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Asymmetric mobilization of arching effect in granular materials: the role of fabric 颗粒材料中拱形效应的非对称调动:织物的作用
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120417
Lin-Jie Deng , Bei-Bing Dai , Feng-Tao Liu , Jun Yang , Wei-Hai Yuan
We present an experimental and DEM investigation of the arching effect by focusing on the trapdoor test, with an emphasis on the effect of fabric orientation which is created by depositing particles at various directions. The results indicate that the arching effect is the weakest when the deposition plane is oriented at θ = 30°, which is manifested by the largest arching ratio for the trapdoor part and the most considerable particle movement. The arching effect mobilization is found to be asymmetric, apart from the cases θ = 0° & 90°. The arching ratio for the left bottom part is on average lower than that for the right bottom part, and the vertical particle displacement for the neighbouring zone at the left of trapdoor is comparably larger. The asymmetric mobilization of arching effect, as well as the occurrence of the weakest arching effect at θ = 30°, is also clarified.
我们以活门试验为中心,对拱起效应进行了实验和 DEM 研究,重点研究了通过在不同方向沉积颗粒而产生的织物取向的影响。结果表明,当沉积面的方向为 θ = 30° 时,拱起效应最弱,表现为活门部分的拱起比率最大,颗粒移动最明显。除了 θ = 0° & 90° 的情况外,拱形效应的移动是不对称的。左侧底部的起拱率平均低于右侧底部,而活门左侧邻近区域的垂直颗粒位移相对较大。拱起效应的非对称调动以及θ = 30°时拱起效应最弱的现象也得到了澄清。
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引用次数: 0
Effect of combined ferrous burden composition and ore-coke interaction on blast furnace burden distribution 综合铁料成分和矿石-焦炭相互作用对高炉炉料分布的影响
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120416
Xiaohui Zhang , Nan Wang , Zongyan Zhou , Zeyao Ning , Min Chen
The distribution of burden materials at the blast furnace throat is highly correlated with the combined ferrous burden with different mass percentages of sinter, pellet, and lump ore. In this work, the motion behavior of the burden particles was studied under different combined ferrous burden composition, and an analysis was conducted on the cooperative influence of the combined ferrous burden composition and ore-coke interaction on the burden distribution characteristics. The results indicate that the particle flow trajectory is stable when the total mass fraction of pellet and lump ore is less than 32 %. Central coke charging can minimize the radial segregation of the combined ferrous burden. At the ore-coke layer interface, the accumulation and percolation behaviors of ore particles are observed. When the pellet ratio is high, the ore particles can easily penetrate into the void structure of the coke layer.
高炉喉部的炉料分布与烧结矿、球团矿和块矿不同质量百分比的综合铁料高度相关。本文研究了不同综合铁料成分下的炉料颗粒运动行为,并分析了综合铁料成分和矿石-焦炭相互作用对炉料分布特征的协同影响。结果表明,当球团矿和块矿的总质量分数小于 32% 时,颗粒的流动轨迹是稳定的。焦炭的集中装填可以最大程度地减少铁矿石结合料的径向偏析。在矿石-焦炭层界面,观察到矿石颗粒的堆积和渗流行为。当球团比高时,矿石颗粒很容易渗入焦炭层的空隙结构中。
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引用次数: 0
Effect of spreader and particle properties on powder bed generation with discrete element method in additive manufacturing 在增材制造中使用离散元素法时,撒布器和颗粒特性对粉末床生成的影响
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120420
Miao Liu , Xingming Yang , Zhongqiu Liu , Baokuan Li
Enhancing the quality of the powder bed can significantly lower the defects in the finished product manufactured by Laser-based powder bed fusion. In this work, the multi-factor effects of particle size distribution, scraper type, laying speed, scraper and substrate separation, and non-spherical particles were investigated using the discrete element method. The results show that the powder bed created by the roller can hold the largest number of particles, with a maximum gap of 67.64 %. The scraper angle will significantly impact the force and volume of the deposited particles. Accelerating the laying speed worsens the powder disturbance and raises the impact on the scraper. Non-spherical particles have less effect than particle size, which raises the force and frequency of pushing on the scraper and the friction between the particles. In addition, the slender particles have the most significant impact on the fluidity.
提高粉末床的质量可以显著降低激光粉末床熔融技术制造的成品中的缺陷。在这项工作中,使用离散元法研究了粒度分布、刮刀类型、铺设速度、刮刀与基底分离以及非球形颗粒等多因素的影响。结果表明,辊筒形成的粉床可以容纳最多的颗粒,最大间隙为 67.64%。刮刀角度会对沉积颗粒的力和体积产生重大影响。加快铺放速度会加剧粉末的扰动,增加对刮刀的冲击。非球形颗粒对颗粒大小的影响较小,这增加了对刮刀的推力和频率以及颗粒之间的摩擦。此外,细长颗粒对流动性的影响最大。
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引用次数: 0
Simulation analysis of damage and energy consumption of rocks during abrasive water jet impacts based on SPH-FDEM method 基于 SPH-FDEM 方法的磨料水射流冲击岩石时的损伤和能耗模拟分析
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120418
Yisheng Hu , Fuzeng Wang , Feng Jiang , Lingbao Hu , Guoqin Huang
This study established a simulation model for abrasive water jet rock breaking based on the SPH-FDEM method. The effects of abrasive concentration and jet velocity on crack and energy consumption were investigated based on the model. The effect of finite and infinite element boundaries on simulation results was compared, and it was found that the infinite element boundary can mitigate the damage caused by stress wave reflection on rocks. During water jet rock breaking, the crack mode inside the rock was dominated by Mode-I crack (opening-mode crack) due to the water wedge effect, and the number of cracks and the broken volume increased with increasing velocity and abrasive concentration. In this study, the specific energy consumption (SEC) was used to evaluated the rock-breaking capacity. Under pure water jetting, the SEC decreased with increasing velocity, while with the addition of abrasive, the SEC increased with increasing velocity and abrasive concentration. These findings provided a basis for optimization of water jet machining parameters in engineering applications.
本研究基于 SPH-FDEM 方法建立了加砂水射流破岩模拟模型。基于该模型研究了磨料浓度和喷射速度对裂缝和能量消耗的影响。比较了有限元边界和无限元边界对模拟结果的影响,发现无限元边界可以减轻应力波反射对岩石造成的破坏。在水射流破岩过程中,由于水的楔形效应,岩石内部的裂缝模式以 Mode-I 裂缝(开口模式裂缝)为主,裂缝数量和破碎体积随着速度和磨料浓度的增加而增加。本研究采用比能量消耗(SEC)来评估破岩能力。在纯水喷射条件下,SEC 随速度的增加而降低,而在添加磨料后,SEC 随速度和磨料浓度的增加而升高。这些发现为优化工程应用中的水射流加工参数提供了依据。
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引用次数: 0
Effects of fluid properties on coarse particles transport in vertical pipe 流体特性对垂直管道中粗颗粒输送的影响
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120421
Xiaodong Chen , Lele Yang , Lian Luo , Liang Yu , Zhiyuan Luo
The mineral resources in deep-seabed are attracting extensive attention. A numerical simulation of particle transport in a vertical pipe for a deep-sea mining system is conducted using the CFD-DEM method. The effects of fluid density, fluid viscosity and rheological parameters of non-Newtonian fluids on the liquid-solid flow behavior in a vertical pipe are investigated. For Newtonian fluids, increasing the density or viscosity enhances the particles' performance in following the fluid and reduces the slip velocity, but also increases the pressure drop. The efficient lifting of particles can be facilitated by adjusting fluid density and viscosity, while considering factors such as energy consumption. For non-Newtonian fluids, an increase in either the flow behavior index n or the consistency coefficient k results in an increase in the fluid's apparent viscosity. This leads to an increase in the particle suspension capacity and local particle velocity, along with a decrease in local particle concentration.
深海海底的矿产资源正受到广泛关注。采用 CFD-DEM 方法对深海采矿系统垂直管道中的颗粒输运进行了数值模拟。研究了流体密度、流体粘度和非牛顿流体的流变参数对垂直管道中液固流动行为的影响。对于牛顿流体,增加密度或粘度可提高颗粒追随流体的性能,降低滑移速度,但同时也会增加压降。在考虑能量消耗等因素的同时,可以通过调整流体密度和粘度来促进颗粒的有效提升。对于非牛顿流体,流动特性指数 n 或稠度系数 k 的增加都会导致流体表观粘度的增加。这会导致颗粒悬浮能力和局部颗粒速度增加,同时局部颗粒浓度降低。
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引用次数: 0
Surface chemistry characterization of AA2014 aluminum alloy powder through triboelectric charging 通过三电荷对 AA2014 铝合金粉末进行表面化学表征
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120411
Ali N. Alagha , Mathilde Rossier , Emilio Galindo , Martin Conlon , José Muñiz , Kamran Azari , Evan Butler-Jones , Mathieu Brochu
Traditional characterization techniques for powders primarily focus on bulk properties, often neglecting the critical role of surface chemistry variations that influence the performance in applications such as additive manufacturing. The method presented in this work addresses this gap by utilizing triboelectric charging concept to gain a comprehensive understanding of powder surface state under varying environmental conditions. In particular, the study investigates the detection of surface chemistry variations of AA2014 powder caused by an exposure to various relative humidity (RH) levels through a change in triboelectric charging behavior. The surface variations are analyzed in parallel with X-ray photoelectron spectroscopy (XPS). The findings reveal a direct correlation between elevated RH and increased hydroxide species content at the surface of the powder. The triboelectric charging experiments demonstrated a significant RH-dependent variations of charge accumulation, with higher humidity levels leading to reduced static charge buildup on the powder particles. The charge accumulation behavior in the powder was fitted with the compressed exponential relaxation model. The results showed that each surface chemical species exhibits a distinct correlation between charging rate and charge accumulation, confirming the effectiveness of the method to detect subtle variations in surface chemistry. The variations in the exponent of the fitted model were shown to be characteristics to the surface scale of the powder particles.
传统的粉末表征技术主要关注块体特性,往往忽视了表面化学变化的关键作用,而这些变化会影响粉末在增材制造等应用中的性能。本研究提出的方法利用三电荷概念来全面了解粉末在不同环境条件下的表面状态,从而弥补了这一不足。特别是,该研究通过改变三电充电行为,检测 AA2014 粉末在不同相对湿度 (RH) 条件下的表面化学变化。在分析表面变化的同时,还使用了 X 射线光电子能谱 (XPS)。研究结果表明,相对湿度升高与粉末表面氢氧化物物种含量增加之间存在直接关联。三电荷实验表明,电荷积累的变化与相对湿度密切相关,湿度越高,粉末颗粒上的静电荷积累越少。粉末中的电荷积累行为采用压缩指数弛豫模型进行拟合。结果表明,每种表面化学物质在充电速率和电荷积累之间都表现出明显的相关性,这证实了该方法在检测表面化学微妙变化方面的有效性。拟合模型指数的变化与粉末颗粒的表面尺度有关。
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引用次数: 0
Measurement and modeling of solids flow behaviors in an aerated standpipe and inclined pipe of circulating fluidized bed full-loop system 循环流化床全循环系统充气立管和斜管中固体流动行为的测量与建模
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-03 DOI: 10.1016/j.powtec.2024.120414
Chunguang Zhou , Christian Jonasson , Marcus Gullberg , Fredrik Ahrentorp , Christer Johansson
To control solids circulation and optimize design and operating parameters in a circulating fluidized bed full-loop system, measurement and modeling of solids flow behaviors in an aerated standpipe and inclined pipe were conducted. Different aeration gas flows were injected at the inclined pipe, which was equipped with different orifice sizes of 37 mm, 54 mm and 75 mm, for regulating solids flow rates. The magnetic tracer-tracking method, which only needs to inject one small magnetic tracer for each measurement to follow the main solids flow, was successfully demonstrated for measuring sand particles' real-time discharge rates, with good accuracy and no calibration requirement. A mathematical model was constructed to predict solids discharge rates and investigate the adverse effect of the pressure gradient in the standpipe bed in a full loop fluidized bed system. The optimization of the solids-return and circulation unit could therefore be achieved with the tools developed in this study.
为了控制循环流化床全环系统中的固体循环并优化设计和运行参数,我们对曝气立管和斜管中的固体流动行为进行了测量和建模。在倾斜管中注入不同的曝气流量,倾斜管配备了 37 毫米、54 毫米和 75 毫米的不同孔径,用于调节固体流量。磁性示踪跟踪法每次测量只需注入一个小的磁性示踪剂即可跟踪固体主流,该方法成功地用于测量沙粒的实时排放率,具有良好的准确性,且无需校准。建立了一个数学模型来预测固体排出率,并研究了全循环流化床系统中立管床压力梯度的不利影响。因此,利用本研究开发的工具可以实现固体回流和循环装置的优化。
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引用次数: 0
Systematic analysis of mixing and segregation patterns of binary mixtures in fluidised beds for multi-functional processes 对流化床中二元混合物的混合和分离模式进行系统分析,以实现多功能工艺
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-02 DOI: 10.1016/j.powtec.2024.120419
Hualun Zhu, Paola Lettieri, Massimiliano Materazzi
Fluidized beds are increasingly used in renewable energy and chemical production due to their versatility in handling different solids for multi-functional industrial applications. The diversity in size and density of solid particles impacts fluidization, influencing mixing and segregation behaviours critical for optimizing chemical processes and reactor design. This study investigates the expansion and segregation behaviours of mixed Geldart group powders in binary systems, simulating polydispersed beds with different materials and catalysts. By applying a modified Cheung equation and an adapted Gibilaro-Rowe model, the study analyzes segregation behaviours of Geldart Group A and B materials at varying mixing rates and gas flow velocities. Results show a good match between experimental data and model predictions. Using novel non-invasive X-ray imaging, the study provides real-time analysis of mixing and segregation at different fluidization regimes and temperatures. These findings aid in designing and optimizing advanced thermochemical conversion technologies, enhancing process efficiency and resilience.
流化床因其处理不同固体的多功能性,越来越多地应用于可再生能源和化工生产领域。固体颗粒尺寸和密度的多样性会影响流化,影响对优化化学过程和反应器设计至关重要的混合和偏析行为。本研究通过模拟含有不同材料和催化剂的多分散床,研究了二元体系中混合 Geldart 组粉末的膨胀和偏析行为。通过应用修改后的 Cheung 方程和改编后的 Gibilaro-Rowe 模型,该研究分析了不同混合速率和气体流速下 Geldart A 组和 B 组材料的偏析行为。结果表明,实验数据与模型预测结果十分吻合。该研究利用新型非侵入式 X 射线成像技术,对不同流化状态和温度下的混合和偏析情况进行了实时分析。这些发现有助于设计和优化先进的热化学转化技术,提高工艺效率和复原能力。
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引用次数: 0
Development and calibration of discrete element model for layered gravel soils in forested areas 林区层状砾石土壤离散元素模型的开发与校准
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-02 DOI: 10.1016/j.powtec.2024.120405
Yuan Zhou , Mohamed A. Shahin , Can Xu , Hongxing Zhu , Zian Ding , Shufa Sun
In this paper, a Discrete Element Method (DEM) model is developed to accurately simulate the interaction between forestry machinery vehicles and forest-layered gravel soils. The soil grains in the DEM model are simulated as spherical particles, while the gravel is represented by nine types of non-spherical particle clusters based on the actual gravel content, size, and shape. The DEM model parameters are calibrated through the indoor angle of repose (AOR) and triaxial shear tests, followed by statistical calibration using Plackett-Burman, Steepest Ascent, and Box-Behnken experiments. The values of the optimal DEM model parameters are determined based on the obtained quadratic regression analysis. Finally, the MED model accuracy is verified by comparing indoor test results with the DEM simulation outputs and mathematical predictions. The results revealed that the DEM model simulated curves closely match the measured values, indicating good agreement.
本文开发了一种离散元素法(DEM)模型,用于精确模拟林业机械车辆与林层砾石土壤之间的相互作用。DEM 模型中的土粒模拟为球形颗粒,而砾石则根据实际的砾石含量、大小和形状由九种类型的非球形颗粒群来表示。DEM 模型参数通过室内静止角 (AOR) 和三轴剪切试验进行校准,然后使用 Plackett-Burman、Steepest Ascent 和 Box-Behnken 试验进行统计校准。根据获得的二次回归分析结果,确定最佳 DEM 模型参数值。最后,通过比较室内测试结果与 DEM 模拟输出和数学预测,验证了 MED 模型的准确性。结果表明,DEM 模型模拟曲线与测量值非常吻合,显示出良好的一致性。
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引用次数: 0
Highly efficient lithium leaching from α-spodumene via binary composite salts low-temperature roasting process 通过二元复合盐低温焙烧工艺从α-锑中高效萃取锂
IF 4.5 2区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-11-02 DOI: 10.1016/j.powtec.2024.120404
Chenquan Ni , Chang Liu , Jieyi Wang , Yinbo Song , Yuting Liang , Weiqi Xie , Hui Zhong , Zhiguo He
With the rapid development and widespread application of lithium-ion batteries, the demand for lithium has surged dramatically, drawing increasing attention to its extraction from spodumene deposits. However, the sustainable development of the lithium industry faces challenges, as traditional processes are hindered by high conversion temperatures, excessive acid consumption, and difficulties in purifying the leachate. Hence, we propose a binary composite additive system based on sodium sulfate‑calcium oxide (Na2SO4-CaO) for roasting α-spodumene at comparative low temperatures. The optimal roasting conditions entailed a mass ratio of spodumene/CaO/Na2SO4 at 1:0.1:0.8, a roasting temperature of 900 °C, a holding time of 2 h, a liquid-to-solid ratio of 5 mL/g, and leaching at 60 °C for 30 min, resulting in an impressive lithium leaching efficiency of 95.45 %. Thermodynamic and kinetic analyses reveal that the roasting formed the product of water-soluble LiNaSO4, which was then dissolved into water, with the leaching process being governed by internal diffusion.
随着锂离子电池的快速发展和广泛应用,对锂的需求急剧增加,从锂辉石矿床中提取锂也日益受到关注。然而,由于传统工艺存在转化温度高、酸消耗量大、浸出液难以净化等问题,锂产业的可持续发展面临挑战。因此,我们提出了一种基于硫酸钠-氧化钙(Na2SO4-CaO)的二元复合添加剂系统,用于在相对较低的温度下焙烧α-锑。最佳焙烧条件包括:质量比为 1:0.1:0.8、焙烧温度为 900 ℃、保温时间为 2 小时、液固比为 5 mL/g、浸出温度为 60 ℃、浸出时间为 30 分钟,锂浸出效率高达 95.45%。热力学和动力学分析表明,焙烧形成了水溶性 LiNaSO4 产物,然后将其溶解到水中,沥滤过程受内部扩散控制。
{"title":"Highly efficient lithium leaching from α-spodumene via binary composite salts low-temperature roasting process","authors":"Chenquan Ni ,&nbsp;Chang Liu ,&nbsp;Jieyi Wang ,&nbsp;Yinbo Song ,&nbsp;Yuting Liang ,&nbsp;Weiqi Xie ,&nbsp;Hui Zhong ,&nbsp;Zhiguo He","doi":"10.1016/j.powtec.2024.120404","DOIUrl":"10.1016/j.powtec.2024.120404","url":null,"abstract":"<div><div>With the rapid development and widespread application of lithium-ion batteries, the demand for lithium has surged dramatically, drawing increasing attention to its extraction from spodumene deposits. However, the sustainable development of the lithium industry faces challenges, as traditional processes are hindered by high conversion temperatures, excessive acid consumption, and difficulties in purifying the leachate. Hence, we propose a binary composite additive system based on sodium sulfate‑calcium oxide (Na<sub>2</sub>SO<sub>4</sub>-CaO) for roasting α-spodumene at comparative low temperatures. The optimal roasting conditions entailed a mass ratio of spodumene/CaO/Na<sub>2</sub>SO<sub>4</sub> at 1:0.1:0.8, a roasting temperature of 900 °C, a holding time of 2 h, a liquid-to-solid ratio of 5 mL/g, and leaching at 60 °C for 30 min, resulting in an impressive lithium leaching efficiency of 95.45 %. Thermodynamic and kinetic analyses reveal that the roasting formed the product of water-soluble LiNaSO<sub>4</sub>, which was then dissolved into water, with the leaching process being governed by internal diffusion.</div></div>","PeriodicalId":407,"journal":{"name":"Powder Technology","volume":"449 ","pages":"Article 120404"},"PeriodicalIF":4.5,"publicationDate":"2024-11-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142587335","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Powder Technology
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