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HIGH-TEMPERATURE RHEOMETRY OF BLAST FURNACE SYNTHETIC SLAGS DOPED WITH TiO2 AND TiN 掺钛锡高炉合成渣的高温流变学研究
Pub Date : 2015-07-10 DOI: 10.7494/MAFE.2015.41.1.17
P. Migas, M. Ślęzak
Streszczenie W pracy zaprezentowano wyniki badan przeprowadzone przy uzyciu reometrii wysokotemperaturowej, w oparciu o metode Searle’a. Przeprowadzono analize reologiczną cieklych systemow CaO-SiO 2 -Al 2 O 3 -MgO-TiO 2 slags domieszkowanych TiN,w zakresie 0,1 -0,7 ulamka objetościowego TiN. Badania przeprowadzono w temperaturze 1310-1500 o C, ktora jest chatakterystyczna dla strefy wysokich temperatur wystepującej w wielkim piecu. Glownym celem prowadzonych badan byla analiza mozliwości pomiarow lepkości dla ukladow heterogenicznych (nietypowych dla zastosowan przemyslowych), a nie zdefiniowanie parametrow reologicznych calkowicie cieklych systemow zuzlowych – ktore wykazują podobienstwo do cieczy idealnej Newtona. Slowa kluczowe: lepkośc zuzla, reometria wysokotemperaturowa, azotek tytanu, reologia Abstract The development of the methodology of rotational measurements with a high temperature rheometer using Searle’s method have been conducted. The rheological analysis of liquid systems - CaO-SiO 2 -Al 2 O 3 -MgO-TiO 2 slags, and solid particles of titanium nitride –TiN are presented, within a range of 0.1-0.7 of volume fraction of TiN. The measurements were conducted at a range between 1310-1500 o C, which is typical for high temperature zones in the blast furnace. The main objective of the study was to analyse the possibilities for viscosity measurements in heterogenic systems (not standard within industrial practice), rather than to determine the rheological character of those systems totally liquid blast furnace slags are similar to ideally viscous Newtonian bodies. Key words: slag viscosity, high-temperature  rheometry, titanium nitride, rheology
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引用次数: 1
Hot cracking of nickel-based superalloy turbine blade 镍基高温合金涡轮叶片的热裂
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.4.181
Ł. Rakoczy, L. Tuz, K. Pańcikiewicz
The aim of this study was to present the hot cracking behavior of a blade originating from a turbine blade segment. The crack was induced by a gas tungsten arc welding process, and the research material was a MAR-M247 nickel based superalloy. This alloy is considered to be difficult to weld because of its high tendency to crack. Light microscopy and scanning electron microscopy show the occurrence of cracking in the melted zone, heat-affected zone, and base alloy. A scanning electron microscopy investigation revealed that cracks are propagated by stresses and liquation of the low temperature constituent.
本研究的目的是提出热裂行为的叶片起源于涡轮叶片段。采用钨气弧焊诱发裂纹,研究材料为MAR-M247镍基高温合金。这种合金被认为是难以焊接的,因为它很容易开裂。光镜和扫描电镜显示,在熔化区、热影响区和基体合金中出现了裂纹。扫描电镜研究表明,裂纹是通过应力和低温成分液化而扩展的。
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引用次数: 0
An assessment of the effectiveness of physical curing methods of molding sand bonded by binders based on starch and aluminosilicates
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.3.133
K. Kaczmarska, B. Grabowska, D. Drożyński, Ž. Kurleto, Ł. Szymański
In this study, based on results of determination selected properties of moulding sand such as permeability, tensile strength and wear resistance, the effectiveness of curing methods: by conventional heating and by innovative of microwave curing were compared. The tested moulding sand used to research was composition of silica sand with a commercial binder in the form of Albertine F/1 (Huttenes Albertus). This binder is a mixture of swellable in water starch derivatives and aluminosilicates. Binding in the moulding sand was occurred by evaporation of the solvent from samples (water). Based on the obtained results were showed a dependence of the properties of moulding sand and selected methods of physical cure, especially after 1 and 4 hours of cured samples storage. However, after 24 hours of samples storage, as apparent from the analysis of the obtained results, both used curing methods are almost the same effective, and marked differences in the properties of the moulding sands were located in the range of measurement uncertainty. Using electromagnetic waves in the microwave range was possible significantly reduce the time of curing and the energy of the drying process.
通过对型砂渗透性、抗拉强度、耐磨性等性能的测定,比较了常规加热和微波固化两种固化方法的有效性。用于研究的测试型砂是硅砂与Albertine F/1 (Huttenes Albertus)形式的商业粘合剂的组合。这种粘合剂是一种可在水中膨胀的淀粉衍生物和硅酸盐铝的混合物。型砂中的粘结是由样品(水)的溶剂蒸发而产生的。结果表明,型砂的性能与所选择的物理固化方法有关,特别是在固化后1和4小时的样品储存后。然而,在样品储存24小时后,从所获得的结果分析中可以看出,两种养护方法的效果几乎相同,并且型砂性能的显着差异位于测量不确定度范围内。在微波范围内使用电磁波可以显著减少固化时间和干燥过程的能量。
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引用次数: 2
FTIR METHOD IN STUDIES OF THE RESOL TYPE PHENOL RESIN STRUCTURE IN THE AIR ATMOSPHERE IN SOME TIME INTERVALS 用红外光谱法研究了树脂型苯酚树脂在空气气氛中一定时间间隔内的结构
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.3.107
A. Bobrowski, B. Grabowska
The paper presents the results of the structural type studies of resol phenolic resin used for the preparation of moulding and core sands exposed to the air. The FTIR study was carried out using a transmittance technique. Recorded changes in the IR spectra of resin can indicate a progressive polycondensation process, the consequence of which, among others, are changes in the aromatic rings of methylene bridges.
本文介绍了用于制备暴露在空气中的型砂和芯砂的酚醛树脂的结构类型研究的结果。FTIR研究采用透射技术进行。在树脂的红外光谱记录的变化可以表明一个渐进的缩聚过程,其结果,除其他外,是在亚甲基桥芳香环的变化。
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引用次数: 9
NUMERICAL ANALYSIS OF ROD UNIAXIAL TENSION CONSIDERING THERMO-MECHANICAL COUPLING EFFECT 考虑热-力耦合效应的杆单轴拉伸数值分析
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.4.189
Hongnam Nguyen, T. Niezgoda, A. Derewońko, J. Jachimowicz
This paper presents numerical analyses of uniaxial tension tests on rods made of a material with elasticplastic characteristics with mapping the temperature fields generated in the fields of plastic strains. The use of thermo-mechanical coupling algorithms implemented in CAE programs that enable us to enter the parameters of materials dependent on temperature and used to visualize the damage of the samples is presented. The numerical models were validated with experimental research.
本文对具有弹塑性特性的材料制成的杆进行了单轴拉伸试验,并绘制了塑性应变场产生的温度场。介绍了在CAE程序中实现的热-机械耦合算法的使用,该算法使我们能够输入依赖于温度的材料参数,并用于可视化样品的损伤。通过实验研究对数值模型进行了验证。
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引用次数: 0
STRUCTURAL CONSTRUCTION OF THE HARDENERS WITH DIFFERENT HARDENING RATES INTENDED FOR GEOPOLIMER BINDER SYSTEMS USED FOR THE PREPARATION OF MOULDING SANDS 用于型砂制备的地高聚物粘结剂体系中具有不同硬化速率的固化剂的结构构造
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.3.115
A. Bobrowski, B. Grabowska, K. Kaczmarska
The paper presents the results of structural investigations of hardeners series of different hardening rate of the geopolymer Geopol, manufactured by the Sand-Team Company. Studies showed that these hardeners have the similar chemical structure and that the hardening rate of the binder depends on the proper selection of the proportions of respective components.
本文介绍了Sand-Team公司生产的不同硬化速率的地聚合物Geopol系列固化剂的结构研究结果。研究表明,这些固化剂具有相似的化学结构,粘结剂的硬化速率取决于适当选择各自组分的比例。
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引用次数: 0
THEORETICAL ANALYSIS OF THE AZ31 MAGNESIUM ALLOY DEFORMATION PROCESS BY A MODIFIED METHOD OF ANGULAR EXTRUSION 改进角挤压法对az31镁合金变形过程的理论分析
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.3.123
T. Bajor, M. Krakowiak, S. Berski
The paper presents the results of the numerical modeling of a chosen magnesium alloy deformation process by a modified method of angular extrusion (AE). The research was made using a die with a circular cross-section, where the channels were arranged at right angles relative to each other. The modification concerned the differing values of applied unit strain obtained by changing the material enter/exit diameter ratio. The extrusion process was analyzed for several temperature-velocity variants. The aim of this work was to determine the most favorable conditions of the extrusion process that result in the most uniform stress and strain distribution in the material.
本文介绍了采用改进的角挤压法对某镁合金变形过程进行数值模拟的结果。这项研究是使用一个圆形横截面的模具进行的,其中通道以相对于彼此的直角排列。这种修正涉及通过改变材料进出直径比获得的不同单位应变值。对几种温度-速度变化的挤压过程进行了分析。这项工作的目的是确定挤压过程中最有利的条件,从而使材料中的应力和应变分布最均匀。
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引用次数: 0
Mechanical properties and structure evolution of the AZ91 magnesium alloy after hot rolling and annealing AZ91镁合金热轧退火后的力学性能与组织演变
Pub Date : 2015-01-01 DOI: 10.7494/MAFE.2015.41.3.143
B. Sułkowski, G. Boczkal
The AZ91 magnesium alloy was processed up to 87.5% of total thickness reduction in several thermodynamic routes, consisted of hot rolling and intermediate annealing. The hot-rolling process was performed at a high strain rate equal to 1.6 s−1 and at a temperature of 430°C. The intermediate annealing was performed at 430°C for 15 minutes after each route. It was found that, during hot rolling, the hardness of the material increased from 32 HV to 40 HV, and the structure investigations showed a huge amount of twins formed inside the grains (which were not observed after annealing). Tensile tests have shown strong anisotropy in mechanical properties of the “as-rolled” samples dependent on the orientation between tension direction (TD) and rolling direction (RD). The samples with TD perpendicular to RD proved higher ultimate tensile strength (UTS) and (on the other hand) worse plastic properties as compared to the samples with TD parallel to RD. The annealing has an effect on the reduction of mechanical properties anisotropy. X-ray investigations have shown texture changes from the basal type with the additional (0001) component for “as-rolled” samples to the texture with the main (0001) component for annealed samples. The texture changes had a great impact on the anisotropy of mechanical properties of the investigated AZ91 magnesium alloy.
对AZ91镁合金进行了热轧和中间退火两种热处理工艺,使其总厚度减少87.5%。热轧过程在高应变速率为1.6 s−1,温度为430℃的条件下进行。每条路线结束后,在430℃下进行中间退火15分钟。结果表明,在热轧过程中,材料的硬度从32 HV提高到40 HV,组织研究表明,晶粒内部形成了大量的孪晶(退火后未观察到)。拉伸试验表明,随拉伸方向(TD)和轧制方向(RD)之间的方向不同,轧制态试样的力学性能具有很强的各向异性。与TD平行于RD的样品相比,TD垂直于RD的样品具有更高的极限拉伸强度(UTS),但塑性性能较差。退火对力学性能各向异性的降低有影响。x射线调查显示,织构从“轧制”样品中含有额外(0001)成分的基本类型转变为退火样品中含有主要(0001)成分的织构。织构的变化对AZ91镁合金力学性能的各向异性有很大影响。
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引用次数: 2
Studies on obtaining Cu-CNT composites by continuous casting method 连铸法制备Cu-CNT复合材料的研究
Pub Date : 2014-11-18 DOI: 10.7494/MAFE.2014.40.2.83
P. Kwaśniewski, G. Kiesiewicz
The progress of civilization force that we look for new materials with higher exploitation properties that can be used in different types of installations and will allow to increase their technological potential. One of the research trends is concentrated on the search of new materials with the above standard electrical conductivity, mechanical and rheological properties, higher thermal resistance and technological properties, all in comparison to pure copper. One of the ideas of such material is composite produced from copper and high quality carbon materials (CNT’s or graphene). Regarding to the above, presented paper refers to the research results concentrated on the metallurgical synthesis of Cu-CNT’s materials obtained with the use of the continuous casting method. Within this paper research works over the synthesis method and obtained material characterization, for electrical, mechanical and structural properties (for both as cast and after cold drawing tempers) are shown.
文明的进步迫使我们寻找具有更高开发性能的新材料,这些材料可以用于不同类型的装置,并允许增加其技术潜力。研究趋势之一是集中于寻找与纯铜相比具有上述标准电导率,机械和流变性能,更高的热阻和技术性能的新材料。这种材料的想法之一是由铜和高质量的碳材料(碳纳米管或石墨烯)制成复合材料。鉴于此,本文参考了利用连铸法对Cu-CNT材料进行冶金合成的研究成果。在本文中,研究工作对合成方法和获得的材料特性,电气,机械和结构性能(铸态和冷拔后回火)进行了展示。
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引用次数: 4
Microstructure and mechanical behavior of a CO2 laser and TIG welded 904L steel CO2激光与TIG焊接904L钢的组织与力学行为
Pub Date : 2014-11-18 DOI: 10.7494/MAFE.2014.40.2.69
Z. Bogdanowicz, P. Jóźwik, B. Nasiłowska
The paper presents the analysis of structural research, micro-hardness and mechanical properties of the base material which is steel 904 L and joints made with CO 2 laser beam and TIG method. The analysis of the equilibrium system created in the Thermo-Calc programme based on chemical composition shows a dominancy of austenite with of Fe α additions, phase σ, P and Laves' and M 23 C 6 and Cr 9 Mo 21 Ni 20 carbides. EBSD (Electron backscatter diffraction) research done by using electron scanning microscope confirmed the presence of pure austenite.
本文对以904l钢为基材,采用co2激光束和TIG法制备的接头进行了组织研究、显微硬度和力学性能分析。基于化学成分的热钙程序建立的平衡体系分析表明,奥氏体以Fe α的加入、σ、P和Laves’相、m23c6和cr9mo21ni20碳化物为主。利用电子扫描显微镜进行电子背散射衍射(EBSD)研究证实了纯奥氏体的存在。
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引用次数: 11
期刊
Metallurgy and Foundry Engineering
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