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Experimental Investigation Into the Fabrication of Porous Biodegradable Fe Scaffold by Microwave Sintering of 3D Printed Green Body 微波烧结3D打印绿色体制备多孔可生物降解铁支架的实验研究
Pub Date : 2021-08-04 DOI: 10.1115/msec2021-63402
D. Mishra, P. M. Pandey
Iron has appealing biodegradable properties that makes compatible for biodegradable implant tools applications. Although, the slow corrosion rate of Fe made obsolete for biomedical applications. The incorporation of the porous structure may result in an enhanced degradation rate. The main advantage offer by the porous structure is to allow to flow the body transportation fluid through it and ease to proliferate the new tissue. Therefore, the current work focused on the development of a porous Fe structures using micro-extrusion based three-dimensional printing (ME3DP) and pressure less microwave sintering. The metallic-based polymeric ink used to fabricate the intent design structure. Subsequently, samples were heated in the microwave sintering furnace. The experimentations were done to evaluate the outcomes of different Fe concentrations (91–95 wt.%) on density and compressive yield strength of developed porous parts. Experimental observation deduced that fabricated part ≥ 94.wt.% of Fe concentration has strong bonding strength between the printed layers. Moreover, the mechanical property of 94 wt.% has found greater than 95 wt.% of Fe concentration. The scanning electron microscopic (SEM) image illustrated the presence of porous morphology into the fabricated body. Additionally, XRD (X-ray diffraction) plots exhibited the purity of sample without any contamination residue.
铁具有吸引人的可生物降解特性,使其与可生物降解植入工具的应用相兼容。尽管如此,铁的缓慢腐蚀速度使其在生物医学应用中过时了。多孔结构的掺入可以提高降解率。多孔结构提供的主要优点是允许身体运输液体通过它,并且易于新组织增殖。因此,目前的工作重点是利用基于微挤压的三维打印(ME3DP)和无压微波烧结技术开发多孔铁结构。用于制造意图设计结构的金属基聚合油墨。随后,样品在微波烧结炉中加热。研究了不同铁浓度(91 ~ 95 wt.%)对多孔件密度和抗压屈服强度的影响。实验观察推断,制件≥94.wt。%的铁浓度具有较强的印刷层之间的结合强度。此外,在94 wt.%的力学性能中发现了大于95 wt.%的铁浓度。扫描电镜(SEM)图像表明,在制备体中存在多孔形态。此外,XRD (x射线衍射)图显示样品纯度高,没有任何污染残留。
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引用次数: 1
Friction Analysis in Needle Insertion Into Soft Tissue 针刺入软组织的摩擦分析
Pub Date : 2021-08-04 DOI: 10.1115/msec2021-63715
Yingda Hu, Murong Li, Yong Lei
As one of the preoperative diagnostic methods, needle insertion is widely used for its safety and effectiveness. Recently, robotic needle insertion systems have been under active developments. Hence needle insertion experiments are essential for system verifications, in which the interactions between needle and tissue is a major focus for needle-tissue interactive models, and the friction between the needle and tissue is an important factor. In these experiments, the friction coefficient can be affected by many factors, such as insertion speed, needle-tissue deformation and contact forces. In this paper, to study and analyze the influence of various variables on friction force and friction coefficient, three variables, i.e., tissue pressure on needle, needle insertion velocity and Young’s modulus of the tissue, are systematically studied by constructing a testbed, in which the radial surface friction is converted into equivalent plane friction based on the assumption that the distribution of the normal force and friction force on the needle is uniform for the whole needle outer surface. The experimental results show that the variation range of friction coefficient is 0.122–0.341. The friction coefficient decreases with the increase of pressure and increases with the increase of velocity, while Young’s modulus have a small effect on the friction coefficient.
针刺作为术前诊断方法之一,因其安全、有效而被广泛应用。近年来,机器人插针系统得到了积极的发展。因此,插针实验对系统验证至关重要,其中针与组织的相互作用是针-组织交互模型的主要关注点,而针与组织之间的摩擦是一个重要因素。在这些实验中,摩擦系数可以受到许多因素的影响,如插入速度、针组织变形和接触力。为了研究和分析各种变量对摩擦力和摩擦系数的影响,本文通过搭建实验平台,系统研究了组织对针的压力、针的插针速度和组织的杨氏模量三个变量。其中,假设针上的法向力和摩擦力在整个针外表面的分布均匀,将径向表面摩擦转化为等效平面摩擦。试验结果表明,摩擦系数的变化范围为0.122 ~ 0.341。摩擦系数随压力的增加而减小,随速度的增加而增大,而杨氏模量对摩擦系数的影响较小。
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引用次数: 0
Ultra-broadband polarisation beam splitters and rotators based on 3D-printed waveguides 基于3D打印波导的超宽带偏振分束器和旋转器
Pub Date : 2021-07-26 DOI: 10.37188/lam.2023.022
Aleksandar Nesic, M. Blaicher, P. Marin-Palomo, Christoph Fullner, S. Randel, W. Freude, C. Koos
Multi-photon lithography has emerged as a powerful tool for photonic integration, allowing to complement planar photonic circuits by 3D-printed freeform structures such as waveguides or micro-optical elements. These structures can be fabricated with high precision on the facets of optical devices and lend themselves to highly efficient package-level chip-chip-connections in photonic assemblies. However, plain light transport and efficient coupling is far from exploiting the full geometrical design freedom that is offered by 3D laser lithography. Here, we extend the functionality of 3D-printed optical structures to manipulation of optical polarization states. We demonstrate compact ultra-broadband polarization beam splitters (PBS) that can be combined with polarization rotators (PR) and mode-field adapters into a monolithic 3D-printed structure, fabricated directly on the facets of optical devices. In a proof-of-concept experiment, we demonstrate measured polarization extinction ratios beyond 11 dB over a bandwidth of 350 nm at near-infrared (NIR) telecommunication wavelengths around 1550 nm. We demonstrate the viability of the device by receiving a 640 Gbit/s dual-polarization data signal using 16-state quadrature amplitude modulation (16QAM), without any measurable optical-signal-to-noise-ratio (OSNR) penalty compared to a commercial PBS.
多光子光刻已经成为光子集成的强大工具,允许通过3D打印的自由形式结构(如波导或微光学元件)来补充平面光子电路。这些结构可以在光学器件的小平面上高精度地制造,并有助于光子组件中高效的封装级芯片-芯片连接。然而,平面光传输和有效耦合远未利用3D激光光刻提供的完全几何设计自由度。在这里,我们将3D打印光学结构的功能扩展到光学偏振态的操作。我们展示了紧凑的超宽带偏振分束器(PBS),该分束器可以与偏振旋转器(PR)和模式场适配器组合成单片3D打印结构,直接在光学器件的小平面上制造。在概念验证实验中,我们证明了在1550 nm左右的近红外(NIR)电信波长下,在350 nm的带宽上测量到的超过11dB的偏振消光比。我们通过使用16态正交幅度调制(16QAM)接收640Gbit/s的双偏振数据信号来证明该设备的可行性,与商业PBS相比,没有任何可测量的光信噪比(OSNR)损失。
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引用次数: 2
Performance of Low-Cost 3D Printer in Medical Application 低成本3D打印机在医疗应用中的性能研究
Pub Date : 2021-07-23 DOI: 10.1115/msec2021-63208
N. A. Sukindar, Azib Azhari Awang Dahan, S. I. S. Shaharuddin, N. F. Halim
Fused Deposition Modelling (FDM) is an additive manufacturing (AM) process that produces a physical object directly from a CAD design using layer-by-layer deposition of the filament material that is extruded via a nozzle. In industry, FDM has become one of the most used AM processes for the production of low batch quantity and functional prototypes, due to its safety, efficiency, reliability, low cost, and ability to process manufacturing-grade engineering thermoplastic. Recently, the market is flooded with the availability of low-cost printers produced by numerous companies. This research aims to investigate the effect of different porosity levels on a scaffold structure produced using a low-cost 3D printer. Comparisons of these porous structures were made in terms of Von-Mises strain, total deformation, as well as compressive stress. Various porosity levels were created by varying printing parameters, including layer height, infill density, and shell thickness by slicing the initial solid CAD file using Repetier Host 3D printing software. Finite Element Analysis (FEA) simulation was then performed on the created scaffold structures by using Ansys Workbench 19.2. The simulation result indicates that the greater porosity level will result in higher total deformation of the structure. Meanwhile, the compression test shows that the minimum strength value obtained was favourable at 22 MPa and had exceeded that of the trabecular femur (15 MPa). However, its porosity level (maximum at 52%) was still below that of the minimum threshold of porosity level of 70 percent. However, the printing parameters currently used can be adjusted in the future. Therefore, it was deduced that the low-cost 3D printer offers promising potential to fabricate different porosity structures with multiple outcomes.
熔融沉积建模(FDM)是一种增材制造(AM)工艺,通过喷嘴挤压长丝材料的逐层沉积,直接从CAD设计中产生物理对象。在工业中,FDM因其安全、高效、可靠、低成本和加工制造级工程热塑性塑料的能力,已成为生产小批量和功能原型的最常用的增材制造工艺之一。最近,市场上充斥着许多公司生产的低成本打印机。本研究旨在研究不同孔隙度对使用低成本3D打印机生产的支架结构的影响。对这些多孔结构进行了Von-Mises应变、总变形和压应力的比较。通过使用Repetier Host 3D打印软件切割初始实体CAD文件,通过不同的打印参数,包括层高、填充密度和外壳厚度,可以创建不同的孔隙度。然后利用Ansys Workbench 19.2对所创建的支架结构进行有限元分析(FEA)仿真。模拟结果表明,孔隙率越大,结构总变形越大。同时,压缩试验表明,得到的最小强度值为22 MPa,超过了股骨小梁的最小强度值(15 MPa)。但其孔隙度(最高为52%)仍低于孔隙度最低阈值70%。但是,目前使用的打印参数可以在将来进行调整。因此,我们推断,低成本的3D打印机在制造不同孔隙结构和多种结果方面具有很大的潜力。
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引用次数: 0
Review of laser powder bed fusion (LPBF) fabricated Ti-6Al-4V: process, post-process treatment, microstructure, and property 激光粉末床熔合(LPBF)制备Ti-6Al-4V的研究进展:工艺、后处理、显微组织和性能
Pub Date : 2021-07-01 DOI: 10.37188/lam.2021.020
S. Cao, Y. Zou, C. V. Lim, Xinhua Wu
Laser powder bed fusion (LPBF) is a timely important additive manufacturing technique that offers many opportunities for fabricating three-dimensional complex shaped components at a high resolution with short lead times. This technique has been extensively employed in manufacturing Ti-6Al-4V parts for aerospace and biomedical applications. However, many challenges, including poor surface quality, porosity, anisotropy in microstructure and property, and difficulty in tailoring microstructure, still exist. In this paper, we review the recent progress in post-process treatment and its influence on the microstructure evolution and material performance, including tensile, fatigue, fracture toughness, creep, and corrosion properties. The contradictions in simultaneously achieving high strength/ductility and strength/fracture toughness/creep resistance have been identified. Furthermore, research gaps in understanding the effects of the emerging bi-modal microstructure on fatigue properties and fracture toughness require further investigation.
激光粉末床熔融(LPBF)是一种重要的增材制造技术,它为在短的交货时间内以高分辨率制造三维复杂形状部件提供了许多机会。该技术已广泛应用于制造用于航空航天和生物医学应用的Ti-6Al-4V部件。但仍存在许多挑战,包括表面质量差、孔隙度、微观结构和性能各向异性、微观结构定制困难等。本文综述了后处理技术的最新进展,以及后处理对材料显微组织演变和材料性能的影响,包括拉伸、疲劳、断裂韧性、蠕变和腐蚀性能。同时实现高强度/延展性和强度/断裂韧性/抗蠕变的矛盾已经被确定。此外,在理解新出现的双峰组织对疲劳性能和断裂韧性的影响方面的研究空白需要进一步研究。
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引用次数: 56
Prediction of Melt-Pool Characteristics in SLM Process for Ti6Al4V Using a Semi-Analytical Model 用半解析模型预测Ti6Al4V合金SLM过程熔池特性
Pub Date : 2021-06-21 DOI: 10.1115/msec2021-63751
Shubhra Kamal Nandi, Rakesh Kumar, Anubhav Anubhav, Anupam Agrawal
Selective Laser Melting (SLM) is a powder-based layer-by-layer manufacturing technique to produce metallic customized shape components. The exceptionally high thermal gradient induces residual stress and distorts the part geometry affecting the yield quality. Computational models are instrumental in optimizing the process controls to fabricate high-quality components, and hence several such methods have been explored to simulate the thermal behavior of the process and the heat transfer in the melt-pool. Most of the practiced techniques are computationally expensive, making it infeasible to perform a parametric study. Based on closed-form exact heat conduction solution and Finite Volume Method (FVM), a pseudo-analytical thermal modeling approach has been employed to estimate the melt-pool characteristics and temperature distribution of the SLM process. A moving volumetric Gaussian heat source laser model and Green’s function have been adopted to model the heat input by conduction. The heat loss by conduction and convection has been calculated by implementing Finite Volume discretized equations on a 2-dimensional thin-walled domain with appropriate part boundary conditions. Additionally, the Alternating Direction Implicit iterative technique has been implemented for the fast convergence of the simulation. The model is used to demonstrate the influence of the process parameters and non-linear material phase change for a single-line single layer and multilayer part fabrication. The computed melt-pool dimensions and temperature distribution for varying laser-power, scanning velocity, and layer thickness for Ti6Al4V are validated with the experimental data from the literature with fair agreements.
选择性激光熔化(SLM)是一种基于粉末的逐层制造技术,用于生产金属定制形状部件。异常高的热梯度会引起残余应力并扭曲零件几何形状,影响产量质量。计算模型有助于优化过程控制,以制造高质量的部件,因此已经探索了几种这样的方法来模拟过程的热行为和熔池中的传热。大多数实践的技术在计算上是昂贵的,使得进行参数化研究是不可行的。基于闭式精确热传导解和有限体积法(FVM),采用拟解析热建模方法估计了SLM过程的熔池特性和温度分布。采用运动体积高斯热源激光模型和格林函数来模拟热传导输入。在适当的局部边界条件下,采用有限体积离散方程计算了二维薄壁区域的传导和对流热损失。此外,还采用交替方向隐式迭代技术,使仿真快速收敛。利用该模型验证了工艺参数和非线性材料相变对单线单层和多层零件加工的影响。计算得到的Ti6Al4V熔池尺寸和温度分布随激光功率、扫描速度和层厚的变化而变化,并与文献中的实验数据进行了比较一致的验证。
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引用次数: 0
Time Domain Study on the Construction Mechanism of Milling Stability Lobe Diagrams With Multiple Modes 多模态铣削稳定波瓣图构造机理的时域研究
Pub Date : 2021-06-21 DOI: 10.1115/msec2021-60227
Weitao Li, Liping Wang, Guang Yu
The stability lobe diagram (SLD) is an important expression way of milling stability prediction result. The SLD obtained by only selecting the most flexible mode fails to predict the chatter if the milling process is dominated by multiple modes. To reveal the relationship between the SLD with multiple modes and the SLDs corresponding to each single mode, this paper studies the construction mechanism of the SLD with multiple modes by using the time domain method. First, the milling dynamic model of the tool with multiple modes is established. Then, the numerical method based on the Newton-Cotes rules is used to solve the milling dynamic model with multiple modes whose solution is in the form of the SLD. It shows that the SLD with multiple modes can be approximated by using the lowest envelope of the SLDs corresponding to each single mode. Finally, two study cases are adopted to verify the construction mechanism of the SLD with multiple modes. To verify the correctness of the SLD with multiple modes, a series of milling tests are carried out. The experimental results agree with the simulation results, which means the proposed time domain method can reveal the construction mechanism of the SLD with multiple modes.
稳定性叶瓣图(SLD)是铣削稳定性预测结果的重要表达方式。当铣削过程由多种模态主导时,仅选择最灵活模态获得的SLD无法预测颤振。为了揭示多模态SLD与各单模态对应的SLD之间的关系,本文采用时域方法研究了多模态SLD的构建机理。首先,建立了刀具多模态的铣削动力学模型。然后,采用基于Newton-Cotes规则的数值方法对多模态铣削动力学模型进行求解,该模型的解为SLD形式。结果表明,多模SLD可以用对应于每个单模SLD的最低包络线来近似。最后,通过两个研究案例验证了多模式SLD的构建机制。为了验证多模态SLD的正确性,进行了一系列铣削试验。实验结果与仿真结果吻合,表明所提出的时域方法能够揭示多模态SLD的构建机理。
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引用次数: 4
Laser Micro Machining Using a Photonic Nanojet in Water Medium 水介质中光子纳米射流的激光微加工
Pub Date : 2021-06-21 DOI: 10.1115/msec2021-60045
T. Uenohara, R. Rahman, Y. Mizutani, Y. Takaya
A photonic nanojet (PNJ) is a fine and high intensity light beam that is generated from a dielectric microsphere irradiated by a laser. A PNJ has a smaller beam diameter than the wavelength of the incident laser and can propagate for longer than 1 μm with high intensity and minimal divergence. In other words, a PNJ has a long depth of focus. Due to its outstanding optical properties, a PNJ is suitable for laser micro machining to create sub-micrometer scale structures. Depth of focus of a PNJ generated in water is longer than in air. In this paper, we experimentally investigated machining characteristics of laser micro machining using a PNJ in water medium. First, electromagnetic simulation was conducted to know the intensity distribution of PNJ in water medium. The simulation demonstrated that PNJ in water mdium has beam diameter of sub-micrometer scale and micrometer scale depth of focus. Next, machining experiments were also conducted on a silicon substrate. A femtosecond laser was used as the machining laser. By controlling the microsphere position, the PNJ position can be controlled in the propagation direction. Sub-micrometer scale hole diameters were obtained even when the PNJ position in the propagation direction was changed by 3 μm. In conclusion, the long depth of focus of a photonic nanojet in water medium enable to create sub-micrometer scale structures.
光子纳米射流(PNJ)是由介质微球经激光照射后产生的一种精细的高强度光束。PNJ的光束直径小于入射激光的波长,传播长度大于1 μm,具有高强度和最小发散。换句话说,PNJ具有较长的聚焦深度。由于其优异的光学性能,PNJ适用于激光微加工,以创建亚微米尺度的结构。在水中产生的PNJ焦深比在空气中产生的焦深长。本文通过实验研究了激光微加工在水介质中的加工特性。首先进行电磁模拟,了解PNJ在水介质中的强度分布。模拟结果表明,水介质中的PNJ具有亚微米尺度的光束直径和微米尺度的聚焦深度。然后,在硅衬底上进行了加工实验。采用飞秒激光作为加工激光。通过控制微球的位置,可以控制PNJ在传播方向上的位置。即使PNJ在传播方向上的位置改变3 μm,也可以获得亚微米尺度的孔径。综上所述,光子纳米射流在水介质中的长聚焦深度可以产生亚微米尺度的结构。
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引用次数: 0
Material Properties of Discarded Textiles for Manufacturing Feedstocks 制造原料用废弃纺织品的材料特性
Pub Date : 2021-06-21 DOI: 10.1115/msec2021-63645
Asad Bashir, Abigail R. Clarke-Sather, Tyler M. Poggogiale, Christopher L. Meehan
Presently, many textiles are discarded, in a condition that would allow a significant percentage of them to be able to be completely reused or recycled. Recent consumption practices embodied by “fast fashion”, fast purchasing, and fast disposal of out of style clothing has increased the volume of discarded clothing, as the repurposing and/or recycling of discarded textile materials has not increased at a proportional rate. Consequently, discarded clothing may have nearly no wear and tear or extensive use before consumers choose to dispose of these textiles. Increasing the recovery of textiles from municipal solid waste streams involves understanding the material properties that discarded textiles possess. Measuring the material properties available from discarded textiles will allow for understanding whether these textiles can be reused. At the same time as disposal of textiles has increased, geotextile purchase and use has been increasing rapidly. In the current study, tensile strength (break force) and permittivity of discarded clothing samples made of cotton, polyester, and cotton-polyester blends were measured and compared with material properties that are commonly specified for geotextile applications. Average break force values measured for discarded cotton and polyester and average permittivity values measured for 50%/50% cotton-polyester blends and polyester are higher than what is commonly recommended for common geotextile applications. Polyester materials showed promise for drainage and erosion control applications that would be commonly serviced by geotextiles, as polyester samples yielded average break force and permittivity values are above typically recommended geotextile minimum values for these applications.
目前,许多纺织品被丢弃,在这种情况下,它们中的很大一部分能够完全重复使用或回收。最近以“快时尚”、快速购买和快速处理过时服装为代表的消费行为增加了废弃服装的数量,因为废弃纺织材料的再利用和/或回收并没有按比例增加。因此,在消费者选择处理这些纺织品之前,被丢弃的衣服可能几乎没有磨损或广泛使用。从城市固体废物流中增加纺织品的回收涉及了解废弃纺织品所具有的材料特性。测量废弃纺织品的材料性能将有助于了解这些纺织品是否可以重复使用。在纺织品处理量增加的同时,土工布的购买量和使用量也在迅速增加。在目前的研究中,测量了棉、聚酯和棉-聚酯混纺制成的废弃衣服样品的拉伸强度(断裂力)和介电常数,并将其与土工布应用中通常指定的材料特性进行了比较。废弃棉和聚酯的平均断裂力值以及50%/50%棉-聚酯混纺和聚酯的平均介电常数值均高于普通土工织物应用的通常推荐值。聚酯材料在通常由土工布提供的排水和侵蚀控制应用中表现出了希望,因为聚酯样品产生的平均断裂力和介电常数值高于这些应用中通常推荐的土工布最小值。
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引用次数: 0
Anisotropic Cutting Force Characteristics in Milling of Maraging Steel Processed Through Selective Laser Melting 选择性激光熔化马氏体时效钢铣削的各向异性切削力特性
Pub Date : 2021-06-21 DOI: 10.1115/msec2021-63704
Shoichi Tamura, T. Matsumura, A. Ezura, K. Mori
Additive manufacturing process of maraging steel has been studied for high value parts in aerospace and automotive industries. The hybrid additive / subtractive manufacturing is effective to achieve tight tolerances and surface finishes. The additive process induces anisotropic mechanical properties of maraging steel, which depends on the laser scanning direction. Because anisotropy in the workpiece material has an influence on the cutting process, the surface finish and the dimension accuracy change according to the direction of the cutter feed with respect to the laser scanning direction. Therefore, the cutting parameters should be determined to control the cutting force considering material anisotropy. The paper discusses the cutting force in milling of maraging steel stacked with selective laser melting, as an additive manufacturing process. Anisotropic effect on the cutting forces is proved with the changing rate of the cutting force in milling of the workpieces stacked by repeating laser scanning at 0/90 degrees and 45/−45 degrees. The cutting forces, then, are analyzed in the chip flow models with piling up of orthogonal cuttings. The force model associates anisotropy with the shear stress on the shear plane. The changes in the cutting forces with the feed direction are discussed in the cutting tests and analysis.
研究了马氏体时效钢的增材制造工艺,用于航空航天和汽车工业的高价值零件。混合增材/减材制造可以有效地实现严格的公差和表面光洁度。添加工艺诱发马氏体时效钢的各向异性力学性能,这种各向异性力学性能与激光扫描方向有关。由于工件材料的各向异性对切割过程有影响,表面光洁度和尺寸精度随刀具进给方向相对于激光扫描方向的变化而变化。因此,应考虑材料的各向异性,确定切削参数以控制切削力。本文讨论了选择性激光熔化堆垛马氏体时效钢增材制造工艺的切削力。通过对0/90度和45/−45度叠置工件的重复激光扫描铣削过程中切削力的变化率,证明了各向异性对切削力的影响。然后,在正交切屑堆积的切屑流模型中对切削力进行了分析。力模型将各向异性与剪切面上的剪应力联系起来。在切削试验和分析中,讨论了切削力随进给方向的变化规律。
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引用次数: 6
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光:先进制造(英文)
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