the findings.
有不同类型的钢板可插入螺钉用于长骨骨折的内固定。这项研究的目的是确定在长骨上以不同角度插入螺钉对拔出强度的影响。我们使用三维打印骨骼模型,通过有限元分析和打印模型实验,测试了长骨中 0 至 40° 插入角度的螺钉拔出强度,并对结果进行了比较。使用 SolidWorks 软件对测试样本和所用皮质螺钉进行建模,并使用 Ansys 软件进行分析。随着螺钉插入角度的增加,测试样本上的拉出力从 0° 时的 61.14 ± 3.5 N 增加到 40° 时的 273 ± 6.8 N,但在 15 至 20° 之间略有下降,从 235.4 ± 6.2 N 下降到 233 ± 6.9 N。两种方法都显示,随着插入角度的增加,螺钉的拔出强度也会增加。这可能适用于骨固定的临床实践。需要对钢板和螺钉固定进行进一步研究,以补充研究结果。
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引用次数: 0
Thermal insulation properties of materials for fishing vessel coolboxes 渔船冷却箱材料的隔热性能
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-18 DOI: 10.1515/mt-2023-0244
P. Manik, T. Tuswan, Muhammad Abdullah Azzam, S. Samuel, Aditya Rio Prabowo
Abstract Effective insulation is critical for traditional fishing boats because it helps to maintain the quality of the fish catch. Inadequate insulation can lead to significant economic losses for fishermen, as they may have to discard or sell the fish at a lower price. This study aimed to compare the thermal conductivity properties of three different insulation materials: Petung bamboo, polystyrene foam, and polyurethane foam. The experiment involved testing the density of the materials and conducting thermal conductivity tests. The results indicated that polyurethane foam is the best material for insulation because it has the lowest thermal conductivity value compared to laminated bamboo and polystyrene foam. The addition of more isocyanate mass fraction to the polyurethane foam material can increase its density and strength. This is because increasing the isocyanate concentration increases the cross-linking density of the foam, making it more durable and resilient. Moreover, higher density polyurethane foams exhibit lower heat conductivity, indicating better insulation qualities. This study highlights the importance of effective insulation to maintain the quality of the fish catch. The findings suggest that polyurethane foam, particularly with increased isocyanate concentration, is the most suitable material for insulation due to its superior insulation qualities.
摘要 有效的隔热对传统渔船至关重要,因为它有助于保持渔获物的质量。隔热性能不足会给渔民带来巨大的经济损失,因为他们可能不得不丢弃或以较低的价格出售鱼类。本研究旨在比较三种不同隔热材料的导热性能:竹子、聚苯乙烯泡沫塑料和聚氨酯泡沫塑料。实验包括测试材料的密度和进行导热性测试。结果表明,聚氨酯泡沫是最好的隔热材料,因为与层压竹和聚苯乙烯泡沫相比,它的导热值最低。在聚氨酯泡沫材料中添加更多的异氰酸酯质量分数可以增加其密度和强度。这是因为增加异氰酸酯浓度可提高泡沫的交联密度,使其更耐用、更有弹性。此外,密度较高的聚氨酯泡沫的导热率较低,表明其隔热性能更好。这项研究强调了有效隔热对保持渔获质量的重要性。研究结果表明,聚氨酯泡沫塑料,尤其是异氰酸酯浓度增加的聚氨酯泡沫塑料,因其卓越的隔热性能,是最合适的隔热材料。
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引用次数: 0
Effects of temperature and strain rate on the deformation microstructure and hardness of Al–Zn eutectoid damping alloy 温度和应变速率对 Al-Zn 共晶阻尼合金变形显微组织和硬度的影响
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-16 DOI: 10.1515/mt-2023-0293
Shuyi Wang, Song Zhang, Yonggang Xu
Abstract The effects of temperature and strain rate on the deformation microstructure and hardness of Al–Zn eutectoid damping alloy was systematically investigated. The results show that the deformed alloy is mainly composed of eutectoid structure with η-Zn distributing on α-Al matrix. There are two forms of η-Zn particles in the eutectoid structure of the deformed alloy. The first type of η-Zn particles (η-ZnI) have relatively large sizes and display irregular morphology; another type of η-Zn particles (η-ZnII) have relatively small sizes and are characterized by dispersion distribution. There exist predominant η-ZnI particles at lower temperature and higher strain rate while dominant η-ZnII particles at higher temperature and lower strain rate. The hardness of the Al–Zn eutectoid damping alloy shows an overall rising trend with increase in temperature and decrease in strain rate. In particular, the highest hardness values (up to 113.07 HB) are obtained at 648 K/0.01 s−1.
摘要 系统研究了温度和应变速率对 Al-Zn 共晶阻尼合金变形显微组织和硬度的影响。结果表明,变形合金主要由η-Zn分布在α-Al基体上的共晶结构组成。在变形合金的共晶结构中,η-Zn 颗粒有两种形式。第一种η-Zn 颗粒(η-ZnI)尺寸相对较大,形态不规则;另一种η-Zn 颗粒(η-ZnII)尺寸相对较小,呈分散分布。在较低温度和较高应变速率下,η-ZnI 颗粒占主导地位,而在较高温度和较低应变速率下,η-ZnII 颗粒占主导地位。随着温度的升高和应变率的降低,Al-Zn 共晶阻尼合金的硬度总体呈上升趋势。尤其是在 648 K/0.01 s-1 时,硬度值最高(达 113.07 HB)。
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引用次数: 0
Interfacial microstructure and mechanical properties of Si3N4/Invar joints using Ag–Cu–In–Ti with Cu foil as an interlayer 以铜箔为中间层的银铜铟锡 Si3N4/Invar 接头的界面微观结构和力学性能
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-11 DOI: 10.1515/mt-2023-0221
Tong Zhao, Defeng Mo, Xue Li, Haimei Gong
Abstract Si3N4 and Invar alloy brazed joints were achieved using two types of Ag-based interlayers: a Ag–Cu–In–Ti foil and a Ag–Cu–In–Ti/Cu/Ag–Cu multi-interlayer. The results showed that when only using a single Ag–Cu–In–Ti filler, the wave-shaped Fe2Ti + Ni3Ti intermetallic compounds are concentrated in the middle of the brazing seam. When adding Cu as the interlayer, the dissolution of the Cu interlayer formed a large number of Cu(s,s) blocks of different sizes in the brazing seam, which hindered the concentrated distribution of Fe2Ti + Ni3Ti intermetallic compounds in the brazing seam. As a result, Fe2Ti and Ni3Ti were dispersedly distributed in the brazing seam, increasing the shear strength of the brazed joint. The shear strength of brazed joints was increased by 82 % compared to joints brazed with a single Ag–Cu–In–Ti filler when the Cu interlayer was added.
摘要 使用两种类型的银基中间膜实现了 Si3N4 和英华合金钎焊接缝:一种是银-铜-铟-钛箔,另一种是银-铜-铟-钛/铜/银-铜多层中间膜。结果表明,只使用单一的银-铜-铟-钛填料时,波浪形的 Fe2Ti + Ni3Ti 金属间化合物集中在钎缝的中间。当加入 Cu 作为中间层时,Cu 中间层的溶解在钎缝中形成了大量大小不一的 Cu(s,s)块,阻碍了 Fe2Ti + Ni3Ti 金属间化合物在钎缝中的集中分布。因此,Fe2Ti 和 Ni3Ti 在钎缝中分散分布,提高了钎焊接头的抗剪强度。当加入铜中间层时,钎焊接头的剪切强度比使用单一银-铜-铟-钛填料钎焊的接头提高了 82%。
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引用次数: 0
Investigation on quasi-static axial crushing of Al/PVC foam-filled Al6063-T5 tubes 铝/聚氯乙烯泡沫填充 Al6063-T5 管的准静态轴向挤压研究
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-11 DOI: 10.1515/mt-2023-0273
M. M. Yalçın
Abstract This study experimentally investigated the energy-absorbing capability of foam-filled 6063-T5 aluminum tubes. Thus, different sample combinations were created with two different foams, PVC (80 kg m−3) and aluminum (200, 350 kg m−3), which were used as filling materials. The first group of samples consisted of uniform foam-filled aluminum tubes. In contrast, tubes were filled with radially graded foams in the second group, which included a ring PVC foam and a cylindrical aluminum foam in the center. Empty tube absorbed 329 J, while it reached the values of 384, 488, and 606 J by using PVC and low- and high-density aluminum foams, respectively. The specific energy absorption value of the empty tube was obtained as 23.2 J g−1. In comparison, it was 19.3 J g−1 in the high-density aluminum foam-filled sample, although it absorbed the highest energy value. This shows that high-density aluminum foam was inefficient in terms of the crashworthiness of the structure. Finally, the best sample regarding the specific energy absorption and crush force efficiency was obtained in the sample where the PVC foam ring and high-density aluminum tube were used together. This sample had 7 % higher specific energy absorption and 34 % higher crush force efficiency than the empty tube.
摘要 本研究通过实验研究了泡沫填充 6063-T5 铝管的能量吸收能力。因此,使用聚氯乙烯(80 kg m-3)和铝(200、350 kg m-3)两种不同的泡沫作为填充材料,制作了不同的样品组合。第一组样品由均匀的泡沫填充铝管组成。与此相反,第二组样品中的管子填充了径向分级泡沫,包括环形聚氯乙烯泡沫和中间的圆柱形铝泡沫。空管吸收的能量为 329 焦耳,而使用聚氯乙烯泡沫和低密度及高密度铝泡沫吸收的能量分别为 384、488 和 606 焦耳。空管的比能量吸收值为 23.2 J g-1。相比之下,填充高密度铝泡沫的样品吸收的能量值最高,为 19.3 J g-1。这表明高密度铝泡沫在结构的耐撞性方面效率较低。最后,PVC 泡沫环和高密度铝管共同使用的样品在比能量吸收和挤压力效率方面都是最好的。与空管相比,该样本的比能量吸收率高出 7%,压溃力效率高出 34%。
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引用次数: 0
Experimental analysis of the effects of different production directions on the mechanical characteristics of ABS, PLA, and PETG materials produced by FDM 不同生产方向对 FDM 生产的 ABS、PLA 和 PETG 材料机械特性影响的实验分析
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-09 DOI: 10.1515/mt-2023-0206
Mehmet Umut Erdaş, B. Yildiz, Ali Rıza Yıldız
Abstract One of the most researched technologies among technologies used for producing complex and diverse parts today is additive manufacturing. In additive manufacturing, production can be carried out using thermoplastic and metal materials without requiring an additional process. Among the additive manufacturing technologies, the Fused Filament Fabrication (FFF) method is the most widely used method worldwide due to its affordability and broad application area. FFF is a method in which part formation is achieved by depositing melted materials on each other. In recent years, polymer materials such as polylactic acid (PLA), polyethylene terephthalate glycol (PETG), and acrylonitrile butadiene styrene (ABS) have been frequently used in many industrial areas in the FFF method because they are lightweight, inexpensive, sustainable, and provide sufficient strength for engineering applications. This study conducted tensile, three-point bending, Charpy, and compression tests on PLA, PETG, and ABS materials at angles of 15°–75° and 30°–60°, and the results were compared.
摘要 在当今用于生产复杂多样零件的技术中,增材制造技术是研究最多的技术之一。在增材制造中,可以使用热塑性和金属材料进行生产,而不需要额外的工序。在增材制造技术中,熔融长丝制造(FFF)方法因其经济实惠和应用领域广泛而成为全球使用最广泛的方法。FFF 是一种通过熔融材料相互沉积来实现零件成型的方法。近年来,聚乳酸(PLA)、聚对苯二甲酸乙二醇酯(PETG)和丙烯腈-丁二烯-苯乙烯(ABS)等高分子材料因其重量轻、价格低廉、可持续发展且具有足够的工程应用强度,在许多工业领域被频繁用于 FFF 法。本研究对聚乳酸、PETG 和 ABS 材料在 15°-75° 和 30°-60° 角度下进行了拉伸、三点弯曲、夏比和压缩测试,并对结果进行了比较。
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引用次数: 0
User independent tool for the analysis of data from tensile testing for database systems 独立于用户的数据库系统拉伸试验数据分析工具
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2024-01-09 DOI: 10.1515/mt-2023-0262
Nima Babaei, Jing Wang, Elisabeth Kisseler, Marc Ackermann, Sebastian Wipp, Alexander Gramlich, Ulrich Krupp
Abstract Data streams in science and economy are becoming increasingly automatized. This has various advantages compared to previous, user-dependent analyses, in which the same results are analyzed differently by different persons. Even though these differences are only of a certain degree, they can lead to false estimations of underlying material and process parameters as well as to missing comparability. In order to automatize previously user-dependent processes in the analysis of material tests, a modular database management system, called idCarl, has been developed. This system places a module as analysis pipeline between the experimental machine and the database. The database management system can be expanded with diverse modules, enabling the generation of user-independent data, which are fed automatically into the database. To provide an example, a module is applied to the common procedure of tensile testing based on DIN EN ISO 6892 and CWA 15261-2. The module determines automatically Young’s modulus and other parameters derived thereof. The method for determining the measurement uncertainties of the Young’s modulus is improved and compatibility with the “Guide to the expression of uncertainty in measurement” (GUM) is achieved. The existing method in ISO and CWA standards provides in some cases an underestimation of about 112 %.
摘要 科学和经济领域的数据流正日益自动化。与以往依赖用户的分析相比,这具有各种优势,在以往的分析中,不同的人对相同的结果进行不同的分析。尽管这些差异仅在一定程度上存在,但它们可能导致对基本材料和工艺参数的错误估算,以及可比性的缺失。为了使以前依赖用户的材料试验分析过程自动化,我们开发了一个模块化数据库管理系统 idCarl。该系统在试验机和数据库之间放置了一个模块作为分析管道。数据库管理系统可通过不同的模块进行扩展,从而生成与用户无关的数据,并自动输入数据库。举例来说,该模块适用于基于 DIN EN ISO 6892 和 CWA 15261-2 标准的拉伸试验常用程序。该模块可自动确定杨氏模量及其衍生的其他参数。杨氏模量测量不确定度的确定方法得到了改进,并实现了与 "测量不确定度表达指南"(GUM)的兼容。ISO 和 CWA 标准中的现有方法在某些情况下会低估约 112%。
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引用次数: 0
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Materials Testing
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