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Electromagnetical and ultrasonic characterizations of concretes subjected to internal swelling reactions 受内膨胀反应影响的混凝土的电磁学和超声波特性分析
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-22 DOI: 10.1016/j.ndteint.2024.103217
X. Dérobert , G. Villain , S. Palma-Lopes , V. Bouvard-Coconet , J.M. Decitre , J. Jabbour , S. Qu , J.L. Geffard , O. Durand , G. Gugole , O. Abraham

Among pathologies of reinforced concrete structures, internal swelling reactions (ISR), including alkali-aggregate reaction and delayed ettringite formation, are at the origin of cracks and major disorders due to rebar corrosion. Visual evaluation of crack density combined to non-destructive testing techniques can be used to characterize the global swelling and then give some structural diagnosis. For the last ones, an intermediate step (assimilated to a calibration step) can be performed at laboratory to evaluate the sensitivity of electromagnetic, electrical and ultrasonic properties of concretes subject to ISR.

This present study focuses on such characterizations of concrete samples presenting different levels of ISR and for several water content. Numerous samples have been extracted from mock-ups representative of two massive concrete structures, affected one by alkali-aggregate reaction and the other by delayed ettringite formation, and conditioned in homogeneous and controlled conditions. After describing the experimental campaign, results are shown and commented.

在钢筋混凝土结构的病变中,内部膨胀反应(ISR),包括碱-骨料反应和延迟蚀变石形成,是钢筋锈蚀导致裂缝和重大病变的根源。裂缝密度的目测评估与非破坏性检测技术相结合,可用于确定整体膨胀的特征,然后给出一些结构诊断。对于最后一种情况,可在实验室进行中间步骤(相当于校准步骤),以评估受 ISR 影响的混凝土的电磁、电气和超声波特性的敏感性。从两个具有代表性的大体积混凝土结构模型中提取了大量样品,其中一个受到碱-集料反应的影响,另一个受到延迟蚀变体形成的影响,并在均匀和受控的条件下进行了调节。在介绍了实验活动之后,对结果进行了说明和评论。
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引用次数: 0
Terahertz spectroscopy and effective medium theory for thickness measurement of adhesive bonds 太赫兹光谱和有效介质理论用于测量粘合剂的厚度
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-22 DOI: 10.1016/j.ndteint.2024.103216
Ji-Yang Zhang , Jiao-Jiao Ren , Li-Juan Li , Dan-Dan Zhang , Jian Gu , Jun-Wen Xue , Qi Chen

This study deals with the characterization of multilayer adhesive structures via terahertz waves, particularly focusing on inversion analysis of the adhesive layer thickness. Terahertz-time-of-flight (THz-TOF), sensitive to the dielectric properties of materials, serves as an excellent device for non-destructive evaluation. Further, the transfer matrix method is introduced to simulate THz propagation through layered materials with various optical properties. An improved model iteration approach and particle swarm optimization algorithm are employed to effectively determine the adhesive layer thickness. This methodology utilizes effective medium theory (EMT), specifically for adhesive penetration into the cushion, thereby enhancing the thickness measurement accuracy. Among the various EMT models, the Lorentz-Lorenz (L-L) model is commonly regarded as the most effective one. An objective function based on combining the Pearson correlation coefficient and the root mean square error is proposed to refine the iterative inversion process. The results of this approach have been benchmarked with traditional THz-TOF calculations and computed tomography imaging, revealing that the proposed methodology is consistent with CT findings and outperforms conventional THz-TOF calculations.

本研究涉及通过太赫兹波表征多层粘合剂结构,尤其侧重于粘合剂层厚度的反演分析。太赫兹飞行时间(THz-TOF)对材料的电介质特性非常敏感,是进行无损评估的绝佳设备。此外,还引入了传递矩阵法来模拟太赫兹在具有不同光学特性的层状材料中的传播。采用改进的模型迭代法和粒子群优化算法来有效确定粘合层厚度。该方法利用有效介质理论 (EMT),特别是针对粘合剂渗入衬垫的情况,从而提高了厚度测量的准确性。在各种 EMT 模型中,洛伦兹-洛伦兹(L-L)模型通常被认为是最有效的模型。我们提出了一种基于皮尔逊相关系数和均方根误差的目标函数,以完善迭代反演过程。该方法的结果已与传统的 THz-TOF 计算和计算机断层扫描成像进行了基准比较,结果表明所提出的方法与 CT 结果一致,并且优于传统的 THz-TOF 计算。
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引用次数: 0
TDOA-based localization of cracking sound events with minimal-error microphone subsets 利用最小误差麦克风子集进行基于 TDOA 的破裂声事件定位
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-20 DOI: 10.1016/j.ndteint.2024.103211
Georg Karl Kocur, Bharath Kumar, Bernd Markert

We present a method based on the time difference of arrival (TDOA) and index minimal-error subsets of microphones to localize sudden cracking sound events, which appear somewhere in flax-fiber reinforced concrete specimens. Validation tests with small-scale pendulum impacts and known impact locations were carried out. Error estimation was performed and error ellipses were calculated. Microphone subsets leading to the smallest localization error were indexed. We validated the localization accuracy against localization results calculated using the delay-and-sum beamforming technique. Further, tension tests on concrete specimens were performed until failure; crack patterns were recorded by photogrammetry. The cracking sound events were localized. With the good match between TDOA-based localization results and crack patterns, we demonstrate that the proposed localization procedure is reliably applicable for real-time localization of concrete cracking.

我们提出了一种基于到达时间差(TDOA)和麦克风最小误差子集索引的方法,用于定位亚麻纤维钢筋混凝土试样中某处出现的突然开裂声音事件。利用小规模摆锤撞击和已知撞击位置进行了验证测试。对误差进行了估计,并计算出误差椭圆。对定位误差最小的麦克风子集进行了索引。我们根据使用延迟和波束成形技术计算出的定位结果验证了定位精度。此外,我们还对混凝土试件进行了拉伸试验,直至其失效;并通过摄影测量法记录了裂纹形态。裂纹声事件被定位。由于基于 TDOA 的定位结果与裂纹图案之间的良好匹配,我们证明了所提出的定位程序可可靠地用于混凝土裂纹的实时定位。
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引用次数: 0
An efficient method for water content estimation of building materials from spectral reflectance 利用光谱反射率估算建筑材料含水量的高效方法
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-17 DOI: 10.1016/j.ndteint.2024.103214
Bikram Koirala, Paul Scheunders

We propose a nondestructive methodology to accurately estimate the water content of building materials from spectral reflectance in the shortwave infrared. The water content of a wet sample is estimated from the relative position of its reflectance spectrum on the curve between 2 reference spectra with known water content. By design, the approach is invariant to variations in illumination and acquisition conditions. Validation is done on datasets of clay powders and bricks. The experimental results provide confirmation of the effectiveness of the proposed method.

我们提出了一种通过短波红外光谱反射率准确估算建筑材料含水量的无损方法。湿样品的含水量是根据其反射光谱在两个已知含水量的参考光谱之间曲线上的相对位置估算出来的。根据设计,该方法不受光照和采集条件变化的影响。在粘土粉和砖块的数据集上进行了验证。实验结果证实了所提方法的有效性。
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引用次数: 0
Ice matrix composites for Cryo-ultrasonic testing 用于低温超声波测试的冰基复合材料
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-17 DOI: 10.1016/j.ndteint.2024.103215
Kaden C. Wells , Francesco Simonetti , Christian Peco , Andrea P. Argüelles

Cryo-ultrasonic testing utilizes polycrystalline ice coupling to enable the inspection of metallic components with complex shape. The relatively high velocity of compressional waves in ice (approximately 4000 m s−1) and its ability to support the propagation of shear waves, significantly strengthen the ultrasonic transmission through curved interfaces over conventional water coupling. This paper explores the possibility of further enhancing the ultrasonic properties of ice by dispersing solid particles in water before it is frozen. Complex physicochemical phenomena occur when aqueous dispersions freeze which can lead to a solid material with microstructural characteristics that may be unfavorable to the propagation of ultrasonic waves. Here, these effects are controlled to produce a composite material consisting of alumina nanoparticles in an ice matrix. The composite exhibits compressional and shear wave velocities of approximately 4800 m s−1 and 2700 m s−1 , respectively. Importantly, the mass density of the material is more than twice as large as the density of water. Finally, it is shown that a phenomenon similar to a glass transition occurs during freezing which results in low ultrasonic attenuation when the temperature approaches – 100 °C.

低温超声波测试利用多晶冰耦合来检测形状复杂的金属部件。冰中压缩波的速度相对较高(约 4000 m s-1),并能支持剪切波的传播,与传统的水耦合相比,大大增强了超声波通过弯曲界面的传输能力。本文探讨了通过在冻结前在水中分散固体颗粒来进一步增强冰的超声波特性的可能性。水分散体冻结时会发生复杂的物理化学现象,这可能导致固体材料具有不利于超声波传播的微观结构特征。在这里,我们通过控制这些效应来生产一种由冰基质中的氧化铝纳米颗粒组成的复合材料。这种复合材料的压缩波速和剪切波速分别约为 4800 m s-1 和 2700 m s-1。重要的是,该材料的质量密度是水密度的两倍多。最后,研究表明,在冷冻过程中会出现类似玻璃转变的现象,当温度接近零下 100 °C 时,超声波衰减较低。
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引用次数: 0
Hybrid multi-modal NDE sensing system for in-motion detection and localization of rolling contact fatigue damage in rails 用于轨道滚动接触疲劳损伤的运动中检测和定位的混合多模态无损检测传感系统
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-14 DOI: 10.1016/j.ndteint.2024.103209
Zebadiah Miles , Zi Li , Lei Peng , Yufei Chu , Takuma Tomizawa , Farzia Karim , Bruce Maxfield , Ming Han , Lalita Udpa , Anish Poudel , Sunil Kishore Chakrapani , Yiming Deng

This article presents a multi-modal hybrid-probe approach to nondestructive inspection of RCF cracks and damage in rails. A combination of electromagnetic (EM) and ultrasonic testing (UT) techniques are presented, which allows for complementary physics to be utilized to enhance detection and characterization of surface and sub-surface cracks in a non-contact manner at high speeds. A novel integrated design which combines the motion-induced eddy current (MIEC) effect and ultrasonic Rayleigh surface waves generated and detected using electromagnetic acoustic transducer (EMAT) is presented. The hybrid probe was tested at low speeds to demonstrate an increased damage localization capability. This was carried out using a data registration and fusion approach between the sensing modalities. Finally, the capability of MIEC effect at high-speeds is demonstrated. The results show that the hybrid probe has a high potential for in-motion, high-speed damage detection and characterization in the future.

本文介绍了一种多模式混合探头方法,用于对钢轨中的 RCF 裂纹和损坏进行无损检测。文章介绍了电磁(EM)和超声波检测(UT)技术的结合,利用互补物理学原理,以非接触方式高速增强表面和次表面裂纹的检测和表征。介绍了一种新颖的集成设计,它结合了运动诱导涡流(MIEC)效应和使用电磁声学传感器(EMAT)产生和检测的超声波瑞利表面波。对混合探头进行了低速测试,以证明其具有更强的损伤定位能力。这是在传感模式之间使用数据注册和融合方法实现的。最后,展示了高速时 MIEC 效应的能力。结果表明,混合探头在未来的运动中高速损伤检测和表征方面具有很大的潜力。
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引用次数: 0
Electromagnetic tomography measuring bench for estimating the density of materials 用于估算材料密度的电磁断层扫描测量台
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-12 DOI: 10.1016/j.ndteint.2024.103212
Cyrille Fauchard , Imen Boughanmi , Nabil Benjelloun , Riah Zouheir , Théau Cousin , Bruno Beaucamp , Vincent Guilbert

In the laboratory, the density of pavement cores (cylindrical samples of hot mix asphalt (HMA) material taken from roads) is assessed using an electromagnetic (EM) bench consisting of two ultra-wideband (UWB) Vivaldi antennas and a vector network analyser (VNA). The main objective is to replace the nuclear gauge system currently used in the laboratory as the standard method for this purpose. Firstly, specific antipodal Vivaldi antennas have been adapted from the literature. Their dimensions are 7 × 7 cm with a bandwidth [1.5–15 GHz]. Secondly, a tomographic approach is compared with an analytical solution and a Finite-Difference Time Domain (FDTD) simulation, based on a time-domain estimation of the dielectric under test (DUT) with a single transmitter/receiver configuration. A laboratory validation is presented and the adapted antennas as well as the time domain approach show acceptable results for assessing the dielectric constant on known materials. Finally, to show that the proposed EM bench is a promising non-ionizing solution, the density or equivalent compactness of HMA cylindrical samples is estimated and compared with nuclear gauge results.

在实验室中,使用由两个超宽带(UWB)维瓦尔第天线和一个矢量网络分析仪(VNA)组成的电磁(EM)工作台对路面芯材(从道路上采集的热拌沥青(HMA)材料的圆柱形样本)的密度进行评估。主要目的是取代实验室目前使用的核测量系统,将其作为这方面的标准方法。首先,从文献中选取了特定的对偶维瓦尔第天线。其尺寸为 7 × 7 厘米,带宽为 [1.5-15 GHz]。其次,将层析法与分析法和有限差分时域(FDTD)模拟法进行了比较,后者基于对被测介质(DUT)的时域估计,采用单一发射器/接收器配置。实验室验证结果表明,适配的天线和时域方法在评估已知材料的介电常数方面显示出了可接受的结果。最后,为了证明所提出的电磁工作台是一种有前途的非电离解决方案,对 HMA 圆柱形样品的密度或等效密实度进行了估算,并与核磁测量结果进行了比较。
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引用次数: 0
Baseline-free damage localization in multilayer metallic spherical shell structures using guided wave tomography 利用导波层析成像技术在多层金属球壳结构中进行无基线损伤定位
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-12 DOI: 10.1016/j.ndteint.2024.103213
Wen Liu , Lishuai Liu , Qiang Wan , Yanxun Xiang , Fu-Zhen Xuan

Multi-layer metal spherical shell structure is widely used as the core component of pressure-bearing equipment, deep-sea exploration equipment and other critical areas due to its plane stress uniformity and high specific strength. Its long-term service in complex and harsh environments will inevitably produce a variety of defects and damages, which will affect the safety of the equipment in service. Ultrasonic guided wave inspection is a potential non-destructive testing method, but the multilayer metal bonding structure between the metal and non-metal bonding layer impedance difference is large, resulting in defects located in the internal reflection signal is difficult to propagate to the outer layer with a sensor, the multilayer spherical shell structure itself leads to the complexity of the guided wave propagation characteristics, it is difficult to extract the individual modes of the time information for the defects of the detection and localization. Therefore, in this paper, we propose a probabilistic damage existence imaging method for spherical shell structures and combine it with the virtual time reversal technique to detect and localize the defects on the inner and outer surfaces of multilayered metallic spherical shell structures without benchmarks. The results show that the newly proposed method can realize the accurate localization imaging of internal/external defects of multilayer metal spherical shell structures.

多层金属球壳结构因其平面应力均匀、比强度高,被广泛用作承压设备、深海勘探设备等关键领域的核心部件。其长期服役于复杂恶劣的环境中,难免会产生各种缺陷和损伤,影响设备的服役安全。超声导波检测是一种潜在的无损检测方法,但由于多层金属结合结构中金属与非金属结合层之间阻抗差较大,导致位于缺陷内部的反射信号很难传播到具有传感器的外层,多层球壳结构本身又导致导波传播特性的复杂性,很难提取单个模态的时间信息进行缺陷的检测和定位。因此,本文提出了一种针对球壳结构的概率损伤存在成像方法,并将其与虚拟时间反演技术相结合,在没有基准的情况下对多层金属球壳结构内外表面的缺陷进行检测和定位。结果表明,新提出的方法可以实现多层金属球壳结构内外缺陷的精确定位成像。
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引用次数: 0
Monitoring damage evolution of SiCf/PyC/SiC mini-composites using electrical resistivity: Crack opening distance and interphase retention rate based electromechanical modeling 利用电阻率监测 SiCf/PyC/SiC 微型复合材料的损伤演变:基于裂缝张开距离和相间滞留率的机电建模
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-05 DOI: 10.1016/j.ndteint.2024.103208
Guoqiang Yu , Beichen Xue , Jiaming Li , Wenbing Ma , Zheng Ni , Yuanhui He , Chuyang Xie , Jinkang Du , Xiguang Gao , Yingdong Song

Electrical resistance is closely related to the damage of ceramic matrix composites (CMC) such as matrix crack, crack opening distance (COD), and interphase retention rate, giving it the potential to become a new non-destructive testing (NDT) technique. An electro-mechanical experiment method was designed for the tensile test of ceramic matrix mini-composites (CMMC). An optical in-situ tensile test was performed to obtain the pattern of matrix crack propagation. The result confirms that matrix crack saturation may not occur before the material fractures. An electromechanical model considering the COD was established to identify the damage situations. A new method for preparing ceramic matrix micro-composites composed of a single fiber and a single-layer pyrolytic carbon (PyC) interphase was realized. The accurate in-situ resistivity of the PyC was measured based on the micro-composites.

电阻与陶瓷基复合材料(CMC)的损伤(如基体裂纹、裂纹开裂距离(COD)和相间滞留率)密切相关,因此有可能成为一种新的无损检测(NDT)技术。为陶瓷基微型复合材料(CMMC)的拉伸测试设计了一种电子机械实验方法。通过光学原位拉伸试验获得了基体裂纹的扩展模式。结果证实,基体裂纹饱和可能不会在材料断裂前发生。建立了一个考虑 COD 的机电模型,以确定损坏情况。实现了一种制备由单根纤维和单层热解碳(PyC)间相组成的陶瓷基体微复合材料的新方法。在微复合材料的基础上精确测量了 PyC 的原位电阻率。
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引用次数: 0
Off-the-shelf UHF RFID-based sensors for corrosion characterization of coated steel 基于 UHF RFID 的现成传感器用于涂层钢的腐蚀鉴定
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-08-05 DOI: 10.1016/j.ndteint.2024.103210
Peilin Hui , Adi Mahmud Jaya Marindra , Chunlei Yang , Mark Robinson , Gui Yun Tian

The application of the UHF RFID technique in non-destructive testing (NDT) and structural health monitoring (SHM) has gained increasing attention due to its wireless, battery-less, and cost-effective attributes. It offers a promising approach for SHM and the Internet of Things (IoTs). This paper reports commercial off-the-shelf (COTS) flexible UHF RFID tag-based sensors for corrosion characterization on coated mild steel. Two types of COTS flexible UHF RFID tags with different bends are fabricated as sensors. The received signal strength indicator (RSSI) measurement is implemented to characterize the corrosion. Three parts (T-match area, dipole arms, and dipole loadings) of the two tags are tested for sensing purposes, and comparison and discussion of sensitivity, read range, and results are provided. This study successfully validates the feasibility of the proposed tag-bent method for corrosion characterization undercoating. It can be concluded that the dipole arm part of the applied COTS tags is the most sensitive area.

超高频射频识别(UHF RFID)技术具有无线、无需电池和成本效益高的特点,因此在无损检测(NDT)和结构健康监测(SHM)中的应用日益受到关注。它为 SHM 和物联网 (IoT) 提供了一种前景广阔的方法。本文介绍了基于商用现货(COTS)柔性超高频 RFID 标签的传感器,用于涂层低碳钢的腐蚀表征。我们制作了两种具有不同弯曲度的 COTS 柔性 UHF RFID 标签作为传感器。采用接收信号强度指示器(RSSI)测量来表征腐蚀情况。对两种标签的三个部分(T 型匹配区、偶极子臂和偶极子负载)进行了传感测试,并对灵敏度、读取范围和结果进行了比较和讨论。这项研究成功验证了拟议的标签弯曲法在涂层下腐蚀表征中的可行性。可以得出结论,应用的 COTS 标签的偶极臂部分是最敏感的区域。
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引用次数: 0
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