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USING SHEEP FACIAL GRIMACE SCALE, INFRARED THERMOGRAPHY AND CORTISOL HORMONE TO MEASURE PAIN IN SHEEP INFECTED WITH MASTITIS DISEASE 使用绵羊面部表情量表、红外热成像和皮质醇激素测量感染乳腺炎疾病的绵羊的疼痛程度
Pub Date : 2024-02-26 DOI: 10.25271/sjuoz.2024.12.1.1185
Nizar J. Hussein, Assel Al-Naqshabendy
The purpose of this study was to apply sheep pain facial expression scales (SPFES) to sheep infected with mastitis, measuring peripheral temperatures and serum cortisol hormone. Twenty-three healthy ewes and 23 infected ewes with clinical mastitis were included in this research from January 2022 to April 2023. Images were taken from each ewe to detect facial grimace scales of ewes. Nasal, eye and ear temperatures were collected using infrared thermal imaging camera. Moreover, serum cortisol hormone was collected from the blood. It was found that there was a significant decrease (p<0.01) in nasal, eye and ear temperatures of infected ewes in comparison to healthy ewes. Additionally, cortisol hormone was found significantly (p<0.01) higher in infected ewes at day 1 and day 7 compared to non-infected animals. The changes in facial expressions for all the determined five regions were significantly (p<0.01) different than healthy ewes. The total pain score was significantly (p<0.05) higher on day 1 and day 7, compared to healthy ewes. It was concluded that sheep facial grimace scale was a useful and practical tool for measuring pain in sheep. In addition, cortisol from the serum and peripheral temperatures were found to be useful pain indicators.
本研究的目的是对感染乳腺炎的绵羊应用绵羊疼痛面部表情量表(SPFES),测量外周温度和血清皮质醇激素。23 只健康母羊和 23 只感染临床乳腺炎的母羊参与了这项研究,研究时间为 2022 年 1 月至 2023 年 4 月。对每只母羊进行拍照,以检测母羊面部的狰狞鳞片。使用红外热像仪采集母羊鼻腔、眼睛和耳朵的温度。此外,还采集了血清皮质醇激素。结果发现,与健康母羊相比,受感染母羊的鼻温、眼温和耳温明显下降(p<0.01)。此外,与未感染的动物相比,受感染母羊在第 1 天和第 7 天的皮质醇激素明显升高(p<0.01)。与健康母羊相比,所有确定的五个区域的面部表情变化均有显著差异(p<0.01)。与健康母羊相比,第 1 天和第 7 天的疼痛总分明显更高(p<0.05)。结论是,绵羊面部表情量表是测量绵羊疼痛的实用工具。此外,血清中的皮质醇和外周温度也是有用的疼痛指标。
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引用次数: 0
ANTIOXIDANTS, BIOCHEMICAL, AND HEMATOLOGICAL PARAMETERS CHANGE IN WORKERS OCCUPATIONALLY EXPOSED TO RADON INHALATION AT CERTAIN CONSTRUCTION MATERIAL INDUSTRIES IN ERBIL, IRAQ 伊拉克埃尔比勒某些建筑材料工业中职业暴露于氡吸入的工人的抗氧化剂、生化和血液参数的变化
Pub Date : 2024-02-18 DOI: 10.25271/sjuoz.2024.12.1.1221
S. Othman, S. I. Mohammed, Ali H. Ahmed
This study examined the effects of radon on the endogenous antioxidants, biochemical, and hematological parameters of workers in Erbil, Iraqi Kurdistan. This was carried out to ascertain how radon affects the health of those who work in certain factories producing building materials. The case study group consisted of 70 workers, who were then divided into seven subgroups (gypsum, cement plant, lightweight block, marble, red brick 1, crushed stone, and concrete block 2), while the control group consisted of 20 healthy volunteers. The total antioxidant capacity (TAC), levels of carcinoembryonic antigen (CEA), superoxide dismutase (SOD), catalase (CAT), and glutathione peroxidase (GPX), the complete blood count (CBC), and liver function tests were evaluated. The statistical analysis revealed that the antioxidant activities and CEA levels between the case study group and the control group differed significantly. Also, antioxidant enzyme activities and indoor radon concentration, the annual effective dosage, were found to be highly significantly correlated by Pearson and Spearman analyses in the case study group. Additionally, the results demonstrated a substantial correlation in the data between the levels of CEA biomarkers and radon (r=0.478, p˂0.000). The present results showed that radon concentration increased alanine aminotransferase (ALT) activity in a radon concentration-dependent manner (r=0.263 and p ˂0.05). The aspartate aminotransferase (AST), alkaline phosphatase (ALP), and total bilirubin activities, on the other hand, were not significantly affected by radon. The most significantly influenced CBC parameter was the low white blood cells (WBC) in the case study group compared to the controls. Low platelet count (PLT) was the second-highest problematic metric. The other CBC values, however, did not significantly differ between the research group and the control group. This study offers a preliminary image of the endogenous antioxidant systems in employees, especially to show a connection between radon and the occurrence of cancer among workers in Iraq Kurdistan Region.
本研究探讨了氡对伊拉克库尔德斯坦埃尔比勒工人的内源性抗氧化剂、生化和血液参数的影响。研究的目的是确定氡对某些建筑材料工厂工人的健康有何影响。案例研究组由 70 名工人组成,然后将他们分为七个分组(石膏组、水泥厂组、轻质砌块组、大理石组、红砖 1 组、碎石组和混凝土砌块 2 组),而对照组由 20 名健康志愿者组成。研究人员评估了总抗氧化能力(TAC)、癌胚抗原(CEA)、超氧化物歧化酶(SOD)、过氧化氢酶(CAT)和谷胱甘肽过氧化物酶(GPX)的水平、全血细胞计数(CBC)和肝功能检测。统计分析显示,病例研究组与对照组的抗氧化活性和 CEA 水平差异显著。同时,通过皮尔逊和斯皮尔曼分析发现,案例研究组的抗氧化酶活性与室内氡浓度(年有效剂量)高度相关。此外,研究结果表明,癌胚抗原生物标志物水平与氡之间的数据也有很大的相关性(r=0.478,p˂0.000)。本研究结果表明,氡浓度以氡浓度依赖性方式增加了丙氨酸氨基转移酶(ALT)活性(r=0.263,p ˂0.05)。而天门冬氨酸氨基转移酶(AST)、碱性磷酸酶(ALP)和总胆红素活性则不受氡的显著影响。与对照组相比,病例研究组受影响最明显的血细胞计数参数是白细胞(WBC)偏低。血小板计数(PLT)低是第二大问题指标。不过,研究组和对照组的其他 CBC 值没有明显差异。这项研究提供了员工内源性抗氧化系统的初步图像,特别是显示了氡与伊拉克库尔德斯坦地区工人癌症发生之间的联系。
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引用次数: 0
EFFICIENT SYNTHESIS OF ZNO AS AN ELECTRODE OF PIEZOELECTRIC NANOGENERATORS 高效合成作为压电纳米发电机电极的 zno
Pub Date : 2024-02-04 DOI: 10.25271/sjuoz.2024.12.1.1205
Ribar A. Salh, M. A. Ibrahem
Piezoelectric nanogenerators (NGs) hold immense promise as self-powered devices for harvesting mechanical energy from the environment. This study introduces an efficient and scalable synthesis method for zinc oxide (ZnO) nanorods, a pivotal material in piezoelectric nanogenerators (NGs), with several key results. A Chemical Bath Deposition technique is employed, optimizing parameters such as growth time, temperature, and precursor concentrations to achieve well-aligned and high-quality ZnO nanorods. The structural and morphological characteristics of the synthesized nanorods are systematically investigated using advanced characterization techniques. The synthesized ZnO nanorods exhibit an average length of 400nm, demonstrating their slender shape. Furthermore, the study determines an energy gap value of 3.5 eV for multilayer zinc oxide thin films, indicating the transition from the valence band to the conduction band. Notably, thermal annealing at 500°C leads to a substantial increase in average output voltage, reaching 1.95 V, a fourfold improvement compared to as-deposited nanopowders. These findings emphasize the efficiency and potential of the proposed synthesis method and underscore its practical applications in enhancing energy harvesting capabilities for sustainable power generation from mechanical sources in piezoelectric NGs.
压电纳米发电机(NGs)作为从环境中获取机械能的自供电设备前景广阔。本研究介绍了压电纳米发电机(NGs)的关键材料--氧化锌(ZnO)纳米棒的高效、可扩展合成方法,并取得了几项关键成果。该研究采用了化学沉积技术,优化了生长时间、温度和前驱体浓度等参数,从而获得了排列整齐的高质量氧化锌纳米棒。利用先进的表征技术系统地研究了合成纳米棒的结构和形态特征。合成的氧化锌纳米棒平均长度为 400 纳米,显示出其细长的形状。此外,研究还确定了多层氧化锌薄膜的能隙值为 3.5 eV,表明其已从价带过渡到导带。值得注意的是,在 500°C 的温度下进行热退火可使平均输出电压大幅提高,达到 1.95 V,与沉积纳米粉体相比提高了四倍。这些发现凸显了所提出的合成方法的效率和潜力,并强调了其在压电负极材料中增强能量收集能力的实际应用,从而实现从机械源持续发电。
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引用次数: 0
EFFICIENT SYNTHESIS OF ZNO AS AN ELECTRODE OF PIEZOELECTRIC NANOGENERATORS 高效合成作为压电纳米发电机电极的 zno
Pub Date : 2024-02-04 DOI: 10.25271/sjuoz.2024.12.1.1205
Ribar A. Salh, M. A. Ibrahem
Piezoelectric nanogenerators (NGs) hold immense promise as self-powered devices for harvesting mechanical energy from the environment. This study introduces an efficient and scalable synthesis method for zinc oxide (ZnO) nanorods, a pivotal material in piezoelectric nanogenerators (NGs), with several key results. A Chemical Bath Deposition technique is employed, optimizing parameters such as growth time, temperature, and precursor concentrations to achieve well-aligned and high-quality ZnO nanorods. The structural and morphological characteristics of the synthesized nanorods are systematically investigated using advanced characterization techniques. The synthesized ZnO nanorods exhibit an average length of 400nm, demonstrating their slender shape. Furthermore, the study determines an energy gap value of 3.5 eV for multilayer zinc oxide thin films, indicating the transition from the valence band to the conduction band. Notably, thermal annealing at 500°C leads to a substantial increase in average output voltage, reaching 1.95 V, a fourfold improvement compared to as-deposited nanopowders. These findings emphasize the efficiency and potential of the proposed synthesis method and underscore its practical applications in enhancing energy harvesting capabilities for sustainable power generation from mechanical sources in piezoelectric NGs.
压电纳米发电机(NGs)作为从环境中获取机械能的自供电设备前景广阔。本研究介绍了压电纳米发电机(NGs)的关键材料--氧化锌(ZnO)纳米棒的高效、可扩展合成方法,并取得了几项关键成果。该研究采用了化学沉积技术,优化了生长时间、温度和前驱体浓度等参数,从而获得了排列整齐的高质量氧化锌纳米棒。利用先进的表征技术系统地研究了合成纳米棒的结构和形态特征。合成的氧化锌纳米棒平均长度为 400 纳米,显示出其细长的形状。此外,研究还确定了多层氧化锌薄膜的能隙值为 3.5 eV,表明其已从价带过渡到导带。值得注意的是,在 500°C 的温度下进行热退火可使平均输出电压大幅提高,达到 1.95 V,与沉积纳米粉体相比提高了四倍。这些发现凸显了所提出的合成方法的效率和潜力,并强调了其在压电负极材料中增强能量收集能力的实际应用,从而实现从机械源持续发电。
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引用次数: 0
VARIATION IN THERMAL STRESS BEHAVIOUR OF COMPOSITE MATERIALS BY THERMOMECHANICAL TECHNIQUE (TMA) 利用热机械技术(TMA)改变复合材料的热应力行为
Pub Date : 2024-01-25 DOI: 10.25271/sjuoz.2024.12.1.1210
R. H. Khalaf, N. M. Abd-Alghafour, Ahmed F. Abdulrahman
In this study, a polymeric-based composite material was made using 80% epoxy polyester 20% and unsaturated polyester resin. The polymeric composites were prepared by manual moulding method by adding a support material of silica powder to the mixture by weight (0%, 5%, 10%, and 15%) to examine one of the thermal properties which are thermal expansion. A comparison was made with the polymeric mixture before and after the reinforcement. The results of the study showed that the coefficient of thermal expansion increases with increasing temperatures, while it decreases at high temperatures. The results also showed that there is a decrease in the degree of glass transition with an increase in the concentration of the additive, and it was also noted that an increase in the percentage of silica at 15% decreases the value of the thermal expansion coefficient compared to other samples.
在这项研究中,使用 80% 的环氧聚酯 20% 和不饱和聚酯树脂制作了一种聚合物基复合材料。聚合物复合材料是通过手工成型法制备的,在混合物中按重量(0%、5%、10% 和 15%)加入二氧化硅粉末作为支撑材料,以检验其中一种热特性,即热膨胀特性。研究人员还对加固前后的聚合物混合物进行了比较。研究结果表明,热膨胀系数随着温度的升高而增大,而在高温下则会减小。研究结果还表明,随着添加剂浓度的增加,玻璃化转变程度会降低,同时还注意到,与其他样品相比,二氧化硅比例增加到 15%时,热膨胀系数值会降低。
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引用次数: 0
ENHANCING WEBSITE USABILITY TESTING: CORRELATING EYE-TRACKING, GSR, AND SUS DATA WITH RESPECT TO GENDER PREFERENCES 加强网站可用性测试:将眼动跟踪、GSR 和 SUS 数据与性别偏好相关联
Pub Date : 2024-01-23 DOI: 10.25271/sjuoz.2024.12.1.1215
Ismael A. Ali
Having a professional team of web developers can produce a professional website, but cannot guarantee an expected usable website. This study presents a comprehensive multilayer approach for examining the correlations between different layers of user consciousness in website usability testing. It utilizes visual attention data from eye-tracking, emotional engagement data from galvanic skin response, and self-reporting data from the system usability scale. Testing AUK and UoZ university websites with 18 users using the Gazepoint GP3 system revealed insightful correlations among different layers of user consciousness, such as high emotional engagement is associated with higher fixation counts and shorter time-to-complete and thus lower SUS scores. Whereas low emotional engagement is associated with lower fixation counts, longer time-to-complete, and thus higher SUS scores. Gender preferences verifies the results from the literature on female users generally experiencing higher emotional arousal thus having lower time-to-complete and lower SUS scores. Design problems are presented in the form of improvement recommendations. The findings of the study highlight the importance of considering different layers of user consciousness in website usability testing, as well as the importance of gender preferences. Finally, current limitations and future works are presented.
拥有专业的网站开发团队可以制作出专业的网站,但并不能保证网站达到预期的可用性。本研究提出了一种多层次的综合方法,用于研究网站可用性测试中不同用户意识层之间的相关性。它利用了眼动跟踪的视觉注意力数据、皮肤电反应的情感投入数据和系统可用性量表的自我报告数据。使用Gazepoint GP3系统对18名用户进行的AUK和UoZ大学网站测试显示,用户意识的不同层次之间存在深刻的关联,例如高情感投入与较高的固定次数和较短的完成时间相关,因此SUS分数较低。而低情感投入与较低的固定次数、较长的完成时间相关,因此 SUS 分数较高。性别偏好验证了文献中的结果,即女性用户的情绪亢奋程度通常较高,因此完成时间较短,SUS 分数较低。设计问题以改进建议的形式呈现。研究结果强调了在网站可用性测试中考虑不同层次用户意识的重要性,以及性别偏好的重要性。最后,介绍了目前的局限性和未来的工作。
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引用次数: 0
INVESTIGATION OF THE IMPACT OF DIFFERENT PARAMETERS ON THE MORPHOLOGY OF ELECTROSPUN POLYURETHANE NANOFIBERS 不同参数对电纺聚氨酯纳米纤维形态影响的研究
Pub Date : 2024-01-16 DOI: 10.25271/sjuoz.2024.12.1.1203
Fatima T. Sabri, M. A. Mahammed
In this research, nonwoven nanofiber mats were prepared using the electrospinning method for the solution of polyurethane polymer dissolved in acetic acid. Effects of solution concentration, solution flow rate, as well as high voltage on the morphonology and wettability of the prepared nanofibers were studied. Nanofiber morphology was investigated through the analysis of scanning electron microscopy (SEM) micrographs using ImageJ software, while the wettability of the nanofiber mat surfaces was studied through the measurement of the contact angle. Results revealed that when the concentration of the solution was changed from 8wt% to 12wt%, the average nanofiber diameter showed a significant increase from 0.326 µm to 0.380 µm, while the contact angle increased from 39 degrees to 79 degrees. Results also showed that when the applied high voltage was changed from 10 KV to 25 KV, the average nanofiber diameter decreased and then increased within the range of 0.380 to 0.497 µm and that the contact angle was increased from 81 degrees to 108 degrees showing an obvious switching from hydrophilic towards hydrophobic surface. When the syringe pump flow rate was changed from 0.012 ml/min to 0.02 ml/min, morphology measurements showed that the average nanofiber diameter showed a significant increase from 0.351 µm to 0.456 µm, and the surface contact angle was also increased from 43 degrees to 98 degrees. Finally, the results of Fourier Transform Infrared Spectroscopy (FTIR) and X-ray diffraction analysis (XRD) tests showed that the electrospun polyurethane polymer material used in this work was not changed during the electrospinning process.  
本研究采用电纺丝方法制备了溶解在醋酸中的聚氨酯聚合物溶液的无纺纳米纤维毡。研究了溶液浓度、溶液流速以及高压对所制备纳米纤维形态和润湿性的影响。纳米纤维的形态是通过使用 ImageJ 软件分析扫描电子显微镜(SEM)显微照片来研究的,而纳米纤维毡表面的润湿性则是通过测量接触角来研究的。结果显示,当溶液浓度从 8wt% 变为 12wt% 时,纳米纤维的平均直径从 0.326 µm 显著增加到 0.380 µm,接触角从 39 度增加到 79 度。结果还显示,当施加的高压从 10 KV 变为 25 KV 时,纳米纤维的平均直径在 0.380 至 0.497 µm 的范围内先减小后增大,接触角从 81 度增大到 108 度,显示出明显的亲水表面向疏水表面的转变。当注射泵的流速从 0.012 毫升/分钟变为 0.02 毫升/分钟时,形态测量结果显示纳米纤维的平均直径从 0.351 微米显著增加到 0.456 微米,表面接触角也从 43 度增加到 98 度。最后,傅立叶变换红外光谱(FTIR)和 X 射线衍射分析(XRD)测试结果表明,电纺聚氨酯聚合物材料在电纺过程中没有发生变化。
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引用次数: 0
ELECTRICAL, OPTICAL, AND CHEMICAL PROPERTIES OF GRAPHENE THIN FILMS FABRICATED BY VACUUM FILTRATION TECHNIQUE 利用真空过滤技术制备的石墨烯薄膜的电学、光学和化学特性
Pub Date : 2024-01-15 DOI: 10.25271/sjuoz.2024.12.1.1198
Shivan H. Haji, Faris A. Kochary, Sabah M. Ahmed
There has been considerable interest in graphene as a transparent electrode material because of its extraordinary features, such as high optical transmittance, high electrical conductivity, excellent thermal conductivity, exceptional mechanical strength, and remarkable electrochemical capacity. In addition, transparent conductors’ graphene thin films have been considered a promising candidate to replace currently utilized indium tin oxide films, which are unlikely to meet future demands because of their rising cost. In this study, a vacuum filtration process along with isopropyl alcohol (IPA)-assisted with direct transfer (IDT) technique is used to prepare wide-area highly conductive graphene thin films on different substrates including (glass, and PET). The graphene thin films' optical, structural, and electrical properties are studied. The graphene sheets are deposited homogeneously on the substrate, and the distribution of small graphene sheets is observed in SEM images. XPS analysis revealed that the amount of oxygen in graphene decreases significantly with annealing at 500°C and treated with HNO3. Furthermore, the graphene transparent conductive films prepared by the adjusted vacuum filtration method show low sheet resistances of 12.2, 1.41, 1.18, and 0.8 kΩ/sq with transmittances of 81%, 70%, 64.3%, and 46.4% respectively after being annealing at 500°C and treated with HNO3.
石墨烯具有高透光率、高导电率、优异的导热性、超强的机械强度和非凡的电化学能力等非凡特性,因此石墨烯作为透明电极材料备受关注。此外,透明导体石墨烯薄膜一直被认为是替代目前使用的氧化铟锡薄膜的理想候选材料,而氧化铟锡薄膜因其成本上升而难以满足未来的需求。本研究采用真空过滤工艺和异丙醇(IPA)辅助直接转移(IDT)技术,在玻璃和 PET 等不同基底上制备了大面积高导电性石墨烯薄膜。研究了石墨烯薄膜的光学、结构和电学特性。石墨烯薄片均匀地沉积在基底上,从 SEM 图像中可以观察到小石墨烯薄片的分布。XPS 分析表明,石墨烯中的氧含量在 500°C 退火并用 HNO3 处理后显著减少。此外,采用调整真空过滤法制备的石墨烯透明导电薄膜在 500°C 退火并用 HNO3 处理后,片电阻分别为 12.2、1.41、1.18 和 0.8 kΩ/sq,透光率分别为 81%、70%、64.3% 和 46.4%。
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引用次数: 0
MINDBOT: DESIGN AND IMPLEMENTATION OF A MIND-CONTROLLED EDUCATIONAL ROBOT TOY FOR DISABLED CHILDREN MINDBOT:残疾儿童心智控制教育机器人玩具的设计与实现
Pub Date : 2024-01-03 DOI: 10.25271/sjuoz.2024.12.1.1195
S. Khalid, Ismael A. Ali
The mindBot robot is a new educational robot toy that can be controlled by brain signals and voice commands. It was evaluated with children with disabilities as well as healthy children as the potential users. The most significant challenge was the size of the used Emotiv Insight electroencephalogram headset when adjusting it on the children’s’ heads. Despite all the challenges, the mindBot robot is a promising technology that could be fun and educational for disabled children. The 11 participants took 36 minutes to finish all tasks on average. This includes the time they spent setting up the robot for the first time, putting on the headset, learning how to use the robot, and using the main educational features. The System Usability Scale usability score for the robot is 71.13, which is considered to be the score of good. The future stages of improving the mindBot includes adding more mobility capabilities and adding the feature of educational assessment.
mindBot 机器人是一种新型教育机器人玩具,可通过大脑信号和语音指令进行控制。该玩具的潜在用户包括残疾儿童和健康儿童。最大的挑战是在儿童头上调节 Emotiv Insight 脑电图耳机时的尺寸。尽管挑战重重,但 mindBot 机器人仍是一项很有前景的技术,对残疾儿童来说,它既有趣又有教育意义。11 名参与者平均用了 36 分钟完成所有任务。这包括他们第一次安装机器人、戴上耳机、学习如何使用机器人以及使用主要教育功能所花费的时间。该机器人的系统可用性量表可用性得分为 71.13,属于良好。未来改进 mindBot 的阶段包括增加更多的移动能力和教育评估功能。
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引用次数: 0
INFLUENCE OF ANNEALING TEMPERATURE ON ZINC OXYSULPHIDE THIN FILMS PROPERTIES DEPOSITED BY THERMAL SPRAY TECHNIQUE 退火温度对热喷涂技术沉积的氧化锌薄膜性能的影响
Pub Date : 2023-12-28 DOI: 10.25271/sjuoz.2023.11.4.1192
M. H. Khalil, Raghad Y. Mohammed, M. Ibrahem
This article studies the effects of annealing temperatures on the stoichiometry, structure, and optical characteristics of Zinc Oxysulphide thin films deposited on glass substrates using the thermal spray method. The annealing was done in the air under a temperature of 150 ºC, 250 ºC and 350 ºC. Field Emission Scanning Electron Microscopy (FESEM), X-ray diffractometry (XRD), and a UV-Vis Spectrophotometer were utilized to examine the thin films' morphological, structure, and optical characteristics as grown and annealed samples. It has been observed that the film thickness decreases as the annealing temperature increases. The XRD pattern demonstrates that as-prepared and annealed samples at 250C, and 350C are amorphous, while film annealed at 150 C is crystalline with the hexagonal phase and orientated along (110) plane. FESEM image of the as-prepared Zinc Oxysulphide thin films shows flower-like sheet nanostructures. However, for the annealed samples, the FESEM images show cone-like with a combination of sheets and aggregate nanoparticles. EDX analysis reveals the presence of Zn, O as well as sulfur. The transmittance of the film decreases from 63% to 37% and the band gap energy reduces slightly from 3.99 to 3.92 eV as the annealing temperature increase.
本文研究了退火温度对采用热喷涂方法沉积在玻璃基底上的氧化锌薄膜的化学计量、结构和光学特性的影响。退火在空气中进行,温度分别为 150 ºC、250 ºC 和 350 ºC。利用场发射扫描电子显微镜 (FESEM)、X 射线衍射仪 (XRD) 和紫外-可见分光光度计来检测薄膜生长和退火样品的形态、结构和光学特性。结果表明,薄膜厚度随着退火温度的升高而减小。XRD 图谱显示,在 250C 和 350C 下制备和退火的样品是无定形的,而在 150 C 下退火的薄膜是晶体,具有六方相,并沿 (110) 平面取向。制备的氧化锌薄膜的 FESEM 图像显示出花朵状的片状纳米结构。然而,退火后的样品的 FESEM 图像则显示出结合了片状和聚合纳米颗粒的锥状。EDX 分析显示了锌、氧和硫的存在。随着退火温度的升高,薄膜的透射率从 63% 降至 37%,带隙能从 3.99 eV 微降至 3.92 eV。
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引用次数: 0
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