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2017 IEEE 17th International Conference on Nanotechnology (IEEE-NANO)最新文献

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Label-free electrochemical detection of brain-derived neurotrophic factor based on a novel immune microelectrode array 基于新型免疫微电极阵列的脑源性神经营养因子无标记电化学检测
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117413
Huiren Xu, Jinping Luo, Yang Wang, Yilin Song, Li Wang, Xinxia Cai
Brain-derived neurotrophic factor (BDNF) has been shown to play an important role in numerous processes of functional and structural synaptic plasticity in the mammalian central nervous system. In this work, we report a novel immune microelectrode array (MEA) for electrochemical detection of BDNF without labeling step. The chitosan-thionine-multi-walled carbon nanotubes (CS-THI-MWCNTs) composite films as the bio-sensitive film are modified onto the MEA by electrochemical deposition and successfully adopted to immobilize anti-BDNF for the fabrication of electrochemical immune MEA. The THI acted as an electrochemical indicator for the immune response of BDNF. Due to surface-controlled process of THI redox reaction, the increasing formation of anti-BDNF-BDNF immunocomplex resulted in the decreased response currents of THI and the response currents were inversely proportional to the concentrations of corresponding BDNF. The test results of performance revealed that the label-free electrochemical immune MEA had a good stability, selectivity and the limit of detections for BDNF is 5 pg/mL. A linear calibration plot for detection of BDNF was obtained in a wide concentration range from 0.01 ng/mL to 100 ng/mL (r = 0.9995). This novel electrochemical immune MEA has potential applications to detect BDNF for neuroscience research.
脑源性神经营养因子(Brain-derived neurotrophic factor, BDNF)在哺乳动物中枢神经系统突触可塑性的许多功能和结构过程中发挥重要作用。在这项工作中,我们报道了一种新的免疫微电极阵列(MEA),用于电化学检测BDNF而不需要标记步骤。通过电化学沉积将壳聚糖-硫代-多壁碳纳米管(cs - ti- mwcnts)复合膜作为生物敏感膜修饰在MEA上,成功地固定化了抗bdnf,制备了电化学免疫MEA。THI可作为BDNF免疫应答的电化学指标。由于THI氧化还原反应的表面控制过程,anti-BDNF-BDNF免疫复合物的形成增加,导致THI的反应电流降低,反应电流与相应的BDNF浓度成反比。性能测试结果表明,无标记电化学免疫MEA具有良好的稳定性和选择性,对BDNF的检出限为5 pg/mL。在0.01 ~ 100 ng/mL的浓度范围内,建立了BDNF检测的线性校准图(r = 0.9995)。这种新的电化学免疫MEA在神经科学研究中检测BDNF具有潜在的应用前景。
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引用次数: 3
High temperature piezoelectric bulk acoustic wave mass sensor for thermogravimetric analysis of nano-layer polymer 用于纳米层聚合物热重分析的高温压电体声波质量传感器
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117353
Hongfei Zu, Qing-Ming Wang, Yanqing Zheng
The acoustic wave (AW) sensors can response to a physical, chemical, or biological stimulus in a sensitive and real-time manner, so they have drawn increasing attraction in recent years. Among the AW sensors, the piezoelectric ones show a lot of extraordinary merits such as high resolution, wide frequency and temperature ranges, high stability, low power consumption, and low cost, and they are able to sense many physical and chemical quantities such as temperature, pressure, mass, gas concentration, and liquid viscosity [1-3]. To date, many surface acoustic wave (SAW) sensors [4], thin film bulk acoustic resonators (FBAR) [5], and bulk acoustic wave (BAW) [6] sensors have been reported as mass sensors. Compared to the former two types, BAW mass sensors are with the property of simple preparation process, easy to use, high temperature-tolerance, high repeatability and durability, and little damping, because neither the interdigitated transducers (IDTs) nor the functional piezoelectric thin film is needed. Therefore, piezoelectric BAW mass sensors that can be used at elevated temperature range are ideal devices for thermogravimetric analysis (TGA) applications.
声波传感器能够对物理、化学或生物刺激作出灵敏、实时的响应,近年来受到越来越多的关注。在AW传感器中,压电传感器表现出高分辨率、宽频率和宽温度范围、高稳定性、低功耗、低成本等非凡的优点,能够感知温度、压力、质量、气体浓度、液体粘度等许多物理和化学量[1-3]。迄今为止,许多表面声波(SAW)传感器[4]、薄膜体声谐振器(FBAR)[5]和体声波(BAW)[6]传感器已被报道为质量传感器。与前两种类型的质量传感器相比,由于不需要交叉换能器(idt)和功能压电薄膜,因此具有制备工艺简单、使用方便、耐高温、重复性和耐用性高、阻尼小等特点。因此,可以在高温范围内使用的压电BAW质量传感器是热重分析(TGA)应用的理想设备。
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引用次数: 0
Numerical modeling and simulation of stable nanowire CdS-CdTe solar cells 稳定纳米线CdS-CdTe太阳能电池的数值模拟与仿真
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117357
Hongmei Dang, E. Ososanya, Nian Zhang, Vijay Singh
Nanowire CdS-CdTe solar cells have been fabricated and their reliability was measured in annealing furnace at 120 °C ambient air for 120 hours. The Numerical simulation models were established to simulate measured J-V characteristics of the nanowire solar cells after fabrication and after the 120 hour thermal annealing. Simulation models demonstrate that donor trap concentration in the CdTe layer is increased from 7.2∗1014/cm3 to 7.6∗1014/cm3 after 120 hour annealing. However, acceptor traps in the CdS nanowires maintain identical concentration after 120 hour annealing. Simulation models indicate that donor traps in the CdTe layer mainly contribute to efficiency loss of the nanowire solar cells. Low defect feature of the CdS nanowires plays a role in device reliability.
制备了纳米线CdS-CdTe太阳能电池,并在120℃环境空气中进行了120小时的可靠性测试。建立数值模拟模型,模拟纳米线太阳能电池制备后和热处理120 h后的J-V特性。模拟模型表明,经过120小时退火后,CdTe层中的供体陷阱浓度从7.2∗1014/cm3增加到7.6∗1014/cm3。然而,CdS纳米线中的受体陷阱在120小时退火后仍保持相同的浓度。仿真模型表明,CdTe层中的供体陷阱是导致纳米线太阳能电池效率损失的主要原因。CdS纳米线的低缺陷特性对器件的可靠性起着重要的作用。
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引用次数: 1
Fabrication and characterization of humidity sensors based on CVD grown MoS2 thin film 基于CVD生长MoS2薄膜的湿度传感器的制备与表征
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117408
Shiqi Guo, A. Arab, S. Krylyuk, A. Davydov, M. Zaghloul
Recent advances in two-dimensional (2D) transition metal dichalcogenides have demonstrated their potential application in chemical sensors. However, the chemical vapor deposition (CVD) grown molybdenum disulfide (MoS2) humidity sensors are still largely unexplored. In this work, MoS2 thin films were grown on 1 cm2 sapphire substrates through sulfurization of e-beam deposited Mo layers. The MoS2 film morphology, thickness, and crystallinity were characterized by AFM and Raman spectroscopy. The two-terminal devices were fabricated with e-beam evaporated interdigitated electrodes (IDEs) on top of the MoS2 surface. The water vapor sensing was tested at various humidity levels with the observed increase in the device resistance response to humidity due to the charge transfer mechanism. We found the devices to be reproducible and with excellent dynamic hysteresis. The sensitivity, fast response and recovery proved that CVD growth MoS2 thin film could be scaled up for humidity and gas sensing applications.
二维(2D)过渡金属二硫族化合物的最新进展证明了它们在化学传感器中的潜在应用。然而,化学气相沉积(CVD)生长的二硫化钼(MoS2)湿度传感器在很大程度上仍未被开发。在这项工作中,通过电子束沉积Mo层的硫化,在1cm2的蓝宝石衬底上生长了MoS2薄膜。利用原子力显微镜和拉曼光谱对二硫化钼薄膜的形貌、厚度和结晶度进行了表征。采用电子束蒸发交叉电极(ide)在二硫化钼表面上制备了双端器件。在不同湿度水平下测试了水蒸气传感,观察到由于电荷转移机制,器件对湿度的电阻响应增加。我们发现该装置具有良好的可重复性和动态迟滞性。灵敏度、快速响应和恢复证明了CVD生长MoS2薄膜可以扩大湿度和气敏应用。
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引用次数: 3
Nanocrystalline and amorphous FeAlSn alloy prepared by mechanical alloying 机械合金化法制备纳米晶和非晶FeAlSn合金
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117450
Z. Hamlati, M. Azzaz, D. Martinez-Bianco, J. Blanco, P. Gorria
A nanostructured disordered FeAlSn solid solution of Fe-26% Al-2% Sn composition was obtained from elemental Fe, Al and Sn powders using a high-energy ball mill. X-ray diffraction and electron microscopy supported by Mössbauer spectroscopy techniques have been applied to follow changes in the microstructure, phase composition and magnetic properties in dependence on milling time. The transformation of the phase depends upon the milling time. With the increase of milling time all Al and Sn atoms dissolved in the bcc Fe and the final product of the MA process was the nanocrystalline Fe (Al, Sn) solid solution in a metastable state with large amount of defects and mean crystallite size of 5 nm. The electron microscope observations show morphology of powder particles and changes in chemical composition during mechanical treatment. The changes in composition are observed at samples formed by mechanical alloying. On the other hand the composition of Fe72Al26Sn2 pieces is influenced by milling. Magnetic properties of the nanocrystalline mechanically alloyed FeAlSn were also investigated and were related to the microstructural changes.
采用高能球磨机将铁、铝、锡单质粉末制备成Fe-26% Al-2% Sn的纳米结构无序FeAlSn固溶体。在Mössbauer光谱技术支持下,x射线衍射和电子显微镜已经被应用于跟踪微观结构、相组成和磁性能随铣削时间的变化。相的转变取决于铣削时间。随着磨矿时间的延长,Al和Sn原子全部溶解在原铁中,MA工艺的最终产物为亚稳态的纳米晶Fe (Al, Sn)固溶体,缺陷较多,平均晶粒尺寸为5 nm。电镜观察显示了机械处理过程中粉末颗粒的形态和化学成分的变化。在机械合金化形成的样品中观察到成分的变化。另一方面,铣削对Fe72Al26Sn2合金的成分也有影响。研究了纳米晶机械合金化FeAlSn的磁性能及其与微观组织变化的关系。
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引用次数: 0
Nylon-6 based nanocomposite films for capacitor applications 电容器用尼龙-6基纳米复合薄膜
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117497
Amoghavarsha Mahadevegowda, C. Johnston, P. Grant
Nylon-6 and Al based nanocomposite films were fabricated via a scalable vacuum co-deposition technique. The relative deposition rates of the constituent phases — nylon-6 (matrix) and Al (filler) — were varied systematically to yield films of different compositions and their dielectric properties, particularly the measured dielectric constants k, were compared with predictions of effective medium expressions. The effect of absorbed water, temperature and heat treatment on k of the nano-films were studied. X-ray photoelectron spectroscopy revealed the presence of an Al-based oxide, which was correlated to the observed enhancement in the dielectric properties of the nanocomposites. The effect of the relative deposition rates of the constituent phases on k and the chemistry of the deposited films fabricated via co-deposition was studied and explained using X-ray photoelectron spectroscopy results.
采用可扩展真空共沉积技术制备了尼龙-6和铝基纳米复合薄膜。系统地改变了组成相-尼龙-6(基体)和Al(填料)的相对沉积速率,以产生不同成分的薄膜,并将其介电性能,特别是测量的介电常数k与有效介质表达式的预测进行了比较。研究了吸收水分、温度和热处理对纳米膜k的影响。x射线光电子能谱显示了al基氧化物的存在,这与观察到的纳米复合材料介电性能的增强有关。利用x射线光电子能谱分析结果,研究了各组分相对沉积速率对k和共沉积膜化学性质的影响。
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引用次数: 0
Fabrication, calibration, and recovery of chemical nanosensor array for ammonia detection 用于氨检测的化学纳米传感器阵列的制造、校准和回收
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117436
Quan Tao, F. Lan, Minlin Jiang, Guangyong Li
The low selectivity of nanosensors is one of their major obstacles for their wide deployment. To enhance the selectivity, nanosensor array made from zinc oxide (ZnO) nanowires and carbon nanotubes (CNTs) was assembled through dielectrophoresis (DEP). The fabricated nanosensor array was used to detect ammonia (NH3) in a well-controlled environment at room temperature. Because of their opposite material types, ZnO nanowire based sensor behaved oppositely to CNT based sensor. In this study, it is also demonstrated that DC biases can quickly recover both sensing elements. After collecting sensing signals from two transducers under different NH3 concentrations, the concentration of NH3 can be estimated through regression methods. It is shown that quadratic model with the lasso performs well on the collected data.
纳米传感器的低选择性是其广泛应用的主要障碍之一。为了提高纳米传感器的选择性,采用介质电泳(DEP)技术将氧化锌(ZnO)纳米线和碳纳米管(CNTs)组装成纳米传感器阵列。所制备的纳米传感器阵列可在室温条件下对氨(NH3)进行检测。由于其材料类型相反,基于ZnO纳米线的传感器与基于碳纳米管的传感器表现相反。在这项研究中,还证明了直流偏置可以快速恢复两个传感元件。采集两个传感器在不同NH3浓度下的传感信号,通过回归方法估算NH3浓度。结果表明,带套索的二次模型对所收集的数据有较好的处理效果。
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引用次数: 1
Amplitude calibration of quartz tuning fork (QTF) force sensor with an atomic force microscope 用原子力显微镜标定石英音叉力传感器的振幅
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117406
Danish Hussain, Hao Zhang, Jianmin Song, Wen Yongbing, Xianghe Meng, F. Xinjian, Hui Xie
Amplitude calibration of the quartz tuning fork (QTF) sensor includes the measurement of the sensitivity factor (αTF). We propose, AFM based methods (cantilever tracking and z-servo tracking of the QTF's amplitude of vibration) to determine the sensitivity factor of the QTF. The QTF is mounted on a xyz-scanner of the AFM and a soft AFM probe is approached on the apex of a tine of the QTF by driving the z-servo and using the normal deflection voltage (Vtb) of position sensitive detector (PSD) as feedback signal. Once the tip contacts the tine, servo is switched off. QTF is electrically excited with a sinusoidal signal from OC4 (Nanonis) and amplitude of the QTF's output at transimpedance amplifier (Vtf) and amplitude of VTB (Vp) is measured by individual lock-in amplifiers which are internally synchronized to the phase of the excitation signal of the QTF. Before, the measurements optical lever is calibrated. By relating the both voltages (Vp & Vtf), sensitivity factor of the QTF (αTF) is determined. In the second approach, after the tip contacts the tine, the z-servo is switched off firstly, then the feedback signal is switched to Vp and frequency sweep for the QTF, Vtb as well as z-servo are started, instantaneously. To keep the Vp at set-point the feedback control moves the z-servo to track the vibration amplitude of the QTF and thus the distance traveled by the z-servo (Δζ) during sweep is equal to the fork's amplitude of vibration (ΔxTF). αtf is determined by relating Δz and VTF. Both approaches can be non-destructively applied for QTF sensor calibration. AFM imaging of the AFM calibration grating TGZ1 (from NT-MDT Russia) has been performed with a calibrated QTF sensor.
石英音叉(QTF)传感器的振幅校准包括灵敏度因子αTF的测量。我们提出了基于AFM的方法(悬臂跟踪和z伺服跟踪QTF的振动幅度)来确定QTF的灵敏度因子。QTF安装在原子力显微镜的z-扫描仪上,利用位置敏感探测器(PSD)的法向偏转电压(Vtb)作为反馈信号,驱动z-伺服装置接近QTF的一个时间顶点上的软AFM探针。一旦尖端接触到时间,伺服被关闭。QTF由来自OC4 (Nanonis)的正弦信号电激励,在透阻放大器(Vtf)处的QTF输出幅度和VTB的幅度(Vp)由单独的锁相放大器测量,这些锁相放大器内部与QTF激励信号的相位同步。之前,测量光杠杆是校准的。通过两个电压(Vp和Vtf)的关联,确定了QTF的灵敏度因子(αTF)。在第二种方法中,在尖端接触时间后,首先关闭z-伺服,然后将反馈信号切换到Vp,并立即启动QTF, Vtb和z-伺服的扫频。为了使Vp保持在设定点,反馈控制移动z伺服器以跟踪QTF的振动幅度,因此z伺服器(Δζ)在扫描期间行进的距离等于叉子的振动幅度(ΔxTF)。αtf由Δz与VTF的关系确定。两种方法均可无损地用于QTF传感器标定。利用校准后的QTF传感器对AFM校准光栅TGZ1(来自NT-MDT俄罗斯)进行了AFM成像。
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引用次数: 1
Competitive intelligence — Understanding current trends in the patent landscape for nanomaterials 竞争情报-了解纳米材料专利领域的当前趋势
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117271
Keith D. Weiss, L. G. Almeda
Identifying the technology trends, key patents to be aware of, the key players active in the field, the product areas that are heavily patented or scarcely addressed, and the focus of a company's competitors represent crucial aspects of developing a successful strategic plan, determining a company's freedom to make and sell their product, and focusing future research & product development efforts. These areas of concern may be addressed by the creation and analysis of a patent landscape associated with the technology behind a company's product. A process for creating and analyzing a patent landscape is provided using the area of nanomaterials as a case study.
确定技术趋势、需要注意的关键专利、活跃在该领域的主要参与者、专利含量高或很少涉及的产品领域,以及公司竞争对手的关注点,这些都是制定成功战略计划的关键方面,决定了公司制造和销售产品的自由,以及关注未来的研究和产品开发工作。可以通过创建和分析与公司产品背后的技术相关的专利景观来解决这些问题。以纳米材料领域为例,提供了一个创建和分析专利景观的过程。
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引用次数: 3
Impact of dielectric material and oxide thickness on the performance of Carbon Nanotube Field Effect Transistor 介质材料和氧化物厚度对碳纳米管场效应晶体管性能的影响
Pub Date : 2017-07-01 DOI: 10.1109/NANO.2017.8117461
Ayesha Shaukat, R. Umer, N. Islam
This paper demonstrates the performance of Carbon Nanotube Field Effect Transistor (CNTFET) in ballistic regime. It shows the effect of dielectric material and oxide thickness on different performance parameters of device like Carrier Injection Velocity (vinj), Drain Induced Barrier Lowering (DIBL), Subthreshold Swing (SS), Transconductance (gm), Output Conductance (gd) and Voltage Gain (Av). The results illustrate that although Silicon dioxide (SiO2) has lowest SS, but still it cannot be used as a dielectric medium in CNTFETs due to high DIBL, lower gm, gd and Av. On the other hand, Zarconium Oxide (ZrO2), Hafnium Oxide (HfO2) and Titanium oxide (TiO2) seem to be better options for dielectric medium of the device. The impact of the said changes is also observed and analyzed in I-V characteristics of the device.
本文论证了碳纳米管场效应晶体管(CNTFET)在弹道状态下的性能。给出了介质材料和氧化物厚度对载流子注入速度(vinj)、漏极势垒降低(DIBL)、亚阈值摆幅(SS)、跨导(gm)、输出导(gd)和电压增益(Av)等器件性能参数的影响。结果表明,二氧化硅(SiO2)虽然SS最低,但由于DIBL高,gm、gd和Av较低,仍不能作为cntfet的介电介质。另一方面,氧化锆(ZrO2)、氧化铪(HfO2)和氧化钛(TiO2)似乎是该器件较好的介电介质选择。在器件的I-V特性中也观察和分析了上述变化的影响。
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引用次数: 7
期刊
2017 IEEE 17th International Conference on Nanotechnology (IEEE-NANO)
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