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IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-03-01 DOI: 10.1016/S2095-2686(24)00036-3
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引用次数: 0
Microdynamic mechanical properties and fracture evolution mechanism of monzogabbro with a true triaxial multilevel disturbance method 用真实三轴多级扰动法研究独居岩的微动态力学性能和断裂演化机理
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-03-01 DOI: 10.1016/j.ijmst.2024.01.001
Zhi Zheng , Bin Deng , Hong Liu , Wei Wang , Shuling Huang , Shaojun Li

The far-field microdynamic disturbance caused by the excavation of deep mineral resources and underground engineering can induce surrounding rock damage in high-stress conditions and even lead to disasters. However, the mechanical properties and damage/fracture evolution mechanisms of deep rock induced by microdynamic disturbance under three-dimensional stress states are unclear. Therefore, a true triaxial multilevel disturbance test method is proposed, which can completely simulate natural geostress, excavation stress redistribution (such as stress unloading, concentration and rotation), and subsequently the microdynamic disturbance triggering damaged rock failure. Based on a dynamic true triaxial test platform, true triaxial microdynamic disturbance tests under different frequency and amplitudes were carried out on monzogabbro. The results show that increasing amplitude or decreasing frequency diminishes the failure strength of monzogabbro. Deformation modulus gradually decreases during disturbance failure. As frequency and amplitude increase, the degradation rate of deformation modulus decreases slightly, disturbance dissipated energy increases significantly, and disturbance deformation anisotropy strengthens obviously. A damage model has been proposed to quantitatively characterize the disturbance-induced damage evolution at different frequency and amplitude under true triaxial stress. Before disturbance failure, the micro-tensile crack mechanism is dominant, and the micro-shear crack mechanism increases significantly at failure. With the increase of amplitude and frequency, the micro-shear crack mechanism increases. When approaching disturbance failure, the acoustic emission fractal dimension changes from a stable value to local large oscillation, and finally increases sharply to a high value at failure. Finally, the disturbance-induced failure mechanism of surrounding rock in deep engineering is clearly elucidated.

深部矿产资源挖掘和地下工程引起的远场微动力扰动会在高应力条件下诱发围岩破坏,甚至导致灾害。然而,三维应力状态下微动力扰动诱发的深部岩石力学性能和破坏/断裂演化机理尚不清楚。因此,我们提出了一种真正的三轴多级扰动试验方法,它可以完全模拟自然地应力、开挖应力重分布(如应力卸载、集中和旋转)以及随后引发受损岩石破坏的微动力扰动。基于动态真三轴试验平台,在单斜辉长岩上进行了不同频率和振幅的真三轴微动力扰动试验。试验结果表明,增加振幅或降低频率都会降低片麻岩的破坏强度。在扰动破坏过程中,变形模量逐渐减小。随着频率和振幅的增加,变形模量的衰减率略有下降,扰动耗散能量显著增加,扰动变形各向异性明显增强。为了定量描述真实三轴应力下不同频率和振幅下扰动诱发的损伤演变,提出了一个损伤模型。扰动破坏前,微拉伸裂纹机制占主导地位,破坏时微剪切裂纹机制显著增加。随着振幅和频率的增加,微剪切裂纹机理也随之增加。当接近扰动破坏时,声发射分形维数从稳定值变为局部大振荡,最后急剧增加到破坏时的高值。最后,清楚地阐明了深部工程中围岩的扰动诱发破坏机理。
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引用次数: 0
An extended micromechanical-based plastic damage model for understanding water effects on quasi-brittle rocks 基于微机械的扩展塑性破坏模型,用于理解水对准脆性岩石的影响
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-03-01 DOI: 10.1016/j.ijmst.2024.02.006
Qiaojuan Yu , Shigui Du , Qizhi Zhu , Zhanyou Luo , Sili Liu , Lunyang Zhao

Water effects on the mechanical properties of rocks have been extensively investigated through experiments and numerical models. However, few studies have established a comprehensive link between the microscopic mechanisms of water-related micro-crack and the constitutive behaviors of rocks. In this work, we shall propose an extended micromechanical-based plastic damage model for understanding weakening effect induced by the presence of water between micro-crack’s surfaces on quasi-brittle rocks, based on the Mori-Tanaka homogenization and irreversible thermodynamics framework. Regarding the physical mechanism, water strengthens micro-crack propagation, which induces damage evolution during the pre- and post-stage, and weakens the elastic effective properties of rock matrix. After proposing a special calibration procedure for the determination of model parameters based on the laboratory compression tests, the proposed micromechanical-based model is verified by comparing the model predictions to the experimental results. The model effectively captures the mechanical behaviors of quasi-brittle rocks subjected to the weakening effects of water.

人们通过实验和数值模型对水对岩石力学性能的影响进行了广泛研究。然而,很少有研究在与水有关的微裂缝的微观机制和岩石的构成行为之间建立了全面的联系。在这项工作中,我们将基于 Mori-Tanaka 均质化和不可逆热力学框架,提出一个基于微观力学的扩展塑性损伤模型,以理解准脆性岩石微裂缝表面之间存在水所诱发的削弱效应。在物理机制方面,水加强了微裂缝的扩展,从而诱发了前后阶段的损伤演化,并削弱了岩石基体的弹性有效特性。在实验室压缩试验的基础上,提出了确定模型参数的特殊校准程序,并通过将模型预测结果与实验结果进行比较,验证了所提出的基于微观力学的模型。该模型有效地捕捉了受水削弱效应影响的准脆性岩石的力学行为。
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引用次数: 0
Experimental investigation on coal pore-fracture variation and fractal characteristics synergistically affected by solvents for improving clean gas extraction 煤炭孔隙裂隙变化与分形特征受溶剂协同影响的实验研究,以提高瓦斯抽采效率
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-03-01 DOI: 10.1016/j.ijmst.2024.02.004
Feilin Han , Sheng Xue , Chunshan Zheng , Zhongwei Chen , Guofu Li , Bingyou Jiang

Chemical solvents instead of pure water being as hydraulic fracturing fluid could effectively increase permeability and improve clean methane extraction efficiency. However, pore-fracture variation features of lean coal synergistically affected by solvents have not been fully understood. Ultrasonic testing, nuclear magnetic resonance analysis, liquid phase mass spectrometry was adopted to comprehensively analyze pore-fracture change characteristics of lean coal treated by combined solvent (NMP and CS2). Meanwhile, quantitative characterization of above changing properties was conducted using geometric fractal theory. Relationship model between permeability, fractal dimension and porosity were established. Results indicate that the end face fractures of coal are well developed after CS2 and combined solvent treatments, of which, end face box-counting fractal dimensions range from 1.1227 to 1.4767. Maximum decreases in ultrasonic longitudinal wave velocity of coal affected by NMP, CS2 and combined solvent are 2.700%, 20.521%, 22.454%, respectively. Solvent treatments could lead to increasing amount of both mesopores and macropores. Decrease ratio of fractal dimension Ds is 0.259%–2.159%, while permeability increases ratio of NMR ranges from 0.1904 to 6.4486. Meanwhile, combined solvent could dissolve coal polar and non-polar small molecules and expand flow space. Results could provide reference for solvent selection and parameter optimization of permeability-enhancement technology.

用化学溶剂代替纯水作为水力压裂液,可有效增加渗透率,提高清洁甲烷抽采效率。然而,贫煤在溶剂协同作用下的孔隙-裂缝变化特征尚未得到充分了解。本研究采用超声波测试、核磁共振分析、液相质谱等方法,全面分析了联合溶剂(NMP 和 CS2)处理贫煤的孔隙-断裂变化特征。同时,利用几何分形理论对上述变化特性进行了定量表征。建立了渗透率、分形维数和孔隙度之间的关系模型。结果表明,经过 CS2 和联合溶剂处理后,煤的端面裂缝发育良好,其中端面箱形计数分形尺寸范围在 1.1227 至 1.4767 之间。受 NMP、CS2 和复合溶剂影响的煤的超声纵波速度最大降幅分别为 2.700%、20.521% 和 22.454%。溶剂处理可增加中孔和大孔的数量。分形维数 Ds 的下降率为 0.259%-2.159%,而 NMR 的渗透率增加率为 0.1904-6.4486。同时,组合溶剂可以溶解煤极性和非极性小分子,扩大流动空间。研究结果可为溶剂选择和增透技术参数优化提供参考。
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引用次数: 0
Experimental study of the damage characteristics of rocks containing non-penetrating cracks under cyclic loading 循环加载下含有非穿透性裂缝的岩石的破坏特性实验研究
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-02-01 DOI: 10.1016/j.ijmst.2024.02.002
Jun Xu , Xiaochun Xiao , Lu Ma , Sen Luo , Jiaxu Jin , Baijian Wu

The damage evolution process of non-penetrating cracks often causes some unexpected engineering disasters. Gypsum specimens containing non-penetrating crack(s) are used to study the damage evolution and characteristics under cyclic loading. The results show that under cyclic loading, the relationship between the number of non-penetrating crack(s) and the characteristic parameters (cyclic number, peak stress, peak strain, failure stress, and failure strain) of the pre-cracked specimens can be represented by a decreasing linear function. The damage evolution equation is fitted by calibrating the accumulative plastic strain for each cycle, and the damage constitutive equation is proposed by the concept of effective stress. Additionally, non-penetrating cracks are more likely to cause uneven stress distribution, damage accumulation, and local failure of specimen. The local failure can change the stress distribution and relieve the inhibition of non-penetrating crack extension and eventually cause a dramatic destruction of the specimen. Therefore, the evolution process caused by non-penetrating cracks can be regarded as one of the important reasons for inducing rockburst. These results are expected to improve the understanding of the process of spalling formation and rockburst and can be used to analyze the stability of rocks or rock structures.

非贯穿性裂缝的破坏演变过程往往会造成一些意想不到的工程灾难。本文采用含有非贯穿性裂缝的石膏试样,研究了循环加载下的破坏演化过程和特征。结果表明,在循环加载下,非穿透裂缝的数量与预开裂试样的特征参数(循环数量、峰值应力、峰值应变、破坏应力和破坏应变)之间的关系可以用一个递减的线性函数来表示。通过校准每个循环的累积塑性应变来拟合损伤演化方程,并通过有效应力的概念提出损伤构成方程。此外,非贯穿性裂缝更容易导致应力分布不均、损伤累积和试样局部破坏。局部破坏会改变应力分布,解除对非穿透裂纹扩展的抑制,最终导致试样的剧烈破坏。因此,非贯穿性裂缝引起的演化过程可视为诱发岩爆的重要原因之一。这些结果有望加深对剥落形成和岩爆过程的理解,并可用于分析岩石或岩石结构的稳定性。
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引用次数: 0
Transfer learning framework for multi-scale crack type classification with sparse microseismic networks 利用稀疏微震网络进行多尺度裂缝类型分类的迁移学习框架
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-02-01 DOI: 10.1016/j.ijmst.2024.01.003
Arnold Yuxuan Xie, Bing Q. Li

Rock fracture mechanisms can be inferred from moment tensors (MT) inverted from microseismic events. However, MT can only be inverted for events whose waveforms are acquired across a network of sensors. This is limiting for underground mines where the microseismic stations often lack azimuthal coverage. Thus, there is a need for a method to invert fracture mechanisms using waveforms acquired by a sparse microseismic network. Here, we present a novel, multi-scale framework to classify whether a rock crack contracts or dilates based on a single waveform. The framework consists of a deep learning model that is initially trained on 2400000+ manually labelled field-scale seismic and microseismic waveforms acquired across 692 stations. Transfer learning is then applied to fine-tune the model on 300000+ MT-labelled lab-scale acoustic emission waveforms from 39 individual experiments instrumented with different sensor layouts, loading, and rock types in training. The optimal model achieves over 86% F-score on unseen waveforms at both the lab- and field-scale. This model outperforms existing empirical methods in classification of rock fracture mechanisms monitored by a sparse microseismic network. This facilitates rapid assessment of, and early warning against, various rock engineering hazard such as induced earthquakes and rock bursts.

岩石断裂机制可从微震事件反演的力矩张量(MT)中推断出来。然而,矩张量只能对波形通过传感器网络获取的事件进行反演。这对地下矿井来说是个限制,因为地下矿井的微震站往往缺乏方位覆盖。因此,需要一种利用稀疏微地震网络获取的波形反演断裂机制的方法。在此,我们提出了一种新颖的多尺度框架,可根据单一波形对岩石裂缝是收缩还是扩张进行分类。该框架由一个深度学习模型组成,该模型最初是在 692 个台站采集的 2400000+ 人工标注的现场尺度地震和微震波形上进行训练的。然后,应用迁移学习对模型进行微调,微调的对象是来自 39 个独立实验的 300,000+ MT 标记的实验室尺度声发射波形,这些实验在训练中使用了不同的传感器布局、载荷和岩石类型。在实验室和现场尺度的未见波形上,最优模型的 F 分数超过 86%。在对稀疏微地震网络监测到的岩石断裂机制进行分类方面,该模型优于现有的经验方法。这有助于对诱发地震和岩爆等各种岩石工程危险进行快速评估和预警。
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引用次数: 0
Three-dimensional stress variation characteristics in deep hard rock of CJPL-II project based on in-situ monitoring 基于原位监测的 CJPL-II 项目深层硬岩三维应力变化特征
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-02-01 DOI: 10.1016/j.ijmst.2023.12.007
Minzong Zheng , Shaojun Li , Zejie Feng , Huaisheng Xu , Yaxun Xiao

In deep hard rock excavation, stress plays a pivotal role in inducing stress-controlled failure. While the impact of excavation-induced stress disturbance on rock failure and tunnel stability has undergone comprehensive examination through laboratory tests and numerical simulations, its validation through in-situ stress tests remains unexplored. This study analyzes the three-dimensional stress changes in the surrounding rock at various depths, monitored during the excavation of B2 Lab in China Jinping Underground Laboratory Phase II (CJPL-II). The investigation delves into the three-dimensional stress variation characteristics in deep hard rock, encompassing stress components and principal stress. The results indicate changes in both the magnitude and direction of the principal stress during tunnel excavation. To quantitatively describe the degree of stress disturbance, a series of stress evaluation indexes are established based on the distances between stress tensors, including the stress disturbance index (SDI), the principal stress magnitude disturbance index (SDIm), and the principal stress direction disturbance index (SDId). The SDI indicates the greatest stress disturbance in the surrounding rock is 4.5 m from the tunnel wall in B2 Lab. SDIm shows that the principal stress magnitude disturbance peaks at 2.5 m from the tunnel wall. SDId reveals that the largest change in principal stress direction does not necessarily occur near the tunnel wall but at a specific depth from it. The established relationship between SDI and the depth of the excavation damaged zone (EDZ) can serve as a criterion for determining the depth of the EDZ in deep hard rock engineering. Additionally, it provides a reference for future construction and support considerations.

在深层硬岩开挖过程中,应力在诱发应力控制破坏方面起着关键作用。虽然开挖引起的应力扰动对岩石破坏和隧道稳定性的影响已通过实验室试验和数值模拟进行了全面研究,但通过原位应力试验对其进行验证的工作仍未开展。本研究分析了中国锦屏地下实验室二期(CJPL-II)B2 实验室开挖过程中监测到的不同深度围岩的三维应力变化。研究深入探讨了深层硬岩的三维应力变化特征,包括应力分量和主应力。结果表明,在隧道开挖过程中,主应力的大小和方向都发生了变化。为了定量描述应力扰动程度,根据应力张量之间的距离建立了一系列应力评价指数,包括应力扰动指数(SDI)、主应力幅度扰动指数(SDIm)和主应力方向扰动指数(SDId)。SDI 表明,在 B2 实验室中,距离隧道壁 4.5 米处围岩的应力扰动最大。SDIm 表明,主应力大小扰动在距离隧道壁 2.5 米处达到峰值。SDId 显示,主应力方向的最大变化并不一定发生在隧道壁附近,而是在距离隧道壁的特定深度。SDI 与开挖破坏带(EDZ)深度之间的既定关系可作为深层硬岩工程中确定开挖破坏带深度的标准。此外,它还为未来的施工和支护考虑提供了参考。
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引用次数: 0
Ash removal from inferior coal via ammonium fluoride roasting and simultaneous yield of white carbon black 通过氟化铵焙烧从劣质煤中除灰并同时获得白碳黑
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-02-01 DOI: 10.1016/j.ijmst.2024.01.005
Xuqin Duan , Shuaiyu Lu , Yuxiao Fu , Jiazhe Zhang , Tong Liu , Jian Ma

The quality upgrading and deashing of inferior coal by chemical method still faces great challenges. The dangers of strong acid, strong alkali, waste water and exhaust gas as well as high cost limit its industrial production. This paper systematically investigates the ash reduction and desilicification of two typical inferior coal utilizing ammonium fluoride roasting method. Under the optimal conditions, for fat coal and gas coal, the deashing rates are 69.02% and 54.13%, and the desilicification rates are 92.64% and 90.27%, respectively. The molar dosage of ammonium fluoride remains consistent for both coals; however, the gas coal, characterized by a lower ash and silica content (less than half that of the fat coal), achieves optimum deashing effect at a reduced time and temperature. The majority of silicon in coal transforms into gaseous ammonium fluorosilicate, subsequently preparing nanoscale amorphous silica with a purity of 99.90% through ammonia precipitation. Most of the fluorine in deashed coal are assigned in inorganic minerals, suggesting the possibility of further fluorine and ash removal via flotation. This research provides a green and facile route to deash inferior coal and produce nano-scale white carbon black simultaneously.

用化学方法对劣质煤进行提质脱灰仍然面临巨大挑战。强酸、强碱、废水、废气的危害以及高昂的成本限制了其工业化生产。本文系统研究了利用氟化铵焙烧法对两种典型劣质煤进行降灰脱硅的过程。在最佳条件下,肥煤和气煤的脱灰率分别为 69.02% 和 54.13%,脱硅率分别为 92.64% 和 90.27%。两种煤的氟化铵摩尔用量保持一致;然而,气煤的灰分和硅含量较低(不到肥煤的一半),因此能在较短时间和较低温度下达到最佳脱灰效果。煤炭中的大部分硅转化为气态氟硅酸铵,随后通过氨沉淀制备出纯度为 99.90% 的纳米级无定形二氧化硅。脱硫煤中的大部分氟被分配在无机矿物中,这表明有可能通过浮选进一步去除氟和灰分。这项研究为劣质煤的脱灰和纳米级白炭黑的生产提供了一条绿色便捷的途径。
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引用次数: 0
Predicting impact forces on pipelines from deep-sea fluidized slides: A comprehensive review of key factors 预测深海流化滑梯对管道的冲击力:关键因素综合评述
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-02-01 DOI: 10.1016/j.ijmst.2024.02.001
Xingsen Guo , Ning Fan , Defeng Zheng , Cuiwei Fu , Hao Wu , Yanjun Zhang , Xiaolong Song , Tingkai Nian

Deep-sea pipelines play a pivotal role in seabed mineral resource development, global energy and resource supply provision, network communication, and environmental protection. However, the placement of these pipelines on the seabed surface exposes them to potential risks arising from the complex deep-sea hydrodynamic and geological environment, particularly submarine slides. Historical incidents have highlighted the substantial damage to pipelines due to slides. Specifically, deep-sea fluidized slides (in a debris/mud flow or turbidity current physical state), characterized by high speed, pose a significant threat. Accurately assessing the impact forces exerted on pipelines by fluidized submarine slides is crucial for ensuring pipeline safety. This study aimed to provide a comprehensive overview of recent advancements in understanding pipeline impact forces caused by fluidized deep-sea slides, thereby identifying key factors and corresponding mechanisms that influence pipeline impact forces. These factors include the velocity, density, and shear behavior of deep-sea fluidized slides, as well as the geometry, stiffness, self-weight, and mechanical model of pipelines. Additionally, the interface contact conditions and spatial relations were examined within the context of deep-sea slides and their interactions with pipelines. Building upon a thorough review of these achievements, future directions were proposed for assessing and characterizing the key factors affecting slide impact loading on pipelines. A comprehensive understanding of these results is essential for the sustainable development of deep-sea pipeline projects associated with seabed resource development and the implementation of disaster prevention measures.

深海管道在海底矿产资源开发、全球能源和资源供应、网络通信和环境保护方面发挥着举足轻重的作用。然而,将这些管道铺设在海床表面,使其面临复杂的深海水动力和地质环境带来的潜在风险,尤其是海底滑坡。历史事故突出表明,滑坡会对管道造成巨大损害。具体而言,深海流体滑动(处于碎屑/泥浆流或浊流物理状态)的特点是速度快,构成了重大威胁。准确评估海底流体化滑坡对管道的冲击力对于确保管道安全至关重要。本研究旨在全面概述在了解流态化深海滑坡造成的管道冲击力方面的最新进展,从而确定影响管道冲击力的关键因素和相应机制。这些因素包括深海流化滑道的速度、密度和剪切行为,以及管道的几何形状、刚度、自重和机械模型。此外,还研究了深海滑道及其与管道相互作用的界面接触条件和空间关系。在全面回顾这些成果的基础上,提出了评估和描述影响管道滑动冲击载荷的关键因素的未来方向。全面了解这些成果对于与海底资源开发相关的深海管道项目的可持续发展和灾害预防措施的实施至关重要。
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引用次数: 0
Experimental and numerical study on dynamic mechanical behaviors of shale under true triaxial compression at high strain rate 高应变率真实三轴压缩条件下页岩动态力学行为的实验和数值研究
IF 11.8 1区 工程技术 Q1 MINING & MINERAL PROCESSING Pub Date : 2024-02-01 DOI: 10.1016/j.ijmst.2023.12.006
Xiaoping Zhou , Linyuan Han , Jing Bi , Yundong Shou

High-energy gas fracturing of shale is a novel, high efficacy and eco-friendly mining technique, which is a typical dynamic perturbing behavior. To effectively extract shale gas, it is important to understand the dynamic mechanical properties of shale. Dynamic experiments on shale subjected to true triaxial compression at different strain rates are first conducted in this research. The dynamic stress-strain curves, peak strain, peak stress and failure modes of shale are investigated. The results of the study indicate that the intermediate principal stress and the minor principal stress have the significant influence on the dynamic mechanical behaviors, although this effect decreases as the strain rate increases. The characteristics of compression-shear failure primarily occur in shale subjected to triaxial compression at high strain rates, which distinguishes it from the fragmentation characteristics observed in shale under dynamic uniaxial compression. Additionally, a numerical three-dimensional Split Hopkinson Pressure Bar (3D-SHPB), which is established by coupling PFC3D and FLAC3D methods, is validated to replicate the laboratory characteristics of shale. The dynamic mechanical characteristics of shale subjected to different confining stresses are systematically investigated by the coupling PFC3D and FLAC3D method. The numerical results are in good agreement with the experimental data.

页岩高能气体压裂是一种新型、高效、环保的开采技术,是一种典型的动态扰动行为。要有效开采页岩气,了解页岩的动态力学特性非常重要。本研究首先对页岩进行了不同应变速率下的真三轴压缩动态实验。研究了页岩的动态应力-应变曲线、峰值应变、峰值应力和破坏模式。研究结果表明,中间主应力和次主应力对动态力学行为有显著影响,但这种影响随着应变速率的增加而减小。压缩-剪切破坏的特征主要发生在高应变速率下受到三轴压缩的页岩中,这区别于在动态单轴压缩下观察到的页岩破碎特征。此外,通过耦合 PFC3D 和 FLAC3D 方法建立的数值三维分裂霍普金森压力棒(3D-SHPB)得到了验证,以复制页岩的实验室特性。通过耦合 PFC3D 和 FLAC3D 方法,系统地研究了页岩在不同约束应力下的动态力学特性。数值结果与实验数据十分吻合。
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引用次数: 0
期刊
International Journal of Mining Science and Technology
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