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INFLUENCE OF HEAT TRANSFER COEFFICIENT ON QUENCHING PROCESSES SIMULATION 传热系数对淬火过程模拟的影响
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3510
I. Danev, D. Gospodinov, R. Radev, M. Ilieva
Currently, heat treatment is the most common and effective method for changing the properties of metals and their alloys. Ferrous alloys most often are heat treated and the most commonly used process of heat treatment is the quenching. At quenching the final structure and material’s properties are formed during the fast cooling process. Therefore, the correct choice of cooling conditions is critical for quality of quenched parts. The simulation of quenching is one of the modern approaches for researching the cooling processes. In order to obtain reliable results, the correct input data for simulation are crucial. It is commonly accepted that the heat transfer coefficient (HTC) plays most significant influence on the simulation results. Meanwhile in the specialized literature there are quite different values of HTC even at equal cooling conditions and a few data regarding its influence on the simulation results. The aim of this paper is to determine to what extent the results obtained after simulation of quenching processes are influenced by HTC. Samples of different dimensions and ratios between length and diameter (L/D), made of medium carbon steel (C45 EN 10083), were studied. Results for the influence of HTC together with geometry of the quenched parts, especially samples with different ratio length/diameter (L/D), are presented in the article.
目前,热处理是改变金属及其合金性能的最常见和最有效的方法。铁合金最常进行热处理,最常用的热处理工艺是淬火。淬火时,材料的最终组织和性能是在快速冷却过程中形成的。因此,正确选择冷却条件对淬火件的质量至关重要。淬火模拟是研究冷却过程的现代方法之一。为了获得可靠的仿真结果,正确的仿真输入数据至关重要。一般认为传热系数(HTC)对模拟结果的影响最为显著。同时,在专业文献中,即使在相同的冷却条件下,HTC的数值也相差很大,关于其对模拟结果影响的数据也很少。本文的目的是确定淬火过程模拟后得到的结果在多大程度上受到HTC的影响。对中碳钢(C45 EN 10083)不同尺寸和长径比(L/D)试样进行了研究。文中给出了HTC和淬火件几何形状的影响,特别是不同长径比(L/D)试样的影响。
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引用次数: 0
TRIP STEEL SPECIMEN PREPARATION FOR ADVANCED SEM AND EBSD 高级sem和ebsd的Trip钢试样制备
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3513
O. Ambrož, Š. Mikmeková, Veronika Hegrová, T. Aoyama
Modern scanning electron microscopy (SEM) allows observations of specimens with high surface sensitivity. The surface sensitivity is significantly affected by the accelerating voltages. With the development of the scanning electron microscopy, the requirements for the surface quality of samples increase. Metallographic methods originally intended for light microscopy become insufficient. The problem occurs especially with multiphase materials having a fine-grained structure. The investigated TRIP steel consists of a ferritic-bainitic matrix, retained austenite and martensite phases. The sizes of the smallest phases are nanometer units. The volume of residual austenite was determined by X-ray diffraction. The basic preparation of all tested samples involved conventional metallographic grinding and very fine mechanical polishing. One sample was analysed in this state. Other samples were subsequently chemically polished, electropolished and chemical-mechanically polished. The specimens were observed in the SEM using a SE and a BSE detector at low energies immediately after the preparation. An EBSD was performed in the same areas to characterize the retained austenite. Topographical imaging by special AFM, integrated into the SEM, demonstrated that the mechanical polishing results in surface deformation and residual austenite is transformed. All other methods have their specifics and for modern sensitive SEM instruments it is necessary to optimize individual procedures.
现代扫描电子显微镜(SEM)允许观察具有高表面灵敏度的标本。加速电压对表面灵敏度有显著影响。随着扫描电镜技术的发展,对样品表面质量的要求越来越高。最初用于光学显微镜的金相方法变得不够。这个问题尤其发生在具有细晶粒结构的多相材料上。所研究的TRIP钢由铁素体-贝氏体基体、残余奥氏体和马氏体相组成。最小相的尺寸为纳米单位。用x射线衍射法测定残余奥氏体的体积。所有测试样品的基本制备都涉及常规金相磨削和非常精细的机械抛光。在这种状态下分析了一个样本。其他样品随后进行化学抛光、电抛光和化学机械抛光。制备后立即使用SE和BSE检测器在低能量下对样品进行扫描电镜观察。在同一区域进行EBSD以表征残留的奥氏体。利用专用原子力显微镜(AFM)与扫描电镜(SEM)结合的形貌分析表明,机械抛光导致表面变形,残余奥氏体发生转变。所有其他方法都有其特点,对于现代灵敏的扫描电镜仪器,有必要优化个别程序。
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引用次数: 1
LASER CUTTING OF RARE-EARTH NdFeB PERMANENT MAGNETS 稀土钕铁硼永磁的激光切割
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3514
I. Belyaev, D. Serov, A. Kireev, A. Kutepov, A. Lyukhter, A. Zhokin, V. Rykov, N. Kolchugina
The possibility of laser cutting of rare-earth NdFeB permanent magnets is studied. An industrial Navigator KS-5VDM1-3 laser complex (VNITER, Russia) is used. Blanks of sintered permanent magnets intended for cutting were 10, 4.5, 3, and 2 mm thick. The cutting was performed in air. The used cutting conditions ensure the cutting of a blank for one pass. The cutting rate was varied in wide range. The magnetic properties of studied blanks were determined via measuring the magnetization reversal curves recorded before and after cutting. Changes in the alloy structure during laser cutting were estimated by X-ray diffraction analysis. The decrease in the magnetic properties during laser cutting was found to depend on the blank thickness. The thinner the magnet blank, the lower the decrease in its magnetic properties. The causes for the decrease in the magnetic properties of NdFeB permanent magnet blanks during laser cutting are local changing the phase composition of alloy and decrease in the degree of texture of blanks. The losses of magnetic properties can be minimized by optimization of laser cutting conditions.
研究了激光切割稀土钕铁硼永磁体的可能性。使用工业导航员KS-5VDM1-3激光复合体(VNITER,俄罗斯)。用于切割的烧结永磁体坯有10、4.5、3和2毫米厚。切割是在空气中进行的。所使用的切削条件保证了一次切削一次毛坯。切削速率变化幅度较大。通过测量切割前后记录的磁化反转曲线,确定了所研究毛坯的磁性能。通过x射线衍射分析估计了激光切割过程中合金组织的变化。发现激光切割过程中磁性能的下降与毛坯厚度有关。磁体坯料越薄,其磁性能的下降幅度越小。导致钕铁硼永磁坯体在激光切割过程中磁性能下降的原因是合金相组成的局部改变和坯体织构程度的降低。通过优化激光切割条件,可以最大限度地降低材料的磁性损失。
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引用次数: 0
FEA analysis of bending stress and deflection in thin steel sheet with reinforcing ribs created by laser treatment 激光加筋薄钢板弯曲应力和挠度的有限元分析
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3533
Oleksandr Kapustynskyi, N. Višniakov
The main objective of the research was to determine the influence of local laser treatment on the process of elastoplastic deflection of the sheets under bending force. FEA modelling results show, that the location of the treated area and the number of laser tracks on a thin-walled sheet surface had a large influence on the stress distribution and sheet deflections during bending. The FEA analysis of equivalent Von-Mises stresses, normal stresses, deflection of steel sheets and applied bending forces confirms that the steel samples with the laser-treated area have greater resistance against bending and reduced deflection under the same bending forces. FEA investigation shows that a greater strengthening effect on thin-walled steel sheets could be achieved through the application of double-sided laser treatment of the sheet surface in comparison with untreated or one-side treated steel sheets.
研究的主要目的是确定局部激光处理对弯曲力作用下板材弹塑性变形过程的影响。有限元模拟结果表明,薄壁薄板表面处理区域的位置和激光轨迹的数量对弯曲过程中的应力分布和薄板挠度有较大的影响。对等效Von-Mises应力、法向应力、钢板挠度和施加的弯曲力进行有限元分析,证实了在相同的弯曲力下,激光处理区域的钢样品具有更大的抗弯曲能力和更小的挠度。有限元分析表明,与未经处理或单面处理的薄壁钢板相比,双面激光处理对薄壁钢板的强化效果更好。
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引用次数: 0
impact of casting speed on mould wall TEMPERATURE FIELD 浇注速度对模壁温度场的影响
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3457
L. Polcar, R. Pyszko
Production of new steel grades and growing demands on productivity require an increasing understanding of heat transfer during the continuous casting process. This work is focused on a mould which has a great influence on the casting process and the final quality of billets. Casting speed has to be adapted to the steel parameters and the format of the product. The temperature field of the mould changes with the casting speed. From the temperature field, the contact of the solid shell with the mould insert and the intensity and symmetry of heat removal can be deduced. Temperature measurements were conducted in the mould walls on site. It was found that increasing the casting speed reduced the temperature gradient in the longitudinal direction and caused a decrease in the unevenness of the temperature field in the transverse direction, which was expressed by the so-called thermal axis. A percentage increase in mould temperatures that followed the increase in casting speed, exhibited close to a linear dependency on the distance from the mould top. Based on the presented data, the increase in casting speed caused a more uniform temperature field in the mould insert, which is related to a more uniform heat removal from the billet.
新钢种的生产和对生产率的日益增长的要求要求对连铸过程中的传热有越来越多的了解。本文主要研究了一种对铸造工艺和钢坯最终质量有很大影响的模具。浇注速度必须与钢的参数和产品的形状相适应。结晶器温度场随浇注速度的变化而变化。由温度场可以推导出实体壳与模具镶件的接触、排热的强度和对称性。现场对模具壁进行了温度测量。结果发现,提高浇注速度使纵向温度梯度减小,使横向温度场的不均匀性减小,即所谓的热轴。随着铸造速度的增加,模具温度的百分比增加与离模具顶部的距离呈线性关系。根据所提供的数据,铸造速度的提高使结晶器内的温度场更加均匀,这与钢坯更均匀地散热有关。
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引用次数: 0
HEAT TREATMENT PROCESSES OF STEEL-SMELTING SLAGS IN THE RECOVERY ENVIRONMENT 钢渣在回收环境下的热处理工艺
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3439
S. Matkarimov
In article questions of development, low-waste technologies of processing of steel-smelting slag are considered, gland allowing by extraction and its connections from steel-smelting slag to receive additional raw materials for production became, and the remains to use in building industry. Complex processing of steelsmelting slags as the main way of engineering-ecological development of society was offered in the mid-sixties the past century, generally by scientists from the CIS countries. Based on their application, it was supposed not only it is most useful to use the consumed raw material resources, but also to try to process formed entirely waste. Thus present at a firm oxidizer iron assimilates with metal and promotes degree increase complex raw materials use. In this case, as firm oxidizers can be used, oxides the connections of iron taken from utilized slags of joint-stock company "Uzbeksteel."
本文讨论了炼钢渣低废处理技术的发展问题,从炼钢渣中提取和连接废渣,可以获得额外的生产原料,剩余物可以用于建筑工业。炼钢渣的复合处理作为社会工程生态发展的主要途径是在上世纪60年代中期由独联体国家的科学家提出的。基于它们的应用,提出了利用已消耗的原料资源的最大限度利用,并尝试对形成的废物进行完全处理的设想。从而存在于牢固的氧化剂铁与金属的同化和促进程度增加复合原料的使用。在这种情况下,作为可以使用的坚固氧化剂,氧化从“乌兹别克钢铁”股份公司的废渣中提取的铁的连接。
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引用次数: 1
EFFECT OF AlTi3B1 INOCULANT ON THE MICROSTRUCTURE AND HARDNESS OF THE AlCu4Mg1 ALLOY AlTi3B1孕育剂对AlCu4Mg1合金显微组织和硬度的影响
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3612
Irena Lysoňková, J. Svobodová, I. Hren
Aluminum alloy EN AW-2024 (AlCu4Mg1 - dural) – Al-Cu-Mg group is one of the most used alloys from this group, which achieves considerable strength after heat treatment. It is an alloy with higher and high strength, but low corrosion resistance. The mechanical properties of Al-Cu alloys depend on whether Cu is present in the aluminum solid solution α in the form of a spheroid, possibly as dispersed particles or if it is forming a network at grain boundaries. The paper is focused on the evaluation (microstructure, grain size, phase fraction, hardness) of this particular alloy using AlTi5B1 inoculant in various concentrations to refine the alloy grain. The heat treatment of the alloy was also performed in the experiment to increase the mechanical properties. Inoculation of aluminum alloys is performed to improve the mechanical and technological properties of the material. In the case of inoculation, this improvement is mainly due to an increase in chemical and structural homogeneity and a decrease in the tendency to segregate individual elements. Optical microscopy and image phase analysis was used to observe the microstructure, which evaluated the microstructure and its changes depending on the content of the inoculant and also the effect of heat treatment in the combination of different amount of inoculant. It is generally known that AlTi5B1 acts in certain amounts to refining the alloy grain. Our work is based on the knowledge of the behaviour of different concentrations of inoculant in this particular AlCu4Mg1 alloy and responds to the requirement from practice. We achieved the best results with a concentration 3 wt% of AlTi5B1. For the other concentrations, the results were almost comparable and not much worse than for the concentration with the best results. It doesn't make sense to add more than 3 wt% of inoculant in this case.
铝合金EN AW-2024 (AlCu4Mg1 -硬膜)- Al-Cu-Mg族是这类合金中应用最多的一种,经热处理后具有相当的强度。它是一种高强度、高强度的合金,但耐腐蚀性较低。Al-Cu合金的力学性能取决于Cu是否以球体的形式存在于铝固溶体α中,可能是分散的颗粒,或者是否在晶界处形成网络。采用不同浓度的AlTi5B1孕育剂细化合金晶粒,对该合金的显微组织、晶粒尺寸、相分数、硬度进行了评价。为了提高合金的力学性能,还对合金进行了热处理。为提高铝合金的力学性能和工艺性能,对铝合金进行了孕育处理。在接种的情况下,这种改善主要是由于化学和结构同质性的增加和单个元素分离倾向的减少。采用光学显微镜和图像相分析方法对其微观组织进行了观察,评价了微观组织及其随孕育剂含量的变化,以及不同孕育剂用量组合时热处理的效果。众所周知,一定量的AlTi5B1对合金晶粒有细化作用。我们的工作是基于对不同浓度孕育剂在这种特殊的AlCu4Mg1合金中的行为的了解,并响应实践的要求。当AlTi5B1的浓度为3wt %时,我们获得了最好的效果。对于其他浓度,结果几乎是相当的,并不比具有最佳结果的浓度差多少。在这种情况下,添加超过3%的接种剂是没有意义的。
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引用次数: 0
Modification of the hydration processes of alkali activated blast furnace slag 碱活化高炉渣水化工艺的改进
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3455
M. Topinková, J. Vlček, M. Klárová, H. Ovčačíková, P. Maierová, V. Blahůšková
Granulated blast furnace slag exhibits latent hydraulic properties and its binding properties can be evoked by the addition of the alkali activator. Subsequent hydration processes during the setting and hardening processes let to origination of the solid products with the mechanical properties comparable or even better than the product obtained with ordinary Portland cement. The dominant product of the hydration processes is so called C-S-H phase. C-S-H phases are non-crystalline products of hydration with variable composition based on CaO, SiO2 and H2O. C-S-H phases are responsible for good mechanical properties of the hydrated products. The paper deals with the effect of the addition of the synthetically produced C-S-H phases on the hydration processes of granulated blast furnace slag. C-S-H phases were synthesized using the sol-gel method and were added to the granulated slag at the beginning of its hydration with the role of the nuclei of the phases responsible for strength of the final hydrated products. The mechanical properties as well as the development of the porous structure of hydrated products were used for the evaluation of the effect of the nuclei addition on the hydration process. It was proved that the addition of the synthetically prepared C-S-H nuclei has a positive effect on the development of the mechanical properties of alkali activated blast furnace slag, especially during the initial period of hardening.
粒状高炉矿渣表现出潜在的水力特性,加入碱性活化剂可诱发其结合特性。在凝结和硬化过程中,后续的水化过程使所生成的固体产品具有与普通硅酸盐水泥相当甚至更好的力学性能。水化过程的主要产物是所谓的C-S-H相。C-S-H相是由CaO、SiO2和H2O组成的非晶态水化产物。C-S-H相是水合产物具有良好力学性能的主要原因。研究了合成的C-S-H相的加入对粒状高炉渣水化过程的影响。采用溶胶-凝胶法合成了C-S-H相,并在矿渣水化初期加入C-S-H相,其相核的作用决定了最终水化产物的强度。通过水化产物的力学性能和多孔结构的发展来评价核加入对水化过程的影响。实验证明,合成的C-S-H核的加入对碱活化高炉渣力学性能的发展有积极的影响,特别是在硬化初期。
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引用次数: 0
Fracture behaviour, structure and mechanical properties of A508 Gr. 4N Class 3 Grade Steel A508 Gr. 4N 3级钢的断裂行为、组织和力学性能
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3534
L. Kander, S. Stejskalová, P. Čížek
Recent increase in output of nuclear power plant has been attained by enlargement of most major components such as pressure vessels. Such large components have almost reached a size limit from the points of manufacturing capacity. In order to solve this problem, it must be beneficial to apply by use of material of higher strength, which brings reduction of pressure vessel thickness and weight A508 Grade 4N is a high nickel pressure vessel steel with relatively high yield strength and a relatively low transition temperature. A study was undertaken to evaluate conventional as well as unconventional material properties of forging made of in our institute. This paper describes results of mechanical properties, structure and fracture behavior including nil-ductility transition temperature.
近年来,核动力装置的产量增加主要是由于压力容器等主要部件的扩大。从制造能力的角度来看,如此大型的部件几乎已经达到了尺寸极限。为了解决这一问题,必须采用更高强度的材料,从而带来压力容器厚度和重量的减轻。A508 4N级是一种高镍压力容器钢,具有较高的屈服强度和较低的转变温度。在我所进行了一项评估常规和非常规锻造材料性能的研究。本文介绍了包括零塑性转变温度在内的力学性能、组织和断裂行为的结果。
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引用次数: 0
Modelling a SAG Grinding System through multiples regressions 通过多元回归对SAG磨削系统进行建模
Pub Date : 2020-01-01 DOI: 10.37904/metal.2020.3665
M. Villanueva, C. Calderon, M. Saldaña, N. Toro
Due to the constant growth of the copper industry, the increase in production costs and complexity in the composition of the feed of the production processes that make up the industry, the analysis of alternatives that improve efficiency by studying the dynamics of the processes represents a significant cost reduction. Then, the generation of analytical models that represent the dynamic behaviour of production processes has the potential to contribute to generating a better understanding of the operating parameters that have a greater impact on the response (s), in addition to identifying operating restrictions and optimal levels of operation. The present work developed a digital model of the SAG milling process by generating multiple regression and quadratic regression models. The relationships between 22 operational variables with production in tons per hour were sampled, and after analysing the impact of the independent variables on the response, water feeding, sump level, percentage of solids in feeding, pebbles and hardness were maintained for fit the analytical models. The multiple linear regression model presents a good fit to the operational data (85.4%), however, the inclusion of the interactions and the quadratic effects of the variables increases the coefficient of determination (93.2%).
由于铜工业的不断发展,生产成本的增加和构成该工业的生产过程的饲料组成的复杂性,通过研究过程的动态来分析提高效率的替代方案代表着显著的成本降低。然后,生成代表生产过程动态行为的分析模型,除了确定操作限制和最佳操作水平外,还可能有助于更好地理解对响应有较大影响的操作参数。本文通过建立多元回归和二次回归模型,建立了SAG铣削过程的数字模型。采样了22个操作变量与产量(吨/小时)之间的关系,并在分析了自变量对响应的影响后,保持了进水,水池液位,进料中固体百分比,卵石和硬度以拟合分析模型。多元线性回归模型与运行数据拟合良好(85.4%),但由于纳入了变量间的相互作用和二次效应,使得决定系数增大(93.2%)。
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引用次数: 1
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METAL 2020 Conference Proeedings
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