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Investigation of stress-induced progressive failure of mine pillars using a Voronoi grain-based breakable block model 利用基于 Voronoi 晶粒的可破块模型研究应力诱发的矿柱渐进式破坏
IF 11.7 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-05-01 DOI: 10.1016/j.ijmst.2024.05.001

The Voronoi grain-based breakable block model (VGBBM) based on the combined finite-discrete element method (FDEM) was proposed to explicitly characterize the failure mechanism and predict the deformation behavior of hard-rock mine pillars. The influence of the microscopic parameters on the macroscopic mechanical behavior was investigated using laboratory-scale models. The field-scale pillar models (width-to-height, W/H=1, 2 and 3) were calibrated based on the empirically predicted stress-strain curves of Creighton mine pillars. The results indicated that as the W/H ratios increased, the VGBBM effectively predicted the transition from strain-softening to pseudo-ductile behavior in pillars, and explicitly captured the separated rock slabs and the V-shaped damage zones on both sides of pillars and conjugate shear bands in core zones of pillars. The volumetric strain field revealed significant compressional deformation in core zones of pillars. While the peak strains of W/H=1 and 2 pillars were relatively consistent, there were significant differences in the strain energy storage and release mechanism. W/H was the primary factor influencing the deformation and strain energy in the pillar core. The friction coefficient of the structural plane was also an important factor affecting the pillar strength and the weakest discontinuity angle. The fracture surface was controlled by the discontinuity angle and the friction coefficient. This study demonstrated the capability of the VGBBM in predicting the strengths and deformation behavior of hard-rock pillars in deep mine design.

提出了基于有限元-离散元组合法(FDEM)的 Voronoi 晶粒可破碎块体模型(VGBBM),以明确描述硬岩矿柱的破坏机制并预测其变形行为。利用实验室尺度模型研究了微观参数对宏观力学行为的影响。根据克雷顿矿柱的经验预测应力-应变曲线,校准了野外规模矿柱模型(宽度-高度,W/H=1、2 和 3)。结果表明,随着 W/H 比的增加,VGBBM 有效地预测了矿柱从应变软化到假韧性行为的转变,并明确捕捉到了分离的岩板和矿柱两侧的 V 型破坏带以及矿柱核心区的共轭剪切带。体积应变场显示了岩柱核心区的显著压缩变形。虽然 W/H=1 和 2 柱的峰值应变相对一致,但应变能的存储和释放机制存在显著差异。W/H 是影响柱心变形和应变能的主要因素。结构平面的摩擦系数也是影响支柱强度和最弱不连续角的重要因素。断裂面受不连续角和摩擦系数的控制。这项研究证明了 VGBBM 在预测深部矿山设计中硬岩柱的强度和变形行为方面的能力。
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引用次数: 0
Effect of dry-wet cycles on dynamic properties and microstructures of sandstone: Experiments and modelling 干湿循环对砂岩动态特性和微观结构的影响:实验与建模
IF 11.7 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-05-01 DOI: 10.1016/j.ijmst.2024.04.008

Underground pumped storage power plant (UPSP) is an innovative concept for space recycling of abandoned mines. Its realization requires better understanding of the dynamic performance and durability of reservoir rock. This paper conducted ultrasonic detection, split Hopkinson pressure bar (SHPB) impact, mercury intrusion porosimetry (MIP), and backscatter electron observation (BSE) tests to investigate the dynamical behaviour and microstructure of sandstone with cyclical dry-wet damage. A coupling FEM-DEM model was constructed for reappearing mesoscopic structure damage. The results show that dry-wet cycles decrease the dynamic compressive strength (DCS) with a maximum reduction of 39.40%, the elastic limit strength is reduced from 41.75 to 25.62 MPa. The sieved fragments obtain the highest crack growth rate during the 23rd dry-wet cycle with a predictable life of 25 cycles for each rock particle. The pore fractal features of the macropores and micro-meso pores show great differences between the early and late cycles, which verifies the computational statistics analysis of particle deterioration. The numerical results show that the failure patterns are governed by the strain in pre-peak stage and the shear cracks are dominant. The dry-wet cycles reduce the energy transfer efficiency and lead to the discretization of force chain and crack fields.

地下抽水蓄能电站(UPSP)是废弃矿井空间回收利用的创新概念。要实现这一目标,需要更好地了解储层岩石的动态性能和耐久性。本文通过超声波探测、分裂霍普金森压力棒(SHPB)冲击、汞侵入孔隙模拟(MIP)和反向散射电子观测(BSE)试验来研究循环干湿破坏砂岩的动力学行为和微观结构。针对重现的中观结构损伤,构建了一个 FEM-DEM 耦合模型。结果表明,干湿循环降低了动态抗压强度(DCS),最大降幅为 39.40%,弹性极限强度从 41.75 兆帕降至 25.62 兆帕。在第 23 次干湿循环期间,筛分碎片的裂缝增长率最高,每个岩石颗粒的可预测寿命为 25 次循环。大孔和微孔的孔隙分形特征在早期和晚期循环中表现出很大差异,这验证了颗粒劣化的计算统计分析。数值结果表明,破坏模式受前峰阶段应变的支配,剪切裂纹占主导地位。干湿循环降低了能量传递效率,导致力链和裂纹场离散化。
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引用次数: 0
Investigation on mechanical properties regulation of rock-like specimens based on 3D printing and similarity quantification 基于三维打印和相似性量化的类岩试样力学性能调控研究
IF 11.7 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-05-01 DOI: 10.1016/j.ijmst.2024.05.004
Duanyang Zhuang , Zexu Ning , Yunmin Chen, Jinlong Li, Qingdong Li, Wenjie Xu

3D printing is widely adopted to quickly produce rock mass models with complex structures in batches, improving the consistency and repeatability of physical modeling. It is necessary to regulate the mechanical properties of 3D-printed specimens to make them proportionally similar to natural rocks. This study investigates mechanical properties of 3D-printed rock analogues prepared by furan resin-bonded silica sand particles. The mechanical property regulation of 3D-printed specimens is realized through quantifying its similarity to sandstone, so that analogous deformation characteristics and failure mode are acquired. Considering similarity conversion, uniaxial compressive strength, cohesion and stress–strain relationship curve of 3D-printed specimen are similar to those of sandstone. In the study ranges, the strength of 3D-printed specimen is positively correlated with the additive content, negatively correlated with the sand particle size, and first increases then decreases with the increase of curing temperature. The regulation scheme with optimal similarity quantification index, that is the sand type of 70/140, additive content of 2.5‰ and curing temperature of 81.6 ℃, is determined for preparing 3D-printed sandstone analogues and models. The effectiveness of mechanical property regulation is proved through uniaxial compression contrast tests. This study provides a reference for preparing rock-like specimens and engineering models using 3D printing technology.

三维打印技术被广泛应用于批量快速制作结构复杂的岩体模型,提高了物理建模的一致性和可重复性。有必要对 3D 打印试样的力学性能进行调节,使其与天然岩石在比例上相似。本研究探讨了呋喃树脂粘结硅砂颗粒制备的三维打印岩石模拟物的力学性能。通过量化三维打印试样与砂岩的相似性,获得相似的变形特征和破坏模式,从而实现对三维打印试样力学性能的调节。考虑到相似性转换,3D 打印试样的单轴抗压强度、内聚力和应力应变关系曲线与砂岩相似。在研究范围内,3D 打印试样的强度与添加剂含量呈正相关,与砂粒粒径呈负相关,且随着固化温度的升高先升高后降低。确定了砂型为 70/140、添加剂含量为 2.5‰、固化温度为 81.6 ℃的最佳相似性量化指标调节方案,用于制备 3D 打印砂岩模拟物和模型。通过单轴压缩对比试验证明了力学性能调节的有效性。该研究为利用三维打印技术制备岩石类试样和工程模型提供了参考。
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引用次数: 0
Enhanced Hoek-Brown (H-B) criterion for rocks exposed to chemical corrosion 受化学腐蚀岩石的强化霍克-布朗(H-B)标准
IF 11.7 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-05-01 DOI: 10.1016/j.ijmst.2024.05.002
Hao Li , Leo Pel , Zhenjiang You , David Smeulders

Underground constructions often encounter water environments, where water–rock interaction can increase porosity, thereby weakening engineering rocks. Correspondingly, the failure criterion for chemically corroded rocks becomes essential in the stability analysis and design of such structures. This study enhances the applicability of the Hoek-Brown (H-B) criterion for engineering structures operating in chemically corrosive conditions by introducing a kinetic porosity-dependent instantaneous mi (KPIM). A multiscale experimental investigation, including nuclear magnetic resonance (NMR), X-ray diffraction (XRD), scanning electron microscopy (SEM), pH and ion chromatography analysis, and triaxial compression tests, is employed to quantify pore structural changes and their linkage with the strength responses of limestone under coupled chemical-mechanical (C-M) conditions. By employing ion chromatography and NMR analysis, along with incorporating the principles of free-face dissolution theory accounting for both congruent and incongruent dissolution, a kinetic chemical corrosion model is developed. This model aims to calculate the kinetic porosity alterations within rocks exposed to varying H+ concentrations and durations. Subsequently, utilizing the generalized mixture rule (GMR), the kinetic porosity-dependent mi is formulated. Evaluation of the KPIM-enhanced H-B criterion using compression test data from 5 types of rocks demonstrated a high level of consistency between the criterion and the experimental results, with a coefficient of determination greater than 0.96, a mean absolute percentage error less than 4.84%, and a root-mean-square deviation less than 5.95 MPa. Finally, the physical significance of the porosity-dependent instantaneous mi is clarified: it serves as an indicator of a rock’s capacity to leverage the confining pressure effect.

地下工程经常会遇到水环境,水与岩石的相互作用会增加孔隙率,从而削弱工程岩石的强度。因此,化学腐蚀岩石的失效准则对于此类结构的稳定性分析和设计至关重要。本研究通过引入动力学孔隙度瞬时值(KPIM),增强了霍克-布朗(Hoek-Brown,H-B)准则对化学腐蚀条件下工程结构的适用性。多尺度实验研究包括核磁共振 (NMR)、X 射线衍射 (XRD)、扫描电子显微镜 (SEM)、pH 值和离子色谱分析以及三轴压缩试验,用于量化孔隙结构变化及其与石灰石在化学-机械耦合 (C-M) 条件下的强度响应之间的联系。通过采用离子色谱法和核磁共振分析,并结合自由面溶解理论的原理,考虑到同向溶解和非同向溶解,建立了一个动力学化学腐蚀模型。该模型旨在计算暴露于不同氢浓度和持续时间的岩石中的动力学孔隙度变化。随后,利用广义混合物规则(GMR),制定了动力学孔隙度依赖性。利用 5 种岩石的压缩试验数据对 KPIM 增强 H-B 标准进行了评估,结果表明该标准与试验结果高度一致,决定系数大于 0.96,平均绝对百分比误差小于 4.84%,均方根偏差小于 5.95 兆帕。最后,澄清了孔隙度瞬时值的物理意义:它是岩石利用约束压力效应能力的指标。
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引用次数: 0
Inverting the rock mass P-wave velocity field ahead of deep buried tunnel face while borehole drilling 钻孔时在深埋隧道工作面前方反转岩体 P 波速度场
IF 11.7 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-05-01 DOI: 10.1016/j.ijmst.2024.06.001
Liu Liu , Shaojun Li , Minzong Zheng , Dong Wang , Minghao Chen , Junbo Zhou , Tingzhou Yan , Zhenming Shi

Imaging the wave velocity field surrounding a borehole while drilling is a promising and urgently needed approach for extending the exploration range of the borehole point. This paper develops a drilling process detection (DPD) system consisting of a multifunctional sensor and a pilot geophone installed at the top of the drilling rod, geophones at the tunnel face, a laser rangefinder, and an onsite computer. A weighted adjoint-state first arrival travel time tomography method is used to invert the P-wave velocity field of rock mass while borehole drilling. A field experiment in the ongoing construction of a deep buried tunnel in southwestern China demonstrated the DPD system and the tomography method. Time-frequency analysis of typical borehole drilling detection data shows that the impact drilling source is a pulse-like seismic exploration wavelet. A velocity field of the rock mass in a triangular area defined by the borehole trajectory and geophone receiving line can be obtained. Both the borehole core and optical image validate the inverted P-wave velocity field. A numerical simulation of a checkerboard benchmark model is used to test the tomography method. The rapid convergence of the misfits and consistent agreement between the inverted and observed travel times validate the P-wave velocity imaging.

在钻探过程中对钻孔周围的波速场进行成像,是扩大钻孔点勘探范围的一种前景广阔且急需的方法。本文开发了一种钻进过程探测(DPD)系统,由安装在钻杆顶部的多功能传感器和先导检波器、隧道面检波器、激光测距仪和现场计算机组成。采用加权邻接态初至旅行时间层析成像法,在钻孔时反演岩体的 P 波速度场。在中国西南部正在进行的深埋隧道施工中进行的现场实验演示了 DPD 系统和层析成像方法。典型钻孔检测数据的时频分析表明,冲击钻孔源是一种脉冲类地震勘探小波。可以获得钻孔轨迹和检波器接收线所定义的三角形区域内岩体的速度场。钻孔岩心和光学图像都验证了反演的 P 波速度场。使用棋盘式基准模型的数值模拟来测试层析成像方法。误差的快速收敛以及反演和观测到的移动时间之间的一致验证了 P 波速度成像。
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引用次数: 0
IFC: Editorial 国际金融公司: 编辑
IF 11.7 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-05-01 DOI: 10.1016/S2095-2686(24)00070-3
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引用次数: 0
A novel box-counting method for quantitative fractal analysis of three-dimensional pore characteristics in sandstone 对砂岩三维孔隙特征进行定量分形分析的新型盒式计数法
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-04-01 DOI: 10.1016/j.ijmst.2024.04.006
Huiqing Liu , Heping Xie , Fei Wu , Cunbao Li , Renbo Gao

Fractal theory offers a powerful tool for the precise description and quantification of the complex pore structures in reservoir rocks, crucial for understanding the storage and migration characteristics of media within these rocks. Faced with the challenge of calculating the three-dimensional fractal dimensions of rock porosity, this study proposes an innovative computational process that directly calculates the three-dimensional fractal dimensions from a geometric perspective. By employing a composite denoising approach that integrates Fourier transform (FT) and wavelet transform (WT), coupled with multimodal pore extraction techniques such as threshold segmentation, top-hat transformation, and membrane enhancement, we successfully crafted accurate digital rock models. The improved box-counting method was then applied to analyze the voxel data of these digital rocks, accurately calculating the fractal dimensions of the rock pore distribution. Further numerical simulations of permeability experiments were conducted to explore the physical correlations between the rock pore fractal dimensions, porosity, and absolute permeability. The results reveal that rocks with higher fractal dimensions exhibit more complex pore connectivity pathways and a wider, more uneven pore distribution, suggesting that the ideal rock samples should possess lower fractal dimensions and higher effective porosity rates to achieve optimal fluid transmission properties. The methodology and conclusions of this study provide new tools and insights for the quantitative analysis of complex pores in rocks and contribute to the exploration of the fractal transport properties of media within rocks.

分形理论为精确描述和量化储层岩石中复杂的孔隙结构提供了强有力的工具,对于了解这些岩石中介质的存储和迁移特征至关重要。面对计算岩石孔隙度三维分形维数的挑战,本研究提出了一种创新的计算流程,从几何角度直接计算三维分形维数。通过采用傅立叶变换(FT)和小波变换(WT)相结合的复合去噪方法,并结合阈值分割、顶帽变换和膜增强等多模态孔隙提取技术,我们成功地制作出了精确的数字岩石模型。然后,改进的盒计数法被用于分析这些数字岩石的体素数据,准确计算出岩石孔隙分布的分形维数。为了探索岩石孔隙分形尺寸、孔隙度和绝对渗透率之间的物理关联性,还进行了进一步的渗透率数值模拟实验。结果表明,分形维数较高的岩石孔隙连通路径更复杂,孔隙分布更宽广、更不均匀,这表明理想的岩石样本应具有较低的分形维数和较高的有效孔隙率,以实现最佳的流体传输特性。本研究的方法和结论为定量分析岩石中的复杂孔隙提供了新的工具和见解,有助于探索岩石内部介质的分形传输特性。
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引用次数: 0
IFC: Editorial 国际金融公司: 编辑
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-04-01 DOI: 10.1016/S2095-2686(24)00053-3
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引用次数: 0
A photogrammetric approach for quantifying the evolution of rock joint void geometry under varying contact states 量化不同接触状态下岩石节理空隙几何形状演变的摄影测量方法
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-04-01 DOI: 10.1016/j.ijmst.2024.04.001
Rui Yong , Changshuo Wang , Nick Barton , Shigui Du

Accurate measurement of the evolution of rock joint void geometry is essential for comprehending the distribution characteristics of asperities responsible for shear and seepage behaviors. However, existing techniques often require specialized equipment and skilled operators, posing practical challenges. In this study, a cost-effective photogrammetric approach is proposed. Particularly, local coordinate systems are established to facilitate the alignment and precise quantification of the relative position between two halves of a rock joint. Push/pull tests are conducted on rock joints with varying roughness levels to induce different contact states. A high-precision laser scanner serves as a benchmark for evaluating the photogrammetry method. Despite certain deviations exist, the measured evolution of void geometry is generally consistent with the qualitative findings of previous studies. The photogrammetric measurements yield comparable accuracy to laser scanning, with maximum errors of 13.2% for aperture and 14.4% for void volume. Most joint matching coefficient (JMC) measurement errors are below 20%. Larger measurement errors occur primarily in highly mismatched rock joints with JMC values below 0.2, but even in cases where measurement errors exceed 80%, the maximum JMC error is only 0.0434. Thus, the proposed photogrammetric approach holds promise for widespread application in void geometry measurements in rock joints.

精确测量岩石节理空隙几何形状的演变,对于理解造成剪切和渗流行为的凸面分布特征至关重要。然而,现有的技术往往需要专业设备和熟练的操作人员,带来了实际挑战。本研究提出了一种具有成本效益的摄影测量方法。特别是建立了局部坐标系,以方便对准和精确量化岩石节理两半之间的相对位置。在不同粗糙度的岩石节理上进行推/拉试验,以诱发不同的接触状态。高精度激光扫描仪是评估摄影测量方法的基准。尽管存在某些偏差,但测量到的空隙几何形状的演变与之前研究的定性结论基本一致。摄影测量的精度与激光扫描相当,孔径的最大误差为 13.2%,空隙体积的最大误差为 14.4%。大多数联合匹配系数(JMC)测量误差低于 20%。较大的测量误差主要出现在高度不匹配的岩石节理中,其 JMC 值低于 0.2,但即使在测量误差超过 80% 的情况下,最大 JMC 误差也仅为 0.0434。因此,拟议的摄影测量方法有望广泛应用于岩石节理空隙几何测量。
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引用次数: 0
Enhancing sustainability in phosphate ore processing: Performance of frying oil as alternative flotation collector for carbonate removal 提高磷矿石加工的可持续性:煎炸油作为替代浮选捕收剂去除碳酸盐的性能
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-04-01 DOI: 10.1016/j.ijmst.2024.04.003
Asmae El-bahi, Yassine Taha, Yassine Ait-Khouia, Abdellatif Elghali, Mostafa Benzaazoua

Recycling waste frying oils for the synthesis of flotation reagents presents a promising avenue for sustainable waste management. Moreover, it offers a cost-effective solution for crafting a specialized collector designed to efficiently remove carbonates and enhance phosphate enrichment in froth flotation processes. This study focuses on the synthesis of an anionic collector using the saponification reaction of a frying oil sample, subsequently applied to the flotation of calcite and dolomite. To elucidate the adsorption mechanisms of the frying oil collector (FrOC) and sodium oleate, a reference collector, on fluorapatite, calcite, dolomite, and quartz surfaces, comprehensive experiments were conducted, including zeta potential measurements and Fourier transform infrared spectroscopy. Results revealed diverse adsorption affinities of the molecules towards these minerals. To assess the practical performance of the collector, flotation tests were conducted using a natural phosphate ore mixture, employing a Box-Behnken experimental design. Notably, under optimized conditions (pH 9, 1000 g/t of FrOC, 3.5 min of conditioning, and 6 min of flotation), FrOC exhibited excellent performance, with calcite and dolomite recoveries exceeding 80%, while apatite recovery in the concentrate fraction remained below 10%. This work exemplifies both circular economy practices and the distinctive approach to sustainable mineral processing.

回收利用废弃煎炸油来合成浮选试剂为可持续废物管理提供了一条前景广阔的途径。此外,它还提供了一种具有成本效益的解决方案,可用于制作专用的捕集剂,以在泡沫浮选工艺中有效去除碳酸盐并提高磷酸盐富集度。本研究的重点是利用煎炸油样品的皂化反应合成阴离子捕收剂,随后将其应用于方解石和白云石的浮选。为了阐明煎炸油捕收剂(FrOC)和参考捕收剂油酸钠在氟磷灰石、方解石、白云石和石英表面的吸附机制,研究人员进行了全面的实验,包括 zeta 电位测量和傅立叶变换红外光谱分析。结果显示,分子对这些矿物的吸附亲和力各不相同。为了评估这种捕收剂的实际性能,采用 Box-Behnken 实验设计,使用天然磷矿混合物进行了浮选测试。值得注意的是,在优化条件下(pH 值为 9、FrOC 的浓度为 1000 克/吨、调节时间为 3.5 分钟、浮选时间为 6 分钟),FrOC 表现出卓越的性能,方解石和白云石的回收率超过 80%,而精矿部分的磷灰石回收率仍低于 10%。这项工作是循环经济实践和可持续矿物加工独特方法的典范。
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引用次数: 0
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International Journal of Mining Science and Technology
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