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PPDiffuse: A Quantitative Prediction Tool for Diffusion of Charged Polymers in a Nanopore. PPDiffuse:一种用于纳米孔中带电聚合物扩散的定量预测工具
IF 1.3 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-06-19 eCollection Date: 2020-01-01 DOI: 10.6028/jres.125.018
David P Hoogerheide
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引用次数: 0
Improvised Long Test Lengths via Stitching Scale Bar Method: Interim Testing of Laser Trackers. 通过缝合刻度条方法改进长测试长度:激光跟踪仪的中期测试。
IF 1.3 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-05-28 eCollection Date: 2020-01-01 DOI: 10.6028/jres.125.016
Vincent D Lee, Daniel Sawyer, Bala Muralikrishnan

Performance verifications of laser tracker systems (LTSs) often rely on calibrated length artifacts that are 2.3 m in length or more, as specified in International Standards Organization (ISO) and American Society of Mechanical Engineers (ASME) standards. The 2.3 m length is chosen as the minimum length that will sufficiently expose inaccuracy in LTSs. Embodiment of these artifacts often comes in the form of scale bars, fixed monuments, or a laser rail. In National Institute of Standards and Technology (NIST) Internal Report (IR) 8016, which was published in 2014 and discusses interim testing of LTSs, it was shown that a scale bar with three nests spaced 1.15 m apart was sufficient for exposing errors in LTSs. In that case, the LTS was placed symmetrically with respect to the scale bar so that both a 2.3 m symmetrical length and a 1.15 m asymmetrical length were presented to the LTS. This paper will evaluate whether a scale bar that is only 1.15 m in length can sufficiently expose errors within the LTS when it is stitched together to create a 2.3 m long test length.

根据国际标准化组织 (ISO) 和美国机械工程师学会 (ASME) 标准的规定,激光跟踪仪系统 (LTS) 的性能验证通常依赖于长度为 2.3 米或更长的校准长度工件。2.3 米长度被选为能充分暴露 LTS 不准确性的最小长度。这些人工制品通常以刻度条、固定石碑或激光导轨的形式出现。美国国家标准与技术研究院(NIST)于 2014 年发布的《内部报告》(IR)8016 中讨论了 LTS 的临时测试,该报告显示,带有三个间距为 1.15 米的嵌套的刻度条足以暴露 LTS 中的误差。在这种情况下,LTS 相对于标尺杆对称放置,这样 LTS 就能看到 2.3 米的对称长度和 1.15 米的不对称长度。本文将评估长度仅为 1.15 米的刻度条在拼接成 2.3 米长的测试长度时,能否充分暴露 LTS 内部的误差。
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引用次数: 0
Influence of Machine Anvil Wear on Charpy Test Results 机械顶砧磨损对Charpy试验结果的影响
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-05-12 DOI: 10.6028/jres.125.015
E. Lucon, R. Santoyo
We investigated the influence of the state of wear of Charpy machine anvils on test results byperforming impact tests on NIST specimens of three energy levels with a machine equipped with new anvils (compliant with both ASTM E23 [1] and ISO 148-2 [2]) and worn anvils (anvil corner radii and distance outside ASTM tolerances, but within ISO tolerances). The results obtained, statistically analyzed, unequivocally show that worn anvils tend to increase absorbed energy at all energy levels. On the other hand, data variability does not appear to be significantly affected by anvil wear. This study represents NIST contribution to an international effort spearheaded by the Japan Iron and Steel Federation Standardization Center (Tokyo, Japan).
我们研究了Charpy机砧的磨损状态对测试结果的影响,方法是在配备新砧(符合ASTM E23[1]和ISO 148-2[2])和磨损砧(砧角半径和距离超出ASTM公差,但在ISO公差范围内)的机器上对NIST三个能级的试样进行冲击试验。所得到的结果,经统计分析,明确表明,磨损的铁砧倾向于增加所有能量水平的吸收能量。另一方面,数据变异性似乎不受铁砧磨损的显著影响。这项研究代表了NIST对由日本钢铁联合会标准化中心(东京,日本)牵头的国际努力的贡献。
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引用次数: 0
Advanced Temperature-Control Chamber for Resistance Standards 高级温控室电阻标准
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-04-10 DOI: 10.6028/jres.125.012
S. Payagala, A. Panna, A. Rigosi, D. Jarrett
Calibration services for resistance metrology have continued to advance their capabilities and establish new and improved methods for maintaining standard resistors. Despite the high quality of these methods, there still exist inherent limitations to the number of simultaneous, measurable resistors and the temperature stability of their air environment. In that context, we report progress on the design, development, and initial testing of a precise temperature-control chamber for standard resistors that can provide a constant-temperature environment with a stability of ± 6 m°C. Achieving this stability involved customizing the chamber design based on air-flow simulations. Moreover, microprocessor programming allowed the air flow to be optimized within an unsealed chamber configuration to reduce chamber temperature recovery times. Further tests were conducted to improve the stability of the control system and the efficiency of the chamber.
电阻计量的校准服务不断提高其能力,并建立了维护标准电阻器的新方法和改进方法。尽管这些方法质量很高,但同时测量的电阻器的数量及其空气环境的温度稳定性仍然存在固有的局限性。在此背景下,我们报告了用于标准电阻器的精确温度控制室的设计、开发和初始测试进展,该温度控制室可以提供稳定度为±6 m°C的恒温环境。实现这种稳定性需要基于气流模拟定制腔室设计。此外,微处理器编程允许在未密封的腔室配置内优化气流,以减少腔室温度恢复时间。进行了进一步的测试以提高控制系统的稳定性和腔室的效率。
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引用次数: 1
Microscale Mapping of Structure and Stress in Barium Titanate 钛酸钡结构和应力的微尺度制图
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-04-04 DOI: 10.6028/jres.125.013
J. A. Howell, M. Vaudin, L. Friedman, R. Cook
Cross-correlation of electron backscatter diffraction (EBSD) patterns was used to generate rotation, strain, and stress maps of single-crystal tetragonal barium titanate (BaTiO3) containing isolated, small, sub-micrometer a domains separated from a c-domain matrix by 90° domain boundaries. Spatial resolution of about 30 nm was demonstrated over 5 μm maps, with rotation and strain resolutions of approximately 10−4. The magnitudes of surface strains and, especially, rotations peaked within and adjacent to isolated domains at values of approximately 10−2, i.e., the tetragonal distortion of BaTiO3. The conjugate stresses between a domains peaked at about 1 GPa, and principal stress analysis suggested that stable microcrack formation in the c domain was possible. The results clearly demonstrate the applicability of EBSD to advanced multilayer ceramic capacitor reliability and strongly support the coupling between the electrical performance and underlying mechanical state of BaTiO3-containing devices.
电子背散射衍射(EBSD)互相关图用于生成单晶四方钛酸钡(BaTiO3)的旋转、应变和应力图,该单晶四方钛酸钡(BaTiO3)含有孤立的、小的、亚微米的a畴,与c畴矩阵以90°畴边界分隔。5 μm图的空间分辨率约为30 nm,旋转和应变分辨率约为10−4。表面应变的大小,尤其是旋转的大小在孤立畴内和邻近区域达到峰值,约为10−2,即BaTiO3的四方畸变。a域之间的共轭应力峰值约为1 GPa,主应力分析表明c域可能形成稳定的微裂纹。结果清楚地证明了EBSD对先进多层陶瓷电容器可靠性的适用性,并有力地支持了含batio3器件的电性能与底层力学状态之间的耦合。
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引用次数: 0
The Statistics of Computer Clocks and the Design of Synchronization Algorithms 计算机时钟统计与同步算法设计
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-02-25 DOI: 10.6028/jres.125.008
J. Levine
In this study, I used standard statistical tools (such as the various forms of the two-sample Allan variance) to characterize the clocks in computers, and I show how the results of this study are used to design algorithms to synchronize the computer clocks. These synchronization algorithms can be used to synchronize the time of a computer to a local reference clock or to a remote server. The algorithms by themselves are not intended to be a simple replacement for software that implements the Network Time Protocol (NTP) or any other similar application. Instead, they describe the statistical principles that should be used to design an algorithm to synchronize any computer clock by using data from any external reference received in any format. These algorithms have been used to synchronize the clocks of the computers that support the Internet Time Service operated by the National Institute of Standards and Technology (NIST), and I illustrate the performance of the algorithm with real-time data from these servers. In addition to presenting the design principles of the algorithm, I illustrate the principles with two specific examples: synchronizing a computer clock to a local reference signal, and the design of a synchronization process that is based on time-difference data received from a remote server over the public Internet. The message exchange between the local system and the remote server in this configuration is realized in NTP format, but that is not a fundamental requirement.
在本研究中,我使用标准的统计工具(如各种形式的双样本Allan方差)来表征计算机中的时钟,我展示了如何使用本研究的结果来设计算法来同步计算机时钟。这些同步算法可用于将计算机的时间同步到本地参考时钟或远程服务器。这些算法本身并不打算简单地替代实现网络时间协议(NTP)或任何其他类似应用程序的软件。相反,它们描述了应该用于设计算法的统计原理,通过使用以任何格式接收的来自任何外部参考的数据来同步任何计算机时钟。这些算法已被用于同步由美国国家标准与技术研究所(NIST)运行的支持互联网时间服务的计算机的时钟,我用来自这些服务器的实时数据说明了算法的性能。除了介绍该算法的设计原则之外,我还用两个具体的示例说明了这些原则:将计算机时钟同步到本地参考信号,以及基于通过公共Internet从远程服务器接收的时差数据的同步过程的设计。在此配置中,本地系统和远程服务器之间的消息交换以NTP格式实现,但这不是基本要求。
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引用次数: 0
So, You Want to Have a Nanofab? Shared-Use Nanofabrication and Characterization Facilities: Cost-of-Ownership, Toolset, Utilization, and Lessons Learned 那么,你想拥有一个纳米fab?共享使用纳米制造和表征设施:拥有成本,工具集,利用和经验教训
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-02-21 DOI: 10.6028/jres.125.009
J. Liddle, Jerry Bowser, B. Ilic, V. Luciani
Nanofabrication/characterization facilities enable research and development activities across a host of science and engineering disciplines. The collection of tools and supporting infrastructure necessary to construct, image, and measure micro- and nanoscale materials, devices, and systems is complex and expensive to establish, and it is costly to maintain and optimize. As a result, these facilities are typically operated in a shared-use mode. We discuss the key factors that must be considered to successfully create and sustain such facilities. These include the need for long-term vision and institutional commitment, and the hands-on involvement of managers in facility operations. We consider startup, operating, and recapitalization costs, together with algorithms for cost recovery and tool-time allocation. The acquisition of detailed and comprehensive project and tool-utilization data is essential for understanding and optimizing facility operations. Only such a data-driven decision-making approach can maximize facility impact on institutional goals. We illustrate these concepts using the National Institute of Standards and Technology (NIST) NanoFab as our test case, but the methodologies and resources presented here should be useful to all those faced with this challenging task.
纳米制造/表征设施使研究和开发活动跨越许多科学和工程学科。构建、成像和测量微纳米级材料、设备和系统所需的工具和支持基础设施的集合是复杂和昂贵的,并且维护和优化成本很高。因此,这些设施通常以共享模式运行。我们讨论了成功创建和维持此类设施必须考虑的关键因素。这包括需要长期的愿景和机构承诺,以及管理人员在设施运营中的实际参与。我们考虑了启动、运营和资本重组成本,以及成本回收和工具时间分配的算法。获取详细而全面的项目和工具使用数据对于了解和优化设施操作至关重要。只有这种数据驱动的决策方法才能最大限度地提高设施对机构目标的影响。我们使用美国国家标准与技术研究所(NIST)的NanoFab作为我们的测试用例来说明这些概念,但是这里提供的方法和资源应该对所有面临这项具有挑战性的任务的人都有用。
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引用次数: 5
Performance of Test Supermartingale Confidence Intervals for the Success Probability of Bernoulli Trials. 伯努利试验成功概率的检验上鞅置信区间的性能
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-02-05 eCollection Date: 2020-01-01 DOI: 10.6028/jres.125.003
Peter Wills, Emanuel Knill, Kevin Coakley, Yanbao Zhang

Given a composite null hypothesis 0, test supermartingales are non-negative supermartingales with respect to 0 with an initial value of 1. Large values of test supermartingales provide evidence against 0. As a result, test supermartingales are an effective tool for rejecting 0, particularly when the p-values obtained are very small and serve as certificates against the null hypothesis. Examples include the rejection of local realism as an explanation of Bell test experiments in the foundations of physics and the certification of entanglement in quantum information science. Test supermartingales have the advantage of being adaptable during an experiment and allowing for arbitrary stopping rules. By inversion of acceptance regions, they can also be used to determine confidence sets. We used an example to compare the performance of test supermartingales for computing p-values and confidence intervals to Chernoff-Hoeffding bounds and the "exact" p-value. The example is the problem of inferring the probability of success in a sequence of Bernoulli trials. There is a cost in using a technique that has no restriction on stopping rules, and, for a particular test supermartingale, our study quantifies this cost.

给定一个复合零假设H0,检验上鞅是相对于H0的非负上鞅,初始值为1。检验上鞅的大值提供了反对H0的证据。因此,检验上鞅是拒绝H0的有效工具,特别是当获得的p值非常小并作为反对原假设的证明时。例子包括拒绝局部实在论作为物理学基础中贝尔测试实验的解释,以及量子信息科学中纠缠的证明。测试超鞅具有在实验过程中适应性强和允许任意停止规则的优点。通过反演可接受区域,它们也可以用来确定置信集。我们使用了一个例子来比较检验上鞅在计算p值和置信区间时与诺夫-霍夫丁界和“精确”p值的性能。这个例子是在一系列伯努利试验中推断成功概率的问题。使用一种没有停止规则限制的技术是有成本的,对于一个特定的测试上鞅,我们的研究量化了这种成本。
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引用次数: 0
Digitizing "The NBS Tables of Chemical Thermodynamic Properties: Selected Values for Inorganic and C1 and C2 Organic Substances in SI Units" 数字化“NBS化学热力学性质表:无机物质、C1和C2有机物质的国际单位选择值”
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-02-04 DOI: 10.6028/jres.125.007
J. J. Reed
The NBS Tables of Chemical Thermodynamic Properties is a collection of thermodynamic properties, published in book form, consisting of 103 tables with 14 330 critically evaluated species. The tables were originally published as a series of NBS Technical Notes As a result of this work, the data is now available in a more accessible spreadsheet format. Enthalpy of formation, ΔfH°, Gibbs energy of formation, ΔfG°, entropy, S°, heat capacity at constant pressure, Cp°, all at 298.15 K, and the enthalpy difference, [H°(298) – H°(0)] are provided where known. Within this collection of data, there are no values given for transuranic elements, Np to Lr (Tables 77–87).
NBS化学热力学性质表是热力学性质的集合,以书籍形式出版,由103个表和14330个严格评估的物种组成。这些表格最初是作为一系列国家统计局技术说明发布的。由于这项工作,这些数据现在以更易于访问的电子表格格式提供。生成焓ΔfH°,吉布斯生成能ΔfG°,熵S°,恒压热容Cp°,均为298.15 K,以及已知的焓差[H°(298)- H°(0)]。在这个数据集合中,没有给出超铀元素的值,从Np到Lr(表77-87)。
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引用次数: 20
In Situ Thermography of the Metal Bridge Structures Fabricated for the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench 2018) 2018增材制造基准测试系列(AM-Bench 2018)金属桥梁结构的原位热成像
IF 1.5 4区 工程技术 Q3 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-01-30 DOI: 10.6028/jres.125.005
J. Heigel, B. Lane, L. Levine, T. Phan, J. Whiting
This document provides details on the files available for download in the data set “In situ thermography of the metal bridge structures fabricated for the 2018 Additive Manufacturing Benchmark Test Series (AM-Bench 2018).” The experiments were performed to support the 2018 AM-Bench1 Class 01 experiments consisting of metal three-dimensional (3D) builds. The modeling community was invited to predict the following: (1) part deflection, (2) residual elastic strains, (3) microstructure, (4) phase fractions, and (5) phase evolution. Details for these proposed challenges and the postprocess measurement results can be found at their respective links on the AM-Bench website.
本文件提供了数据集“2018年增材制造基准测试系列(AM-Bench 2018)制造的金属桥梁结构的原位热成像”中可下载文件的详细信息。这些实验是为了支持2018年AM-Bench1 01级实验,该实验由金属三维(3D)构建组成。邀请建模界预测以下内容:(1)零件挠度,(2)残余弹性应变,(3)微观结构,(4)相分数,(5)相演化。这些提议的挑战和后处理测量结果的详细信息可以在AM-Bench网站上的相应链接中找到。
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引用次数: 10
期刊
Journal of Research of the National Institute of Standards and Technology
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