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Heterogeneous fracture toughness of human cortical bone tissue 人皮质骨组织的非均匀断裂韧性
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-24 DOI: 10.1007/s10704-024-00836-w
Maxime Levy, Zohar Yosibash

CT-based finite element analysis (FEA) of human bones helps estimate fracture risk in clinical practice by linking bone ash density ((rho _{ash})) to mechanical parameters. However, phase field models for fracture prediction require the heterogeneous fracture toughness (G_{Ic}), which can be derived from the critical stress intensity factor (K_{Ic}), determined through various experimental methods. Due to a lack of standards for determining cortical bone’s (K_{Ic}), an experimental campaign is presented using 53 cortical specimens from two fresh frozen femurs to investigate whether a correlation exists between (K_{Ic}) and (rho _{ash}). We investigated various experimental techniques for correlating (K_{Ic}) with (rho _{ash}). We conducted FEAs employing the phase field method (PFM) to determine the most suitable correlation among the five possible ones stemming from the experimental methods. The ASTM standard using displacement at force application point was found to be the recommended experimental method for the estimation of (K_{Ic}) perpendicular to osteons’ direction

$$begin{aligned} K_{Ic} [MPasqrt{m}]{=}1.89left( rho _{ash} [gr/cc] right) ^{1.88} ,, R^2{=}0.5374. end{aligned}$$

The corresponding statistical critical energy release rate bounds were determined:

$$begin{aligned} G_{Ic}[N/m]= 321.94 (rho _{ash}[gr/cc])^{1.69} times exp(pm 2SD), end{aligned}$$

with a standard deviation (SD= 0.30) representing a 95.4% confidence interval. The average (G_{Ic}) resulted in good correlations between the predicted fracture force by PFM-FEA of four representative specimens and experimental fracture forces. The proposed correlations will be used in CT-based PFM FEA to estimate the risk of hip and humeral fractures.

基于ct的人骨有限元分析(FEA)通过将骨密度((rho _{ash}))与力学参数联系起来,有助于在临床实践中估计骨折风险。然而,用于断裂预测的相场模型需要非均质断裂韧性(G_{Ic}),该韧性可由各种实验方法确定的临界应力强度因子(K_{Ic})导出。由于缺乏确定皮质骨(K_{Ic})的标准,本文提出了一项实验,使用来自两个新鲜冷冻股骨的53个皮质标本来研究(K_{Ic})和(rho _{ash})之间是否存在相关性。我们研究了将(K_{Ic})与(rho _{ash})相关联的各种实验技术。我们采用相场法(PFM)进行了有限元分析,以确定从实验方法得出的五种可能的相关性中最合适的相关性。发现使用施力点位移的ASTM标准是估计(K_{Ic})垂直于骨方向$$begin{aligned} K_{Ic} [MPasqrt{m}]{=}1.89left( rho _{ash} [gr/cc] right) ^{1.88} ,, R^2{=}0.5374. end{aligned}$$的推荐实验方法。确定相应的统计临界能量释放率界限:$$begin{aligned} G_{Ic}[N/m]= 321.94 (rho _{ash}[gr/cc])^{1.69} times exp(pm 2SD), end{aligned}$$,标准差(SD= 0.30)代表95.4% confidence interval. The average (G_{Ic}) resulted in good correlations between the predicted fracture force by PFM-FEA of four representative specimens and experimental fracture forces. The proposed correlations will be used in CT-based PFM FEA to estimate the risk of hip and humeral fractures.
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引用次数: 0
An investigation of crack propagation in porous quasi-brittle structures using isogeometric analysis and higher-order phase-field theory 用等几何分析和高阶相场理论研究多孔准脆性结构中的裂纹扩展
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-22 DOI: 10.1007/s10704-024-00824-0
Khuong D. Nguyen, Tran Minh Thi

This article introduces a novel method for investigating crack propagation in porous quasi-brittle structures. The method combines isogeometric analysis (IGA) with higher-order phase-field theory. IGA is particularly useful for representing complex geometries through high-order Non-Uniform Rational B-Spline (NURBS)-based elements. It gives it an advantage over conventional methods that rely on enriched nodes. The phase-field approach uses a scalar field to implicitly define the trajectory of cracks, eliminating the need to predefine an initial crack location. The study was conducted on a porous plate model with multiple perforations. The porosity level significantly affects the structural integrity of the domain under consideration. The degradation functions that characterize material softening concerning porosity are obtained through careful examination. These degradation functions are further implemented into numerical problems to observe the effect of porosity on crack initiation and propagation behavior. The results have demonstrated the proposed approach’s efficiency and accuracy in analyzing porous concrete’s failure behavior. The analysis results contribute to advancing our understanding of crack propagation and showcase the efficacy of the presented methodological framework in enhancing predictive capabilities in structural mechanics.

本文介绍了一种研究多孔准脆性结构裂纹扩展的新方法。该方法将等几何分析与高阶相场理论相结合。IGA对于通过基于高阶非均匀有理b样条(NURBS)的元素表示复杂几何图形特别有用。它比依赖于富节点的传统方法有一个优势。相场方法使用标量场来隐式定义裂纹的轨迹,从而消除了预先定义初始裂纹位置的需要。该研究是在多孔板模型上进行的。孔隙度水平对研究区域的结构完整性有显著影响。通过仔细研究,得到了表征材料软化与孔隙率关系的降解函数。将这些退化函数进一步应用到数值问题中,观察孔隙率对裂纹萌生和扩展行为的影响。结果表明,该方法对分析多孔混凝土的破坏行为具有较高的效率和准确性。分析结果有助于提高我们对裂纹扩展的理解,并展示了所提出的方法框架在增强结构力学预测能力方面的有效性。
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引用次数: 0
Interpretable crack features for the representation of kinematic fields in the case of fatigue overloads 疲劳超载情况下运动场的可解释裂纹特征表示
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-22 DOI: 10.1007/s10704-024-00830-2
Ghita Bahaj Filali, Michel Coret, Adrien Leygue, Julien Réthoré

Many engineering structures are subjected to variable amplitude loading. A number of studies investigate the effects of post overload, even-though it is crucial to describe what occurs during the overloading. The aim of this paper is to provide effective independent descriptors based on purely kinematic measurements for the analysis of overloading. Fatigue tests were conducted on a SENT specimen. Investigating crack propagation was through direct measurements using Digital Image Correlation and Linear Elastic Fracture Mechanics via Williams’ series expansion. The higher terms in Williams’ series expansion, referred to as crack features were analyzed in cycles with and without overload. In a case without overload, all features exhibit a proportional regime. Singular value decomposition (SVD) analysis confirms that a single feature is adequate to characterize the mechanism. In a cycle with overload, the regime changes during the overloading phase, making it a signature of this phase. In this case, the SVD analysis reveals that two descriptors are needed for these cycles. A subsequent analysis allows the definition of two physically interpretable features. This work presents a robust method to identify, based on kinematic measurements and SVD analysis, independent descriptors for the processes that occur during a cycle with overload.

许多工程结构都要承受变幅荷载。许多研究调查了超载后的影响,尽管描述超载期间发生的事情至关重要。本文的目的是为超载分析提供基于纯运动学测量的有效独立描述符。对SENT试样进行了疲劳试验。通过Williams级数扩展,使用数字图像相关和线弹性断裂力学直接测量裂缝扩展。威廉姆斯级数展开中的较高项,即裂纹特征,在有和没有过载的循环中进行了分析。在没有过载的情况下,所有的特征都呈现成比例。奇异值分解(SVD)分析证实单个特征足以表征该机制。在具有过载的循环中,状态在过载阶段发生变化,使其成为该阶段的签名。在这种情况下,SVD分析揭示了这些循环需要两个描述符。随后的分析允许定义两个物理上可解释的特征。这项工作提出了一种鲁棒的方法来识别,基于运动学测量和SVD分析,独立描述符的过程中发生的循环与过载。
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引用次数: 0
A dialogue between Finite Fracture Mechanics and Phase Field approaches to fracture for predicting crack nucleation at the microscale 有限断裂力学与相场断裂方法在微观尺度上预测裂纹成核的对话
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-20 DOI: 10.1007/s10704-024-00819-x
Sara Jiménez-Alfaro, Dominique Leguillon, Corrado Maurini, José Reinoso

Unraveling the material behavior at the microscale is one of the challenges of this century, demanding progress in experimental and computational strategies. Among the latter, two approaches are commonly applied for predicting crack nucleation. The Coupled Criterion (CC) and the Phase Field (PF) model, both depending on a material length parameter. In brittle materials at the macroscale, this parameter is significantly smaller than the specimen size. However, when the scale decreases, this material length might approach the structural dimensions. In this context, a comprehensive comparison between the two models is conducted, changing the ratio between the material length parameter and the dimensions of the specimen. Results indicate that when this ratio is sufficiently small predictions from both models coincide, otherwise both the CC and the PF model predict different results. Despite their differences, an agreement with experiments reported in the literature have been observed.

揭示微观尺度下的材料行为是本世纪的挑战之一,需要在实验和计算策略方面取得进展。其中,裂纹形核预测常用两种方法。耦合准则(CC)和相场(PF)模型,两者都依赖于材料长度参数。在宏观尺度的脆性材料中,该参数明显小于试样尺寸。然而,当尺度减小时,该材料长度可能接近结构尺寸。在此背景下,对两种模型进行综合比较,改变材料长度参数与试件尺寸的比值。结果表明,当该比值足够小时,两种模型的预测结果一致,否则CC和PF模型的预测结果不同。尽管它们存在差异,但已观察到与文献中报告的实验一致。
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引用次数: 0
Understanding regularized crack initiation through the lens of finite fracture mechanics 从有限断裂力学的角度理解正则化裂纹起裂
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-16 DOI: 10.1007/s10704-024-00837-9
Aurelien Doitrand, Gergely Molnár

As a remedy to pathological sharp crack configurations such as strong singularities or anti-plane shear cracks, where crack initiation is driven solely by energy, a regularized crack description can be adopted to study crack initiation. The nucleation of a regularized crack at a V-notch is studied using the coupled criterion through matched asymptotic expansions. The process zone around the crack is described by crack regularization usually employed in phase-field models. The effective crack length increases with increasing regularization length so that the incremental energy release rate decreases, which in turn increases the critical generalized stress intensity factor at initiation. Decreasing incremental energy release rate is also obtained with increasing Poisson’s ratio. For a given material characteristic length, it is shown that the initiation crack length only depends on the V-notch angle and Poisson’s ratio. For a given geometry and Poisson’s ratio, the initiation length is proportional to the regularization length. The proposed description of regularized crack initiation shows good correspondence to the generalized stress intensity factor obtained by phase-field calculation, the only difference being in the description of the process zone prior to crack initiation.

作为病态尖锐裂纹形态的补救措施,如强奇点或反平面剪切裂纹,其中裂纹起裂完全由能量驱动,可采用正则化裂纹描述来研究裂纹起裂。通过匹配渐近展开,利用耦合准则研究了v型缺口处正则裂纹的形核问题。裂纹周围的过程区用相场模型中常用的裂纹正则化来描述。有效裂纹长度随着正则化长度的增加而增加,使得增量能量释放率减小,从而增加了初始临界广义应力强度因子。随着泊松比的增大,能量的增量释放率也减小。在材料特征长度一定的情况下,初始裂纹长度只与v形缺口角和泊松比有关。对于给定的几何形状和泊松比,起始长度与正则化长度成正比。本文提出的正则裂纹起裂描述与相场计算得到的广义应力强度因子具有良好的符合性,唯一不同的是对裂纹起裂前过程区的描述。
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引用次数: 0
How to measure fracture toughness of soft materials: a comparison of six different approaches using blood clot as a model material 如何测量软材料的断裂韧性:使用血凝块作为模型材料的六种不同方法的比较
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-13 DOI: 10.1007/s10704-024-00820-4
Matthew J. Lohr, Grace N. Bechtel, Berkin Dortdivanlioglu, Manuel K. Rausch

Soft materials are an important class of materials. They play critical roles both in nature, in the form of soft tissues, and in industrial applications. Quantifying their mechanical properties is an important part of understanding and predicting their behavior, and thus optimizing their use. However, there are often no agreed upon standards for how to do so. This also holds true for quantifying their fracture toughness; that is, their resistance to crack propagation. The goal of our work is to fill this knowledge gap using blood clot as a model material. In total, we compared three general approaches, some with multiple different implementations. The first approach is based on Griffith’s definition of the critical energy release rate. The second approach makes use of the J-Integral. The last approach uses cohesive zones. We applied these approaches to 12 pure shear experiments with notched samples (some approaches were supplemented with unnotched samples). Finally, we compared these approaches by their intra- and inter-approach variability, the complexity of their implementation, and their computational cost. Overall, we found that the simplest method was also the most consistent and the least costly one: the Griffith-based approach, as proposed by Rivlin and Thomas in 1953.

软质材料是一类重要的材料。它们在自然界中发挥着至关重要的作用,以软组织的形式,在工业应用中。量化它们的力学性能是理解和预测它们的行为,从而优化它们的使用的重要组成部分。然而,对于如何这样做,通常没有商定的标准。这也适用于量化它们的断裂韧性;也就是说,它们对裂纹扩展的抵抗力。我们工作的目标是用血凝块作为模型材料来填补这一知识空白。总的来说,我们比较了三种通用方法,其中一些有多种不同的实现。第一种方法是基于格里菲斯对临界能量释放率的定义。第二种方法利用j积分。最后一种方法使用内聚区域。我们将这些方法应用于12个带缺口样品的纯剪切实验(一些方法补充了未缺口样品)。最后,我们比较了这些方法的内部和内部可变性、实现的复杂性和计算成本。总的来说,我们发现最简单的方法也是最一致和成本最低的方法:Griffith-based方法,由Rivlin和Thomas在1953年提出。
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引用次数: 0
In situ characterisation of dynamic fracture in (Al_2O_3) using ultra-fast X-ray phase contrast radioscopy: effects of porosity and crack speed 使用超快速x射线相衬放射镜对(Al_2O_3)动态裂缝的原位表征:孔隙率和裂纹速度的影响
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-13 DOI: 10.1007/s10704-024-00816-0
Q. Henry, J.-B. Kopp, L. Le Barbenchon, J. Girardot, B. Lukić, A. Cohen, A. Cosculluela, P. Viot

The dynamic fracture properties of porous ceramics were studied using single bunch synchrotron X-ray phase contrast imaging. The modified brazilian geometry was used to initiate and propagate a pure mode I crack. The specimen was compressed using the Split Hopkinson bars at strain rates of the order of (10^2) s(^{-1}). Main cracks were isolated for four different grades of (Al_2O_3), one dense alumina, and three porous grades with (20~%) to (60~%) porosity. The maximum measured crack velocities for three grades is of the order of (0.6c_R) and (0.4c_R) for the most porous. The fracture energy was estimated using a FE numerical simulation to quantify the influence of inertial effects induced by crack propagation. The results show that these inertial effects are far from negligible (up to (80~%) of the stored energy) and that the dynamic correction factors known from the literature tend to overestimate the fracture energy. The values obtained vary from 22 J/m(^2) for the densest to 5 J/m(^2) for the most porous.

采用单束同步x射线相衬成像技术研究了多孔陶瓷的动态断裂特性。采用修正巴西几何模型对纯I型裂纹进行了初始化和扩展。试样使用劈裂霍普金森杆压缩,应变速率为(10^2) s (^{-1})数量级。对4种不同等级的(Al_2O_3)、1种致密氧化铝和3种孔隙度为(20~%) ~ (60~%)的多孔氧化铝进行了主裂缝隔离。三个等级的最大测量裂纹速度为(0.6c_R)和(0.4c_R)数量级。利用有限元数值模拟估算了裂纹扩展引起的惯性效应对断裂能的影响。结果表明,这些惯性效应远非可以忽略不计(高达储存能量的(80~%)),并且从文献中已知的动态修正因子往往高估了断裂能。得到的数值从密度最大的22 J/m (^2)到最多孔的5 J/m (^2)不等。
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引用次数: 0
Finite element simulation of rate-dependent damage in elastomers 弹性体速率相关损伤的有限元模拟
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-13 DOI: 10.1007/s10704-024-00818-y
Pinyi Wang, Shawn R. Lavoie, Tian Tang

Predicting the mechanical response and damage evolution of elastomers under large deformation is of great significance in engineering applications. In this work, a finite element (FE) scheme is formulated and used to simulate rate-dependent damage in elastomers. While based on the theoretical model of Lavoie et al. (Extrem Mech Lett 8:114–124, 2016) and maintaining the key features such as kinetics of chain scission and polydispersity, the FE scheme presented here includes the consideration of finite compressibility. Both implicit and explicit algorithms are derived and implemented as user subroutines in ABAQUS. Validated against existing numerical results as well as experimental data on homogeneous deformation, the capability of the FE scheme to solve problems involving inhomogeneous deformation is further explored by simulating samples with pre-existing defects. The numerical results can successfully capture several interesting phenomena, such as crack blunting, stress reduction near defect caused by damage, and rate-dependent damage evolution. Good agreement is also found with experimental data on the strain field near a crack tip.

预测弹性体在大变形作用下的力学响应和损伤演化在工程应用中具有重要意义。在这项工作中,制定了一个有限元(FE)方案,并用于模拟弹性体的速率相关损伤。虽然基于Lavoie等人的理论模型(extreme Mech Lett 8:114-124, 2016),并保持了链断裂动力学和多分散性等关键特征,但本文提出的有限元方案考虑了有限可压缩性。隐式和显式算法都是在ABAQUS中作为用户子程序派生和实现的。通过对已有的均匀变形数值结果和实验数据的验证,通过模拟存在缺陷的样品,进一步探讨了有限元格式解决非均匀变形问题的能力。数值结果可以很好地捕捉到裂纹钝化、损伤引起的缺陷附近应力减小和损伤演化速率相关等现象。裂纹尖端附近的应变场与实验数据吻合较好。
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引用次数: 0
Interfacial cavitation during peeling of soft viscoelastic adhesives 软粘弹性胶粘剂剥离过程中的界面空化
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-12 DOI: 10.1007/s10704-024-00834-y
Xingwei Yang, Huiqi Shi, Yuan Qi, Rong Long

Peel tests are commonly used to characterize the performance of adhesive tapes. The force required to peel a tape from a substrate depends on not only interface adhesion but also mechanics of the tape. Typically, adhesive tapes consist of a stiff backing film and a layer of adhesive material that is soft and viscoelastic. While mechanics of the backing film has been extensively studied, mechanics of the soft adhesive layer is less understood. In this work, finite element simulations are carried out to study large deformation of the soft adhesive layer during 90-degree peeling and its implication on the peel force. We find that debonding can occur ahead of the peel front when the peel front is still adhered to the substrate. This phenomenon, referred to as “interfacial cavitation”, causes the peel front to advance in a stepwise manner despite that a constant peeling velocity is prescribed. Consequently, the peel force follows an oscillatory history resembling the “stick–slip” behavior widely observed in peel tests. Further investigations reveal that interfacial cavitation originates from a non-monotonic distribution of interfacial traction ahead of the peel front. Moreover, emergence of interfacial cavitation can be controlled by three factors: interfacial slip, adhesive layer thickness and peeling velocity. These results can provide insights towards designing adhesive tapes with desired adhesion performance or release mechanisms.

剥离试验通常用于表征胶带的性能。从基板上剥离胶带所需的力不仅取决于界面附着力,还取决于胶带的力学性质。通常,胶带由一层坚硬的背膜和一层柔软的粘弹性粘合材料组成。虽然背膜的力学已被广泛研究,但软粘接层的力学却鲜为人知。本文通过有限元模拟研究了软胶层在90度剥离过程中的大变形及其对剥离力的影响。我们发现,当剥离面仍然粘附在基材上时,剥离可以发生在剥离面前面。这种现象被称为“界面空化”,尽管规定了恒定的剥离速度,但仍会导致剥离前沿以逐步的方式前进。因此,剥离力遵循类似于剥离试验中广泛观察到的“粘滑”行为的振荡历史。进一步的研究表明,界面空化起源于剥离锋前方界面牵引力的非单调分布。界面空化的产生受界面滑移、胶层厚度和剥离速度三个因素的控制。这些结果可以为设计具有理想粘附性能或释放机制的胶带提供见解。
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引用次数: 0
Effect of notch root radius on apparent fracture toughness of Ti6Al4V alloy: experiments and simulations 缺口根半径对Ti6Al4V合金表观断裂韧性的影响:实验与模拟
IF 2.2 3区 工程技术 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-01-11 DOI: 10.1007/s10704-024-00838-8
Akash Kumar, Jyoti S. Jha, Sushil K. Mishra, Parag Tandaiya

Ti6Al4V is a widely used titanium alloy known for its excellent combination of mechanical properties, corrosion resistance, and biocompatibility. However, to ensure its effectiveness in various applications, it is important to understand the mechanical and fracture behavior of the alloy in the presence of a notch. In the present study, the effect of notch root radius on mode I fracture toughness of Ti6Al4V alloys with a nearly bimodal microstructure has been investigated. Fracture toughness tests were conducted on compact tension (CT) specimens with five different notch root radii. The experimental results demonstrate that the apparent fracture toughness, (K_{IA}), increases linearly with the square root of the notch root radius. Further to elucidate the results, a 2D elastoplastic finite element analysis is performed on the CT specimens using cohesive zone model. The simulation results are in good agreement with the experimental data. The study also reveals that the apparent fracture toughness is independent of the notch root radius below a critical value, estimated to be approximately (50 mu m). Finally, the scanning electron microscopy of the fracture surfaces has been examined. The micrographs reveal void coalescence and dimple regions indicating the ductile nature of the fracture process.

Ti6Al4V是一种广泛使用的钛合金,以其优异的机械性能、耐腐蚀性和生物相容性而闻名。然而,为了确保其在各种应用中的有效性,了解缺口存在时合金的力学和断裂行为是很重要的。本文研究了缺口根半径对近双峰组织Ti6Al4V合金I型断裂韧性的影响。对5种不同缺口根半径的致密拉伸(CT)试样进行了断裂韧性试验。实验结果表明,表观断裂韧性(K_{IA})随缺口根半径的平方根线性增加。为了进一步阐明结果,采用内聚区模型对CT试件进行了二维弹塑性有限元分析。仿真结果与实验数据吻合较好。研究还表明,在一个临界值(估计约为(50 mu m))以下,表观断裂韧性与缺口根半径无关。最后,对断口表面进行了扫描电镜观察。显微图显示孔洞合并和韧窝区域,表明断裂过程具有延展性。
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引用次数: 0
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International Journal of Fracture
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