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Plasma Spraying of Metal-Ceramic Composite Powders Produced by MA Method 等离子喷涂法制备金属陶瓷复合粉末的研究
Pub Date : 1900-01-01 DOI: 10.2207/qjjws.9.489
M. Fukumoto, Noriaki Yaegashi, Makoto Shimanuki, M. Umemoto, I. Okane
High performance metal matrix composite coatings could be fabricated by using the highly mixed metal-ceramic composite powders. In this study, composite powders both of Cu-Al2O3 system and of Cu-AlN system were produced by mechanical alloying (MA) method. The composite coating were made by plasma spraying of these pre-composite powders. To compare with these composite coatings, conventional coatings were made by using the conventional Cu and Al2O3 powder. The quality of the coatings obtained were evaluated by abrasion were test and the electric properties were also investigated.The main results of this study are summarized as follows, (1) In the case of spraying of MA powders, the separation of the ceramics from the metal occured due to the relative difference of specific gravity between them. Nonetheless, the sprayed coating made with MA pre-composite powders had finer microstructure and higher were resistance than made with conventional powders.(2) The electric resistivity values of the coatings made with MA powders did not scatter largely compared with those of the conventional coatings because of the homogeneous structures. Therefore, it was found that highquality composite coatings with fine and homogeneous structure can be obtained using MA powders.
利用高度混合的金属陶瓷复合粉末可以制备高性能的金属基复合涂层。采用机械合金化(MA)法制备了Cu-Al2O3体系和Cu-AlN体系的复合粉末。将预复合粉末等离子喷涂制成复合涂层。为了与这些复合涂层进行比较,采用常规的Cu和Al2O3粉末制备了常规涂层。通过磨损试验和电性能测试来评价涂层的质量。本研究的主要结果总结如下:(1)在喷涂MA粉末的情况下,陶瓷与金属的分离是由于两者比重的相对差异造成的。(2)与常规涂层相比,MA预复合粉末制备的涂层具有更细的微观结构和更高的电阻率。(2)MA预复合粉末制备的涂层由于结构均匀,其电阻率值没有出现较大的分散。因此,发现使用MA粉末可以获得结构精细均匀的高质量复合涂层。
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引用次数: 0
Correlation between Arc Phenomena and Welding Parameters in Submerged-Arc Welding 埋弧焊中电弧现象与焊接参数的关系
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS1943.50.520
K. Akahide, Teruo Uke Ukibe, J. Tsuboi
In submerged arc welding, the direction of arc column and the position of molten metal in the crater have been examined using a X-ray image intensifier TV system in order to regulate weld bead shape by controlling welding parameters.Arcs are classified into the open and buried arcs depending on the position of electrode tip to the plate surface. The arc at high welding current and high travel speed, is buried in the plate and is generated forward between the front of crater and the electrode tip, which results in a knife like shape of electrode tip. The arc at high welding current and low travel speed, is buried deeply in the plate and strikes radially between the weld pool and the electrode tip melted like a pencil. On the other hand, the open arc with low welding current is generated between the weld pool and the electrode tip over the plate surface. The direction of the arc column and the shape of the electrode tip at the open arc change in accordance with the position of molten metal in the crater.
在埋弧焊中,为了通过控制焊接参数来调节焊头形状,利用x射线图像增强电视系统检测了电弧柱的方向和熔坑内金属液的位置。根据电极端头在极板表面的位置,电弧分为开弧和埋弧。在高焊接电流和高运动速度下,电弧埋藏在焊板中,在熔坑前部和电极尖端之间向前产生,使电极尖端呈刀状。在大焊接电流和低移动速度下,电弧深埋在焊板中,在焊池和电极尖端之间呈放射状击打,像铅笔一样熔化。另一方面,焊池和电极尖端之间在板材表面产生低焊接电流的开弧。电弧柱的方向和开弧处电极尖端的形状随熔池中熔融金属的位置而变化。
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引用次数: 5
Implementation in Hardware and Its Evaluation of Dual Lines Scanning Method : Perimeter Measurement by Dual Lines Scanning Method (Second Report) 双线扫描法的硬件实现及其评价——用双线扫描法测量周长(第二报告)
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS.9.228
K. Nakashima, Yutaka Obuchi, Katsunori Inoue
The development of the high-speed algorithm, using dual lines scanning, called DLS, of perimeter measurement for the figures of binary image was described in the previous report. And also it was proved theoretically that the accuracy of the measurement with that algorithm increases by employing rectangular pixel of large vertical-horizontal ratio in the same report.At this time, the algorithm is implemented in the simple hardware and the measuring characteristics is evaluated for various shape of figures. The experimental results closely agree with the estimation by the computer simulation made beforehand.There are two ways for realizing rectangular pixel with large vertical-horizontal ratio in the present raster scanning video system, they are to increase the horizontal or to decrease the vertical resolution respectively. It is confirmed experimentally that the accuracy of measurement is improved even in latter case, in which the total resolution is decreased.As the results of experimental investigation, it can be substantiated that the DLS algorithm is practically effective for the perimeter measurement of figures.
采用双线扫描(DLS)对二值图像图形进行周长测量的高速算法的发展已在上一篇报告中进行了描述。并从理论上证明了在同一报告中采用大纵横比的矩形像元可以提高该算法的测量精度。该算法在简单的硬件上实现,并对各种形状图形的测量特性进行了评价。实验结果与事先计算机模拟的估计基本吻合。在目前的光栅扫描视频系统中,实现纵横比大的矩形像素有两种方法,分别是提高水平分辨率或降低垂直分辨率。实验证明,即使在后一种情况下,总分辨率降低,测量精度也有所提高。实验研究结果表明,DLS算法对于图形周长测量是切实有效的。
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引用次数: 0
Construction of 3-dimensional Image by Using A Characteristics of Secondary Electron Intensity with SEM and It's Application 利用扫描电镜二次电子强度特征构建三维图像及其应用
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS.9.452
M. Murata, Y. Mukai, Y. Taguchi, M. Hotta
Intensity of secondary electron induced by incident electron beam depends on a degree of inclina-tion of surface. In the present work, 3-dimensional image for fracture surface was tried to constitute by applying this secondary elecron property with improved type SEM equipment which had four secondary electron detectors to remove a image distortion caused by observating direction. As the results, we could obtain 3-dimensional image and measured direction depth of fracture surfaces by real time treatment with 32 bit personal computer. In the case, the calculation time for one fractograph analysis was about only 5 minutes.
入射电子束诱导的二次电子强度与表面倾斜度有关。本文尝试利用这一二次电子性质,利用改进型四次电子探测器的扫描电镜设备,构建断口表面的三维图像,以消除观测方向引起的图像畸变。结果表明,利用32位个人计算机对裂缝表面进行实时处理,可以获得裂缝表面的三维图像和测量方向深度。在这种情况下,一次断口分析的计算时间仅为5分钟左右。
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引用次数: 0
Brazing of Commercial Pure Titanium with Zr-based Filler Metal. 纯钛与锆基钎料的钎焊。
Pub Date : 1900-01-01 DOI: 10.2207/qjjws.9.372
Takehiko Watanabe, M. Hoshino
The work in this paper was designed to develop the brazing filler metal for commercial pure titanium (CPTi) from the viewpoint that the filler metal is composed of simpler alloy system having lower melting point and sufficient wettability comparing with Ti-based filler metals which have been developed so far. In this work, we investigated the Zr-based eutectic system filler metal and the wettability. The results of this work show that the Zr-47Cu filler metal allows brazing of CPTi below the α-β transfomation temperature and provides us with the joint possessing sufficient mechanical properties and corrosion resistance.
本文的工作是为了开发一种与目前已开发的纯钛(CPTi)钎料相比,由更简单的合金体系组成,熔点更低,润湿性更强的钎焊钎料。本文研究了锆基共晶体系填充金属及其润湿性。结果表明,Zr-47Cu钎料可以在α-β转变温度以下钎焊CPTi,并提供具有足够力学性能和耐腐蚀性的接头。
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引用次数: 1
Initiation and Propagation Characteristics of Lamellar Tearing and Root Cracking in Corner Joint 角接头片层撕裂和根部开裂的萌生和扩展特性
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS1943.49.621
Y. Ueda, Iwao Nishimura, Hideaki Iiyama, Naomichi Chiba
Lamellar tearing of opening type and root cracking occasionally occur in multipass welded corner joints.In this paper, initiation and propagation characteristics of these cracks are examined by measurement of acoustic emission (AE) or weld cracking test, and effects of diffusible hydrogen and preheat-interpass temperature on them are investigated. The result of AE measurement reveais well initiation and propagation characteristics of these cracks. Effects of diffusible hydrogen and preheat-interpass temperature are hardly observed on lamellar tearing of opening type which occurs at the position away from the heat-affected zone. The lamellar tearing is initiated and propagated principally by the developement of welding stress and strain. Root cracking in multipass welded corner joints is initiated mainly by these stress and strain.It is propagated under them, being subjected to the influence of diffusible hydrogen and preheat-interpass temperature.
在多道次焊接角接头中,偶尔会出现开口型片层撕裂和根部开裂。本文通过声发射(AE)测量或焊接裂纹试验研究了裂纹的萌生和扩展特性,并研究了扩散氢和预热间道温度对裂纹的影响。声发射测量结果揭示了这些裂缝的良好起裂和扩展特征。在远离热影响区的位置,几乎没有观察到扩散氢和预热间温度对开口型片层撕裂的影响。片层撕裂主要是由焊接应力和应变的发展引起和扩展的。多道次焊接角接头的根部开裂主要是由这些应力和应变引起的。它在它们的作用下传播,受到扩散氢和预热间温度的影响。
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引用次数: 0
Tensile Deformation Analysis of Bead Weld Based on Simple Three Zone Model 基于简单三区模型的焊缝拉伸变形分析
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS1943.50.354
Shigeo Matsushima, K. Nozawa, Kenzo Nakamura, T. Enjo
From a simple model of the bead weld constructed by three zones (base metal (BM) without heat affected zone, heat affected zone (HAZ) and weld metal (WM)), the approximate analysis for the tensile deformation of bead welds (mild steel (arc): three.zones, and copper (TIG and electron beam) and aluminum (TIG): two zones of BM and WM) have been carried out. And the confirmation for the propriety of this analysis is made by the tensile test of their bead welds.As the results, it is found that absolute values of both ratios (σ/σx) and (e/ex) are larger than 0.85 (σ and e: equivalent stress and strain, and σx and ex: normal stress and longitudinal strain), and that the tensile deformation of bead weld is approximately expressed by the tensile deformation of the heterogeneity distribution. Moreover, it is found that initial yield for mild steel, copper (TIG) and aluminum occurs in BM in the vicinity of WM, and yield for copper (electron beam) occurs near the ditch (made by the weld), and that the yielding progresses along the boundary of HAZ (for arc and TIG). Also, it is recognized that the inclination (not perpendicular in the tensile direction) of boundary of HAZ and the contignity between HAZ and WM are necessary for the occurrence of the initial yield and for the yield progress and that the variations of the stress and the strain near boundaries between their zones occurs remarkably.
从由三个区域(母材(BM)无热影响区、热影响区(HAZ)和焊缝金属(WM)构成的简单焊头模型出发,对低碳钢(电弧)焊头的拉伸变形进行了近似分析:铜(TIG和电子束)和铝(TIG): BM和WM两个区)进行了实验。并通过焊接头的拉伸试验验证了分析结果的正确性。结果表明,焊缝拉伸变形的绝对值(σ/σx)和(e/ex)均大于0.85 (σ和e分别为等效应力和应变,σx和ex分别为法向应力和纵向应变),焊缝拉伸变形近似表示为非均匀分布的拉伸变形。此外,还发现低碳钢、铜(TIG)和铝的初始屈服发生在焊缝附近的BM中,铜(电子束)的初始屈服发生在焊缝形成的沟槽附近,屈服沿热影响区边界进行(电弧和TIG)。同时,热影响区边界的倾斜(不垂直于拉伸方向)和热影响区与WM之间的亲缘关系是产生初始屈服和屈服过程的必要条件,热影响区与WM之间的边界附近应力和应变发生显著变化。
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引用次数: 0
Thermal Stresses Developed In High-strength Steels Subjected To Thermal Cycles Simulating Weld Heat-affected Zone 高强度钢在模拟焊接热影响区的热循环下产生的热应力
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS1943.35.9_780
K. Satoh, S. Matsui, T. Machida
Residual stress less than tensile yield stress of the material is obtained for usual groove welds of high-strength steels (See Fig. 1). In the present research attention was focused on the difference in thermal stress cycle between mild steel and high-strength steel welds. Experiments were made in such manner that a round bar specimen (Fig. 3) set in a rigid frame (Fig.2) was subjected to a thermal cycle simulating weld heat-affected zone. The thermal cycle was given by high frequency induction heating and air-cooling or controled-cooling. Thermal stress developed in the specimen was measured by a load-cell (capacity 2 tons) connected to the specimen. A mild steel and HY-80 steel were used for the experiments (See Table 1.)Thermal cycles measured at several points on the specimen are shown in Figs. 4 and 5. Free expan-sions as shown in Figs. 6 and 7 were obtained between end chucks of the specimen during thermal cycles. Uniform temperature distribution along parallel part of the specimen was not expected because of high frequency induction heating. Peculiar shape of the free expansion curves is obtained as the result of nonuniform temperature distribution (See Fig. 8.).Figs. 9 thru 11 show thermal stress cycles plotted for surface temperature at the center of the specimen. It was found that factors by which residual stress is lowered are the decrease in Ar transformation temperature range over which yield stress of the material is rather small and the increase in expansion during the transformation. Therefore, rapid cooling from higher temperature than Ac1 point lowers residual stress level in high yield-strength steel welds (See Fig. 12).Degree of restraint for the rigid frame used was investigated by an analogical system shown in Fig. 13. The restraint was about one-third as large as a bar with uniform temperature fixed at the ends.
高强钢一般坡口焊缝的残余应力小于材料的拉屈服应力(见图1)。本研究主要关注低碳钢与高强钢焊缝热应力循环的差异。将圆杆试件(图3)置于刚性框架(图2)中,进行模拟焊接热影响区的热循环试验。热循环采用高频感应加热和风冷或控制冷却。通过连接到试样上的负载传感器(容量2吨)测量试样中产生的热应力。实验采用低碳钢和HY-80钢(见表1)。在试样上几个点测量的热循环如图4和图5所示。在热循环过程中,试样两端卡盘之间的自由膨胀如图6和7所示。由于高频感应加热,试样平行部分的温度分布不均匀。由于温度分布不均匀,导致自由膨胀曲线形状奇特(见图8)。图9至11显示了试样中心表面温度的热应力循环。结果表明,降低残余应力的主要因素是减小相变温度范围(该温度范围内材料的屈服应力较小)和增大相变过程中的膨胀。因此,在高于Ac1点的温度下快速冷却可以降低高屈服强度钢焊缝的残余应力水平(见图12)。所使用的刚性框架的约束程度由图13所示的类比系统进行了研究。约束的大小约为棒材的三分之一,两端固定均匀温度。
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引用次数: 31
Experimental Study on the Mechanical Behavior and the Tensile Strength of Partial Penetration Groove Welded Joint 部分熔透槽焊接接头力学性能及抗拉强度试验研究
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS1943.42.302
K. Satoh, K. Seo, Genichi Higuchi, T. Yatagai
This report deals with the strength of partial penetration groove welded joint which has become a subject of general interest in architecture but of which little information is available. In this report it is found that the theoretical evaluation of the strength based on the theory of localized necking agrees with the experimental results. In the series of experiments the results obtained are as follows.1) The yield strength and the maximum strength of throat area increase with an increase of the depth of penetration (p) and decrease with an increase of the leg length (f) (cf. Fig. 8, 12, 14, 20).2) The maximum laod of the welded joint increases with an increase of the depth of penetration (p) and the leg length (f) (cf. Fig. 9, 13, 15 21).3) The fracture mode is affected with a ratio of p/f. When p/f is smaller than 1.5, the fracture arises in the fillet weld metal, and when p/f is larger than 1.5, the fracture arises between the base matel and the heat affected zone. (cf. Photo. 1, 2, 3, 5).4) In the usual design of the joint, the theoretical equation (2) or Fig. 4 is well applicable.
本报告涉及部分熔透槽焊接接头的强度,这已成为建筑界普遍感兴趣的主题,但可获得的信息很少。本文发现,基于局部颈缩理论的强度理论评价与实验结果吻合。在一系列的实验结果是follows.1)屈服强度和最大强度的喉咙区域增加渗透的深度的增加(p)和减少增加腿部长度(f) (cf,图8、12、14、20)。2)焊接接头的最大负荷增加而增加的深度(p)和腿的长度(f) (13 cf,无花果。9日,15 21)。3)断裂模式影响的比率p / f。当p/f小于1.5时,角焊缝金属发生断裂,当p/f大于1.5时,母材与热影响区之间发生断裂。(参见图1、2、3、5)。4)在通常的节点设计中,理论方程(2)或图4是适用的。
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引用次数: 1
Effect of Grain Boundary Structure on Weld Decay of Austenitic Stainless Steel (Part 1) : Crain Boundary Structure and Intergranular Corrosion in a Type 304 Stainless Steel Weld Heat Affected Zone 晶界组织对奥氏体不锈钢焊缝腐蚀的影响(一):304型不锈钢焊缝热影响区的晶界组织与晶间腐蚀
Pub Date : 1900-01-01 DOI: 10.2207/QJJWS.9.258
H. Kokawa, T. Kuwana
Grain boundary carbide precipitation and corrosion in weld heat affected zone of a type 304 austenitic stainless steel were investigated using optical and scanning electron microscopy to discuss effects of grain boundary structure on precipitation and corrosion from a crystallographic viewpoint. In the grain boundary precipitation region, the frequency of grain boundary carbide precipitation had a maximum near the coarse grained region and decreased gradually with the distance from there to the unaffected base metal region. The frequency increased with weld heat input. Strauss test of 304 steel HAZ showed that all the cracked grain boundaries after bend test had carbide precipitates and that the frequency of cracked boundary was roughly proportional to the frequency of grain boundary precipitation. Electron channel-ling pattern analyses in scanning electron microscopy showed that grain boundaries with ordered atomic structures were hardly etched after 10% oxalic acid etching test. These facts have suggested that grain boundary precipitation and corrosion in stainless steel weld heat affected zone depend sensitively on crystallographic character of grain boundary.
采用光学显微镜和扫描电镜对304型奥氏体不锈钢焊缝热影响区晶界碳化物析出和腐蚀进行了研究,从晶体学的角度探讨了晶界组织对析出和腐蚀的影响。在晶界析出区,晶界碳化物析出频率在粗晶区附近最大,随着距粗晶区距离的增加而逐渐降低。频率随焊缝热输入的增加而增加。304钢HAZ Strauss试验表明,弯曲试验后的裂纹晶界均有碳化物析出,且裂纹晶界出现的频率与晶界析出的频率大致成正比。扫描电镜的电子通道图分析表明,10%草酸腐蚀试验后,具有有序原子结构的晶界几乎没有被腐蚀。这些事实表明,不锈钢焊缝热影响区晶界的析出和腐蚀与晶界的结晶学特征密切相关。
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引用次数: 4
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Transactions of the Japan Welding Society
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