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Multi-scale fatigue damage analysis in filament-wound carbon fiber reinforced epoxy composites for hydrogen storage tanks 用于储氢罐的丝状缠绕碳纤维增强环氧树脂复合材料的多尺度疲劳损伤分析
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100537
Imen Feki , Mohammadali Shirinbayan , Samia Nouira , Robert Tie Bi , Jean-Baptiste Maeso , Cedric Thomas , Joseph Fitoussi
This article presents the findings of a multi-scale experimental study on carbon fiber-reinforced epoxy composites (CFRP) used in lightweight hydrogen storage pressure vessels produced via filament winding. The research employs a combination of tension-tension load-controlled fatigue tests and high-resolution physical-chemical characterization and porosity quantification to assess the impact of porosity on mechanical performance. The findings demonstrate that porosity has a detrimental impact on mechanical properties, acting as nucleation sites for damage mechanisms such as crack initiation, fiber-matrix separation and fiber breakage. At the mesoscopic level, microdefects coalesce into transverse cracks and delamination, resulting in complex failure modes under cyclic loading. The results of the tensile tests demonstrated that the orientation of the fibers has a significant impact on the mechanical behavior of the material. The ±15° configuration demonstrated superior tensile strength and modulus, while the ±30° and multilayer configurations exhibited higher ductility. The results of the fatigue testing confirmed that fiber orientation has a significant impact on fatigue life, with the ±15° configuration proving to be the most resistant. Microscopic analysis indicated that pores act as damage initiation points, accelerating failure through matrix cracking, fiber-matrix debonding, and delamination. This study highlights the need for improved porosity control during manufacturing to enhance the durability of hydrogen storage systems. Additionally, it provides valuable insights for optimizing fiber orientation to improve fatigue performance in practical applications.
本文介绍了对通过长丝缠绕生产的轻质储氢压力容器中使用的碳纤维增强环氧树脂复合材料(CFRP)进行多尺度实验研究的结果。研究结合了拉伸-张力负载控制疲劳试验、高分辨率物理化学表征和孔隙率量化,以评估孔隙率对机械性能的影响。研究结果表明,孔隙率对机械性能有不利影响,是裂纹萌发、纤维基质分离和纤维断裂等损伤机制的成核点。在中观层面,微缺陷会凝聚成横向裂缝和分层,从而在循环加载下产生复杂的破坏模式。拉伸试验结果表明,纤维的取向对材料的机械性能有重大影响。±15°配置表现出更高的拉伸强度和模量,而±30°和多层配置则表现出更高的延展性。疲劳测试结果证实,纤维取向对疲劳寿命有显著影响,±15°结构的抗疲劳能力最强。显微分析表明,孔隙是破坏的起始点,通过基体开裂、纤维与基体脱粘和分层加速破坏。这项研究强调了在制造过程中改进孔隙率控制以提高储氢系统耐久性的必要性。此外,它还为优化纤维取向以提高实际应用中的疲劳性能提供了宝贵的见解。
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引用次数: 0
High-throughput in-situ mechanical evaluation and parameter optimization for 3D printing of continuous carbon fiber composites 用于连续碳纤维复合材料三维打印的高通量原位力学评估和参数优化
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100536
Yuichiro Yuge, Ryosuke Matsuzaki
The mechanical properties of carbon fiber reinforced thermoplastic (CFRTP) molded parts produced by thermal fusion lamination 3D printing vary with printing conditions. This study assesses the influence of the 3D printing parameters on the mechanical properties of resulting CFRTP products through parameter evaluation testing. An in-situ three-point bending test mechanism was developed to enhance the efficiency of these tests, allowing the same 3D printer to handle all processes from printing multiple CFRTP specimens simultaneously to conducting a bending test, reducing manual handling time to about one minute. Using this modified 3D printer, 700 specimens with varying printing conditions were produced, and their flexural strength was measured semi-automatically. Results revealed that the flexural strength of the 3D-printed CFRTP object varied with nozzle temperature, printing pitch, and stacking pitch, but not with printing speed. Machine learning was then employed to predict the maximum flexural strength and determine optimal printing parameters using the collected data as training data.
通过热熔层压 3D 打印技术生产的碳纤维增强热塑性塑料(CFRTP)模塑件的机械性能随打印条件的不同而变化。本研究通过参数评估测试评估了三维打印参数对所生产的 CFRTP 产品机械性能的影响。为了提高这些测试的效率,我们开发了一种原位三点弯曲测试机制,使同一台 3D 打印机能够处理从同时打印多个 CFRTP 试样到进行弯曲测试的所有过程,将人工处理时间减少到约一分钟。使用这种改进的三维打印机,制作了 700 个不同打印条件的试样,并对其抗弯强度进行了半自动测量。结果显示,三维打印 CFRTP 物体的抗弯强度随喷嘴温度、打印间距和堆叠间距的变化而变化,但与打印速度无关。随后,利用机器学习预测了最大弯曲强度,并以收集到的数据作为训练数据确定了最佳打印参数。
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引用次数: 0
Genetic programming-based algorithms application in modeling the compressive strength of steel fiber-reinforced concrete exposed to elevated temperatures 基于遗传编程算法的钢纤维加固混凝土高温抗压强度建模应用
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100529
Mohsin Ali , Li Chen , Qadir Bux Alias Imran Latif Qureshi , Deema Mohammed Alsekait , Adil Khan , Kiran Arif , Muhammad Luqman , Diaa Salama Abd Elminaam , Amir Hamza , Majid Khan
Steel-fiber-reinforced concrete (SFRC) has replaced traditional concrete in the construction sector, improving fracture resistance and post-cracking performance. However, extreme temperatures degrade concrete's material characteristics including stiffness and strength. The construction industry increasingly embraces machine learning (ML) to estimate concrete properties and optimize cost and time accurately. This study employs independent ML methods, gene expression programming (GEP), multi-expression programming (MEP), XGBoost, and Bayesian estimation model (BES) to predict SFRC compressive strength (CS) at high temperatures. 307 experimental data points from published studies were utilized to develop the models. The models were trained using 70 % of the dataset, with 15 % for validation and 15 % for testing. Iterative hyperparameter adjustment and trial-and-error refining achieved optimum predictions. All the models were evaluated using correlation (R) values for training, validation, and testing datasets. MEP showed slightly lower R-values of 0.923, 0.904, and 0.949 than GEP, which performed consistently with 0.963, 0.967, and 0.961. XGBoost had the greatest training R-value of 0.997 but dropped in validation (0.918) and testing (0.896). BES model exhibited commendable performance with scores of 0.986, 0.944, and 0.897. GEP and XGBoost exhibited great accuracy, with GEP sustaining constant accuracy across all datasets, highlighting its potency in predicting CS. Interpreting model predictions using SHapley Additive exPlanation (SHAP) highlighted temperature over heating rate. CS improved significantly as the steel fiber volume fraction (Vf) reached 1.5 %, plateauing thereafter. The proposed models are valid and accurate, providing designers and builders with a practical and adaptable method for estimating strength in SFRC structural applications, particularly under high-temperature conditions.
在建筑领域,钢纤维增强混凝土(SFRC)已经取代了传统混凝土,提高了抗断裂性能和开裂后性能。然而,极端温度会降低混凝土的材料特性,包括刚度和强度。建筑行业越来越多地采用机器学习(ML)来估算混凝土特性,并准确优化成本和时间。本研究采用独立的 ML 方法、基因表达编程(GEP)、多表达编程(MEP)、XGBoost 和贝叶斯估计模型(BES)来预测 SFRC 在高温下的抗压强度(CS)。模型的开发利用了已发表研究中的 307 个实验数据点。模型使用 70% 的数据集进行训练,其中 15% 用于验证,15% 用于测试。迭代超参数调整和试错改进实现了最佳预测。所有模型都使用训练、验证和测试数据集的相关性(R)值进行评估。MEP 的 R 值分别为 0.923、0.904 和 0.949,略低于 GEP,后者的 R 值分别为 0.963、0.967 和 0.961。XGBoost 的训练 R 值最大,为 0.997,但在验证(0.918)和测试(0.896)中有所下降。BES 模型的表现值得称赞,得分分别为 0.986、0.944 和 0.897。GEP 和 XGBoost 表现出了极高的准确性,其中 GEP 在所有数据集上都保持了恒定的准确性,突出了其预测 CS 的能力。使用 SHapley Additive exPlanation(SHAP)解释模型预测结果时,温度比加热速率更重要。当钢纤维体积分数(Vf)达到 1.5 % 时,CS 得到明显改善,之后趋于平稳。所提出的模型有效且准确,为设计人员和建筑商提供了一种实用且适应性强的方法,用于估算 SFRC 结构应用中的强度,尤其是高温条件下的强度。
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引用次数: 0
Assessment of chitosan-PVA hydrogels infused with marine collagen peptides for potential wound healing applications 评估注入海洋胶原蛋白肽的壳聚糖-PVA 水凝胶在伤口愈合方面的潜在应用
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100528
Farhana Islam, Ehsanur Rahman, Tanjina Tarannum, Nafisa Islam
Ideal wound dressings should show enhanced moisture management at the wound site, antibacterial and physical barrier, and mechanical robustness. Additionally, it should be easy to apply to the wound and be biocompatible and non-toxic. In this study, a linker-free freeze-thaw procedure was used to create an array of chitosan/PVA hydrogels blended with commercially available marine collagen peptides. Marine collagen peptides (CP) are easily available as by-products of the marine food industry and are an inexpensive and novel source of biomaterial in this field. The different weight ratios of chitosan, PVA, and CP influenced the hydrogel properties such as swelling, gel content, evaporation, and mechanical properties. Furthermore, SEM and ATR-FTIR were used to characterize the hydrogels generated under ideal conditions. After 24 h, the optimum hydrogel (chitosan:PVA:CP ratio of 1:5:1) showed a water absorption capacity of up to 900 %, a gel content of 80 %, and a 40 % evaporation rate. The physical interactions between marine collagen peptide and gel-forming components were validated by ATR-FTIR spectra, and the hydrogel kept a sufficient porous structure for potential wound dressing application. To test the mechanical integrity of the hydrogels, compression testing was carried out showing a compressive modulus of up to ∼40 kPa. The addition of marine collagen peptide in the chitosan/PVA hydrogel increased its wettability, antimicrobial capabilities, and hemostatic properties. Furthermore, the hydrogel preparation procedure is simple and does not use toxic chemicals, serving as a model for developing safe and effective hydrogel wound dressing.
理想的伤口敷料应能加强伤口部位的湿度管理、抗菌、物理屏障和机械强度。此外,这种敷料还应该易于在伤口上使用,并具有生物相容性和无毒性。在这项研究中,我们采用了无连接剂冻融程序来制造一系列壳聚糖/PVA 水凝胶,并与市面上的海洋胶原蛋白肽混合。海洋胶原蛋白肽(CP)作为海洋食品工业的副产品很容易获得,是该领域生物材料的一种廉价而新颖的来源。壳聚糖、PVA 和 CP 的不同重量比会影响水凝胶的特性,如溶胀、凝胶含量、蒸发和机械特性。此外,还利用扫描电镜和 ATR-FTIR 对理想条件下生成的水凝胶进行了表征。24 小时后,最佳水凝胶(壳聚糖:PVA:CP 的比例为 1:5:1)的吸水能力高达 900%,凝胶含量为 80%,蒸发率为 40%。ATR-FTIR 光谱验证了海洋胶原蛋白肽和凝胶形成成分之间的物理相互作用,水凝胶保持了足够的多孔结构,可用于伤口敷料。为了测试水凝胶的机械完整性,进行了压缩测试,结果显示压缩模量高达 40 千帕。在壳聚糖/PVA 水凝胶中添加海洋胶原蛋白肽可提高其润湿性、抗菌能力和止血性能。此外,该水凝胶的制备过程简单,不使用有毒化学物质,是开发安全有效的水凝胶伤口敷料的典范。
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引用次数: 0
A review of AI for optimization of 3D printing of sustainable polymers and composites 人工智能在优化可持续聚合物和复合材料 3D 打印方面的应用综述
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100513
Malik Hassan , Manjusri Misra , Graham W. Taylor , Amar K. Mohanty
In recent years, 3D printing has experienced significant growth in the manufacturing sector due to its ability to produce intricate and customized components. The advent of Industry 4.0 further boosted this progress by seamlessly incorporating artificial intelligence (AI) in 3D printing processes. As a result, design precision and production efficiency have significantly improved. Although numerous studies have explored the integration of AI and 3D printing, the literature still lacks a comprehensive overview that emphasizes material selection and formulation, predictive modeling, design optimization, and quality control. To fully understand the impacts of these emerging technologies on advanced manufacturing, a thorough assessment is required. This review aims to examine the intersection of AI and 3D printing to create a technologically advanced and environment-friendly manufacturing environment. It examines factors such as material, process efficiency, and design enhancements to highlight the benefits of combining these technologies. By focusing on predictive modeling, material selection and quality control, this analysis aims to unlock the potential for a sustainable and efficient 3D printing process. This review provided a thorough analysis of the challenges and potential benefits, proving valuable for academics and practitioners alike. It presents solutions that may establish a foundation for sustained growth and outlines a strategy for leveraging 3D printing and AI capabilities in the manufacturing sector.
近年来,3D 打印技术凭借其生产复杂和定制化组件的能力,在制造业中取得了长足的发展。工业 4.0 的出现将人工智能(AI)无缝融入 3D 打印流程,进一步推动了这一进步。因此,设计精度和生产效率显著提高。虽然已有大量研究探讨了人工智能与三维打印的融合,但文献中仍缺乏对材料选择和配方、预测建模、设计优化和质量控制等方面的全面概述。要充分了解这些新兴技术对先进制造业的影响,需要进行全面评估。本综述旨在研究人工智能与 3D 打印的交叉点,以创建技术先进、环境友好的制造环境。它研究了材料、流程效率和设计改进等因素,以突出这些技术相结合的优势。通过重点关注预测建模、材料选择和质量控制,本分析旨在发掘可持续高效 3D 打印工艺的潜力。本综述对挑战和潜在益处进行了透彻分析,对学术界和从业人员都很有价值。它提出了可为持续增长奠定基础的解决方案,并概述了在制造业中利用 3D 打印和人工智能能力的战略。
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引用次数: 0
Cure-induced residual stresses and viscoelastic effects in repaired wind turbine blades: Analytical-numerical investigation 修复风力涡轮机叶片中的固化诱导残余应力和粘弹性效应:分析-数值研究
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100521
Ayush Varshney , Daniel Paul , Puneet Mahajan , Leon Mishnaevsky Jr.
During scarf repair of wind turbine blades, the difference in coefficients of thermal expansion and chemical shrinkage between the original part and the repair patch leads to the development of residual stresses. These residual stresses are detrimental when the repaired composite structures are subjected to operational cyclic loads and affect their post-repair lifetime. This paper uses a hybrid analytical-numerical model to evaluate the residual stresses in a scarf-repaired composite panel. A Prony series-based viscoelastic model is used to describe the material behaviour of the composite undergoing cure to replicate real-life effects more closely. Experiments on the repaired composite samples and numerical simulations on a model of the same are performed to study the post-repair mechanical behaviour. It is found that the damage initiates at the adhesive interface between the scarf patch and the base composite. The resulting debonding and damage to the base composite leads to the failure of the repaired section.
在风力涡轮机叶片的疤痕修复过程中,原部件和修复补丁之间的热膨胀系数和化学收缩系数的差异会导致残余应力的产生。当修复后的复合材料结构承受运行循环载荷时,这些残余应力会对其造成损害,并影响其修复后的使用寿命。本文采用分析-数值混合模型来评估疤痕修复复合材料面板中的残余应力。使用基于 Prony 系列的粘弹性模型来描述正在固化的复合材料的材料行为,以更接近地复制现实生活中的影响。对修复后的复合材料样品进行了实验,并对同一模型进行了数值模拟,以研究修复后的机械性能。研究发现,损坏始于疤痕修补层和基底复合材料之间的粘合界面。由此产生的基底复合材料的脱粘和损坏导致了修复部分的失效。
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引用次数: 0
Bioinspired surface modification of mussel shells and their application as a biogenic filler in polypropylene composites 受生物启发的贻贝壳表面改性及其作为生物填料在聚丙烯复合材料中的应用
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100520
Jing Xu , Michael R. Mucalo , Kim L. Pickering
This study explores the potential of mussel shells (MS) as biogenic fillers in polymer composites. The chemical composition and crystal structures of MS were characterised. To improve MS filler dispersion and adhesion within a polypropylene (PP) matrix, three surface modification methods were evaluated: polydopamine (PDA) coating, maleic anhydride-grafted polypropylene (MAPP) modification, and PDA/MAPP co-modification. The PDA coating, inspired by the adhesive properties of mussel foot proteins, successfully functionalized the MS surface, as confirmed by X-ray photoelectron spectroscopy (XPS). Thermodynamic analysis, based on contact angle measurements, revealed that MAPP and PDA/MAPP modifications reduced surface energies and potential energy differences. These changes enhanced filler dispersion and interfacial bonding by increasing hydrophobicity and reducing agglomeration in the PP matrix. Consequently, PP composites with 20% PDA/MAPP-modified MS fillers exhibited a 2.9% increase in tensile strength and a 7.5% increase in flexural strength compared to neat PP. Scanning electron microscopy (SEM) also showed reduced filler-matrix debonding and fewer voids. The proposed mechanism attributes these macroscopic property enhancements to the ability of the PDA coating to facilitate chemical and hydrogen bonding between MS fillers and MAPP.
本研究探讨了贻贝壳(MS)作为聚合物复合材料中生物填料的潜力。对贻贝的化学成分和晶体结构进行了表征。为了改善 MS 填料在聚丙烯(PP)基体中的分散性和粘附性,对三种表面改性方法进行了评估:聚多巴胺(PDA)涂层、马来酸酐接枝聚丙烯(MAPP)改性和 PDA/MAPP 共改性。PDA 涂层受贻贝足蛋白粘附特性的启发,成功地对 MS 表面进行了功能化,X 射线光电子能谱(XPS)证实了这一点。基于接触角测量的热力学分析表明,MAPP 和 PDA/MAPP 改性降低了表面能量和势能差。这些变化通过增加疏水性和减少聚丙烯基体中的团聚,提高了填料的分散性和界面结合力。因此,与纯 PP 相比,含有 20% PDA/MAPP 改性 MS 填料的 PP 复合材料的拉伸强度提高了 2.9%,弯曲强度提高了 7.5%。扫描电子显微镜(SEM)还显示,填料与基体之间的脱粘现象有所减少,空隙也更少。所提出的机理将这些宏观性能的提高归因于 PDA 涂层能够促进 MS 填料和 MAPP 之间的化学键和氢键。
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引用次数: 0
Structural health monitoring of scarf bonded repaired glass/epoxy laminates interleaved with carbon non-woven veil 用碳纤维无纺布纱交错粘接修复的玻璃/环氧层压板的结构健康监测
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100526
Ozan Can Zehni , Oğuzcan İnal , Kali Babu Katnam , Mark A. Bissett , Ian A. Kinloch
Bonded repair patches/joints often introduce vulnerabilities in composite laminates, making them prime candidates for structural health monitoring (SHM). In this study, stepped-scarf bonded joints were manufactured using glass fibre-reinforced epoxy laminates as representative repair patches, and a novel SHM approach through the electrical resistance change method was applied. To establish an electrically conductive path within the stepped-scarf joint, non-woven carbon fibre veils with areal weights of 10 g/m² and 20 g/m² were interlaid along the stepped bondline. Two types of tensile tests were performed. In the first set of tests, the stepped-scarf joints underwent monotonic quasi-static tensile loading until the bondline was completely fractured (catastrophic failure) and the change in electrical resistance was continuously monitored. The failure stress of the joint with a 10 g/ m² carbon veil was only marginally decreased (∼2 %) in comparison with that of the joints without a carbon veil, while the failure stress of the joint with a 20 g/m² carbon non-woven veil was considerably decreased (by ∼9 %). However, the joints with 10 g/m² and 20 g/m² carbon veils exhibited a significant change in electrical resistance (∼200 % and ∼1000 %, up to full failure, respectively). Simultaneously, the change in electrical resistance was used for the detection of damage initiation and progression, supported by digital images taken during the tests. In the second set of tests, the joints were subjected to a cyclic tensile loading/unloading regime and the change in electrical resistance was monitored. A significant amount of permanent change in resistance during the unloading phases (up to 120 % in the bondline with a 20 g/m² veil) was observed, providing insights into the laminate and bondline damage evolution. In addition, thermal images obtained with the joule heating method in the cyclic tensile tests were used to confirm the damage detected with the electrical resistance change method. Moreover, the micrographs from the fracture surfaces indicated that the variations in electrical resistance change are largely caused by damage occurring within or near the carbon veils. In conclusion, the results demonstrate that the presented SHM approach, which incorporates carbon non-woven fibre veils within non-conductive laminate composites, holds promise for monitoring damage initiation and propagation in repaired composite laminates as well as adhesively bonded composite laminate joints, without adversely influencing the structural integrity of the bondline.
粘接修复补丁/接合点通常会在复合材料层压板中引入薄弱环节,使其成为结构健康监测(SHM)的主要候选对象。在这项研究中,使用玻璃纤维增强环氧树脂层压板作为代表性修复补丁,制造了阶梯式围巾粘接接头,并通过电阻变化法应用了一种新型 SHM 方法。为了在阶梯式围巾接合处内建立导电路径,沿着阶梯式粘合线交错铺设了面积重量分别为 10 克/平方米和 20 克/平方米的无纺碳纤维纱。进行了两种拉伸试验。在第一组试验中,阶梯形碳纤维纱接头承受单调的准静态拉伸负荷,直至粘合线完全断裂(灾难性破坏),并持续监测电阻的变化。与未使用碳纱的接头相比,使用 10 克/平方米碳纱的接头的破坏应力仅略有下降(∼2%),而使用 20 克/平方米碳纤维无纺布的接头的破坏应力则大幅下降(∼9%)。然而,使用 10 克/平方米和 20 克/平方米碳纱的接合处的电阻发生了显著变化(分别为 ∼200 % 和 ∼1000 %,直至完全失效)。同时,在测试期间拍摄的数字图像的支持下,电阻的变化被用于检测损坏的开始和发展。在第二组测试中,对接头进行周期性拉伸加载/卸载,并监测电阻的变化。在卸载阶段,观察到电阻发生了显著的永久性变化(在带有 20 g/m² 薄膜的粘合线中高达 120%),为了解层压板和粘合线的损坏演变提供了依据。此外,在循环拉伸试验中用焦耳加热法获得的热图像也用于确认电阻变化法检测到的损伤。此外,断裂表面的显微照片表明,电阻变化的主要原因是碳纱内部或附近发生的损坏。总之,研究结果表明,所介绍的 SHM 方法在非导电层压复合材料中加入了碳无纺布纤维纱,有望监测修复后的复合材料层压板以及粘合复合材料层压板接合处的损伤发生和扩展情况,同时不会对粘合线的结构完整性产生不利影响。
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引用次数: 0
Predicting tensile and fracture parameters in polypropylene-based nanocomposites using machine learning with sensitivity analysis and feature impact evaluation 利用机器学习的敏感性分析和特征影响评估预测聚丙烯基纳米复合材料的拉伸和断裂参数
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100535
Pouya Rajaee , Faramarz Ashenai Ghasemi , Amir Hossein Rabiee , Mohammad Fasihi , Behnam Kakeh , Alireza Sadeghi
This study examines the efficacy of decision tree and AdaBoost algorithms in predicting mechanical and fracture parameters of polypropylene nanocomposites toughened with ethylene-based and propylene-based thermoplastic elastomers and reinforced with fumed silica and halloysite nanotube nanoparticles. The essential work of the fracture approach was utilized to study the fracture parameters, including elastic and plastic works of the blended polymer nanocomposites. The data were divided into 80 % for training and 20 % for testing. AdaBoost consistently achieved superior performance compared to the decision tree model in all variables throughout both the training and testing stages. During the testing phase, the AdaBoost model obtained R2 values of 0.90 for Young's modulus, 0.93 for elongation at break, 0.87 for tensile strength, 0.86 for plastic work, and 0.60 for elastic work. Also, the mean absolute percentage error for the AdaBoost model during the test phase was 3.10 % for Young's modulus, 3.25 % for tensile strength, 10.34 % for elastic work, 13.55 % for plastic work, and 24.78 % for elongation at break. Furthermore, a sensitivity analysis examining the effects of various features such as TPO type, nanoparticles, and nanoparticle type on mechanical properties reveals that TPO has the most significant overall influence. The results also include an analysis of the impact of the key features on each mechanical property based on the sensitivity analysis.
本研究探讨了决策树和 AdaBoost 算法在预测用乙烯基和丙烯基热塑性弹性体增韧并用气相二氧化硅和埃洛石纳米管纳米颗粒增强的聚丙烯纳米复合材料的力学和断裂参数方面的功效。利用断裂法的基本工作来研究断裂参数,包括混合聚合物纳米复合材料的弹性和塑性工作。数据分为 80% 用于训练,20% 用于测试。与决策树模型相比,AdaBoost 在整个训练和测试阶段的所有变量中都取得了优异的性能。在测试阶段,AdaBoost 模型的杨氏模量 R2 值为 0.90,断裂伸长率 R2 值为 0.93,拉伸强度 R2 值为 0.87,塑性功 R2 值为 0.86,弹性功 R2 值为 0.60。此外,AdaBoost 模型在测试阶段的平均绝对百分比误差为:杨氏模量 3.10%,拉伸强度 3.25%,弹性功 10.34%,塑性功 13.55%,断裂伸长率 24.78%。此外,对 TPO 类型、纳米粒子和纳米粒子类型等各种特征对机械性能影响的敏感性分析表明,TPO 的总体影响最大。结果还包括基于敏感性分析的关键特征对各项机械性能影响的分析。
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引用次数: 0
Analysis of the deformation of conical shells made by 4D Printing of composites 复合材料 4D 印刷锥形壳体的变形分析
IF 5.3 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-10-01 DOI: 10.1016/j.jcomc.2024.100522
Mohammad Hamidpour, Suong V Hoa
4D printing of composites (4DPC) is a technique that allows the manufacturing of composite structures to shape without the use of a complex-shaped mold. Instead, only a flat mold is utilized. This innovative technique has been employed to make composite leaf springs with performance comparable to metallic springs, omega stiffeners, and corrugated core for flexible wings. Recently, this technique was applied to fabricate composite conical shells. While experimental work has successfully demonstrated the transformation from flat to conical shape, the development of a numerical method to replicate this transformation is highly desirable. The availability of such method not only provides theoretical support for the experimental result, it also provides means to develop other shapes. The lay-up sequence for transforming flat to conical shapes involves curvilinear fibers. Most if not all finite elements currently available deal only with straight fibers (even though the boundaries of the element may be curved). The objective of this research is to examine the efficiency of the analysis for the deformation of composite from flat to curve made by 4DPC by special finite elements containing curved fibers. The developed finite elements were used to determine the shapes of conical shells made using multiple distinct lay-up sequences. The direction of bending in curvilinear fiber structures is significantly influenced by the orientation of the fibers. This highlights the critical role of fiber orientation and layer composition in achieving desired shapes in 4D printed composites.
复合材料 4D 打印(4DPC)是一种无需使用复杂形状模具即可制造复合材料结构形状的技术。相反,只需使用一个平面模具。这种创新技术已被用于制造性能可与金属弹簧媲美的复合材料板簧、欧米茄加强筋和柔性机翼的波纹芯。最近,这种技术又被用于制造复合材料锥形壳。虽然实验工作已经成功证明了从平面到圆锥形的转变,但开发一种数值方法来复制这种转变是非常可取的。这种方法的出现不仅为实验结果提供了理论支持,还为开发其他形状提供了手段。将平面形状转化为锥形形状的铺层顺序涉及曲线纤维。目前可用的有限元即使不是全部,也大多只处理直线纤维(即使元件的边界可能是弯曲的)。本研究的目的是通过包含曲线纤维的特殊有限元,检查 4DPC 所制成的复合材料从平面到曲线变形的分析效率。所开发的有限元用于确定采用多种不同铺层顺序制成的锥形壳体的形状。曲线纤维结构的弯曲方向在很大程度上受纤维取向的影响。这凸显了纤维取向和铺层组成在实现 4D 打印复合材料理想形状中的关键作用。
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引用次数: 0
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Composites Part C Open Access
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