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Removal Efficiency for Micro-Polystyrene in Water by the Oil-Based Ferrofluid Employ Response Surface Methodology 采用响应面法研究油基铁磁流体对水中微聚苯乙烯的去除效果
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-08-31 DOI: 10.17576/jsm-2023-5208-03
Natasha Nizam, Sumithra Mohanasunthar, Alyza A. Azmi, Sabiqah Tuan Anuar, Yusof Shuaib Ibrahim, Wan Mohd Afiq Wan Mohd Khalik
This research article presents a study on the potential use of oil-based ferrofluid for the efficient removal of microplastics from water. The targeted analyte, micro-polystyrene (micro-PS), was chosen along with palm oil as the carrier liquid. Fourier Transform Infrared (FTIR) analysis was conducted to identify the main peaks in the ferrofluid, including carboxyl group (1542 cm-1), C-H bonding (1022 cm-1), CH2 bonding (2941 cm-1), CH3 bonding (3461 cm-1), C=C bonding (1255 cm-1), and Fe-O (597.34 cm-1). A comprehensive investigation of the synergistic effect of six variables was performed: volume of oil (4-15 mL), weight of magnetite nanoparticles (0.1-0.2 g), stirring rate (132-468 rpm), contact time (3-12 min), pH value of water samples (pH 6-8), and effect on ionic strength (0-16 g/L). Response surface methodology, including 26-Plackett-Burman and 24-central composite design, were employed to establish the relationship between the variables. The optimum operational settings proposed by the model were as follows: volume of oil (14.6 mL), weight of magnetite nanoparticles (0.1 g), stirring rate (216 rpm), contact time (3.29 min), pH value of water samples (pH 6-6.5), and effect on ionic strength (16 g/L), resulting in a remarkable removal efficiency of 91.09 ± 0.99%. The method exhibited desirable figures of merit, including a low bias (%RSD) of below 5% and the ability to reuse the ferrofluids for up to five cycles. Additionally, an analytical greenness metric was employed to assess the environmental impact of the sample preparation process, with a green score of 0.69/1.0 (indicating a light green colour). Future work in this field could focus on the scalability of the developed method and its applicability to real-wastewater treatment.
本文介绍了油基铁磁流体在高效去除水中微塑料方面的潜在应用。选择目标分析物微聚苯乙烯(micro-PS)和棕榈油作为载体液。傅里叶红外(FTIR)分析确定了铁磁流体中的主要峰,包括羧基(1542 cm-1)、C- h键(1022 cm-1)、CH2键(2941 cm-1)、CH3键(3461 cm-1)、C=C键(1255 cm-1)和Fe-O (597.34 cm-1)。研究了油体积(4-15 mL)、磁铁矿纳米颗粒重量(0.1-0.2 g)、搅拌速度(132-468 rpm)、接触时间(3-12 min)、水样pH值(pH 6-8)和对离子强度(0-16 g/L)的影响。采用响应面法,包括26-Plackett-Burman和24中心复合设计,建立变量之间的关系。模型提出的最佳操作设置为:油体积(14.6 mL)、纳米磁铁矿质量(0.1 g)、搅拌速度(216 rpm)、接触时间(3.29 min)、水样pH值(pH 6 ~ 6.5)和离子强度影响(16 g/L),去除率为91.09±0.99%。该方法表现出令人满意的优点,包括低于5%的低偏置(%RSD)和重复使用铁磁流体多达五个循环的能力。此外,采用分析绿色度指标来评估样品制备过程的环境影响,绿色评分为0.69/1.0(表示浅绿色)。该领域未来的工作将重点关注所开发方法的可扩展性及其在实际废水处理中的适用性。
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引用次数: 0
The Effects of Abelmoschus esculentus (L.) Moench Seed on High Fat Diet Induced Metabolic and Cognitive Impairments in C57BL/6J Mice 绿僵鼠(L.)的防治效果高脂饮食对C57BL/6J小鼠代谢和认知损伤的影响
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-08-31 DOI: 10.17576/jsm-2023-5208-10
Paweena Wongwitwichot, Supattra Prom-in, Jasadee Kaewsrichan, Nuntika Wangpradit, Kien Hui Chua, Mohamad Fairuz Yahaya, Azizah Ugusman, Jaya Kumar
Okra is known for its neuroprotective and antioxidant properties. We aimed to investigate the potential effects of okra seed powder in alleviating high far diet (HFD) induced cognitive deficit and hypercholesterolemia. We randomly allocated thirty-six C57BL/6J male mice into: (i) control, mice fed with a normal fat level diet; (ii) HFD, mice fed with HFD; (iii) HFD-OS1; (iv) HFD-OS2; (v) HFD-OS3, mice fed with HFD and okra seed powder (200, 400, or 800 mg/kg/day, respectively); (vi) HFD-SIM, mice fed with HFD and simvastatin (20 mg/kg/day). After 10 weeks of treatment period, the mice were tested with an episodic-like memory test (EMT) and Morris water maze (MWM). We found significantly higher total and LDL cholesterol levels in mice fed with HFD. Compared to the HFD group, the control group performed better in the EMT test, and also learned and retrieved spatial reference memory better in the MWM test. The okra seed powder significantly improved spatial learning in four days of acquisition trials and the highest dose of okra profoundly improved spatial reference memory retention during the probe trial. Contrary to the MWM results, the okra-treated animals did not perform significantly better than the HFD-treated animals in EMT. At present, we recommend future studies testing the potential neuroprotective or cognitive enhancing effects of okra to assess different cognitive domains using various disease models to have a better understanding on the potential neuroprotective properties of okra.
秋葵以其神经保护和抗氧化特性而闻名。我们的目的是研究秋葵籽粉在缓解高脂饮食(HFD)诱导的认知障碍和高胆固醇血症中的潜在作用。我们将36只C57BL/6J雄性小鼠随机分为两组:(i)对照组,喂食正常脂肪水平的饲料;(ii) HFD,饲喂HFD的小鼠;(3) HFD-OS1;(四)HFD-OS2;(v) HFD- os3,分别饲喂HFD和秋葵籽粉(200、400、800 mg/kg/d);(vi) HFD- sim, HFD +辛伐他汀(20mg /kg/d)喂养小鼠。治疗10周后,进行情景样记忆测试(EMT)和Morris水迷宫测试(MWM)。我们发现喂食HFD的小鼠的总胆固醇和低密度脂蛋白胆固醇水平显著升高。与HFD组相比,对照组在EMT测试中表现更好,在MWM测试中学习和检索空间参考记忆也更好。在4天的习得试验中,秋葵籽粉显著提高了空间学习能力,在探针试验中,最高剂量的秋葵籽粉显著提高了空间参考记忆的保留。与MWM的结果相反,秋葵治疗的动物在EMT中的表现并不明显好于hfd治疗的动物。目前,我们建议未来的研究测试秋葵潜在的神经保护或认知增强作用,利用各种疾病模型评估不同的认知领域,以更好地了解秋葵潜在的神经保护特性。
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引用次数: 0
Hybrid Multistep Block Method for Solving Neutral Volterra Integro-Differential Equation with Proportional and Mixed Delays 求解具有比例和混合时滞的中立型Volterra积分微分方程的混合多步分块法
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-08-31 DOI: 10.17576/jsm-2023-5208-13
Nur Inshirah Naqiah Ismail, Zanariah Abdul Majid
The neutral Volterra integro-differential equation with proportional and mixed delays (NDVIDE) is being solved by a newly proposed technique in numerical method, namely, the two-point one off-point block multistep method (1OBM3). The method is also known as a hybrid multistep block method. Subsequently, Lagrange interpolating polynomial is utilized in order to develop the hybrid block method. The foundation of the technique is taken from predictor and corrector formulae. The proposed method will solve NDVIDE in two steps simultaneously, with three predictor formulae including one off-point. The NDVIDE problems are solved via the constant step size technique. In order to solve the integral and differential parts of the problems, two alternative numerical approaches are applied. The differentiation part is approximated by deriving the divided difference formula, while the integration part is interpolated using composite Simpson’s rule. Note that the proposed method has been analysed thoroughly regarding its order, consistency, zero stability and convergence of the method. The stability region for 1OBM3 has been constructed based on the stability polynomial obtained. Consequently, numerical results are presented to demonstrate the effectiveness of the proposed method, 1OBM3.
采用一种新的数值方法,即两点一离点块多步法(1OBM3),求解具有比例和混合延迟的中立型Volterra积分微分方程(NDVIDE)。该方法也被称为混合多步块方法。在此基础上,利用拉格朗日插值多项式建立了混合块法。该技术的基础来自于预测和校正公式。该方法采用了包括一个离点在内的三个预测公式,分两步求解NDVIDE。采用恒步长技术解决了NDVIDE问题。为了解决问题的积分和微分部分,采用了两种可选的数值方法。微分部分采用微分除差公式逼近,积分部分采用复合辛普森规则插值。值得注意的是,所提出的方法已经对其顺序、一致性、零稳定性和收敛性进行了深入的分析。根据得到的稳定性多项式,构造了1OBM3的稳定区域。最后给出了数值结果,验证了该方法的有效性。
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引用次数: 0
Kajian Terhadap Eis dan Kaedah Kehilangan Berat: Novel Perencat Kakisan Hijau daripada Ekstrak Etlingera Elatior 关于 Eis 和减肥方法的研究:提取自 Etlingera Elatior 的新型绿色甜味剂
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-08-31 DOI: 10.17576/jsm-2023-5208-12
Syahidah Nabila Rosli, Norinsan Kamil Othman, Ahmad Rifqi Md Zain
Perencatan kakisan berasaskan bahan pengekstrakan tumbuhan telah mendapat perhatian penyelidik sejak beberapa tahun kebelakangan ini disebabkan tidak bertoksik dan biodegredasi. Hasil ekstrak Etlingera elatior telah digunAakan dalam kajian ini sebagai perencat kakisan hijau dalam medium 0.5 M asid hidroklorik (HCl). Dalam kajian ini, bahan ekstrak yang diperoleh telah dicirikan menggunakan analisis spektroskopi inframerah Fourier-transformasi (FTIR) dan spektroskopi jisim-kromatografi gas (GC-MS) untuk mengenal pasti kumpulan berfungsi dan sebatian kimia yang wujud. Keberkesanan bahan ekstrak dalam perencatan kakisan keluli berkarbon rendah telah dikaji melalui ujian kehilangan berat dan ujian impedans (EIS) dalam medium berasid mengikut parameter suhu (25 °C, 45 °C dan 65 °C) dan kepekatan ekstrak (250 ppm, 450 ppm, 650 ppm, 950 ppm dan 1050 ppm) yang berbeza. Spesimen keluli berkarbon rendah dicirikan melalui mikroskop elektron imbasan (SEM) dan serakan x penyebaran tenaga (EDX). Spektroskopi inframerah Fourier-transformasi (FTIR) telah menunjukkan kehadiran kumpulan berfungsi seperti hidroksil dan alkena. Sebatian organik yang mempunyai ikatan π dengan kepadatan elektron tinggi akan memudahkan proses penjerapan. Analisis GC-MS pula mendedahkan empat sebatian utama yang terdapat dalam ekstrak Etlingera elatior iaitu N-asid hexadekanoik, siklododekan, 9,12-asid oktadekadienoik dan asid dodekanoik. Kecekapan perencatan yang diperoleh dari ujian kehilangan berat mendapati bahawa peratusan kecekapan perencatan tertinggi adalah 93.6%, manakala bagi ujian impedans (EIS) adalah 90.5% pada kepekatan 950 ppm. Suhu yang tinggi juga mempercepatkan kadar kakisan dan kecekapan perencatan (IE%) menurun. Morfologi pembentukan lapisan pelindung dilihat pada permukaan berkarbon rendah apabila dengan kehadiran perencat kakisan ekstrak Etlingera elatior. Secara keseluruhannya, perencat kakisan daripada ekstrak Etlingera elatior berupaya menghalang kakisan berlaku disokong pula dengan sifat yang mesra alam.
自过去几年以来,基于植物提取物的杮酱重组由于其无毒性和生物降解性而受到研究人员的关注。本研究将 Etlingera elatior 的提取物用作 0.5 M 盐酸(HCl)培养基中的绿色杮酱受体。本研究使用傅立叶变换红外光谱(FTIR)和气相色谱-气相色谱(GC-MS)分析法对获得的提取物材料进行了表征,以确定其中存在的官能团和化合物。在酸性介质中,根据不同的温度(25 °C、45 °C 和 65 °C)和提取物浓度(250 ppm、450 ppm、650 ppm、950 ppm 和 1050 ppm)参数,通过失重测试和阻抗测试(EIS)评估了提取物材料处理低碳钢屑的功效。低碳钢试样通过扫描电子显微镜(SEM)和能量色散 X 射线(EDX)进行表征。傅立叶变换红外光谱(FTIR)显示了羟基和烯基等官能团的存在。具有高电子密度 π 键的有机化合物会促进吸附过程。气相色谱-质谱分析还揭示了 Etlingera elatior 提取物中存在的四种主要化合物,即 N-酸十六烷酸、环十二烷酸、9,12-酸十八烷二烯酸和十二烷酸。通过失重测试得出的规划效率最高,为 93.6%,而阻抗测试(EIS)在 950 ppm 浓度时的规划效率为 90.5%。高温也加快了腐蚀速度,绝缘效率(IE%)下降。在有 Etlingera elatior 提取物 kakisan 稀释剂存在的情况下,低碳表面观察到了保护层形成的形态。总之,Etlingera elatior 提取物缓蚀剂以其自然友好的特性防止了腐蚀的发生。
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引用次数: 0
Genomic Analysis of a Novel Antarctic Bacterium, Cyrobacterium sp.SO2 Provides Insights into its Genomic Potential for Production of Antimicrobial Compounds 一种新的南极细菌,环状细菌sp.SO2的基因组分析为其生产抗菌化合物的基因组潜力提供了见解
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-07-31 DOI: 10.17576/jsm-2023-5207-05
C.P. Teoh, P. Lavin, M. González-Aravena, C.M.V.L. Wong
A novel strain of Cryobacterium designated as SO2, was isolated from the Antarctic. Hence, this study was undertaken to gain further insight into the antimicrobial compounds and secondary metabolites produced by Cryobacterium sp. SO2. It was found that strain SO2 is a Gram-positive that exhibits an irregular rod shape, which formed yellow to orange pigmented colonies on semi-solid media. Strain SO2 grows at temperatures ranging from 4 to 25 ºC. It has a complete genomic size of 4.097 Mb. SO2 has a DNA G+C content of 68.43%, and genomic annotation showed that the genome contained 3,862 CDS, 10 rRNA, 55 tRNA and 1 tm-RNA. Phylogenetic and OrthoANI analysis suggested Cryobacterium sp. strains SO1, N22, TMB1-8, LW097, TMN39-1, C. zongtaiiTMN-42, C. arcticumPAMC27867 and C. soli GCJ02 as its closest phylogenetic neighbour. Genome annotation shows that strain SO2 confers β-lactamase class A, cephalosporin-C deacetylases, and 27 drug-resistance encoding genes, and allows resistance to ceftazidime. Functional annotation identifies 28.74% of predicted genes are of unknown functions. Genome mining indicates that there are six putative secondary metabolite gene clusters in strain SO2. They are made up of RRE-containing, terpene, beta-lactone, T3PKS, NAPAA, and 2dos. This finding shows strain SO2 harbours genes that may be involved in the production of compounds with antibacterial and antioxidant activities.
从南极分离出一种名为SO2的低温细菌新菌株。因此,本研究旨在进一步了解Cryobacterium sp. SO2产生的抗菌化合物和次生代谢物。结果表明,菌株SO2为革兰氏阳性,呈不规则棒状,在半固体培养基上形成黄色至橙色的色素菌落。菌株SO2在4到25℃的温度范围内生长。完整基因组大小为4.097 Mb, SO2的DNA G+C含量为68.43%,基因组注释显示该基因组包含3862个CDS、10个rRNA、55个tRNA和1个tm-RNA。系统发育和正位分析表明,其最近的系统发育邻居是Cryobacterium sp.菌株SO1、N22、TMB1-8、LW097、TMN39-1、C. zongtaiiTMN-42、C. arcticumPAMC27867和C. soli GCJ02。基因组注释显示,菌株SO2具有β-内酰胺酶A类、头孢菌素- c去乙酰化酶和27个耐药编码基因,对头孢他啶具有耐药性。功能注释发现28.74%的预测基因功能未知。基因组挖掘表明,菌株SO2可能存在6个次生代谢物基因簇。它们由含rre、萜烯、-内酯、T3PKS、NAPAA和2do组成。这一发现表明菌株SO2含有可能参与产生具有抗菌和抗氧化活性的化合物的基因。
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引用次数: 0
Exogenous Gibberellic Acid Stimulates Bulb Dormancy Breaking and the Role of Paclobutrazol in Maintaining the Size of Harvested Bulb of Lily (Lilium sp.) cv. Tisento 外源赤霉素酸刺激百合球茎休眠打破及多效唑在维持百合收获球茎大小中的作用。Tisento
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-07-31 DOI: 10.17576/jsm-2023-5207-06
Siti Nur Anisah Siti Nur Anisah, Diah Ratnadewi, Ence Darmo Jaya Supena
Lilies are increasingly demanded in Indonesia. However, the production of lily seedlings in Indonesia still needs to be improved, causing a strong dependence on imported bulbs as the planting material and low competitiveness in foreign flower markets. Insufficient lily production is due to the decreasing quality of the bulb as the planting material and the time required for vernalization to break the bulb dormancy. The study aimed to accelerate the time of bulb dormancy breaking and maintain the size of the lily bulb to get an efficient flower production with good quality. The research was conducted in a greenhouse during the rainy and dry seasons. Various exogenous gibberellic acid (GA3) concentrations with different soaking times were applied to lily bulbs to shorten the dormancy period. The most efficient treatment was soaking the bulbs in 100 mg/L of GA3 for 16 hours, from 19-20 weeks to 12-13 weeks. Further, paclobutrazol (PBZ) was sprayed on the plants to decelerate vegetative growth and grow bulb size. The results showed that GA3 could partly substitute vernalization to break bulb dormancy, and PBZ maintained the bulb size after plant harvesting. Additionally, the plant height was suppressed, and the stem diameter, leaf chlorophyll, and bulb carbohydrate content were significantly increased under 300 mg/L PBZ treatment, resulting in the bulbs' bigger size.
印尼对百合的需求量越来越大。然而,印尼百合种苗的生产仍有待提高,导致其种植材料严重依赖进口球茎,在国外花卉市场竞争力较低。百合产量不足是由于作为种植材料的球茎质量下降以及春化打破球茎休眠所需的时间。本研究旨在加快百合球茎休眠的时间,保持球茎的大小,以获得高效优质的花卉生产。这项研究是在雨季和旱季在温室里进行的。采用不同浓度和浸泡时间的外源赤霉素(GA3)处理百合球茎,以缩短百合的休眠时间。用100 mg/L的GA3浸泡球茎16小时,从19-20周到12-13周,效果最好。此外,施用多效唑(PBZ)可以减缓植株的营养生长,使鳞茎变大。结果表明,GA3能部分替代春化来打破球茎休眠,PBZ能维持收获后的球茎大小。此外,300 mg/L PBZ处理抑制了植株高度,显著提高了茎粗、叶片叶绿素和球茎碳水化合物含量,使球茎尺寸增大。
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引用次数: 0
Mechanical Characteristics of Developed Brick from Drinking Water Sludge Under Different Firing Temperatures and Rice Husk Ash Contents 不同烧成温度和稻壳灰分掺量下饮用水污泥发育砖的力学特性
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-07-31 DOI: 10.17576/jsm-2023-5207-17
Zulfahmi Ali Rahman, Hafis Nazarah, Wan Mohd Razi Idris, Tukimat Lihan
There is a considerable interest in making alternative bricks using wastes. Firing temperature has been significantly improved the mechanical qualities of bricks. The aim of this study was to investigate into the impact of firing temperature and rice husk ash content on the mechanical properties of drinking water sludge bricks (DWS). Two types of bricks were produced; bricks made of 100% DWS (DWS100) and bricks with 80% DWS and 20% RHA (DWS80). These samples were subjected to different thermal variations of 300 °C and 700 °C for three hours. The unfired brick samples were also prepared for reference. The volume changes of the DWS100 bricks increased as the firing temperature climbed up to 500 °C, before dropped at 700 °C. A similar behaviour was also exhibited by DWS80 bricks, however it shrunk at earlier temperature of 500 °C. At 500 °C and 700 °C, the density of bricks decreased dramatically, with DWS80 bricks consistently being lesser than DWS100 bricks. The water absorption of DWS80 brick began to decrease at 500 °C, a lower temperature than that of DWS100, as the firing temperature climbed. RHA-added bricks (DWS80) were anticipated to absorb more water than DWS100 bricks, but this did not occur. This presumably induced by the constriction of clay mineral structure rather than organic matter removal at high temperature per se. The compressive strength increased with the increase in temperature. It can be inferred that RHA can decrease the compressive strength of RHA-added bricks, despite the fact that a higher fire temperature significantly increased their strength.
人们对利用废料制造替代砖很感兴趣。烧成温度大大提高了砖的机械质量。研究了烧制温度和稻壳灰分含量对饮用水污泥砖(DWS)力学性能的影响。生产了两种类型的砖;100% DWS砖(DWS100)和80% DWS和20% RHA砖(DWS80)。这些样品经受300°C和700°C的不同温度变化3小时。并制备了未烧结砖样品供参考。DWS100砖的体积变化随着烧成温度的升高而增大,在700℃时减小。DWS80砖也表现出类似的行为,但它在500°C的较早温度下收缩。在500°C和700°C时,砖的密度急剧下降,DWS80砖的密度始终小于DWS100砖。随着烧成温度的升高,DWS80砖的吸水率在低于DWS100砖的500℃时开始下降。添加rhaa的砖(DWS80)预计比DWS100砖吸收更多的水,但这并没有发生。这可能是由于粘土矿物结构的收缩,而不是在高温下有机物本身的去除。抗压强度随温度升高而升高。可以推断,尽管较高的火灾温度会显著提高添加了RHA的砖的强度,但RHA会降低砖的抗压强度。
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引用次数: 0
Adsorption of Ciprofloxacin Using Composite Film from PVA, Agarose and Maltodextrin 聚乙烯醇-琼脂糖-麦芽糊精复合膜对环丙沙星的吸附研究
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-07-31 DOI: 10.17576/jsm-2023-5207-11
Bich Ngoc Hoang, Dieu Tran Huong, Thi Cam Quyen Ngo, Thi Nhu Dung Nguyen, Long Giang Bach
Antibiotic resistance is one of the most alarming problems today. Therefore, composite membranes have been widely applied for the removal of antibiotics from water. PVA/Agarose/Maltodextrin films have been synthesized by casting with various component ratios. They were evaluated for characteristics through moisture, solubility, expansion, and BET results. The results showed that PVA/Agarose/Maltodextrin films exhibited the best viability in the aquatic environment through low solubility (68.88% ± 0.03), high swelling (431.77% ± 5.89) and pore volume (0.034969 cm³/g). The adsorption capacity of PVA/Agarose/Maltodextrin was tested for several antibiotics such as Ciprofloxacin, Tetracycline, Oxy-Tetracycline, and Chloramphenicol. The results showed that Ciprofloxacin was removed by the PVA/Agarose/Maltodextrin films better than other antibiotics. The highest antibiotic adsorption was obtained at 20 min, temperature of 30 °C, dosage of 2 g/L, pH 6, and antibiotic concentration of 40 mg/L. Ciprofloxacin adsorption was predicted through adsorption kinetic and isothermal models. The compatibility of the Pseudo First Order kinetic and Dubinin-Radushkevich isothermal has shown that adsorption takes place according to a physical adsorption mechanism with electrostatic interactions on the surface of the material. The maximum adsorption capacity recorded at 4.48 mg/g based on the Dubinin-Radushkevich isothermal.
抗生素耐药性是当今最令人担忧的问题之一。因此,复合膜在水中抗生素的去除中得到了广泛的应用。采用浇铸法制备了不同配比的PVA/琼脂糖/麦芽糊精薄膜。通过水分、溶解度、膨胀和BET结果来评估它们的特性。结果表明,PVA/琼脂糖/麦芽糊精膜溶解度低(68.88%±0.03),溶胀度高(431.77%±5.89),孔体积为0.034969 cm³/g,在水环境中具有最佳的生存能力。考察了PVA/琼脂糖/麦芽糖糊精对环丙沙星、四环素、氧四环素、氯霉素等抗生素的吸附能力。结果表明,PVA/琼脂糖/麦芽糊精膜对环丙沙星的去除效果较好。在温度为30℃、用量为2 g/L、pH为6、抗生素浓度为40 mg/L、20 min时,抗生素的吸附效果最佳。通过吸附动力学和等温模型对环丙沙星的吸附进行了预测。伪一级动力学和杜比宁-拉杜什克维奇等温的相容性表明,吸附是根据材料表面静电相互作用的物理吸附机制进行的。根据Dubinin-Radushkevich等温线测定的最大吸附量为4.48 mg/g。
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引用次数: 0
Seed Germination Characteristics as Affected by Interaction of Moisture Stress and Temperature in Sethoxydim-Resistant Biotype of Goosegrass (Eleusine indica (L.) Gaertn.) from Malaysia 湿度和温度对抗乙醛生物型鹅草种子萌发特性的影响来自马来西亚的Gaertn
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-07-31 DOI: 10.17576/jsm-2023-5207-08
Tse Seng Chuah, Chee Nam Hiew, Nursyafiqah Izzati Norzaidi, Sunny Goh Eng Giap
Understanding temperature and moisture stress that influence sethoxydim-resistant (R) goosegrass (Eleusine indica) germination is crucial for effective weed control, but little research has been done on the impact of these environmental factors on germination of the R goosegrass biotype. This research aims to confirm sethoxydim resistance in goosegrass and to examine interaction effects of different temperatures and water potentials on germination of the R goosegrass biotype. Dose–response tests showed that the R goosegrass biotype exhibited high resistance level to sethoxydim with 17-fold. In laboratory bioassays, the R goosegrass biotype germinated by 88-100% at 35 °C with water potentials ranging from 0 to -0.80 MPa, but no seed germination occurred at 10 °C and 40 °C under all water potential treatments. With rising water potentials from 0 to -0.80 MPa, seed germination at 15 to 30 °C decreased markedly. The time it took to achieve 50% seed germination (T 50) increased drastically when decreasing temperature from 35 to 15 °C. The T50 at 20 to 30 °C also increased as the water potential increased from -0.20 to -0.80 MPa. At 35 °C, however, the water potential level had no impact on T 50, implying that the R goosegrass biotype seed is water stress tolerant at 35 °C. The base temperature and base water potentials estimated were 10.6 °C and -1.28 MPa, respectively. These findings can help in determining the optimal time to apply pre-emergent and early post-emergent controls when a large proportion of R goosegrass biotype have already germinated or emerged.
了解温度和水分胁迫对耐乙氧基(sethoxydium -resistant, R)鹅毛草(Eleusine indica)萌发的影响是有效防治鹅毛草杂草的关键,但这些环境因素对鹅毛草生物型萌发的影响研究甚少。本研究旨在证实鹅草对乙氧霉素的抗性,并研究不同温度和水势对R型鹅草萌发的交互作用。剂量效应试验表明,R型鹅草对乙氧基醚具有17倍的高抗性。在实验室生物测定中,R型鹅草在35℃、水势为0 ~ -0.80 MPa条件下的萌发率为88% ~ 100%,但在10℃和40℃条件下,所有水势处理均未萌发。随着水势从0 ~ -0.80 MPa的升高,种子在15 ~ 30℃的萌发率显著降低。当温度从35°C降低到15°C时,达到50%种子发芽所需的时间(t50)急剧增加。随着水势从-0.20 MPa增加到-0.80 MPa, 20 ~ 30℃时的T50也随之增加。在35℃条件下,水势水平对t50没有影响,说明R型鹅草种子在35℃条件下具有耐水胁迫能力。碱基温度和碱基水势分别为10.6℃和-1.28 MPa。这些发现有助于确定当大部分R型鹅草已经发芽或出现时,应用发芽前和发芽后早期控制的最佳时间。
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引用次数: 0
A Comparison Between Two Discordancy Tests to Identify Outlier in Wrapped Normal (WN) Samples 两种不一致检验在包裹正态(WN)样本中识别异常值的比较
4区 综合性期刊 Q3 MULTIDISCIPLINARY SCIENCES Pub Date : 2023-07-31 DOI: 10.17576/jsm-2023-5207-19
Nurisha Mohd Zulkefli, Adzhar Rambli, Mohamad Ismeth Khan Azhar Suhaimi, Ibrahim Mohamed, Raiha Shazween Redzuan
This study focuses on comparing the performance of the Robust Circular Distance (RCDU*) (simplified version) and A statistics in detecting a single outlier in the Wrapped Normal (WN) samples. Firstly, this study proposes a simplified version of RCDU statistic. Then, the paper generates the cut-off points for both statistics taken from WN samples via a simulation study. This study also evaluates the performance of both statistics using the proportion of a correct outlier detection. As a result, for a small sample size, the performance of RCDU* and A statistics do not have a huge difference. However, for a large sample size of n=250, A statistic performs slightly better than RCDU* statistic. As an illustration of a practical example, both statistics successfully detected one outlier present in the wind direction data at Kota Bharu station.
本研究的重点是比较鲁棒圆距离(RCDU*)(简化版)和A统计量在包裹正态(WN)样本中检测单个异常值的性能。首先,本研究提出了一个简化版本的RCDU统计。然后,本文通过模拟研究生成了从WN样本中获取的两种统计数据的截止点。本研究还使用正确离群值检测的比例来评估两种统计数据的性能。因此,对于小样本量,RCDU*和a统计的性能并没有太大的差异。但是,对于n=250的大样本量,a统计性能略好于RCDU*统计。作为一个实际例子的说明,两种统计都成功地检测到Kota Bharu站风向数据中的一个异常值。
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引用次数: 0
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Sains Malaysiana
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