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Investigation of NS-single-point laser ablation of bronze under different incidence angles and pulses 不同入射角和脉冲下青铜的 NS 单点激光烧蚀研究
IF 2.1 4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001146
Esmaeil Ghadiri Zahrani, Bahman Azarhoushang
A fundamental understanding of ablation in different incidence angles is indispensable to expand the result to volume ablation where nonperpendicular irradiation exists. So far, no study with this orientation has been conducted in the category of volume laser machining. In this study, a nanosecond laser with different fluencies was utilized for single-point ablation experiments. The effect of incidence angles of 0°, 30°, and 60° on the ablation depth and the crater geometry was evaluated. Different laser pulse numbers are also considered. The results show that the ablation depth for 0° and 30° angles is almost in the same range for the initial pulses, but afterward, the ablation depth for the incidence 30° drops considerably. As the number of incident pulses increases, the ablation depth first develops approximately linearly and then grows exponentially. By changing the incident from 0° to 60°, the affecting area changes as well. The affecting area could be categorized into two distinct areas: (1) ablation area (A.A) where the crater ablation depth rapidly increases for the first 20 pulses and then, as more incident pulses arrive, it does not grow anymore and reaches a plateau due to the increase in the ablation depth. The second area (2) is the heat-affected area (H.A.A) of the crater where no further ablation occurs, but due to heat accumulation, it becomes constantly bigger when more incident pulses strike the crater. This heat-affected area tends to stay almost constant for the first incident pulses (up to 10) and, after a sharp increase, tends to enlarge steadily as the number of incident pulses rises to 70.
要将这一成果推广到非垂直照射的体烧蚀领域,就必须从根本上了解不同入射角的烧蚀情况。迄今为止,在体积激光加工领域还没有进行过这种方向的研究。在这项研究中,使用了不同通量的纳秒激光进行单点烧蚀实验。评估了 0°、30° 和 60°入射角对烧蚀深度和凹坑几何形状的影响。还考虑了不同的激光脉冲数。结果表明,0° 和 30° 角的烧蚀深度在初始脉冲时几乎处于相同的范围内,但之后,入射角为 30° 的烧蚀深度大幅下降。随着入射脉冲数的增加,烧蚀深度先是近似线性增长,然后呈指数增长。将入射角度从 0° 改为 60°,影响区域也会发生变化。影响区域可分为两个不同的区域:(1) 烧蚀区域 (A.A),在最初的 20 个脉冲中,陨石坑的烧蚀深度迅速增加,然后随着更多入射脉冲的到来,烧蚀深度不再增加,并由于烧蚀深度的增加而达到一个高点。第二个区域(2)是陨石坑的热影响区域(H.A.A),在这里不会发生进一步的烧蚀,但由于热量积累,当更多入射脉冲撞击陨石坑时,该区域会不断变大。在最初的入射脉冲(最多 10 个)中,热影响区域几乎保持不变,在急剧增加之后,随着入射脉冲数增加到 70 个,热影响区域逐渐扩大。
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引用次数: 0
Cutting thick aluminum plates using laser fusion cutting enhanced by dynamic beam shaping 利用动态光束整形增强的激光熔融切割技术切割厚铝板
IF 2.1 4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001095
M. Kardan, N. Levichev, Sylvie Castagne, Joost R. Duflou
Cutting thick plates is affected not only by the laser power but also by the cut kerf width and the melt flow dynamics that determine the ejection of the molten material. Employing the same laser beam intensity distribution for various thicknesses is the limiting factor when cutting thicker plates. This paper investigates fiber laser fusion cutting of 25 mm thick aluminum with dynamic beam shaping (DBS). While both static and longitudinal dynamic intensity distributions fail to cut this thickness with a 4 kW laser power, a cut through is achieved using annular and elliptical intensity distributions. However, an improvement of 45% in cutting speed can be achieved using an elliptical intensity distribution compared to an annular one. In order to understand the effect of the beam shape, an infrared thermal camera is used to study lateral heat propagation when using different process parameters. Moreover, to analyze the melt flow when changing the DBS frequency, high-speed imaging is utilized to observe the molten material inside the cut kerf. Finally, the cut edge quality is investigated for different cutting conditions.
切割厚板不仅受到激光功率的影响,还受到切割切口宽度和熔融材料喷射的熔流动力学的影响。对不同厚度的板材采用相同的激光束强度分布是切割较厚板材时的限制因素。本文研究了使用动态光束整形(DBS)对 25 毫米厚的铝材进行光纤激光熔融切割。在 4 kW 激光功率下,静态和纵向动态光束强度分布都无法切割这一厚度的板材,而使用环形和椭圆形光束强度分布则可以实现切割。不过,与环形强度分布相比,使用椭圆形强度分布可将切割速度提高 45%。为了了解光束形状的影响,使用了红外热像仪来研究使用不同工艺参数时的横向热传播。此外,为了分析改变 DBS 频率时的熔体流动情况,还利用高速成像技术观察切割切口内的熔融材料。最后,研究了不同切割条件下的切割边缘质量。
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引用次数: 0
Parametric investigation and optimization in laser based directed energy deposition of tungsten carbide-cobalt 激光定向能沉积碳化钨-钴的参数研究与优化
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001179
Ankit Shrivastava, Anirban Changdar, Abhijit Datta, Samik Dutta, Shitanshu Shekhar Chakraborty
Cemented carbide (WC-Co), the widely used tool-die material, is difficult to be machined by conventional and nonconventional techniques. This inspired exploring additive manufacturing (AM) of this material. However, porosity, brittleness due to cobalt depletion, etc. have been reported in the literature with rare success. For the AM of WC-Co, the current work focuses on directed energy deposition, which can be implemented with existing laser cutting-welding workstations, with modifications. To ensure the retention of cobalt even after inevitable vaporization of some of its initial content during deposition, 20 wt. % of Co was mixed with WC powder by low-energy ball milling. Laser power, scan speed, and powder flow rate were varied following a full-factorial design of experiments. The analysis of variance revealed that the experimental model and most of the parameters were significant. Only the laser power came out to be insignificant for the contact angle. The track height and width increased with the laser power and reduced with the scan speed. The contact angle increased with the scan speed and reduced with the powder flow rate. Cross sections of the deposited track showed no pores or cracks. Multiobjective optimization with gray relational analysis was conducted to get the parameter combination giving high values of the contact angle, track height, and width simultaneously. The optimum parameter combination, thus, obtained is 700 W laser power, 5 mm/s scan speed, and 5 g/min powder flow rate. This yielded 305 ± 40 μm track height, 2132 ± 33 μm width, and 152° ± 2° contact angle.
硬质合金(WC-Co)是一种常规和非常规工艺都难以加工的广泛应用的模具材料。这激发了对这种材料的增材制造(AM)的探索。然而,由于钴耗尽导致的孔隙度、脆性等在文献中已经报道过,但很少成功。对于WC-Co的增材制造,目前的工作重点是定向能沉积,可以在现有的激光切割焊接工作站上进行修改。为了确保即使在沉积过程中不可避免地汽化了一些钴的初始含量后仍能保留钴,通过低能球磨将20wt . %的Co与WC粉末混合。激光功率、扫描速度和粉末流速随实验全因子设计而变化。方差分析表明,实验模型和大部分参数均显著。只有激光功率对接触角的影响不显著。轨迹高度和宽度随激光功率的增大而增大,随扫描速度的增大而减小。接触角随扫描速度的增加而增大,随粉末流量的增加而减小。沉积轨迹的横截面未见孔隙和裂纹。采用灰色关联分析法进行多目标优化,得到接触角、轨迹高度和轨迹宽度同时高值的参数组合。因此,得到的最佳参数组合为700 W激光功率,5 mm/s扫描速度,5 g/min粉末流速。结果显示,履带高度为305±40 μm,宽度为2132±33 μm,接触角为152°±2°。
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引用次数: 0
Fatigue strength and impact toughness dependence of powder bed fusion with laser beam-manufactured 316L stainless steel on orientation and layer thickness 激光加工316L不锈钢粉末床熔接疲劳强度和冲击韧性与取向和层厚的关系
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001113
Timo Rautio, Matias Jaskari, Markku Keskitalo, Joonas Päkkilä, Antti Järvenpää
Additive manufacturing is an enticing way of producing complex geometries and optimized parts for special applications. Even though the achievable static properties for the printed material are usually good when compared to wrought materials, in many cases dynamic properties are known to be much worse. Often, the quality is sacrificed in respect of printing speed. Furthermore, printed materials have usually anisotropic behavior, caused by the remelting and fast cooling of each deposited layer. This means that the mechanical properties need to be measured in several directions in respect of the printing direction for attaining a more holistic approach to the achieved static and dynamic behavior. As a demonstration, this study focuses on determining the properties of 316L stainless steel-manufactured with laser powder bed fusion. A comprehensive set of samples for various testing methods were manufactured to investigate the effect of the layer thickness and printing orientation on the microstructure, mechanical properties, impact strength, and fatigue life. Fatigue performance of the material was evaluated in both axial and flexural bending comparing as-built and polished surface conditions. Bending fatigue testing revealed that a fatigue limit of 100 MPa at best can be achieved with the as-built surface quality, but with a polished surface and lower layer thickness, it could be doubled. Impact toughness and mechanical strength of the material are heavily dependent on the layer thickness, and while the best results were obtained with the lower layer thickness, the printing orientation can have a detrimental effect on it.
增材制造是一种生产复杂几何形状和特殊应用优化零件的诱人方法。尽管与变形材料相比,印刷材料的可实现的静态性能通常是好的,但在许多情况下,动态性能要差得多。通常情况下,质量是在印刷速度方面牺牲的。此外,印刷材料通常具有各向异性行为,这是由每层沉积的重熔和快速冷却引起的。这意味着机械性能需要在印刷方向的几个方向上进行测量,以获得更全面的方法来获得静态和动态行为。作为示范,本研究的重点是确定316L不锈钢的性能与激光粉末床熔化。制作了一套全面的样品,用于各种测试方法,以研究层厚度和印刷方向对微观结构,力学性能,冲击强度和疲劳寿命的影响。材料的疲劳性能在轴向和弯曲弯曲两方面进行了评估,比较了建成和抛光的表面条件。弯曲疲劳试验表明,在原有表面质量条件下,弯曲疲劳极限最高可达到100 MPa,但在抛光表面和较低的层厚条件下,弯曲疲劳极限可提高一倍。材料的冲击韧性和机械强度很大程度上取决于层厚,而层厚越低,效果越好,但印刷方向对其有不利影响。
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引用次数: 0
Laser cladding: A high-speed-imaging examination of powder catchment efficiency as a function of the melt pool geometry and its position under the powder stream 激光熔覆:作为熔池几何形状及其在粉末流下位置的函数的粉末收集效率的高速成像检查
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001199
Daniel Koti, John Powell, Himani Naesstroem, Chiara Spaccapaniccia, K. T. Voisey
This paper provides quantitative information about the paths taken by blown powder particles during laser cladding. A proportion of the powder is “wasted” by bouncing off the solid areas surrounding the melt pool. This wastage reduces the productivity and profitability of the process. In this paper, specially developed software was used to analyze high-speed imaging videos of the cladding process, to monitor the directions of powder particle flight toward and away from the melt pool area. This information has been correlated to the geometry and position of the melt pool zone for three different cladding techniques: single track cladding (A tracks), standard overlapping track cladding (AAA cladding), and a recently developed technique called ABA cladding. The results show that the melt pool geometry, and particularly the overlap between the melt pool and the incoming powder stream, has a strong influence on powder catchment efficiency. ABA cladding was found to have considerably better powder catchment efficiency than standard AAA cladding and this improvement can be explained by consideration of the geometries and positions of the melt pools and surrounding solid material in each case. As powder costs are an important factor in industrial laser cladding, the adaption of the ABA technique, and/or control of pool/powder stream overlap (e.g., by making the powder stream not coaxial with the laser beam), could improve the profitability of the process.
本文提供了激光熔覆过程中吹散粉末颗粒路径的定量信息。一部分粉末在熔池周围的固体区域反弹而“浪费”了。这种浪费降低了流程的生产率和盈利能力。本文采用专门开发的软件对熔覆过程的高速成像视频进行分析,监测粉末颗粒向熔池区域和远离熔池区域的飞行方向。这些信息与三种不同覆层技术的熔池区域的几何形状和位置相关:单轨道覆层(A轨道),标准重叠轨道覆层(AAA覆层)和最近开发的称为ABA覆层的技术。结果表明,熔池的几何形状,特别是熔池与入射粉末流之间的重叠,对粉末集集效率有很大影响。发现ABA包层比标准AAA包层具有更好的粉末集集效率,这种改进可以通过考虑每种情况下熔池和周围固体材料的几何形状和位置来解释。由于粉末成本是工业激光熔覆的一个重要因素,采用ABA技术和/或控制熔池/粉末流重叠(例如,通过使粉末流与激光束不同轴)可以提高工艺的盈利能力。
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引用次数: 0
Fatigue behavior of 8 mm thick steel butt joints performed with hybrid laser arc welding 混合激光弧焊8mm厚钢对接接头的疲劳行为
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001084
J. M. Sánchez-Amaya, A. Gómez-Parra, C. Churiaque, S. R. Fernández-Vidal, A. J. Gámez
In the present research, the hybrid laser arc welding (HLAW) process has been applied to join 8 mm thick structural S355J2N steel under 1G configuration. Welding tests were performed at the Laser Welding Advanced Center available at the University of Cadiz, Spain. Different experimental welding parameters were fitted to obtain sound butt welds. The welds were subjected to different quality control tests, including visual inspection, metallographic characterization, microhardness measurements, and tensile and fatigue tests. The HLAW tests were performed at higher welding rates in 1G configuration than previously reported for 8 mm thick steels. Complete penetration was achieved in all welds, presenting suitable geometries without defects such as cracks, root humps, or porosities. Microhardness values measured at different welding zones were always below 350 HV. All welds broke at the base metal in the tensile tests. The present contribution reports novel fatigue results for these butt hybrid welds. The samples welded at the highest welding rate (2.5 m/min) were the ones providing the best fatigue response, due to the lower heat input applied under this condition.
在本研究中,采用混合激光弧焊(HLAW)工艺对8mm厚的S355J2N结构钢在1G组态下进行了焊接。焊接试验在西班牙加的斯大学的激光焊接先进中心进行。拟合了不同的实验焊接参数,得到了声音良好的对接焊缝。焊缝进行了不同的质量控制测试,包括目视检查、金相表征、显微硬度测量、拉伸和疲劳测试。HLAW试验在1G配置下进行,比以前报道的8毫米厚钢的焊接速率更高。所有焊缝都实现了完全渗透,呈现出合适的几何形状,没有裂纹、根峰或孔隙等缺陷。不同焊接区测得的显微硬度值均低于350hv。在拉伸试验中,所有焊缝都在母材处断裂。本文报道了这些对接混合焊缝的新疲劳结果。在最高焊接速率(2.5 m/min)下焊接的样品提供了最好的疲劳响应,因为在此条件下施加的热量较低。
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引用次数: 0
New possibilities for laser welding of highly loaded transmission components by strategic use of simulation methods 通过战略性地使用仿真方法,为高负载传输部件的激光焊接提供了新的可能性
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-11-01 DOI: 10.2351/7.0001189
Markus Wagner, Fabian Günther, Rishabh Rajesh Rao, Uwe Stamm, Dirk Dittrich, Axel Jahn
Laser welding in transmission manufacturing opens up completely new kinds of product solutions with excellent properties in terms of wear, corrosion resistance, and service life. Current welding designs are characterized in particular by difficult-to-weld material combinations (e.g., steel versus cast iron) and a high component stiffness, which is correlated with high residual welding stresses. The major challenge for these mass-produced components remains both their crack-free weldability and their complex cyclic load capacity [U. Stamm, “Rissfreies Laserstrahlschweißen von Mischverbindungen aus Gusseisen und Einsatzstahl, Jahresbericht Fraunhofer IWS 2006” (2006); X. Shu, “Untersuchungen zum Laserstrahlschweißen von Werkstoffkombinationen aus Gußeisen und Stahl,” Dissertation, Shaker, Band 4/94 (1994), ISBN: 3-8265-0098-9; G. Göbel, “Erweiterung der Prozessgrenzen beim Laserstrahlschweißen heißrissgefährdeter Werkstoffe,” Dissertation, Fraunhofer-IRB-Verlag (2007), ISBN: 978-3-8167-7671-0]. Therefore, this contribution presents practical solutions for weld-compatible joint constructions and the reduction of residual stresses on the basis of a representative transmission design. Specifically, a systematic study is being conducted to understand and qualitatively evaluate effective methods for reducing residual weld stresses in circumferential welds. The recommendations developed as part of this study take particular account of the influence of process modifications, material conditions, and geometric aspects on weldability and component distortion. Here, structural welding simulations are performed and verified by experimental welding trials, including metallographic examinations. To ensure the required component fatigue strength, a practical concept for determining Wöhler curves is presented, which is based on structural mechanical simulations and multiaxial fatigue strength tests on simplified test specimens. The adaptations developed in this way facilitate the production of difficult-to-weld and highly stressed transmission components. In particular, time-consuming and cost-intensive iterations of laser welding tests can be significantly reduced or even eliminated [Brenner et al., “Neuere Ergebnisse zum Schweißen von Eisenbasiswerkstoffen mit Faserlasern, 5. Laser-Anwenderforum,” Strahltechnik Band 28 (2006), pp. 139–148, ISBN: 3-933762-18-9, S]. Furthermore, the systematic investigations provide effective recommendations for phenomenological understanding and solving typical welding challenges in practice [J. Standfuß, “Ganzheitliche innovative fügetechnische Konzepte am Beispiel des PKW-Antriebsstranges,” Fraunhofer Verlag (2010), ISBN: 978-3-8396-0125-9]. This applies, in particular, to load-transmitting components in the fields of e-mobility, aerospace, and industrial engineering [Wagner et al., “Entwickeln und Auslegen von lasergeschweißten Getriebe-komponenten für die Luftfahrt,” DVS-Berichte Band 365 (2020), pp. 62–69, ISBN: 978-3-96144
激光焊接在传动制造中开辟了全新的产品解决方案,在耐磨、耐腐蚀和使用寿命方面具有优异的性能。当前的焊接设计尤其以难以焊接的材料组合(例如,钢与铸铁)和高部件刚度为特征,这与高残余焊接应力相关。这些量产部件面临的主要挑战是其无裂纹焊接性和复杂的循环载荷能力。斯塔姆,“激光辐射与激光辐射”,德国劳恩霍夫学会(2006);舒欣,“Untersuchungen zum Laserstrahlschweißen von Werkstoffkombinationen aus Gußeisen und Stahl”,博士论文,振动,第4/94期(1994),ISBN: 3-8265-0098-9;G. Göbel,“Erweiterung der Prozessgrenzen beim Laserstrahlschweißen heißrissgefährdeter Werkstoffe”,Dissertation, Fraunhofer-IRB-Verlag (2007), ISBN: 978-3-8167-7671-0]。因此,这一贡献为焊接兼容接头结构和减少残余应力提供了实用的解决方案,并以代表性传动设计为基础。具体来说,正在进行一项系统的研究,以了解和定性评估减少环向焊缝残余应力的有效方法。作为本研究的一部分,提出的建议特别考虑了工艺修改、材料条件和几何方面对可焊性和部件变形的影响。在这里,进行了结构焊接模拟,并通过实验焊接试验进行了验证,包括金相检查。为了保证构件所需的疲劳强度,提出了一种基于结构力学模拟和简化试件多轴疲劳强度试验的Wöhler曲线确定的实用概念。以这种方式开发的适应性有助于生产难以焊接和高应力的传动部件。特别是,激光焊接测试的耗时和成本密集的迭代可以大大减少甚至消除[Brenner等人,“Neuere Ergebnisse zum schweien von Eisenbasiswerkstoffen mit faserlasen, 5]。Laser-Anwenderforum, " Strahltechnik Band 28 (2006), pp. 139-148, ISBN: 3-933762-18-9, S]。此外,系统的研究为理解现象学和解决实践中的典型焊接挑战提供了有效的建议[J]。斯坦弗斯,“Ganzheitliche innovative f getechnische Konzepte am Beispiel des PKW-Antriebsstranges”,弗劳恩霍夫出版社(2010),ISBN: 978-3-8396-0125-9。这尤其适用于电动汽车、航空航天和工业工程领域的负载传输组件[Wagner等人,“Entwickeln und Auslegen von lasergeschweißten Getriebe-komponenten f r die Luftfahrt,”DVS-Berichte Band 365 (2020), pp. 62-69, ISBN: 978-3-96144-098-6]。
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引用次数: 0
Evaluation of an ultrashort pulsed laser robot system for flexible and large-area micromachining 柔性大面积微加工超短脉冲激光机器人系统评价
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-10-30 DOI: 10.2351/7.0001171
Daniel Franz, Yongting Yang, Luis Michel, Cemal Esen, Ralf Hellmann
We report for the first time on the realization, characterization and application of an ultrashort pulsed laser robot system for flexible and large-area 2D and 3D laser micromachining with 6 articulated axes. To characterize the dynamic positioning of the laser beam during and after axes movement, CMOS image sensors were integrated into the beam path. A method introduced for the alignment of the optical axes allows a reduction of the deviations in laser beam positioning to less than 141.8 ± 92.9 μm within a 110° rotation range of axis 4. In addition, a high laser beam positioning repeatability of less than 102.2 μm is demonstrated over a total period of 14 h for a movement of axis 5 within a range of 0° to 90°. Initial laser cutting, laser structuring and laser marking applications on automotive dashboards and glass substrates are presented for flexible and large area 2D and 3D manufacturing. By applying a special laser cutting strategy for processing AF 32 eco thin glass, high cutting quality is achieved with a taper of up to 96.3% without the generation of cracks, demonstrating the innovative potential of the high-precision laser robot system. Nonetheless, different identified inherent influences of each axis 1–5 during robot axis movement demand for an innovative beam stabilization concept to achieve high precision in laser beam positioning.
本文首次报道了一种用于柔性、大面积、六轴关节激光微加工的超短脉冲激光机器人系统的实现、表征和应用。为了表征激光束在轴向运动期间和运动后的动态定位,将CMOS图像传感器集成到光束路径中。介绍了一种光轴对准方法,在轴4旋转110°范围内,将激光束定位偏差减小到141.8±92.9 μm以内。此外,在0°到90°的范围内,在14 h的总周期内,5轴的运动具有小于102.2 μm的高激光束定位重复性。介绍了在汽车仪表板和玻璃基板上的初始激光切割,激光结构和激光打标应用,用于灵活和大面积的2D和3D制造。通过应用特殊的激光切割策略来加工AF 32生态薄玻璃,实现了高切割质量,锥度高达96.3%而不会产生裂纹,展示了高精度激光机器人系统的创新潜力。然而,在机器人轴线运动过程中,每个轴1-5的不同固有影响需要一个创新的光束稳定概念,以实现高精度的激光束定位。
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引用次数: 0
Influence of post-processing heat-treatment on the mechanical performance of AISI 410L stainless steel manufactured by the L-DED process 后处理热处理对L-DED工艺生产的AISI 410L不锈钢力学性能的影响
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-10-30 DOI: 10.2351/7.0001135
Jurandir Marcos Sá de Sousa, Milton Pereira, Juliane Ribeiro da Cruz, Anselmo Thiesen Júnior, Henrique Santos Ferreira, Jhonattan Gutjahr
Additively manufactured martensitic stainless steel components can combine complex geometry with superior mechanical and corrosion performance. In this work, the mechanical performance of AISI 410L processed by laser directed energy deposition (L-DED) additive manufacturing using previously optimized parameters is assessed. Microstructure, hardness, tensile strength, and Charpy impact toughness are evaluated in the as-built and heat-treated conditions. Four heat-treatment routes are investigated: (I) austenitization and water quenched, and austenitization, water quenched, and tempered at (II) 300, (III) 450, and (IV) 600 °C, followed by air cooling. The results show that, for tempering temperatures up to 450 °C, the hardness, yield strength, and ultimate tensile strength show an increasing trend when compared with the as-built condition and reference commercial standard (annealed AISI 410) because of microstructure refinement induced by recrystallization. Tempering at 600 °C, on the other hand, enhances the ductility of the specimens, accounting for an increased deformation until fracture and superior Charpy impact toughness. In summary, this work demonstrates that, for all tested conditions, the tensile strength of the AISI 410L additively manufactured by L-DED outperforms that of the standardized commercial AISI 410 martensitic stainless steel, and that post-processing heat-treatments can be used to further enhance toughness and ductility, making it even more competitive.
增材制造的马氏体不锈钢部件可以将复杂的几何形状与优异的机械和腐蚀性能结合起来。在这项工作中,利用先前优化的参数,对激光定向能沉积(L-DED)增材制造的AISI 410L的机械性能进行了评估。显微组织,硬度,抗拉强度和夏比冲击韧性在制造和热处理条件下进行评估。研究了四种热处理路线:(I)奥氏体化和水淬,以及(II) 300°C、(III) 450°C和(IV) 600°C的奥氏体化、水淬和回火,然后进行空气冷却。结果表明,当回火温度达到450℃时,由于再结晶引起的组织细化,合金的硬度、屈服强度和极限抗拉强度均较原位状态和参考商业标准(退火后的AISI 410)有所提高。另一方面,在600°C回火,提高了试样的延展性,增加了变形,直到断裂和优越的夏比冲击韧性。总之,这项工作表明,在所有测试条件下,由L-DED制造的AISI 410L添加剂的抗拉强度优于标准化的商用AISI 410马氏体不锈钢,并且后处理热处理可用于进一步提高韧性和延展性,使其更具竞争力。
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引用次数: 0
Influence of ultraviolet irradiation on the optical properties and biological activity of copper nanoparticles prepared by pulsed laser ablation 紫外光照射对脉冲激光烧蚀制备的铜纳米颗粒光学性能和生物活性的影响
4区 工程技术 Q2 Physics and Astronomy Pub Date : 2023-10-26 DOI: 10.2351/7.0001221
Khalaf Ajaj, Mushtaq Abed Al-Jubbori, Abdullah M. Ali
In this study, we synthesized colloidal copper nanoparticles (CuNPs) utilizing Q-switched Nd:YAG laser ablation on a copper plate immersed in double-distilled water at energies of 200 and 400 mJ, respectively, with 100, 200, 300, 400, and 500 pulses. The size and optical properties of nanoparticles were determined using a UV–Vis spectrophotometer, a transmission electron microscope (TEM), and a field emission scanning electron microscope (FE-SEM). The absorption spectra exhibited two surface plasmon resonance peaks (λSPR), one at 217 nm for copper oxide nanoparticles (CuONPs) and the other at 636 nm for CuNPs, with the increase in laser pulses. Consequently, the optical bandgap increased by roughly 3 eV. The TEM and FE-SEM analyses showed nearly spherical Cu nanoparticles with average diameters of 33 and 38 nm for laser energies of 200 and 400 mJ, respectively. An analysis of x-ray diffraction patterns revealed that CuONPs contained the crystallographic planes of a monoclinic and an orthorhombic crystal system. Additionally, the mean crystallite size of laser-ablated nanoparticles increased with increasing pulse energy. Furthermore, the absorption and optical bandgap of CuNPs increased slightly with an increase in ultraviolet irradiation exposure. The results of our study showed an increased inhibitory effect against both Staphylococcus aureus bacteria and Escherichia coli bacteria when CuNPs were irradiated by ultraviolet type C.
在这项研究中,我们利用调q Nd:YAG激光烧蚀在铜板上合成了胶体铜纳米粒子(CuNPs),分别在能量为200和400 mJ的双蒸发水中,脉冲分别为100、200、300、400和500。采用紫外-可见分光光度计、透射电子显微镜(TEM)和场发射扫描电子显微镜(FE-SEM)对纳米颗粒的尺寸和光学性质进行了测定。随着激光脉冲的增加,吸收光谱呈现出两个表面等离子体共振峰(λSPR),分别为氧化铜纳米粒子(CuONPs)和铜纳米粒子(CuNPs)的217 nm和636 nm。因此,光学带隙增加了大约3ev。TEM和FE-SEM分析表明,当激光能量为200和400 mJ时,Cu纳米粒子的平均直径分别为33和38 nm。x射线衍射图分析表明,CuONPs包含单斜晶系和正交晶系的晶体平面。此外,激光烧蚀纳米粒子的平均晶粒尺寸随着脉冲能量的增加而增加。此外,随着紫外照射量的增加,光子晶体的吸收和光带隙略有增加。我们的研究结果表明,在C型紫外线照射下,CuNPs对金黄色葡萄球菌和大肠杆菌的抑制作用增强。
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Journal of Laser Applications
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