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Thermomigration of non-oriented aluminium-rich liquid zones through (110) silicon wafers 通过(110)硅片的无取向富铝液体区热迁移
O. S. Polukhin, V. V. Kravchina
The paper analyzes the reasons and factors that allow avoiding faceting of non-oriented linear zones. It is shown that in the manufacture of semiconductor chips with a large perimeter and a reverse voltage of 2000 V, the conditions sine qua non to create isolating walls on silicon wafers with an orientation different from (111) are to form an ensemble of linear zones by the method of high-temperature selective forced wetting (HSV) and to fulfill a number of requirements to the “thermomigration” photomask and zones immersion stage during TM at high temperatures. It is shown that these factors provide a stable migration of an ensemble of linear zones through wafers (110) even in a stationary temperature gradient field.For the first time in the world, the authors practically demonstrate the possibility of stable migration of an ensemble of non-oriented linear zones through silicon (110) in a stationary temperature gradient conditions, outlining the conditions and factors necessary for this process. It is assumed that when the conditions for the formation of linear zones and their immersion are met, the crystallographic orientation of the silicon wafers does not matter at all.
本文分析了无取向线状带避免饰面的原因和因素。研究表明,在制造大周长、反向电压为2000 V的半导体芯片时,在不同于(111)取向的硅片上形成隔离壁的必要条件是,通过高温选择性强制润湿(HSV)方法形成线性区集合,并满足高温TM过程中对“热迁移”掩模和区浸入阶段的一系列要求。结果表明,即使在稳定的温度梯度场中,这些因素也提供了线性区系综在晶圆中的稳定迁移(110)。在世界上第一次,作者实际证明了在固定温度梯度条件下,无取向线性带的集合通过硅(110)稳定迁移的可能性,并概述了这一过程所需的条件和因素。假设当满足线性区形成和浸入的条件时,硅片的晶体取向完全无关紧要。
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引用次数: 1
Heat transfer characteristics of miniature two-phase thermosyphons with nanofluids 纳米流体微型两相热虹吸管的传热特性
V. Kravets, D. Hurov
This paper presents and analyzes experimental data on the total thermal resistances of two-phase miniature thermosyphons with nanofluids; the geometric parameters of the thermosyphons for all experimental samples are identical: total length 700 mm, internal diameter 5 mm. The following nanofluids used as heat carriers are: aqueous nanofluid based on carbon nanotubes, aqueous nanofluid based on synthetic diamond, and aqueous nanofluid based on amorphous carbon. Much attention is also paid to the influence of the filling ratio on the heat transfer characteristics of the thermosyphons. The influence of filling ratio and types of nanofluid on the performance of miniature closed two-phase thermosyphons is demonstrated.
本文介绍并分析了纳米流体两相微型热虹吸管总热阻的实验数据;所有实验样品的热虹吸管几何参数相同:总长度700 mm,内径5 mm。用作热载体的纳米流体有:基于碳纳米管的纳米流体、基于合成金刚石的纳米流体和基于非晶碳的纳米流体。本文还着重研究了填充率对热虹吸管传热特性的影响。研究了填充率和纳米流体类型对微型封闭两相热虹吸管性能的影响。
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引用次数: 3
Evaluation of metrological characteristics of spectral analysis method for determining erythrocyte morphology 光谱分析法测定红细胞形态的计量特性评价
Y. Sokol, K. Kolisnyk, T. V. Bernads’ka
Spectral photometry is currently widely used for quantitative and qualitative analysis of biological molecules in medical biology. The method is based on the ability of molecules to absorb electromagnetic radiation. Modern clinical laboratory diagnostics extensively uses optical methods of analysis that rely on these physical properties of semitransparent objects, such as blood components. Knowing the absorption spectra of blood and its components, it is possible to quantify the concentration of all the components by solving the mathematical system of equations corresponding to these spectra. However, the existing methods of optical analysis of erythrocytes do not allow quantifying their geometric parameters, which may also indicate certain diagnostic signs and be used to analyze the clinical condition of the patient's body.The aim of this work is to evaluate the metrological characteristics of the newly developed method of determining the geometric parameters of erythrocytes, which combines spectral analysis and double annealing.The input data for the 3D imaging of erythrocytes were taken from the images of the sample both made in natural light and illuminated by a coherent light source with different wavelengths. The latter, after some additional image correlation, increases the reliability of the result. The calculation results on the errors and the measuring channel resolution of the digital interference microscope indicate an acceptable accuracy of the method. The accuracy of the three-dimensional image obtained by the proposed method is more than 20% higher than that of other known methods. This allows determining the informative geometric parameters of the structure of erythrocytes more accurately and using them to obtain additional clinical diagnostic characteristics of the patient's body.
光谱光度法在医学生物学中广泛应用于生物分子的定量和定性分析。这种方法是基于分子吸收电磁辐射的能力。现代临床实验室诊断广泛使用依赖于这些半透明物体(如血液成分)的物理特性的光学分析方法。了解血液及其成分的吸收光谱,就可以通过求解与这些光谱相对应的数学方程组来量化所有成分的浓度。然而,现有的红细胞光学分析方法不允许量化其几何参数,这些几何参数也可能指示某些诊断征象,并用于分析患者身体的临床状况。这项工作的目的是评估新开发的方法,确定红细胞的几何参数,它结合了光谱分析和双重退火的计量特性。红细胞三维成像的输入数据取自样品在自然光和不同波长的相干光源照射下的图像。后者,在一些额外的图像相关之后,增加了结果的可靠性。对数字干涉显微镜的误差和测量通道分辨率的计算结果表明,该方法具有可接受的精度。该方法获得的三维图像精度比其他已知方法提高20%以上。这可以更准确地确定红细胞结构的信息几何参数,并利用它们获得患者身体的额外临床诊断特征。
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引用次数: 0
Using a layer based on materials with a metal to semiconductor phase transition for electrothermal protection of solar cells 采用金属到半导体相变材料层,用于太阳能电池的电热保护
A. Tonkoshkur, A. Ivanchenko
One of the main problems in ensuring the reliability of solar electrical power sources is local overheating, when hot spots form in photovoltaic cells of solar arrays. It is currently considered that these negative phenomena are caused, among other things, by overvoltage in the electrical circuits of solar arrays. This leads to the appearance of defective elements and a significant decrease in the functionality of the entire power generation system up to its complete failure.This study considers the possible ways to increase the reliability of solar arrays by using thermistor thermocontacting layers for preventing overvoltage events and overheating. The authors use simulation to study electrical characteristics of a photovoltaic cell in thermal contact with an additional layer based on thermistor materials with a metal to semiconductor phase transition. Vanadium dioxide with a phase transition temperature of ~340 K is considered to be a promising material for this purpose. During the phase transition, electrical resistance sharply decreases from the values characteristic of dielectrics to the values associated with metal conductors.It is shown that such thermistor layers can be used for protecting solar cells from electrical overheating under the following basic conditions:— the layer’s resistance in the «cold» state significantly exceeds that of the lightened forward-biased solar cell;— the layer’s resistance in the «heated» state is sufficiently low compared to those of the reverse-biased photovoltaic cell and of the power source.The current and temperature of the reverse-biased photovoltaic cell are limited and stabilized, and the voltage drop sharply decreases from the moment when the temperature of the thermistor layer reaches the values close to the temperature of its transition to the low-conductivity state.The obtained results substantiate the potntial of the described approach to protect photovoltaic cells of solar modules against electric thermal overloads.
保证太阳能电源可靠性的主要问题之一是局部过热,当太阳能电池阵列的光伏电池形成热点时。目前认为,除其他因素外,这些负现象是由太阳能电池阵列电路中的过电压引起的。这导致出现有缺陷的元件,并在整个发电系统的功能显著下降,直至其完全失败。本研究考虑了通过使用热敏电阻热接触层来防止过电压事件和过热来提高太阳能电池阵列可靠性的可能方法。作者利用模拟技术研究了光伏电池在与金属到半导体相变的热敏电阻材料的附加层热接触时的电特性。相变温度为~340 K的二氧化钒被认为是一种很有前途的材料。在相变过程中,电阻从电介质的特征值急剧下降到与金属导体相关的值。研究表明,在以下基本条件下,这种热敏电阻层可以用于保护太阳能电池免受电过热的影响:-层在“冷”状态下的电阻明显超过轻化的正偏太阳能电池的电阻;-层在“热”状态下的电阻与反向偏置光伏电池和电源的电阻相比足够低。反偏光伏电池的电流和温度受到限制和稳定,从热敏电阻层温度达到接近其向低电导率状态过渡的温度的时刻起,电压降急剧下降。所获得的结果证实了所述方法保护太阳能组件的光伏电池免受电热过载的潜力。
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引用次数: 0
Particular aspects of designing longitudinal-coaxial waveguide-microstrip connectors 设计纵向-同轴波导-微带连接器的特殊方面
E. M. Glushechenko
The authors justify the use of combined longitudinal-coaxial connectors — waveguide-coaxial or waveguide-microstrip type — in new modern antenna-feeder microwave paths.Using the example of a basic coaxial waveguide-coaxial connector based on a section of a regular rectangular waveguide, the study considers the process of converting an electromagnetic wave of a regular waveguide of the main waveguide type H10 into a transverse electromagnetic wave of a coaxial line with a wave resistance (impedance) Z0 = 50 Ohm. Such a connector allows implementing good electrical parameters — matching (standing wave ratio, SWR) and linear losses — but its design is difficult to configure and cannot be reliably reproduced. However, the basic operation principles of this connector make it possible to use it as a prototype when creating modern coaxial waveguide-coaxial or waveguide-microstrip connectors.One example of such a modern connector is the sealed longitudinal-coaxial waveguide-microstrip connector based on a segment of H-shaped waveguide, shorted by an end wall on one end. Correcting the reactive component of both inductive and capacitive nature will allow achieving the required parameters of the wave impedance of the connector. With this in mind, the author has built an inductive-capacitive system consisting of a matching element in the form of a staggered fin and a corrective element in the form of a rectangular parallelepiped. To ensure the air tightness of the connector design, the segment of the coaxial line was replaced by a sealed coaxial insert, which is a serial electronic component.Particular attention was paid to the layout and design of this sealed waveguide-microstrip connector, as well as to the calculation of the overall dimensions of its elements.The article proposes an original technique for measuring the main parameters of both waveguide-coaxial and waveguide-microstrip connectors. The author forms a mathematical model of combined type connectors based on the scattering wave matrix and presents the parameters of real hermetically sealed longitudinally coaxial waveguide-microstrip connectors based on waveguide segments of various standard sizes and measured at various frequencies.
作者证明了在新型现代天线馈线微波路径中使用波导-同轴或波导-微带型组合纵向-同轴连接器。本研究以基于规则矩形波导截面的基本同轴波导-同轴连接器为例,考虑将主波导类型H10的规则波导的电磁波转换为波阻(阻抗)Z0 = 50欧姆的同轴线的横向电磁波的过程。这样的连接器可以实现良好的电气参数-匹配(驻波比,SWR)和线性损耗-但其设计难以配置,无法可靠地再现。然而,这种连接器的基本工作原理使得在创建现代同轴波导-同轴或波导-微带连接器时可以将其用作原型。这种现代连接器的一个例子是基于一段h形波导的密封纵向同轴波导微带连接器,一端被端壁缩短。纠正电感和电容性质的无功成分将允许实现所需的连接器波阻抗参数。考虑到这一点,作者建立了一个由交错翅片形式的匹配元件和矩形平行六面体形式的校正元件组成的电感-电容系统。为了保证连接器设计的气密性,将同轴线段替换为密封的同轴插件,这是一种串行电子元件。特别注意的是这种密封波导微带连接器的布局和设计,以及其元件的整体尺寸的计算。本文提出了一种测量波导同轴连接器和波导微带连接器主要参数的新方法。基于散射波矩阵建立了组合式连接器的数学模型,并根据不同标准尺寸、不同频率测量的波导段,给出了实际密封纵向同轴波导微带连接器的参数。
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引用次数: 0
Quasi-synchronous thermocompensation for ISFET-based ionometric devices. Part 1: Theory and simulation 基于isfet的离子测量器件的准同步热补偿。第1部分:理论和仿真
O. S. Pavluchenko, О. L. Kukla
Solid-state ion selective transducers, as an alternative to the traditional liquid electrolyte-filled glass electrodes, are known for over four decades now, and find their use in various areas of industry and applied science, such as in vivo analysis of the ions activity in biological and medical research, monitoring of toxic and aggressive environments, and biosensors design. However, along with potential advantages — short response time, small size, chemical inertness and durability — solid-state devices also possess certain inherent drawbacks — namely intrinsic noise, drift and instability of sensing properties, and cross-sensitivity to various interfering environmental conditions — that inhibit their widespread acceptance. Further improvement of the fabrication technology and methodology of application of these devices is thus still an important practical task even today. This paper is a first part of the two-part work dedicated to the problem of compensating the temperature dependence of a solid-state ion selective transducer output. Specifically, presented work considers the possibility of using ion-selective field-effect transistors (ISFET) that serve as primary transducers in an ionometric device, as temperature sensors. This allows compensating the temperature dependence of ionometric signal without substantial complication of the ionometer structure, and eliminates the need to include a separate thermometric channel as part of the instrument. Ionometric and thermometric channels are combined into a unified measuring path, with the sensor functions separated in time. The ISFET operation modes are switched by changing polarity of the bias voltage, and thus direction of the current flowing through the sensor. The authors propose a corresponding secondary transducer structure and simplified schematic illustrating the implementation of its key components. The concept’s applicability is supported by the circuit simulation results. Some aspects of the practical implementation of the proposed concept will be presented further in the upcoming second part of the paper.
固态离子选择性换能器作为传统液体电解质填充玻璃电极的替代品,已经有四十多年的历史了,并且在工业和应用科学的各个领域都有应用,例如生物和医学研究中离子活性的体内分析,有毒和侵袭性环境的监测以及生物传感器的设计。然而,随着潜在的优势-响应时间短,尺寸小,化学惰性和耐用性-固态器件也具有某些固有的缺点-即固有的噪声,漂移和传感特性的不稳定性,以及对各种干扰环境条件的交叉敏感性-阻碍了它们的广泛接受。因此,即使在今天,进一步改进这些器件的制造技术和应用方法仍然是一项重要的实际任务。本文是两部分工作的第一部分,致力于补偿固态离子选择性换能器输出的温度依赖问题。具体地说,提出的工作考虑了使用离子选择性场效应晶体管(ISFET)作为离子测量装置的主要换能器,作为温度传感器的可能性。这允许补偿电离信号的温度依赖性,而没有电离计结构的实质性复杂性,并消除了需要包括一个单独的测温通道作为仪器的一部分。离子通道和测温通道合并成一个统一的测量路径,传感器功能在时间上分离。通过改变偏置电压的极性来切换ISFET的工作模式,从而改变流过传感器的电流的方向。作者提出了相应的二次换能器结构,并给出了其关键部件的简化原理图。电路仿真结果验证了该概念的适用性。本文的第二部分将进一步介绍拟议概念的实际实施的一些方面。
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引用次数: 0
Influence of electrolyte nature on electrochemical properties of carbon material of plant origin 电解液性质对植物源碳材料电化学性能的影响
I. V. Semkiv, V. Vashchynskyi, A. Kashuba, Н. A. Ilchuk, M. Solovyov
Non-aqueous electrolytes are advantageous for power sources due to the increase in the operating voltage since their electrochemical stability range is much wider. It should be noted that the capacitor’s capacitance depends on the capacitance provided by the electrode material, expressed in F/g, while its voltage and resistance depend on the electrolyte. Therefore, it is very important to study the electrochemical properties of carbon material in aqueous and organic electrolytes and to determine the effect of the electrolyte on the capacitance of the capacitor formed on its basis.The cathode mixture was made of porous carbon material obtained from biomass and a binding additive. Then, it was pressed onto a nickel grid with an area of 0,5 cm2. A 30% aqueous solution of potassium hydroxide (KOH) and a 0,7-molar solution of tetraethyl ammonium tetrafluoroborate ([C2 H5 ]4 NBF4) in acetonitrile (CH3CN) was used as the electrolyte. The measurements were carried out using two- and three-electrode schemes with a silver chloride reference electrode. Modeling impedance data to equivalent electrical circuits has assisted to establish the influence of the volume charge region in the electrode material on the capacitor’s capacitive characteristics. The specific capacitance values of 125 F/g in KOH and 101 F/g in [C2 H5 ]4 NBF4 are determined by the electrolyte type used and the nature of salts and bases dissolved in it. The practical significance of the obtained results is the application of the developed methods for obtaining carbon material with developed micro- and mesoporous structures and improved physicochemical properties.
由于非水电解质的电化学稳定范围更广,其工作电压的提高对电源是有利的。需要注意的是,电容器的电容取决于电极材料提供的电容,以F/g表示,而其电压和电阻取决于电解质。因此,研究碳材料在水性和有机电解质中的电化学性能,确定电解质对在其基础上形成的电容器电容的影响是非常重要的。阴极混合物由从生物质中获得的多孔碳材料和结合添加剂制成。然后,它被压在一个面积为0.5平方厘米的镍网格上。以30%的氢氧化钾(KOH)水溶液和0.7摩尔的四氟硼酸四乙基铵([C2 H5]4 NBF4)在乙腈(CH3CN)中的溶液为电解质。测量采用二电极和三电极方案与氯化银参比电极进行。对等效电路的阻抗数据进行建模有助于确定电极材料中体积电荷区域对电容器电容特性的影响。KOH溶液的比电容值为125 F/g, [C2 H5]4 NBF4溶液的比电容值为101 F/g,这是由所使用的电解质类型和溶解在其中的盐和碱的性质决定的。所得结果的实际意义在于应用所开发的方法获得了微孔和介孔结构发达、物理化学性质改善的碳材料。
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引用次数: 0
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Технология и конструирование в электронной аппаратуре
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