Pub Date : 2021-11-24DOI: 10.52571/ptq.v18.n39.2021.04_arrieta_pgs_43_55.pdf
A. Arrieta, J. Mendoza, Manuel Palencia
Background: Composite materials make it possible to modulate the properties of the source materials and expand their technological potential. In this sense, composite materials made from solid biopolymeric electrolytes and graphene oxide can be an attractive alternative for applications in organic electronics due to their electrochemical properties. Aim: The present work aims to evaluate the electrochemical behavior of a composite material made of solid biopolymeric electrolyte of cassava starch and graphene oxide at different concentrations to determine the effect of this concentration and the pH used in the production process. Methods: The composite material was made from the use of cassava starch plasticized with glycerol, glutaraldehyde, polyethylene glycol and with lithium perchlorate as electrolytes. During the synthesis process, graphene oxide was added in different concentrations (0, 0.25, 0.50, 1.00, 1.25, 1.50, and 1.75 %w/w) to evaluate the effect of the concentration of this component. The synthesis was carried out by thermochemical method with constant heating in an oven at 75 ° C for 48 hours. Films were prepared using synthesis solutions at different pH (5.0 and 9.0). The pH was regulated by adding HCl or NaOH to the synthesis solution as appropriate. Results and Discussion: The results showed that the cassava starch biopolymeric solid electrolyte films without plasticizers were stiff and brittle, so they broke easily. The films with plasticizers and the films of the composite material were stable to the manual traction, allowing their easy manipulation without breaking. The films presented a similar electrochemical behavior in terms of oxide reduction processes; however, the films with graphene oxide presented signals with higher peak currents. Films made at pH 9.0 showed 50 % more intensity in peak currents. The addition of graphene oxide affected the current parameters and peak potentials, being more marked in the films prepared at pH 9.0; at this pH the films with concentrations of graphene oxide lower than 1.00 %w/w presented variable Ep and Ip, while at concentrations of graphene oxide greater than 1%w/w, the behavior did not show significant variations. Conclusions: The addition of graphene oxide modulates or modifies the electrochemical behavior of cassava starch biopolymeric solid electrolyte films, and the processing pH can vary the effect of the graphene oxide addition.
{"title":"ELECTROCHEMICAL BEHAVIOR OF A COMPOSITE MATERIAL OF SOLID BIOPOLYMER ELECTROLYTE FROM CASSAVA STARCH / GRAPHENE OXIDE PREPARED AT DIFFERENT pH","authors":"A. Arrieta, J. Mendoza, Manuel Palencia","doi":"10.52571/ptq.v18.n39.2021.04_arrieta_pgs_43_55.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n39.2021.04_arrieta_pgs_43_55.pdf","url":null,"abstract":"Background: Composite materials make it possible to modulate the properties of the source materials and expand their technological potential. In this sense, composite materials made from solid biopolymeric electrolytes and graphene oxide can be an attractive alternative for applications in organic electronics due to their electrochemical properties. Aim: The present work aims to evaluate the electrochemical behavior of a composite material made of solid biopolymeric electrolyte of cassava starch and graphene oxide at different concentrations to determine the effect of this concentration and the pH used in the production process. Methods: The composite material was made from the use of cassava starch plasticized with glycerol, glutaraldehyde, polyethylene glycol and with lithium perchlorate as electrolytes. During the synthesis process, graphene oxide was added in different concentrations (0, 0.25, 0.50, 1.00, 1.25, 1.50, and 1.75 %w/w) to evaluate the effect of the concentration of this component. The synthesis was carried out by thermochemical method with constant heating in an oven at 75 ° C for 48 hours. Films were prepared using synthesis solutions at different pH (5.0 and 9.0). The pH was regulated by adding HCl or NaOH to the synthesis solution as appropriate. Results and Discussion: The results showed that the cassava starch biopolymeric solid electrolyte films without plasticizers were stiff and brittle, so they broke easily. The films with plasticizers and the films of the composite material were stable to the manual traction, allowing their easy manipulation without breaking. The films presented a similar electrochemical behavior in terms of oxide reduction processes; however, the films with graphene oxide presented signals with higher peak currents. Films made at pH 9.0 showed 50 % more intensity in peak currents. The addition of graphene oxide affected the current parameters and peak potentials, being more marked in the films prepared at pH 9.0; at this pH the films with concentrations of graphene oxide lower than 1.00 %w/w presented variable Ep and Ip, while at concentrations of graphene oxide greater than 1%w/w, the behavior did not show significant variations. Conclusions: The addition of graphene oxide modulates or modifies the electrochemical behavior of cassava starch biopolymeric solid electrolyte films, and the processing pH can vary the effect of the graphene oxide addition.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43095614","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-11-24DOI: 10.52571/ptq.v18.n39.2021.01_berezina_pgs_01_13.pdf
D. I. Berezina, Luybov Leonidovna Fomina
Background: The mortality of freshwater fish due to stress during various production manipulations is a severe problem, which requires a thorough understanding of the basic mechanisms involved, including the hemostasis system. Therefore, on the application level, the study of blood clotting can perform fish coagulopathies diagnostics and develop practical preventive and therapeutic anticoagulation methods for fish farming. Aim: The goal of this research was a comparative assessment of the reaction of some hemostasis parameters of two commercial fish species, carp Cyprinus carpio and tilapia Oreochromis niloticus, to the stress of different duration induced by corticosteroids. Methods: The fishes were divided into three groups: chronically stressed (induction by betamethasone), acutely stressed (induction by dexamethasone), and control animals with blood taken from the caudal hemal canal before hormone treatment(by dexamethasone and betamethasone), then 7 and 21 days after. Results and Discussion: Changes in the following parameters were studied: thrombin time, prothrombin time, activated partial thromboplastin time, the concentration of fibrinogen, soluble fibrin monomer complexes, antithrombin. It was found that both hormone-induced stress and handling stress associated with blood sampling strongly increased blood clotting ability in carps (prothrombin time decrease by 78,5-86,1%, fibrinogen increase by 12,7-100%, thrombin time decrease by 83,4-85%, and antithrombin III decreases by 15,3-21,7%), while in tilapias, acceleration of blood clotting by intrinsic and extrinsic pathways were recorded by the end of the experiment only in fishes with imitation of chronic stress (prothrombin time decrease by 76,8%, activated partial thromboplastin time decrease by 20,0%, and 2,3 multiplying soluble fibrin monomer complexes). Conclusions: It was concluded that the adaptive mechanisms of the tilapia (Oreochromis niloticus) organism allowed the clotting function to recover in most cases by the end of the experiment in all groups of fish, in contrast to carps (Cyprinus carpio).
{"title":"COMPARATIVE ANALYSIS OF THE EFFECT OF HORMONE-INDUCED STRESS ON HEMOSTASIS IN THE CYPRINUS CARPIO AND THE OREOCHROMIS NILOTICUS","authors":"D. I. Berezina, Luybov Leonidovna Fomina","doi":"10.52571/ptq.v18.n39.2021.01_berezina_pgs_01_13.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n39.2021.01_berezina_pgs_01_13.pdf","url":null,"abstract":"Background: The mortality of freshwater fish due to stress during various production manipulations is a severe problem, which requires a thorough understanding of the basic mechanisms involved, including the hemostasis system. Therefore, on the application level, the study of blood clotting can perform fish coagulopathies diagnostics and develop practical preventive and therapeutic anticoagulation methods for fish farming. Aim: The goal of this research was a comparative assessment of the reaction of some hemostasis parameters of two commercial fish species, carp Cyprinus carpio and tilapia Oreochromis niloticus, to the stress of different duration induced by corticosteroids. Methods: The fishes were divided into three groups: chronically stressed (induction by betamethasone), acutely stressed (induction by dexamethasone), and control animals with blood taken from the caudal hemal canal before hormone treatment(by dexamethasone and betamethasone), then 7 and 21 days after. Results and Discussion: Changes in the following parameters were studied: thrombin time, prothrombin time, activated partial thromboplastin time, the concentration of fibrinogen, soluble fibrin monomer complexes, antithrombin. It was found that both hormone-induced stress and handling stress associated with blood sampling strongly increased blood clotting ability in carps (prothrombin time decrease by 78,5-86,1%, fibrinogen increase by 12,7-100%, thrombin time decrease by 83,4-85%, and antithrombin III decreases by 15,3-21,7%), while in tilapias, acceleration of blood clotting by intrinsic and extrinsic pathways were recorded by the end of the experiment only in fishes with imitation of chronic stress (prothrombin time decrease by 76,8%, activated partial thromboplastin time decrease by 20,0%, and 2,3 multiplying soluble fibrin monomer complexes). Conclusions: It was concluded that the adaptive mechanisms of the tilapia (Oreochromis niloticus) organism allowed the clotting function to recover in most cases by the end of the experiment in all groups of fish, in contrast to carps (Cyprinus carpio).","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"45480608","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-11-24DOI: 10.52571/ptq.v18.n39.2021.03_martinez_pgs_33_42.pdf
Fredy Martinez
Background: The academic activity of students and professors constitutes the basis of professional training in engineering. Training in electrical engineering has always been of less interest to university students compared to other professional training programs. However, in recent years, this interest has decreased beyond previous trends, an effect detected in all engineering programs, which has been accelerated by the distance learning mechanisms adopted in the face of the spread of COVID-19. Therefore, among the incentive mechanisms for young people, the promotion of research activity has been included. This study describes the model proposed within the Electrical Technology and Engineering programs of the Universidad Distrital Francisco José de Caldas as a distinctive element of its research training strategy. Aims: To offer alternatives tending to promote the current research activities of the research groups of the electrical engineering area of the Universidad Distrital (Colombia) to increase the performance of the formative research processes, in particular with motivational aspects, development of critical awareness, and strengthening of resilience. Methods: A strategic plan was developed to increase the activity related to research processes within the academic program. It was based on the dynamics shown in the last seven years, and a set of strategies aimed at strengthening and encouraging this trend was projected for the next seven years. Results and Discussion: This strategic plan is expected to increase academic activity, particularly related to scientific production indicators. Projections for the next seven years indicate an increase in student participation related to scientific publications, the population in research groups, and project development. Conclusions: The proposed scheme corresponds to a model adjusted to higher education institutions with student populations of low academic strata and under national standards that prioritize quality in education from the point of view of both physical and human resources, particularly those that promote critical awareness of local and national reality. In this sense, the proposed plan is highly relevant and promotes one of the strengths identified in the academic program.
{"title":"STRATEGIC PLAN TO STRENGTHEN RESEARCH AS A MECHANISM TO INCREASE MEANINGFUL TRAINING BASED ON FORMATIVE RESEARCH","authors":"Fredy Martinez","doi":"10.52571/ptq.v18.n39.2021.03_martinez_pgs_33_42.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n39.2021.03_martinez_pgs_33_42.pdf","url":null,"abstract":"Background: The academic activity of students and professors constitutes the basis of professional training in engineering. Training in electrical engineering has always been of less interest to university students compared to other professional training programs. However, in recent years, this interest has decreased beyond previous trends, an effect detected in all engineering programs, which has been accelerated by the distance learning mechanisms adopted in the face of the spread of COVID-19. Therefore, among the incentive mechanisms for young people, the promotion of research activity has been included. This study describes the model proposed within the Electrical Technology and Engineering programs of the Universidad Distrital Francisco José de Caldas as a distinctive element of its research training strategy. Aims: To offer alternatives tending to promote the current research activities of the research groups of the electrical engineering area of the Universidad Distrital (Colombia) to increase the performance of the formative research processes, in particular with motivational aspects, development of critical awareness, and strengthening of resilience. Methods: A strategic plan was developed to increase the activity related to research processes within the academic program. It was based on the dynamics shown in the last seven years, and a set of strategies aimed at strengthening and encouraging this trend was projected for the next seven years. Results and Discussion: This strategic plan is expected to increase academic activity, particularly related to scientific production indicators. Projections for the next seven years indicate an increase in student participation related to scientific publications, the population in research groups, and project development. Conclusions: The proposed scheme corresponds to a model adjusted to higher education institutions with student populations of low academic strata and under national standards that prioritize quality in education from the point of view of both physical and human resources, particularly those that promote critical awareness of local and national reality. In this sense, the proposed plan is highly relevant and promotes one of the strengths identified in the academic program.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47470747","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-11-24DOI: 10.52571/ptq.v18.n39.2021.06_orekhova_pgs_71_87.pdf
Yelena Yurievna Orekhova, S. M. Sysoev, Maxim Mikhailovich Alekseev
Background: Being an essential part of the educational process, blended learning still faces some problems concerning the interaction between teachers and students. They include a decrease in the level of knowledge and in the number of graduates as students experience a lack of live communication with the teacher, lack of sufficient experience of independent work, lack of interactive assessment. Aim: This study aimed to elaborate the model of enhanced feedback in an e-learning course, “Fundamentals of Molecular Physics and Thermodynamics,” to increase student educational achievements. Methods: The effectiveness of the model of enhanced feedback in the learning process was measured with the methodology for calculating statistical indicators of the quality of education: knowledge quality, level of student proficiency, progress, and average grade. To measure the emotional and evaluative attitude of students to educational activities and interaction with the teacher in an electronic course, a test-questionnaire satisfaction with learning activity was employed. Results and Discussion: the results of the initial and final control of the statistical indicators of the quality of education including knowledge quality, level of student proficiency, progress, and average grade in students showed a significant difference between the control and the experimental groups. At the end of the semester, the difference in knowledge quality was 23%, student proficiency level – 13%, progress – 3.5%, average grade – 0.6 scores. The analysis of student satisfaction with the learning process also confirms an increase in satisfaction with the learning process and with the interaction with the lecturer. Thus, the experimental methodology contributes to a significant improvement in the learning process results. Conclusions: The experiment demonstrated that replacing formative assessment with the model of enhanced feedback raises student educational achievements and compensates for lack of live communication with the teacher.
{"title":"USE OF ENHANCED FEEDBACK IN AN ELECTRONIC LEARNING COURSE “FUNDAMENTALS OF MOLECULAR PHYSICS AND THERMODYNAMICS”","authors":"Yelena Yurievna Orekhova, S. M. Sysoev, Maxim Mikhailovich Alekseev","doi":"10.52571/ptq.v18.n39.2021.06_orekhova_pgs_71_87.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n39.2021.06_orekhova_pgs_71_87.pdf","url":null,"abstract":"Background: Being an essential part of the educational process, blended learning still faces some problems concerning the interaction between teachers and students. They include a decrease in the level of knowledge and in the number of graduates as students experience a lack of live communication with the teacher, lack of sufficient experience of independent work, lack of interactive assessment. Aim: This study aimed to elaborate the model of enhanced feedback in an e-learning course, “Fundamentals of Molecular Physics and Thermodynamics,” to increase student educational achievements. Methods: The effectiveness of the model of enhanced feedback in the learning process was measured with the methodology for calculating statistical indicators of the quality of education: knowledge quality, level of student proficiency, progress, and average grade. To measure the emotional and evaluative attitude of students to educational activities and interaction with the teacher in an electronic course, a test-questionnaire satisfaction with learning activity was employed. Results and Discussion: the results of the initial and final control of the statistical indicators of the quality of education including knowledge quality, level of student proficiency, progress, and average grade in students showed a significant difference between the control and the experimental groups. At the end of the semester, the difference in knowledge quality was 23%, student proficiency level – 13%, progress – 3.5%, average grade – 0.6 scores. The analysis of student satisfaction with the learning process also confirms an increase in satisfaction with the learning process and with the interaction with the lecturer. Thus, the experimental methodology contributes to a significant improvement in the learning process results. Conclusions: The experiment demonstrated that replacing formative assessment with the model of enhanced feedback raises student educational achievements and compensates for lack of live communication with the teacher.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-11-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42694900","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-07-28DOI: 10.52571/ptq.v18.n38.2021.10_arrieta_pgs_137_148.pdf
A. Arrieta
Background: Solid biopolymer electrolytes are a type of material with high technological potential used in the development of solar cells, batteries, fuel cells, among others, due to their biodegradable nature and low environmental impact. Aim: This study aimed to evaluate the effect of the botanical origin of the starch used to prepare solid biopolymeric electrolyte films on its electrochemical and thermal properties and to establish the variations in thermal decomposition temperatures and redox potentials depending on the botanical origin of the starch used. Methods: Films of solid biopolymer electrolyte were made by thermochemical synthesis processes using corn starch, cassava starch, potato starch, glycerol, polyethylene glycol, and glutaraldehyde as plasticizers and lithium perchlorate salt. The synthesis solutions were taken to an oven at 70 °C for 48 hours. The films were characterized electrochemically by cyclic voltammetry using a dry electrochemical cell and thermally by differential scanning calorimetry and thermogravimetric analysis. Results and Discussion: The results showed that the electrochemical behavior of the films was similar in terms of registered redox processes. However, the potential values of the oxidation and reduction were different, as are the stability and intensity of the processes. On the other hand, the thermal analysis allowed establishing two decomposition processes in each of the films studied; the first process was due to dehydration and depolymerization phenomena in the films. The temperatures recorded were 59.0 °C, 58.9 °C, and 89.9 °C for potato starch, cassava starch, and corn starch films. The second process evidenced the thermal decomposition at different temperatures, 267.7 °C in potato starch films, 280.6 °C in corn starch films, and 287.1 °C in cassava starch films. Conclusions: It could be concluded that the botanical origin of the starch used in the synthesis of solid biopolymer electrolyte films affects its behavior and electrochemical and thermal stability.
{"title":"THERMAL AND ELECTROCHEMICAL PROPERTIES OF SOLID BIOPOLYMER ELECTROLYTES FROM STARCH OF DIFFERENT BOTANICAL ORIGIN","authors":"A. Arrieta","doi":"10.52571/ptq.v18.n38.2021.10_arrieta_pgs_137_148.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n38.2021.10_arrieta_pgs_137_148.pdf","url":null,"abstract":"Background: Solid biopolymer electrolytes are a type of material with high technological potential used in the development of solar cells, batteries, fuel cells, among others, due to their biodegradable nature and low environmental impact. Aim: This study aimed to evaluate the effect of the botanical origin of the starch used to prepare solid biopolymeric electrolyte films on its electrochemical and thermal properties and to establish the variations in thermal decomposition temperatures and redox potentials depending on the botanical origin of the starch used. Methods: Films of solid biopolymer electrolyte were made by thermochemical synthesis processes using corn starch, cassava starch, potato starch, glycerol, polyethylene glycol, and glutaraldehyde as plasticizers and lithium perchlorate salt. The synthesis solutions were taken to an oven at 70 °C for 48 hours. The films were characterized electrochemically by cyclic voltammetry using a dry electrochemical cell and thermally by differential scanning calorimetry and thermogravimetric analysis. Results and Discussion: The results showed that the electrochemical behavior of the films was similar in terms of registered redox processes. However, the potential values of the oxidation and reduction were different, as are the stability and intensity of the processes. On the other hand, the thermal analysis allowed establishing two decomposition processes in each of the films studied; the first process was due to dehydration and depolymerization phenomena in the films. The temperatures recorded were 59.0 °C, 58.9 °C, and 89.9 °C for potato starch, cassava starch, and corn starch films. The second process evidenced the thermal decomposition at different temperatures, 267.7 °C in potato starch films, 280.6 °C in corn starch films, and 287.1 °C in cassava starch films. Conclusions: It could be concluded that the botanical origin of the starch used in the synthesis of solid biopolymer electrolyte films affects its behavior and electrochemical and thermal stability.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47852064","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-07-28DOI: 10.52571/ptq.v18.n38.2021.04_teixeira_pgs_38_46.pdf
É. C. Teixeira, R. Ferreira
Introduction: Galling insects manipulate the development of their host plants. Galls are rich in secondary metabolites, such as phenolic compounds and terpenes. Caryocar brasiliense acts as a host of galling insects. Few studies report the impacts of this plant-insect interaction on the species' morphology, physiology, and secondary metabolism. Objective: The purpose of this study was to verify if there is a correlation between the levels of total phenols and flavonoids in C. brasiliense leaf extracts and environmental variables, such as temperature and precipitation, throughout the year, and to evaluate how galling insects can interfere in this seasonality. Methods: Ethanol extracts from leaves were obtained by soxhlet extraction. The main classes of secondary metabolites were detected by phytochemical prospecting. The levels of total phenols and flavonoids were quantified by the Folin-Dennis tests and complexation reaction with aluminum chloride, respectively. Pearson 's correlation coefficient shows that the levels of phenols and flavonoids were correlated with the average monthly maximum temperatures and precipitation accumulation, respectively, recorded in Gurupi - Tocantins. Results and Discussion: Phytochemical prospecting indicated flavonoids, saponins, tannins, triterpenes, steroids, and alkaloids in both extracts. In C. brasiliense, the samples of healthy leaves suffered a greater variation in the levels of phenols (68.39±2.3 to 279.34±3.1 mg GAE g-1 extract) and flavonoids (164.06± 3.0 at 269.03±3.6 mg QE g-1 extract) compared to leaf samples with galls. A strong positive correlation was found between the contents of total phenols and maximum temperatures and a strong negative correlation with precipitation through Pearson's correlation. Conclusions: The variations observed in the levels of phenols and flavonoids in the extracts of C. brasiliense seem to be related to abiotic factors and the herbivory promoted by the galling insect.
昆虫可以操纵寄主植物的发育。虫瘿富含次生代谢物，如酚类化合物和萜烯。Caryocar brasiliense是一群昆虫。很少有研究报道这种植物-昆虫相互作用对物种形态、生理和次生代谢的影响。目的:本研究的目的是验证巴西螺叶提取物中总酚和总黄酮的含量是否与全年的环境变量(如温度和降水)相关，并评估昆虫对这种季节性的干扰程度。方法:采用索氏提取法提取乙醇提取物。利用植物化学方法对次生代谢物进行了检测。用福林-丹尼斯法和与氯化铝络合反应分别测定其总酚和总黄酮的含量。Pearson相关系数表明，古鲁皮-托坎坦斯的酚类和黄酮类含量分别与月平均最高气温和降水量相关。结果与讨论:两种提取物中均含有黄酮类、皂苷类、单宁类、三萜类、甾体和生物碱。在巴西松香中，健康叶片的酚类含量(68.39±2.3 ~ 279.34±3.1 mg QE g-1)和黄酮类含量(164.06±3.0 mg QE g-1, 269.03±3.6 mg QE g-1)比有虫瘿的叶片差异更大。Pearson相关分析表明，总酚含量与最高气温呈显著正相关，与降水量呈显著负相关。结论:巴西香提取物中酚类和黄酮类含量的变化可能与非生物因素和昆虫促进的草食作用有关。
{"title":"SEASONAL VARIATION OF PHENOLS AND FLAVONOIDS IN NON-GALLED AND GALLED LEAVES OF CARYOCAR BRASILIENSE (CARYOCARACEAE)","authors":"É. C. Teixeira, R. Ferreira","doi":"10.52571/ptq.v18.n38.2021.04_teixeira_pgs_38_46.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n38.2021.04_teixeira_pgs_38_46.pdf","url":null,"abstract":"Introduction: Galling insects manipulate the development of their host plants. Galls are rich in secondary metabolites, such as phenolic compounds and terpenes. Caryocar brasiliense acts as a host of galling insects. Few studies report the impacts of this plant-insect interaction on the species' morphology, physiology, and secondary metabolism. Objective: The purpose of this study was to verify if there is a correlation between the levels of total phenols and flavonoids in C. brasiliense leaf extracts and environmental variables, such as temperature and precipitation, throughout the year, and to evaluate how galling insects can interfere in this seasonality. Methods: Ethanol extracts from leaves were obtained by soxhlet extraction. The main classes of secondary metabolites were detected by phytochemical prospecting. The levels of total phenols and flavonoids were quantified by the Folin-Dennis tests and complexation reaction with aluminum chloride, respectively. Pearson 's correlation coefficient shows that the levels of phenols and flavonoids were correlated with the average monthly maximum temperatures and precipitation accumulation, respectively, recorded in Gurupi - Tocantins. Results and Discussion: Phytochemical prospecting indicated flavonoids, saponins, tannins, triterpenes, steroids, and alkaloids in both extracts. In C. brasiliense, the samples of healthy leaves suffered a greater variation in the levels of phenols (68.39±2.3 to 279.34±3.1 mg GAE g-1 extract) and flavonoids (164.06± 3.0 at 269.03±3.6 mg QE g-1 extract) compared to leaf samples with galls. A strong positive correlation was found between the contents of total phenols and maximum temperatures and a strong negative correlation with precipitation through Pearson's correlation. Conclusions: The variations observed in the levels of phenols and flavonoids in the extracts of C. brasiliense seem to be related to abiotic factors and the herbivory promoted by the galling insect.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"46685574","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-07-28DOI: 10.52571/ptq.v18.n38.2021.13_mohamadimoghadam_pgs_176_187.pdf
Marzieh Mohamadimoghadam, Seyed hojjat Shakib, F. Salmani
Background: Periodontal infection leads to adverse pregnancy outcomes such as preterm delivery, low birth weight, preeclampsia, miscarriage, or early pregnancy loss. Aim: The aim of this study was to investigate the knowledge, attitude, and practice of pregnant women about periodontal health and oral health and their effect on the fetus. Methods: The present study is a descriptive-analytical study on 210 pregnant women in the first and second trimesters referring to health centers in Birjand in 2019. The tool used in this study was a researchermade questionnaire with four parts: women's demographic information, and women's knowledge, attitude, and practice, the validity, and reliability of which were confirmed. After data collection, it was entered into SPSS software version 22 and then analyzed using descriptive statistics, independent t-test, and one-way analysis of variance. The significance level was considered 0.05 in all tests. Results and Discussion: In this study, the mean scores of knowledge, attitude, and practice of pregnant women were 5.6 ±1.92, 55.9 ± 5.1, and 25.9± 3.7, respectively. There was a significant difference between the mean attitude score and mothers' age. There was also a significant difference between the mean scores of knowledge, attitude, and practice of women and significant difference in knowledge, attitude, and practice of employee and housewife pregnant women; In terms practice, there were significant differences between pregnant housewives and self-employed women. There was a significant relationship between the mean of these scores and mothers' jobs so that the mean scores were higher in employed women than others. Conclusions: The results of our study showed that the average score of knowledge, attitude, and practice of pregnant women in Birjand regarding oral hygiene during pregnancy is not satisfactory and appropriate.
{"title":"INVESTIGATING THE KNOWLEDGE, ATTITUDE, AND PRACTICE OF PREGNANT WOMEN ABOUT PERIODONTAL HEALTH AND ORAL HEALTH, AND THEIR EFFECT ON THE FETUS DURING PREGNANCY","authors":"Marzieh Mohamadimoghadam, Seyed hojjat Shakib, F. Salmani","doi":"10.52571/ptq.v18.n38.2021.13_mohamadimoghadam_pgs_176_187.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n38.2021.13_mohamadimoghadam_pgs_176_187.pdf","url":null,"abstract":"Background: Periodontal infection leads to adverse pregnancy outcomes such as preterm delivery, low birth weight, preeclampsia, miscarriage, or early pregnancy loss. Aim: The aim of this study was to investigate the knowledge, attitude, and practice of pregnant women about periodontal health and oral health and their effect on the fetus. Methods: The present study is a descriptive-analytical study on 210 pregnant women in the first and second trimesters referring to health centers in Birjand in 2019. The tool used in this study was a researchermade questionnaire with four parts: women's demographic information, and women's knowledge, attitude, and practice, the validity, and reliability of which were confirmed. After data collection, it was entered into SPSS software version 22 and then analyzed using descriptive statistics, independent t-test, and one-way analysis of variance. The significance level was considered 0.05 in all tests. Results and Discussion: In this study, the mean scores of knowledge, attitude, and practice of pregnant women were 5.6 ±1.92, 55.9 ± 5.1, and 25.9± 3.7, respectively. There was a significant difference between the mean attitude score and mothers' age. There was also a significant difference between the mean scores of knowledge, attitude, and practice of women and significant difference in knowledge, attitude, and practice of employee and housewife pregnant women; In terms practice, there were significant differences between pregnant housewives and self-employed women. There was a significant relationship between the mean of these scores and mothers' jobs so that the mean scores were higher in employed women than others. Conclusions: The results of our study showed that the average score of knowledge, attitude, and practice of pregnant women in Birjand regarding oral hygiene during pregnancy is not satisfactory and appropriate.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42109014","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-07-28DOI: 10.52571/ptq.v18.n38.2021.03_miftakhov_pgs_27_37.pdf
E. Miftakhov, S. Mustafina, I. Nasyrov, A. Daminov
Background: the polymer product obtained in the presence of microheterogeneous catalytic systems is characterized by fairly molecular weight distribution (MWD), resulted from kinetically nonequivalent active centers (ACs) in the system that initiate the polymerization process. The nature and composition of ACs are determined by setting and solving an inverse problem on the formation of MWD. This problem is acute because revealing the nature of the kinetic heterogeneity explains changes in the molecular and consumer parameters of the product for different catalyst compositions and propagation modes in polymerizations. Aim: This study aimed to develop methods and algorithms for interpreting gel chromatograms to analyze the kinetic heterogeneity of a polymer product obtained industrially in microheterogeneous catalytic systems. Methods: the solution method is based on the assumption that the formed MWD is a superposition of distributions inherent in each type of ACs. Since the problem in the final formulation refers to the Fredholm integral equations of the first kind, the regularization method of A. N. Tikhonov is used for its numerical solution, with the original problem being preliminary discretized. This methodology and the developed software algorithms were used to determine the kinetic heterogeneity of titanium- and neodymium-containing catalytic systems. Results and discussion: The MWD analysis revealed two types of ACs with an average molecular weight of ATi-lnM = 11.3 and BTi-lnM = 13.2 in the titanium catalyst and three types of ACs ANd-lnM = 11.1, BNd-lnM = 12.7 and CNd-lnM = 14 for the neodymium catalyst, respectively. Conclusions: repeated computational experiments under different polymerization conditions and requirements for the preparation of a catalytic system make it possible to reveal a relationship with the resulting heterogeneity of ACs. It allows us to set and solve problems of controlling the molecular characteristics of the resulting polymer product.
{"title":"KINETIC HETEROGENEITY OF POLYMER PRODUCTS OBTAINED IN THE PRESENCE OF MICROHETEROGENIC CATALYTIC SYSTEMS BASED ON GEL CHROMATOGRAMS","authors":"E. Miftakhov, S. Mustafina, I. Nasyrov, A. Daminov","doi":"10.52571/ptq.v18.n38.2021.03_miftakhov_pgs_27_37.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n38.2021.03_miftakhov_pgs_27_37.pdf","url":null,"abstract":"Background: the polymer product obtained in the presence of microheterogeneous catalytic systems is characterized by fairly molecular weight distribution (MWD), resulted from kinetically nonequivalent active centers (ACs) in the system that initiate the polymerization process. The nature and composition of ACs are determined by setting and solving an inverse problem on the formation of MWD. This problem is acute because revealing the nature of the kinetic heterogeneity explains changes in the molecular and consumer parameters of the product for different catalyst compositions and propagation modes in polymerizations. Aim: This study aimed to develop methods and algorithms for interpreting gel chromatograms to analyze the kinetic heterogeneity of a polymer product obtained industrially in microheterogeneous catalytic systems. Methods: the solution method is based on the assumption that the formed MWD is a superposition of distributions inherent in each type of ACs. Since the problem in the final formulation refers to the Fredholm integral equations of the first kind, the regularization method of A. N. Tikhonov is used for its numerical solution, with the original problem being preliminary discretized. This methodology and the developed software algorithms were used to determine the kinetic heterogeneity of titanium- and neodymium-containing catalytic systems. Results and discussion: The MWD analysis revealed two types of ACs with an average molecular weight of ATi-lnM = 11.3 and BTi-lnM = 13.2 in the titanium catalyst and three types of ACs ANd-lnM = 11.1, BNd-lnM = 12.7 and CNd-lnM = 14 for the neodymium catalyst, respectively. Conclusions: repeated computational experiments under different polymerization conditions and requirements for the preparation of a catalytic system make it possible to reveal a relationship with the resulting heterogeneity of ACs. It allows us to set and solve problems of controlling the molecular characteristics of the resulting polymer product.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47353526","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-07-28DOI: 10.52571/ptq.v18.n38.2021.9_vostrikova_pgs_123_136.pdf
T. Vostrikova, V. Kalaev, A. Potapov, Gizacheu M. Manakhelokhe, K. Shikhaliev
Background: Productivity is increased with breeding techniques and modes for obtaining highly productive cultivars, various agricultural activities, and the use of new technologies for growing planting material. Some of modes to increase productivity are simple. They use different growth stimulants. Many methods were developed to synthesize organic compounds that have stimulating biological activity and can be used as growth stimulants for agricultural crop. Aim: The purpose of this research was to study the effect of synthesized organic compounds of the general formula: 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2-dihydroquinoline and 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2,3,4-tetrahydroquinoline on growth indicators (by which we meant seed germination and plant height, length, width, and the number of leaves) and the yield of the agricultural crop. Methods: To identify the biological effects of the synthesized organic compounds, morphometric parameters of an annual vegetable crop (Solanum melongena L.) were selected. It is investigated seed germination, growth processes, and yield. Growth processes were studied by biometric indicators. Biometric indicators included the plant height, length, width, and the number of leaves. Results and Discussion: The most effective growth stimulators from compounds of the series 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2-dihydroquinoline and 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2,3,4-tetrahydroquinoline for common eggplant were revealed. The most effective substances for Solanum melongena are 1,2,2,4-tetramethyl-6-(1-piperidinylcarbothioyl)-1,2,3,4-tetrahydroquinoline hydrochloride and 4-[(1,2,2,4-tetramethyl-1,2-dihydro-6-quinolinyl)carbothioyl]-1-piperazinylcarbaldehyde hydrochloride in tested concentrations (0,01 %; 0,05 % and 0,1 %), as well as the compounds of the general formula: 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2,3,4-tetrahydroquinoline in concentrations of 0,05 % and 0,1 %. It was established that the synthesized chemical substances cause stimulation of the eggplant growth compared with existing commercial preparation. Compounds of the series 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2- dihydroquinoline and 1-alkyl-2,2,4-trimethyl-6-aminocarbothioil-1,2,3,4-tetrahydroquinoline increase the seed germination of Solanum melongena from 30 to 80 %, the vegetative mass - from 10 to 40 %, yield - from 28 to 46 %. Conclusions: Tetrahydroquinolines are most effective as stimulants of growth processes (and productivity) for common eggplant. Compounds containing a dihydro-6-quinolinyl substituent stimulate the growth and also increase the yield of Solanum melongena. The expediency of quinoline series compounds for the production of vegetable growing is shown. Used growth stimulators increase the adaptive potential of Solanum melongena.
{"title":"USE OF NEW COMPOUNDS OF THE QUINOLINE SERIES AS GROWTH AND YIELD STIMULANTS OF AGRICULTURAL CROP","authors":"T. Vostrikova, V. Kalaev, A. Potapov, Gizacheu M. Manakhelokhe, K. Shikhaliev","doi":"10.52571/ptq.v18.n38.2021.9_vostrikova_pgs_123_136.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n38.2021.9_vostrikova_pgs_123_136.pdf","url":null,"abstract":"Background: Productivity is increased with breeding techniques and modes for obtaining highly productive cultivars, various agricultural activities, and the use of new technologies for growing planting material. Some of modes to increase productivity are simple. They use different growth stimulants. Many methods were developed to synthesize organic compounds that have stimulating biological activity and can be used as growth stimulants for agricultural crop. Aim: The purpose of this research was to study the effect of synthesized organic compounds of the general formula: 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2-dihydroquinoline and 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2,3,4-tetrahydroquinoline on growth indicators (by which we meant seed germination and plant height, length, width, and the number of leaves) and the yield of the agricultural crop. Methods: To identify the biological effects of the synthesized organic compounds, morphometric parameters of an annual vegetable crop (Solanum melongena L.) were selected. It is investigated seed germination, growth processes, and yield. Growth processes were studied by biometric indicators. Biometric indicators included the plant height, length, width, and the number of leaves. Results and Discussion: The most effective growth stimulators from compounds of the series 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2-dihydroquinoline and 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2,3,4-tetrahydroquinoline for common eggplant were revealed. The most effective substances for Solanum melongena are 1,2,2,4-tetramethyl-6-(1-piperidinylcarbothioyl)-1,2,3,4-tetrahydroquinoline hydrochloride and 4-[(1,2,2,4-tetramethyl-1,2-dihydro-6-quinolinyl)carbothioyl]-1-piperazinylcarbaldehyde hydrochloride in tested concentrations (0,01 %; 0,05 % and 0,1 %), as well as the compounds of the general formula: 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2,3,4-tetrahydroquinoline in concentrations of 0,05 % and 0,1 %. It was established that the synthesized chemical substances cause stimulation of the eggplant growth compared with existing commercial preparation. Compounds of the series 1-alkyl-2,2,4-trimethyl-6-aminocarbothioyl-1,2- dihydroquinoline and 1-alkyl-2,2,4-trimethyl-6-aminocarbothioil-1,2,3,4-tetrahydroquinoline increase the seed germination of Solanum melongena from 30 to 80 %, the vegetative mass - from 10 to 40 %, yield - from 28 to 46 %. Conclusions: Tetrahydroquinolines are most effective as stimulants of growth processes (and productivity) for common eggplant. Compounds containing a dihydro-6-quinolinyl substituent stimulate the growth and also increase the yield of Solanum melongena. The expediency of quinoline series compounds for the production of vegetable growing is shown. Used growth stimulators increase the adaptive potential of Solanum melongena.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"44466190","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2021-07-28DOI: 10.52571/ptq.v18.n38.2021.12_roni_pgs_164_175.pdf
K. Roni, Elfidiah Elfidiah, Ryan Pasongko, Dian Kharisma, S. Martini
Background: Indonesia is a country that has a tropical climate throughout the year along with relatively less difference of temperature during both dry and rainy seasons. The mobile community influences people’s interest in packaged drinks, including canned fruit juice. However, the first obstacle is the condition of the place and the temperature-related heavy metal lead (Pb) migration in canned orange juice drinks. Methods: This study focused on the relationship between Pb metal content, storage treatment, storage temperature, and storage time. This study used a canned orange juice drink from the distributor warehouse of Palembang city, standard Pb(NO3)2 (Merck) powder, 0.5 mol/l concentrated HNO3 solutions (Merck), concentrated HCl solution (Merck), demineralized water, Buffer pH 4.7, and 10. The sample was conducted from 5 °C to 40 °C with the testing period within 1-30 days. The sample at certain day intervals would then be tested to change pH and Pb ion concentration using the Atomic Absorption Spectrophotometry (AAS) test. Results and Discussion: In this study, the sample of orange juice was given different treatments, and each treatment has a differentiated analysis code consisting of S-SBJ-1-1 (Distributor warehouse) for one day of storage time, and the codes for 10 of storage time are SSBJ-10-1 (Freezer, temperature 5 °C), S-SJB-10-2 (Refrigerator, temperature 20 °C), S-SJB-10-3 (Homeroom, temperature 28 °C), S-SJB-10-4 (Oven, temperature 40 °C), S-SJB-10-5 (Open space, temperature 22°C - 38 °C). Furthermore, codes for 30 days of sample storage are S-SBJ-30-1 (Freezer, temperature 5 °C), S-SJB-30-2 (Refrigerator, temperature 20 °C), S-SJB-30-3 (Room house, temperature 28 °C, S-SJB-30-4 (Oven, temperature 40°C), and S-SJB-30-5 (Open space, temperature 22 °C-38 °C). Conclusions: Temperature and time have a significant influence on the migration of the heavy metal lead (Pb) from the can to orange juice drinks, and, for the minimum pH value, there is a less significant change. Overall, canned fruit juice should be stored at a temperature below 28 °C, and the drink is protected from direct sunlight and high humidity.
{"title":"THE EFFECT OF TEMPERATURE AND TIME ON THE MIGRATION OF LEAD METAL (PB) IONS IN CANNED ORANGE JUICE DRINK USING ATOMIC ABSORPTION SPECTROPHOTOMETRY ANALYSIS","authors":"K. Roni, Elfidiah Elfidiah, Ryan Pasongko, Dian Kharisma, S. Martini","doi":"10.52571/ptq.v18.n38.2021.12_roni_pgs_164_175.pdf","DOIUrl":"https://doi.org/10.52571/ptq.v18.n38.2021.12_roni_pgs_164_175.pdf","url":null,"abstract":"Background: Indonesia is a country that has a tropical climate throughout the year along with relatively less difference of temperature during both dry and rainy seasons. The mobile community influences people’s interest in packaged drinks, including canned fruit juice. However, the first obstacle is the condition of the place and the temperature-related heavy metal lead (Pb) migration in canned orange juice drinks. Methods: This study focused on the relationship between Pb metal content, storage treatment, storage temperature, and storage time. This study used a canned orange juice drink from the distributor warehouse of Palembang city, standard Pb(NO3)2 (Merck) powder, 0.5 mol/l concentrated HNO3 solutions (Merck), concentrated HCl solution (Merck), demineralized water, Buffer pH 4.7, and 10. The sample was conducted from 5 °C to 40 °C with the testing period within 1-30 days. The sample at certain day intervals would then be tested to change pH and Pb ion concentration using the Atomic Absorption Spectrophotometry (AAS) test. Results and Discussion: In this study, the sample of orange juice was given different treatments, and each treatment has a differentiated analysis code consisting of S-SBJ-1-1 (Distributor warehouse) for one day of storage time, and the codes for 10 of storage time are SSBJ-10-1 (Freezer, temperature 5 °C), S-SJB-10-2 (Refrigerator, temperature 20 °C), S-SJB-10-3 (Homeroom, temperature 28 °C), S-SJB-10-4 (Oven, temperature 40 °C), S-SJB-10-5 (Open space, temperature 22°C - 38 °C). Furthermore, codes for 30 days of sample storage are S-SBJ-30-1 (Freezer, temperature 5 °C), S-SJB-30-2 (Refrigerator, temperature 20 °C), S-SJB-30-3 (Room house, temperature 28 °C, S-SJB-30-4 (Oven, temperature 40°C), and S-SJB-30-5 (Open space, temperature 22 °C-38 °C). Conclusions: Temperature and time have a significant influence on the migration of the heavy metal lead (Pb) from the can to orange juice drinks, and, for the minimum pH value, there is a less significant change. Overall, canned fruit juice should be stored at a temperature below 28 °C, and the drink is protected from direct sunlight and high humidity.","PeriodicalId":45103,"journal":{"name":"Periodico Tche Quimica","volume":" ","pages":""},"PeriodicalIF":0.4,"publicationDate":"2021-07-28","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"47753655","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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