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Efficient defect reconstruction from temporal non-uniform pulsed thermography data using the virtual wave concept 利用虚拟波概念从时间非均匀脉冲热成像数据中高效重建缺陷
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-30 DOI: 10.1016/j.ndteint.2024.103200
L. Gahleitner , G. Mayr , G. Mayr , P. Burgholzer , U. Cakmak

In this study, we present an extension of the virtual wave concept to enable photothermal reconstruction from temporal non-uniform pulsed thermography data. Therefore, we introduce a generalized discrete transformation kernel, which allows to account for arbitrary temporal sampling strategies. First, we show the evidence of the proposed strategy for analytical temperature signals. Moreover, we demonstrate the advantages of the strategy for simulated temperature signals, obtained from an orthotropic sample with defect interfaces at various depth positions. For experimental verification, we apply pulsed thermography in the pulse-echo configuration for a carbon fiber-reinforced polymer sample with different embedded defects. It can be shown that efficient time sampling in the virtual wave concept allows a significant reduction in the number of data points compared to uniform sampling, without compromising the quality of the reconstruction results.

在这项研究中,我们对虚拟波概念进行了扩展,以便能够从时间非均匀脉冲热成像数据中进行光热重建。因此,我们引入了一个广义离散变换核,它允许考虑任意的时间采样策略。首先,我们展示了所提出的分析温度信号策略的证据。此外,我们还展示了该策略在模拟温度信号方面的优势,模拟温度信号是从正交各向同性样品中获得的,缺陷界面位于不同深度位置。为了进行实验验证,我们对具有不同嵌入缺陷的碳纤维增强聚合物样品采用脉冲回波配置的脉冲热成像技术。结果表明,与均匀采样相比,虚拟波概念中的高效时间采样可以显著减少数据点的数量,而不会影响重建结果的质量。
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引用次数: 0
Measurement of through-thickness electrical properties of carbon fiber reinforced thermoplastics using transmission method based on electromagnetic induction testing 利用基于电磁感应测试的传输方法测量碳纤维增强热塑性塑料的厚度电特性
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-25 DOI: 10.1016/j.ndteint.2024.103202
Wataru Matsunaga , Satoshi Imai , Yoshihiro Mizutani, Akira Todoroki

In this study, we proposed an electromagnetic induction testing method for measuring the electrical properties of carbon fiber reinforced thermoplastics (CFRTPs) along the through-thickness direction. The effectiveness of the transmission method, wherein the coil is placed opposite to the object to be measured, was demonstrated through finite element analysis and experimental measurements. The simulation results indicated that the output voltage of an interlaminar non-electrically conductive specimen exceeded that of an interlaminar conductive specimen due to the electromagnetic shielding effect. In the experiments, the impedance along the through-thickness direction depended on the lamination configuration and the presence of the PA-6 layer. Our findings indicate that the proposed method can be used to measure the changes in the electrical properties of CFRTP along the through-thickness direction.

在这项研究中,我们提出了一种电磁感应测试方法,用于测量碳纤维增强热塑性塑料(CFRTPs)沿厚度方向的电气特性。通过有限元分析和实验测量,证明了线圈与待测物体相对放置的传输方法的有效性。模拟结果表明,由于电磁屏蔽效应,层间非导电试样的输出电压超过了层间导电试样的输出电压。在实验中,沿厚度方向的阻抗取决于层叠结构和 PA-6 层的存在。我们的研究结果表明,所提出的方法可用于测量 CFRTP 沿厚度方向的电特性变化。
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引用次数: 0
The volumetric ultrasound imaging strategy for quantification of the defects in concrete based on the optimized cumulative kurtosis method 基于优化累积峰度法的混凝土缺陷量化体积超声成像策略
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-25 DOI: 10.1016/j.ndteint.2024.103203
Lu Zhang , Shangda Jia , Chong Qiao , Yongze Tang , Hongyu Li , Tonghao Zhang

Currently, ultrasonic tomography is widely used for quantifying the status of damage/flaw in various materials including metal, concrete, and composite. It is capable of visualizing the internal damage or flaws by reconstructing the velocity of ultrasound. For most cases, the conventional ultrasonic tomography is adapted for slice-based investigations. Though 3D image can be generated by slice-based method, the involvement of multi-scan interpolation caused high computational cost and unexpected errors. Moreover, for 3D imaging, two essential factors are dominant: (i) reconstructing the velocity; and (ii) scheme of forming up the 3D image. To this end, this study proposed to develop a novel volumetric ultrasound imaging strategy with high accuracy. To obtain more accurate Time-of-Flight (TOF) for ultrasonic velocity, an improved method based on cumulative kurtosis is proposed. With the proposed method, the adverse influence of internal complexity within samples on ultrasound was reduced. The proposed novel volumetric ultrasound imaging strategy was verified numerically and experimentally. Finally, the performance of the proposed method has been evaluated by the comparison of three-dimensional imaging results with different inclusion. Additionally, the parametric study was conducted using path average velocity, voxel velocity, and image accuracy. The results show a positive correlation between the number of voxels and imaging accuracy. However, as the number of voxels increases, the errors introduced by the Simultaneous Algebraic Reconstruction Technique (SART) increase. The influential factors on the imaging accuracy were discussed, such as inclusion eccentricity, the relationship among the reduced volume imaging quantity, and accuracy in voxel inversion result. For further application, the recommendations were also provided.

目前,超声波断层扫描被广泛用于量化各种材料(包括金属、混凝土和复合材料)的损伤/缺陷状况。它能够通过重建超声波的速度来观察内部损伤或缺陷。在大多数情况下,传统的超声断层扫描适用于基于切片的调查。虽然基于切片的方法可以生成三维图像,但由于涉及多扫描插值,导致计算成本高和意外误差。此外,三维成像有两个关键因素:(i) 重建速度;(ii) 形成三维图像的方案。为此,本研究提出了一种新型高精度容积超声成像策略。为了获得更精确的超声波速度飞行时间(TOF),提出了一种基于累积峰度的改进方法。利用所提出的方法,减少了样本内部复杂性对超声波的不利影响。通过数值和实验验证了所提出的新型容积超声成像策略。最后,通过比较不同样本的三维成像结果,评估了所提方法的性能。此外,还利用路径平均速度、体素速度和图像精度进行了参数研究。结果显示,体素数量与成像精度之间存在正相关。然而,随着体素数量的增加,同步代数重建技术(SART)带来的误差也随之增加。讨论了影响成像准确性的因素,如纳入偏心率、缩小体积成像量之间的关系以及体素反演结果的准确性。此外,还提出了进一步应用的建议。
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引用次数: 0
Edge blurring suppression of ultrasonic reflection coefficients in contact state measurement 在接触状态测量中抑制超声波反射系数的边缘模糊
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-22 DOI: 10.1016/j.ndteint.2024.103201
Xingyuan Wang , Chonglin Xu , Fulai Yang

Ultrasonic reflection coefficient is the key to contact state evaluation of mechanical devices. Edge blurring can lead to contact state (such as stress concentrations) measurement errors. This reduces the reliability of performance evaluations and introduces potential security risks. In this study, an edge blurring suppression method based on matching pursuit algorithm was proposed. Firstly, the interference signal prediction model is built based on the Nakagami model. Then, a blurred signal separation algorithm based on matching pursuit is proposed to obtain the effective signal. Finally, the reflection coefficient with and without edge blurring effect were obtained. The simulation results show that the maximum relative error of the reflection coefficient is reduced from 219 % to 15 %. The effectiveness of the proposed method is also verified by experiments. The experimental results show that the relative error of the reflection coefficient after edge blurring suppression is reduced from 64 % to 16 %. This indicates that the proposed method can effectively suppress edge blurring, which provides an effective method for edge blurring suppression in various application fields of ultrasonic measurement and improve the reliability of product quality evaluation.

超声波反射系数是评估机械设备接触状态的关键。边缘模糊会导致接触状态(如应力集中)测量误差。这会降低性能评估的可靠性,并带来潜在的安全风险。本研究提出了一种基于匹配追求算法的边缘模糊抑制方法。首先,基于中神模型建立干扰信号预测模型。然后,提出一种基于匹配追寻的模糊信号分离算法,以获得有效信号。最后,得到了有边缘模糊效应和无边缘模糊效应的反射系数。仿真结果表明,反射系数的最大相对误差从 219% 降至 15%。实验也验证了所提方法的有效性。实验结果表明,抑制边缘模糊后,反射系数的相对误差从 64% 减小到 16%。这表明所提出的方法能有效抑制边缘模糊,为超声波测量的各种应用领域提供了一种有效的边缘模糊抑制方法,提高了产品质量评价的可靠性。
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引用次数: 0
FTnet: An integrated network for fusing multi-modal NDE data of lightning damage in aircraft composite materials FTnet:融合飞机复合材料雷击损伤多模态无损检测数据的综合网络
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-20 DOI: 10.1016/j.ndteint.2024.103196
Yanshuo Fan , Rakiba Rayhana , Catalin Mandache , Marc Genest , Zheng Liu

Lightning strikes pose a significant challenge for aircraft and wind turbine blades with Carbon Fiber Reinforced Polymer (CFRP) structures, requiring reliable damage detection techniques. Non-destructive evaluation (NDE) methods, including X-ray and Ultrasonic Testing, are effective in identifying material damage in aircraft. However, X-ray requires access to both sides of the structure, and UT requires a coupling medium between the transducer and the structure, as well as a relatively smooth surface, making both methods less feasible for routine aircraft maintenance. Other NDE techniques, such as eddy current testing and infrared thermography, can detect damage on the side struck by lightning but lack the precision needed for a comprehensive assessment. To address these challenges, this paper introduces a two-stage Fusion-Translation network (FTnet), which integrates NDE 4.0 innovations, including data fusion and advanced imaging algorithms, to optimize the NDE process. By integrating infrared and eddy current data, FTnet characterizes lightning-induced damage with enhanced depth and contour detail, demonstrating superior performance over existing methods in both qualitative and quantitative evaluations. The implementation of FTnet marks an advancement in NDE 4.0, potentially enhancing aircraft safety and streamline maintenance protocols by providing a more reliable and comprehensive assessment of lightning strike damage.

雷击对采用碳纤维增强聚合物(CFRP)结构的飞机和风力涡轮机叶片构成重大挑战,需要可靠的损坏检测技术。包括 X 射线和超声波测试在内的无损评价 (NDE) 方法可有效识别飞机的材料损伤。然而,X 射线需要进入结构的两侧,UT 需要传感器和结构之间的耦合介质以及相对光滑的表面,因此这两种方法在飞机的日常维护中都不太可行。其他无损检测技术,如涡流测试和红外热成像技术,可以检测雷击侧的损坏情况,但缺乏全面评估所需的精度。为了应对这些挑战,本文介绍了一种两阶段融合-转换网络(FTnet),它集成了无损检测 4.0 创新技术,包括数据融合和先进的成像算法,以优化无损检测流程。通过整合红外和涡流数据,FTnet 以更高的深度和轮廓细节来描述雷电引起的损伤,在定性和定量评估方面都显示出优于现有方法的性能。FTnet 的实施标志着无损检测 4.0 的进步,通过提供更可靠、更全面的雷击损伤评估,有可能提高飞机安全性并简化维护协议。
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引用次数: 0
Non-destructive characterisation of pearlitic steel microstructure at room temperature and in-situ microstructure development during heat treatment using electromagnetic sensors 利用电磁传感器对珠光体钢室温下的微观结构和热处理过程中的原位微观结构发展进行无损表征
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-18 DOI: 10.1016/j.ndteint.2024.103199
L. Zhou , F. Wu , M.A. Jolfaei , S. Hobson , C.L. Davis

Pearlitic steels are important engineering materials in various high-strength applications. Their mechanical properties are influenced by microstructure control using chemical composition and/or thermomechanical processing. In the current study, a novel, non-destructive technique is presented for the characterisation of key microstructure parameters that are essential for strength, both at room temperature and during dynamic heat treatment. The pearlite interlamellar spacing in a 0.81 wt% C steel has been accurately measured at room temperature using an electromagnetic (EM) sensor. Furthermore, the spheroidisation process in 100Cr6 pearlitic steel has been monitored at elevated temperatures. A strong linear relationship between the EM sensor signal and the pearlite interlamellar spacing is demonstrated, indicated by an R2 value of 0.91. Additionally, the capability of this method to track the spheroidisation process in real-time during constant heat treatment offers potential avenues for process optimisation in pearlitic steels.

珠光体钢是各种高强度应用中的重要工程材料。它们的机械性能受到使用化学成分和/或热机械加工控制微观结构的影响。在本研究中,介绍了一种新颖的非破坏性技术,用于表征在室温和动态热处理过程中对强度至关重要的关键微观结构参数。使用电磁(EM)传感器可在室温下精确测量 0.81 wt% C 钢中的珠光体层间间距。此外,还监测了 100Cr6 珠光体钢在高温下的球化过程。电磁传感器信号与珠光体层间间距之间存在很强的线性关系,R2 值为 0.91。此外,这种方法能够在恒定热处理过程中实时跟踪球化过程,为珠光体钢的工艺优化提供了潜在的途径。
{"title":"Non-destructive characterisation of pearlitic steel microstructure at room temperature and in-situ microstructure development during heat treatment using electromagnetic sensors","authors":"L. Zhou ,&nbsp;F. Wu ,&nbsp;M.A. Jolfaei ,&nbsp;S. Hobson ,&nbsp;C.L. Davis","doi":"10.1016/j.ndteint.2024.103199","DOIUrl":"10.1016/j.ndteint.2024.103199","url":null,"abstract":"<div><p>Pearlitic steels are important engineering materials in various high-strength applications. Their mechanical properties are influenced by microstructure control using chemical composition and/or thermomechanical processing. In the current study, a novel, non-destructive technique is presented for the characterisation of key microstructure parameters that are essential for strength, both at room temperature and during dynamic heat treatment. The pearlite interlamellar spacing in a 0.81 wt% C steel has been accurately measured at room temperature using an electromagnetic (EM) sensor. Furthermore, the spheroidisation process in 100Cr6 pearlitic steel has been monitored at elevated temperatures. A strong linear relationship between the EM sensor signal and the pearlite interlamellar spacing is demonstrated, indicated by an R<sup>2</sup> value of 0.91. Additionally, the capability of this method to track the spheroidisation process in real-time during constant heat treatment offers potential avenues for process optimisation in pearlitic steels.</p></div>","PeriodicalId":18868,"journal":{"name":"Ndt & E International","volume":"147 ","pages":"Article 103199"},"PeriodicalIF":4.1,"publicationDate":"2024-07-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141729847","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of light source wavelength on surface defect imaging in deep-water concrete dams 光源波长对深水混凝土大坝表面缺陷成像的影响
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-17 DOI: 10.1016/j.ndteint.2024.103198
Dong Chen , Fei Kang , Jing Chen , Sisi Zhu , Hongjun Li

This study explores the relationship between surface defect imaging in deep-water concrete dams and the wavelength of the light source, aiming to improve concrete defect image quality by varying the wavelength. The underwater optical imaging model of concrete dam surfaces was developed by applying the principle of object reflection and the underwater optical propagation model. This model reflects the effect of different light wavelengths on underwater concrete defect imaging. Through a self-designed underwater optical darkroom test platform, defect image acquisition tests were conducted under various color light conditions. The results reveal the significant influence of light source wavelength on images captured in both air and water. Furthermore, under the same initial illuminance, blue light significantly enhanced the average gray value, sharpness, contrast, and the number of feature points in underwater defect images, exhibiting increments of 2.97 times, 0.48 times, 2.70 times, and 2.95 times, respectively, compared to white light. These findings can serve as a reference for the selection of color-light for the non-destructive testing of surface defects in actual underwater concrete dams.

本研究探讨了深水混凝土大坝表面缺陷成像与光源波长之间的关系,旨在通过改变波长提高混凝土缺陷成像质量。应用物体反射原理和水下光学传播模型,建立了混凝土坝表面的水下光学成像模型。该模型反映了不同波长的光对水下混凝土缺陷成像的影响。通过自行设计的水下光学暗室测试平台,在不同色光条件下进行了缺陷图像采集测试。结果表明,光源波长对在空气和水中拍摄的图像都有显著影响。此外,在相同的初始照度下,蓝光能显著提高水下缺陷图像的平均灰度值、清晰度、对比度和特征点数量,与白光相比,分别提高了 2.97 倍、0.48 倍、2.70 倍和 2.95 倍。这些研究结果可为实际水下混凝土大坝表面缺陷的无损检测选择色光提供参考。
{"title":"Effect of light source wavelength on surface defect imaging in deep-water concrete dams","authors":"Dong Chen ,&nbsp;Fei Kang ,&nbsp;Jing Chen ,&nbsp;Sisi Zhu ,&nbsp;Hongjun Li","doi":"10.1016/j.ndteint.2024.103198","DOIUrl":"10.1016/j.ndteint.2024.103198","url":null,"abstract":"<div><p>This study explores the relationship between surface defect imaging in deep-water concrete dams and the wavelength of the light source, aiming to improve concrete defect image quality by varying the wavelength. The underwater optical imaging model of concrete dam surfaces was developed by applying the principle of object reflection and the underwater optical propagation model. This model reflects the effect of different light wavelengths on underwater concrete defect imaging. Through a self-designed underwater optical darkroom test platform, defect image acquisition tests were conducted under various color light conditions. The results reveal the significant influence of light source wavelength on images captured in both air and water. Furthermore, under the same initial illuminance, blue light significantly enhanced the average gray value, sharpness, contrast, and the number of feature points in underwater defect images, exhibiting increments of 2.97 times, 0.48 times, 2.70 times, and 2.95 times, respectively, compared to white light. These findings can serve as a reference for the selection of color-light for the non-destructive testing of surface defects in actual underwater concrete dams.</p></div>","PeriodicalId":18868,"journal":{"name":"Ndt & E International","volume":"147 ","pages":"Article 103198"},"PeriodicalIF":4.1,"publicationDate":"2024-07-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141736444","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Characterization of electro-adhesion using surface waves generated and detected by Laser-Ultrasonics 利用激光超声波产生和检测的表面波表征电附着力
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-17 DOI: 10.1016/j.ndteint.2024.103191
Mustapha Baher, Meriem Chrifi Alaoui, Frédéric Jenot, Mohammadi Ouaftouh, Marc Duquennoy

Studying and understanding adhesion characteristics between a coating and its substrate is important for improving the reliability of a thin film’s adhesion. To the best of the authors’ knowledge, this work studies for the first time a specific electro-adhesion process using Laser-Ultrasonics. An electric field source is applied to a convenient sample composed of a polyvinyl chloride (PVC) layer on an aluminum (Al) substrate. The aim is to investigate the impact of different electro-adhesion levels on the propagation of surface acoustic waves (SAW), which are generated by a pulsed laser and detected using an interferometer. This non-destructive and non-contact experimental setup allows us to determine the surface modes dispersion curves for each adhesion level. A theoretical model is developed to numerically solve the dispersion relation in order to analyze the influence of the interface quality on the dispersion curves. These ones have also been obtained by the finite element method (FEM) allowing us to predict the shape of the experimental signals. This research paves the way for future studies of specific adhesion phenomena across different materials.

研究和了解涂层与其基底之间的附着特性对于提高薄膜附着的可靠性非常重要。据作者所知,这项研究首次使用激光超声波技术对特定的电附着过程进行了研究。电场源被施加到由铝基板上的聚氯乙烯(PVC)层组成的方便样品上。目的是研究不同的电附着水平对表面声波(SAW)传播的影响,SAW 由脉冲激光产生,并使用干涉仪进行检测。通过这种非破坏性和非接触式实验装置,我们可以确定每个附着水平的表面模式频散曲线。为了分析界面质量对频散曲线的影响,我们开发了一个理论模型来数值求解频散关系。我们还通过有限元法(FEM)获得了这些曲线,从而可以预测实验信号的形状。这项研究为今后研究不同材料间的特殊粘附现象铺平了道路。
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引用次数: 0
Identifying grain size in ASTM A36 steel using ultrasonic backscattered signals and machine learning 利用超声波反向散射信号和机器学习识别 ASTM A36 钢中的晶粒尺寸
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-15 DOI: 10.1016/j.ndteint.2024.103181
M.C.A. Viana , P. Pereira , A.A. Buenos , A.A. Santos

Ultrasonic nondestructive techniques can be useful tools in the microstructural classification of metallic alloys. Among the most common techniques for characterizing materials, backscattered signal analysis stands out because it does not require a back surface echo. This study classifies five ASTM A36 steel samples with varying grain sizes using ultrasonic waves. For each sample, ultrasound signals were obtained using two ultrasonic array probes with center frequencies of 5 and 10 MHz. An extensive feature engineering process was conducted using the tfresh package in Python, which extracts a wide range of features from time series data, transforming raw ultrasound signals into a structured format. Seven machine learning models were evaluated based on accuracy, precision, recall, and F1 score, with performances ranging from 70 to 100%. The XGBoost model exhibited the best performance with 10 MHz probe signals, achieving 100% accuracy. An additional validation test was conducted to evaluate the models’ generalization capability, considering inter-specimen variabilities. Despite a slight reduction in prediction metrics, the XGBoost model maintained good performance, with accuracy between 89% and 100% across all frequencies. Such findings demonstrate that backscattered grain noise can effectively identify grain sizes provided that an adequate machine learning model is used.

超声波无损技术是金属合金微观结构分类的有用工具。在最常见的材料表征技术中,背散射信号分析因其不需要背面回波而脱颖而出。本研究利用超声波对五种晶粒大小不同的 ASTM A36 钢样本进行了分类。每个样品都使用两个中心频率分别为 5 和 10 MHz 的超声阵列探头获取超声信号。使用 Python 中的 tfresh 软件包进行了广泛的特征工程处理,该软件包可从时间序列数据中提取各种特征,将原始超声波信号转换为结构化格式。根据准确度、精确度、召回率和 F1 分数,对七个机器学习模型进行了评估,其性能从 70% 到 100% 不等。XGBoost 模型在使用 10 MHz 探头信号时表现最佳,准确率达到 100%。考虑到样本间的差异,还进行了额外的验证测试,以评估模型的泛化能力。尽管预测指标略有下降,但 XGBoost 模型仍然保持了良好的性能,在所有频率下的准确率都在 89% 到 100% 之间。这些研究结果表明,只要使用适当的机器学习模型,反向散射晶粒噪声就能有效识别晶粒尺寸。
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引用次数: 0
A comparison of X-ray attenuation, differential phase, and dark-field contrast imaging for the detection of porosity in carbon fiber reinforced cyanate ester X 射线衰减、差分相位和暗场对比成像在检测碳纤维增强氰酸酯中孔隙率方面的比较
IF 4.1 2区 材料科学 Q1 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-07-15 DOI: 10.1016/j.ndteint.2024.103194
Jonathan Glinz , Bernhard Plank , Josephine Gutekunst , Michael Scheerer , Simon Zabler , Johann Kastner , Sascha Senck

In this work we explore the capabilities of Talbot-Lau grating interferometry (TLGI) radiography for the inspection of porosity in structural specimens of cyanate ester carbon fiber reinforced polymer. The influence of system resolution and varying specimen thicknesses on mean values and standard deviations (STDV) in all three image modalities acquired by TLGI are addressed. Results show that mean absorption contrast (AC) values are highly affected by specimen thickness and strong negative correlation (r ≤ −0.8) is found only after correction via preliminary thickness measurements. Although dark-field contrast (DFC) is affected by changes in specimen thickness as well, the signal can be corrected by normalization with the inherently available AC. Consequently, strong positive correlation with porosity was found both in high- and low-resolution imaging (r = 0.83 and 0.71 respectively). Without the need for high image resolution or thickness measurements, the normalized DFC is a promising option for large field of view inspections. Investigations of STDV revealed strong positive correlations between porosity and AC STDV as well as differential phase contrast (DPC) STDV (r = 0.95 and 0.92 respectively) but high image resolution is required. Furthermore, results suggest increased robustness against variations in specimen thickness of AC and DPC STDV analyses.

在这项工作中,我们探索了塔尔博特-劳光栅干涉仪(TLGI)射线照相术在检测氰酸酯碳纤维增强聚合物结构试样孔隙率方面的能力。研究探讨了系统分辨率和不同试样厚度对 TLGI 获得的所有三种图像模式的平均值和标准偏差 (STDV) 的影响。结果表明,平均吸收对比度(AC)值受试样厚度的影响很大,只有在通过初步厚度测量进行校正后才会发现两者之间存在很强的负相关(r ≤ -0.8)。虽然暗场对比度(DFC)也会受到试样厚度变化的影响,但可以通过对固有的 AC 值进行归一化来校正信号。因此,在高分辨率和低分辨率成像中都发现了与孔隙率的强正相关性(r = 0.83 和 0.71)。在不需要高图像分辨率或厚度测量的情况下,归一化 DFC 是大视场检测的理想选择。对 STDV 的研究表明,孔隙率与 AC STDV 以及差分相衬 (DPC) STDV 之间存在很强的正相关性(r 分别为 0.95 和 0.92),但需要很高的图像分辨率。此外,结果表明 AC 和 DPC STDV 分析对试样厚度变化的鲁棒性增强。
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