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Stress based fracture criteria for mixed-mode I/II delamination of unidirectional composite laminates 基于应力的单向复合材料层压板 I/II 混合模式分层断裂标准
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-25 DOI: 10.1016/j.compstruct.2024.118325
Tiancheng Cao , Yu Gong , Libin Zhao , Linjuan Wang , Ning Hu

Mixed mode delamination is prone to occur in composite laminates subjected to complicated loading. In current study, the modified maximum principal stress (M-MPS) criterion and the modified maximum shear stress (M-MSS) criterion considering the effect of mode ratio on the critical distance are developed to predict the mixed mode delamination of unidirectional laminates. The accuracy of the proposed fracture criteria is validated by the comparison of the predicted fracture locus curve with extensive experimental data available in the literatures, a higher correlation is observed between the predicted results and the experimental data. Finally, comprehensive discussion on the capability of the proposed M-MPS and M-MSS criteria is conducted, a dimensionless parameter named fracture index composed of the difference of elastic properties and the difference of pure mode fracture toughness is proposed to reveal the fracture mechanisms of the unidirectional composites.

在承受复杂载荷的复合材料层压板中,混合模式分层很容易发生。在本研究中,考虑到模式比对临界距离的影响,开发了修正的最大主应力(M-MPS)准则和修正的最大剪应力(M-MSS)准则,用于预测单向层压板的混合模式分层。通过将预测的断裂位置曲线与文献中的大量实验数据进行比较,验证了所提出的断裂准则的准确性,并观察到预测结果与实验数据之间具有较高的相关性。最后,对所提出的 M-MPS 和 M-MSS 标准的能力进行了全面讨论,并提出了一个由弹性特性差值和纯模式断裂韧性差值组成的无量纲参数--断裂指数,以揭示单向复合材料的断裂机制。
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引用次数: 0
Frequency trajectory and modal analysis of variable stiffness composite cylindrical shells with flange 带翼缘的变刚度复合圆柱壳的频率轨迹和模态分析
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-25 DOI: 10.1016/j.compstruct.2024.118315
Xiaofeng Liu, Wei Sun, Honghao Liu, Hongwei Ma, Hui Li

Variable stiffness composite structures show great application potential due to their flexible spatial stiffness adjustment ability. In this paper, the accurate and efficient dynamic models of variable stiffness composite cylindrical shells considering the effects of the flange are established based on a semi-analytic frame. Then, the finite element models of the corresponding structures are established by using the ANSYS commercial software. Through the comparison of the calculation results between models under two analytical frameworks, the correctness and efficiency of the proposed modeling method are well verified and reflected. In addition, an instant hammering test of a composite cylindrical shell with flange is carried out to verify the accuracy of the modeling method at the experimental level. Then, the influence of design parameters on frequency trajectories and modals of the variable stiffness composite cylindrical shell with flange is studied. The analysis results show rich and interesting phenomena, among which, the circumferential variable stiffness composite cylindrical shell with and without flange exhibits complex frequency veering behavior under continuous variations of design parameters. The research work has a certain guiding significance for the dynamic optimization design of the variable stiffness composite cylindrical shell with flange.

变刚度复合材料结构因其灵活的空间刚度调节能力而显示出巨大的应用潜力。本文基于半解析框架,建立了考虑翼缘效应的变刚度复合材料圆柱壳体精确高效的动力学模型。然后,利用 ANSYS 商业软件建立了相应结构的有限元模型。通过比较两种分析框架下模型的计算结果,很好地验证和反映了所提出建模方法的正确性和高效性。此外,还对带凸缘的复合圆柱壳体进行了瞬时锤击试验,在实验层面验证了建模方法的准确性。然后,研究了设计参数对带凸缘的变刚度复合圆柱壳的频率轨迹和模态的影响。分析结果显示了丰富而有趣的现象,其中,有翼缘和无翼缘圆周变刚度复合材料圆柱壳在设计参数连续变化的情况下表现出复杂的频率矢量行为。该研究工作对带凸缘变刚度复合圆柱壳的动态优化设计具有一定的指导意义。
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引用次数: 0
A mode localization inspired vibration control method based on the axially functionally graded design for beam structures 基于梁结构轴向功能分级设计的模态定位启发振动控制方法
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-23 DOI: 10.1016/j.compstruct.2024.118300
Xiao Mi, Zhiguang Song

Vibration control plays a vital role in engineering structures, especially for low-frequency range, because designing structures with small dimensions makes it difficult to control large-wavelength vibrations. The present study seeks another road to realize low-frequency vibration control from the view of the real vibration responses. Similar to mode shapes, deflection modes are the main distributions of vibration amplitudes on structures in low frequency. Therefore, they are also essential vibration characteristics of structures. This paper proposes an effective passive vibration control method under both non-resonant and resonant excitations based on deflection mode theory and optimal algorithm. In fact, it is just like an axially functionally graded design for structures. The equations of motion for non-uniform beam structures are formulated by Hamilton’s principle. Firstly, a desired deflection mode is artificially designed, and the beam structure is discretely divided into subunits. Then, by adjusting the thickness or elastic modulus of each subunit to make the deflection mode of the beam coincide with that of the desired one. This process is completed by the genetic algorithm (GA). After that, by experimental and simulation analyses, the deflection mode of the optimally designed beam structures coincides with that of the desired one. Therefore, the present vibration control method is verified to be correct and effective.

振动控制在工程结构中起着至关重要的作用,尤其是在低频范围内,因为设计尺寸小的结构很难控制大波长振动。本研究从真实振动响应的角度出发,寻求实现低频振动控制的另一条道路。与模态振型类似,挠度模态是结构低频振动振幅的主要分布。因此,它们也是结构的基本振动特性。本文基于挠度模态理论和最优算法,提出了一种在非共振和共振激励下的有效被动振动控制方法。事实上,这就如同结构的轴向功能分级设计。非均匀梁结构的运动方程是根据汉密尔顿原理制定的。首先,人为设计出所需的挠曲模式,并将梁结构离散地划分为若干子单元。然后,通过调整每个子单元的厚度或弹性模量,使梁的挠曲模式与所需模式相吻合。这一过程由遗传算法(GA)完成。之后,通过实验和模拟分析,优化设计的梁结构的挠曲模式与所需模式一致。因此,验证了本振动控制方法的正确性和有效性。
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引用次数: 0
Static strength assessment of short glass fibre-reinforced polyphenilenesulphide in presence of notches according to different approaches 根据不同方法对存在缺口的短玻璃纤维增强聚苯硫醚进行静态强度评估
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-22 DOI: 10.1016/j.compstruct.2024.118312
A. Resente, M. Ricotta, M. Sorgato, G. Meneghetti

In this paper the static behaviour of polyphenylenesulfide reinforced by 40% wt. short glass fibre net-shaped plain and notched specimens was investigated. The specimen geometries were obtained by injection moulding and the experimental results were compared with data obtained from machined specimens with the same material and geometries. All data were reanalysed according to several models available in the literature for orthotropic materials, to find a rapid and efficient assessment tool for predicting the strength of short glass fibre reinforced materials in the early design stages. To this end, approaches based on orthotropic linear elastic stress analysis were considered, namely the linear elastic peak stress criterion, the nominal net-stress criterion, the point stress criterion, the average stress criterion, the strain energy density criterion, the generalized stress intensity factor-based approach, the inherent flaw model, the damaged zone criterion and the Hitchen criterion. Among the models, the average stress criterion and the generalized stress intensity factor-based approach provided the most accurate predictions of the static strength, ranging from −10% to +9% and from −19% to +2%, respectively, compared to the experimental data.

本文研究了由重量占 40% 的短玻璃纤维网状平纹和缺口试样增强的聚苯硫醚的静态性能。试样的几何形状是通过注塑成型获得的,实验结果与相同材料和几何形状的机加工试样获得的数据进行了比较。所有数据都根据文献中的几个正交材料模型进行了重新分析,以找到一种快速有效的评估工具,用于在早期设计阶段预测短玻璃纤维增强材料的强度。为此,考虑了基于正交线性弹性应力分析的方法,即线性弹性峰值应力准则、名义净应力准则、点应力准则、平均应力准则、应变能密度准则、基于广义应力强度因子的方法、固有缺陷模型、受损区准则和希钦准则。在这些模型中,平均应力准则和基于广义应力强度因子的方法对静态强度的预测最为准确,与实验数据相比分别为-10%至+9%和-19%至+2%。
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引用次数: 0
A novel hybrid-stress method using an eight-node solid-shell element for nonlinear thermoelastic analysis of composite laminated thin-walled structures 使用八节点固壳元素的新型混合应力法,用于复合材料层状薄壁结构的非线性热弹性分析
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-20 DOI: 10.1016/j.compstruct.2024.118303

Composite laminated thin-walled structures, widely used in high-speed aircrafts, undergo a complex thermal–mechanical coupling environment. Geometrical nonlinearities with a thermal effect bring significant challenge to finite element analysis of structures. In this paper, a novel hybrid-stress method based on the solid-shell element is proposed for nonlinear thermoelastic analysis. An eight-node solid-shell element (CSSH8) is developed based on the assumed natural strain method and hybrid-stress formulations to overcome various locking problems and achieve an effective 3D simulation for structures with a large span-thickness ratio. The Green–Lagrange displacement-strain relation is selected to take the geometrical nonlinearities into account. The modified generalized laminate constitutive model is extended to consider both the thermal expansion and temperature-dependent material properties. A temperature variation along the laminate thickness can also be assumed in the constitutive model. Nonlinear thermoelastic equilibrium equations are derived using the Hellinger–Reissner variational principle, in which five different coupling cases for thermal–mechanical loads can be fully involved. Numerical examples demonstrate that the proposed method with CSSH8 element is insensitive to various distorted meshes and numerically robust to pass the buckling point; meanwhile large step sizes can be achieved in the path-following nonlinear thermoelastic analysis.

在高速飞行器中广泛使用的复合材料层压薄壁结构经历着复杂的热机械耦合环境。带有热效应的几何非线性给结构的有限元分析带来了巨大挑战。本文提出了一种基于固壳元素的新型混合应力法,用于非线性热弹性分析。基于假定自然应变法和混合应力公式开发了一种八节点固壳元素(CSSH8),以克服各种锁定问题,实现对大跨度-厚度比结构的有效三维模拟。选择格林-拉格朗日位移-应变关系来考虑几何非线性。修改后的广义层压板构成模型被扩展到同时考虑热膨胀和随温度变化的材料特性。构成模型中还可以假设沿层压板厚度的温度变化。利用海灵格-赖斯纳变分原理推导出非线性热弹性平衡方程,其中可完全涉及五种不同的热机械载荷耦合情况。数值实例表明,采用 CSSH8 元素的拟议方法对各种扭曲网格不敏感,在数值上稳健地通过了屈曲点;同时,在路径跟随非线性热弹性分析中可以实现大步长。
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引用次数: 0
Flexible sandwich structure MXene-Aramid Nanofiber-MXene film for adjusting infrared camouflage and multifunctional application 用于调整红外线伪装和多功能应用的柔性夹层结构 MXene-Aramid 纳米纤维-MXene 薄膜
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-20 DOI: 10.1016/j.compstruct.2024.118299
Zhenqian Lu , Xu Shen , Zhihui Li , Qi Jia

As the rapid developing in infrared detection technology, infrared camouflage has attracted increasing attention in militarily. The two-dimensional transition metal carbide/nitride (MXene)-based film have been developed in IR stealth due to the low IR emissivity. However, the adjusting thermal camouflage is still a great challenge. In this study, we successfully fabricated a sandwich-structured MXene-ANF-MXene nanocomposite film by the vacuum-assisted filtration process. The composite film displayed remarkable infrared stealth performance of large reduction in radiation temperature. The lowest IR emissivity was 0.21. Additionally, adjusting infrared disguise and temperature modulation of the film were achieved by a stable and reliable Joule heating capability. The resulting composite film also exhibited multifunctionality including an impressively high electromagneticinterference(EMI) shielding efficiency of up to 56.2 dB, excellent mechanical properties, flame retardancy, and hydrophobicity. This work offers a simple avenue for preparing multifunctional sandwich-structured composite film by vacuum-assisted filtration method, demonstrating the great promise of MXene film for multifunctional application.

随着红外探测技术的飞速发展,红外伪装在军事上越来越受到重视。基于二维过渡金属碳化物/氮化物(MXene)的薄膜由于具有较低的红外发射率,在红外隐身方面得到了发展。然而,如何调整热伪装仍然是一个巨大的挑战。在这项研究中,我们采用真空辅助过滤工艺成功制备了一种夹层结构的 MXene-ANF-MXene 纳米复合薄膜。该复合薄膜具有显著的红外隐身性能,辐射温度大幅降低。最低红外发射率为 0.21。此外,通过稳定可靠的焦耳加热能力,还实现了薄膜的红外伪装和温度调节。由此产生的复合薄膜还具有多功能性,包括令人印象深刻的高达 56.2 dB 的电磁干扰(EMI)屏蔽效率、优异的机械性能、阻燃性和疏水性。这项研究为利用真空辅助过滤法制备多功能夹层结构复合薄膜提供了一种简单的途径,证明了 MXene 薄膜在多功能应用方面的巨大前景。
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引用次数: 0
Effect of various admixtures on selected mechanical properties of medium viscosity bone cements: Part 2 – Hydroxyapatite 各种外加剂对中粘度骨水泥选定机械性能的影响:第 2 部分 - 羟基磷灰石
IF 6.3 2区 材料科学 Q1 Engineering Pub Date : 2024-06-20 DOI: 10.1016/j.compstruct.2024.118308
Robert Karpiński , Jakub Szabelsk , Przemysław Krakowski , Józef Jonak , Katarzyna Falkowicz , Mariusz Jojczuk , Adam Nogalski , Agata Przekora

Poly methyl-methacrylate (PMMA) is one of the most widely used polymer composite materials in orthopaedic and trauma surgery. However, this material can change its mechanical properties when exposed to the highly aggressive environment of the human body, which may result in joint implant loosening and thus in a need for revision surgery. Therefore, in recent years, numerous researchers have investigated the effect of adding various particles to PMMA in order to obtain a composite bone cement with enhanced mechanical properties. In our study, we examined the effect of adding different grain sizes of hydroxyapatite (HA) to the commercially available PMMA (Palamed, Heraeus) on the mechanical properties of the fabricated PMMA/HA bone cement composite. Samples were subjected to compressive loading, as this type of load reflects typical conditions in the human body after joint prosthesis implantation. Hydroxyapatite of two different grain sizes was used: 5 µm (HA5) and 10 µm (HA10). Being a naturally occurring bone mineral, hydroxyapatite can improve the biocompatibility of bone cements, which would prolong the total joint replacement (TJR) survival rate. However, when added to PMMA, HA can affect its mechanical properties. In this study, the effects of adding HA was added in 0, 1, 2, 3, 5, 8, 10 % of dry mass were analysed. Obtained results demonstrated that only the addition of 2 % HA had a significant impact on the mechanical properties of PMMA. The other percentage concentrations had no effect on PMMA properties.

聚甲基丙烯酸甲酯(PMMA)是骨科和创伤外科应用最广泛的聚合物复合材料之一。然而,当这种材料暴露在人体的高侵蚀性环境中时,其机械性能会发生变化,可能导致关节植入物松动,从而需要进行翻修手术。因此,近年来,许多研究人员都在研究在 PMMA 中添加各种颗粒的效果,以获得具有更强机械性能的复合骨水泥。在我们的研究中,我们考察了在市售的 PMMA(Palamed,Heraeus)中添加不同粒度的羟基磷灰石(HA)对制成的 PMMA/HA 骨水泥复合材料机械性能的影响。对样品进行压缩加载,因为这种类型的载荷反映了关节假体植入后人体的典型状况。使用了两种不同粒度的羟基磷灰石:5 微米(HA5)和 10 微米(HA10)。羟基磷灰石是一种天然骨矿物质,可以改善骨水泥的生物相容性,从而延长全关节置换术(TJR)的存活率。然而,当羟基磷灰石添加到 PMMA 中时,会影响其机械性能。本研究分析了添加 HA 的影响,添加量分别为干物质的 0%、1%、2%、3%、5%、8%、10%。结果表明,只有添加 2% 的 HA 才会对 PMMA 的机械性能产生显著影响。其他浓度对 PMMA 的性能没有影响。
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引用次数: 0
Experimental investigation on axial quasi-static compression and low-velocity impact behaviors of perforated thermoplastic composite cylindrical shells 穿孔热塑性复合材料圆柱壳轴向准静态压缩和低速冲击行为的实验研究
IF 6.3 2区 材料科学 Q1 Engineering Pub Date : 2024-06-19 DOI: 10.1016/j.compstruct.2024.118311
Xin Pan , Wanqi Zhao , Liming Chen , Tao Liu , Jianqiang Deng , Yan Zhang , Shaowei Zhu , Weiguo Li

Perforation in cylindrical shells is commonly a typical technique to fulfill relevant functional requirements. However, how the perforation influence the mechanical performance of thermoplastic composite cylindrical shells (TPCCS) is incompletely understood. Hence, a systematic investigation through quasi-static compression and low-velocity impact (LVI) experiments was carried out in this paper. The full-field strain distributions of TPCCS intact tubes (IT) and perforated tubes (PT) were monitored by using 3D-DIC, and the residual properties were also characterized by compression-after-impact (CAI) tests. The results show that under quasi-static compression, the structural stiffness decreases significantly with increasing perforation diameter. The perforation reduces the interference of internal random defects on the structural deformation mode, which leads to a significant strain concentration in PT. The peak force and initial stiffness under LVI are smaller than those under quasi-static compression, with IT displaying higher sensitivity to dynamic loading compared to PT. At the impact energy of 100 J, IT and PT exhibit “S”- and “X”-shaped deformation modes, respectively. CAI tests indicate that although PT has a poorer residual load-carrying capacity than IT, it retains good structural integrity and secondary energy absorption capacity. This study provides a valuable reference for the assessment and application of perforated TPCCS.

在圆柱形壳体中穿孔通常是满足相关功能要求的一种典型技术。然而,人们对穿孔如何影响热塑性复合材料圆柱形壳体(TPCCS)的机械性能还不甚了解。因此,本文通过准静态压缩和低速冲击(LVI)实验进行了系统研究。利用 3D-DIC 监测了 TPCCS 完整管(IT)和穿孔管(PT)的全场应变分布,并通过压缩后冲击(CAI)试验表征了其残余特性。结果表明,在准静态压缩条件下,结构刚度随着穿孔直径的增加而显著降低。穿孔减少了内部随机缺陷对结构变形模式的干扰,从而导致 PT 中出现明显的应变集中。LVI 条件下的峰值力和初始刚度均小于准静态压缩条件下的峰值力和初始刚度,与 PT 相比,IT 对动态加载的敏感性更高。在 100 J 的冲击能量下,IT 和 PT 分别表现出 "S "形和 "X "形变形模式。CAI 测试表明,虽然 PT 的残余承载能力比 IT 差,但它保持了良好的结构完整性和二次能量吸收能力。这项研究为评估和应用带孔 TPCCS 提供了有价值的参考。
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引用次数: 0
Effect of various admixtures on selected mechanical properties of medium viscosity bone cements: Part 3 – Glassy carbon 各种外加剂对中粘度骨水泥选定机械性能的影响:第 3 部分--玻璃碳
IF 6.3 2区 材料科学 Q1 Engineering Pub Date : 2024-06-19 DOI: 10.1016/j.compstruct.2024.118307
Robert Karpiński , Jakub Szabelski , Przemysław Krakowski , Józef Jonak , Katarzyna Falkowicz , Mariusz Jojczuk , Adam Nogalski , Agata Przekora

Bone cements based on poly methyl-methacrylate (PMMA) are among the most widely used polymer composites in orthopaedic surgery. They play a key role in fixing the endoprosthesis with the bone, and, as such, are the weakest link in total joint replacement (TJR) surgeries. A fast, premature decrease in the mechanical properties of PMMA in an aggressive environment, such as the human body, can lead to TJR loosening, which results in the necessity for revision surgery. In recent years researchers have undertaken studies on the possibility of enhancing the mechanical properties of PMMA by adding various admixtures in different concentrations. In this study we present the results of the mechanical properties of samples made of the commercially available and widely used in orthopaedic surgery PMMA bone cement (Palamed® Heraeus) that was admixed with glassy carbon (GC) using different concentrations. All samples were subjected to compression testing. Compression reflects the load mechanism acting on PMMA in the human body after TJR implantation. The study involved comparing selected mechanical parameters of both samples prepared according to the manufacturer’s instructions and samples prepared with the addition of GC with grain sizes of 0.4–12 μm and 20–50 μm. Although this material can potentially increase the mechanical strength of PMMA, serious contamination with GC can lead to PMMA polymerization impairment due to the thermal properties of GC and, consequently, affect the mechanical properties of PMMA. GC was added in the following w/w concentrations: 1, 2, 3, 5, 8 and 10 %. Results revealed a significant decrease in the compression strength of PMMA following the addition of 20–50 μm GC, which resulted from the disturbances in standard polymerization process conditions (time and temperature). Interestingly, the addition of 0.4–12 μm GC did not affect significantly the compressive strength of the material in the tested range of concentration.

基于聚甲基丙烯酸甲酯(PMMA)的骨水泥是骨科手术中使用最广泛的聚合物复合材料之一。它们在固定骨内假体方面起着关键作用,因此是全关节置换(TJR)手术中最薄弱的环节。在人体等侵蚀性环境中,PMMA 的机械性能过快、过早地下降会导致全关节置换术松动,从而导致翻修手术的必要性。近年来,研究人员对通过添加不同浓度的各种外加剂来增强 PMMA 机械性能的可能性进行了研究。在本研究中,我们展示了在骨科手术中广泛使用的市售PMMA骨水泥(Palamed® Heraeus)样品的机械性能结果,这些样品中掺入了不同浓度的玻璃碳(GC)。所有样品都进行了压缩测试。压缩反映了植入 TJR 后 PMMA 在人体中的负载机制。研究包括比较按照制造商说明制备的样品和添加了晶粒尺寸为 0.4-12 μm 和 20-50 μm 的 GC 后制备的样品的选定机械参数。虽然这种材料有可能提高 PMMA 的机械强度,但由于 GC 的热特性,GC 的严重污染会导致 PMMA 聚合受阻,进而影响 PMMA 的机械特性。添加 GC 的重量百分比浓度如下:1%、2%、3%、5%、8% 和 10%。结果表明,添加 20-50 μm GC 后,PMMA 的压缩强度明显降低,这是标准聚合工艺条件(时间和温度)受到干扰所致。有趣的是,在测试的浓度范围内,添加 0.4-12 μm GC 对材料的压缩强度并无明显影响。
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引用次数: 0
Effect of various admixtures on selected mechanical properties of medium viscosity bone cements: Part 1 – α/β tricalcium phosphate (TCP) 各种外加剂对中粘度骨水泥选定机械性能的影响:第 1 部分 - α/β 磷酸三钙 (TCP)
IF 6.3 2区 材料科学 Q1 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-06-19 DOI: 10.1016/j.compstruct.2024.118306
Robert Karpiński , Jakub Szabelski , Przemysław Krakowski , Józef Jonak , Katarzyna Falkowicz , Mariusz Jojczuk , Adam Nogalski , Agata Przekora

Every year millions of people around the world suffer from joint and bone diseases and require orthopaedic surgery. Owing to its unique properties such as biocompatibility and ability to bond bones with orthopaedic implants, poly methyl-methacrylate (PMMA) is among the most widely used polymer composites for bone cements in orthopaedic and trauma surgery. On the other hand, this material is characterized by low mechanical properties, which can lead to accelerated implant loosening in aggressive environments, such as the human body. Over the years, researchers have studied PMMA, especially its failure mechanism. Various additives to PMMA have been proposed to enhance the mechanical properties of this material. This study investigated the effect of mixing PMMA with α-TCP (PMMA/α-TCP bone cement composite) and β-TCP (PMMA/β-TCP bone cement composite) on its mechanical properties. The study was conducted on commercially available PMMA (Haraeus Palamed) mixed with α-TCP and β-TCP in different concentrations. TCP has bacteriostatic properties and, as a bone compatible material, it stimulates bone regeneration and bone ingrowth, which highly increases the survival rate of PMMA bonding. However, the addition of particles to PMMA can affect mechanical properties of bone cements. In this study, the effects of 0, 1, 2, 3, 5, 8 and 10% dry mass concentration of TCP in bone cement on the mechanical properties of PMMA were investigated. Samples were subjected to compressive loading. This loading mode is typical of the human body after joint prosthesis implantation. The analysis involved comparing selected mechanical parameters of samples prepared according to manufacturer’s instructions and of samples prepared with the addition of α-TCP and β-TCP. Results demonstrated that the addition of β-TCP, whose crystals are triangular, did not affect the mechanical properties of PMMA. On the other hand, the addition of more than 3% dry mass α-TCP, the inner structure of which is hexagonal, led to a slight yet significant decrease in the compressive strength of PMMA.

全世界每年都有数百万人罹患关节和骨骼疾病,需要进行矫形手术。聚甲基丙烯酸甲酯(PMMA)具有独特的生物相容性和骨骼与骨科植入物粘合的能力等特性,是骨科和创伤手术中使用最广泛的骨水泥聚合物复合材料之一。另一方面,这种材料的机械性能较低,在人体等侵蚀性环境中会导致植入物加速松动。多年来,研究人员一直在研究 PMMA,尤其是其失效机制。人们提出了各种添加剂来提高 PMMA 的机械性能。本研究调查了 PMMA 与 α-TCP (PMMA/α-TCP 骨水泥复合材料)和 β-TCP (PMMA/β-TCP 骨水泥复合材料)混合对其机械性能的影响。研究对象是混合了不同浓度的 α-TCP 和 β-TCP 的市售 PMMA(Haraeus Palamed)。TCP 具有抑菌特性,作为一种骨兼容材料,它能刺激骨再生和骨生长,从而大大提高 PMMA 粘合剂的存活率。然而,在 PMMA 中添加颗粒会影响骨水泥的机械性能。本研究调查了骨水泥中 TCP 干质量浓度为 0、1、2、3、5、8 和 10% 时对 PMMA 机械性能的影响。对样品进行了压缩加载。这种加载模式是关节假体植入后人体的典型加载模式。分析包括比较根据制造商说明制备的样品和添加了 α-TCP 和 β-TCP 的样品的选定机械参数。结果表明,添加晶体为三角形的 β-TCP 不会影响 PMMA 的机械性能。另一方面,添加超过 3% 干重的 α-TCP(其内部结构为六角形)会导致 PMMA 的抗压强度轻微但显著地降低。
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Composite Structures
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