Pub Date : 2026-01-23DOI: 10.3103/S1068366625700552
V. G. Burov, S. V. Stankevich, I. A. Bataev, M. L. Kheifetz, K. I. Emurlaev, E. A. Drobyaz, D. I. Kotov, A. A. Bataev
A novel friction tester has been developed that simultaneously implements three types of mechanical effects on metal samples: oblique impact, rolling friction, and sliding friction. The main unit of the installation is a driver mounted on a shaft with indenters located in its sockets, steel rollers with a diameter of 32 mm and a weight of 0.2 kg. The mechanism is actuated by a servodrive, which allows a smooth adjustment of the angular rotation speed in the range from 0 to 1500 min–1. The indenters are made of quenched and ShKh15SG low-tempered ball bearing steel (64 HRC). During the testing process, the rollers, freely located in the driver sockets, have the ability to rotate relative to their axes and roll along the surfaces of the samples. Under the action of the centrifugal force generated by the rotation of the driver, the rollers come into contact with the studied samples and wear them out. During one revolution of the driver, each of the samples is subjected to roller impacts twice. The impacts are carried out simultaneously, which reduces vibrations of the parts of the device. Tribological tests of Hadfield steel in the austenitic state, 95Cr6Mo3V3SiTi steel quenched and tempered at 545°C, as well as boron- and chromium-alloy formed by the method of non-vacuum electron beam cladding were carried out using the developed device. The samples made of 95Cr6Mo3V3SiTi steel possessed the highest level of wear resistance. The features of the mechanisms of destruction of the surface layers of metal alloys are revealed.
{"title":"A Device for Studying the Mechanisms of Surface Fracture of Materials That Combines Impact Loading, Rolling, and Sliding Friction","authors":"V. G. Burov, S. V. Stankevich, I. A. Bataev, M. L. Kheifetz, K. I. Emurlaev, E. A. Drobyaz, D. I. Kotov, A. A. Bataev","doi":"10.3103/S1068366625700552","DOIUrl":"10.3103/S1068366625700552","url":null,"abstract":"<p>A novel friction tester has been developed that simultaneously implements three types of mechanical effects on metal samples: oblique impact, rolling friction, and sliding friction. The main unit of the installation is a driver mounted on a shaft with indenters located in its sockets, steel rollers with a diameter of 32 mm and a weight of 0.2 kg. The mechanism is actuated by a servodrive, which allows a smooth adjustment of the angular rotation speed in the range from 0 to 1500 min<sup>–1</sup>. The indenters are made of quenched and ShKh15SG low-tempered ball bearing steel (64 HRC). During the testing process, the rollers, freely located in the driver sockets, have the ability to rotate relative to their axes and roll along the surfaces of the samples. Under the action of the centrifugal force generated by the rotation of the driver, the rollers come into contact with the studied samples and wear them out. During one revolution of the driver, each of the samples is subjected to roller impacts twice. The impacts are carried out simultaneously, which reduces vibrations of the parts of the device. Tribological tests of Hadfield steel in the austenitic state, 95Cr6Mo3V3SiTi steel quenched and tempered at 545°C, as well as boron- and chromium-alloy formed by the method of non-vacuum electron beam cladding were carried out using the developed device. The samples made of 95Cr6Mo3V3SiTi steel possessed the highest level of wear resistance. The features of the mechanisms of destruction of the surface layers of metal alloys are revealed.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"221 - 226"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027175","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S106836662570059X
N. K. Krioni, A. A. Mingazheva, A. Dzh. Mingazhev
The article presents results of studies on the wear resistance of structural steels used to manufacture shafts for rotary positive‑displacement pumps. A characteristic feature of these pumps is the extremely small clearances between their working elements, on the order of about 10–25 µm, which depend on the amount of wear of the shafts at the bearing interfaces. Glow‑discharge nitriding (plasma nitriding) is the most efficient method for providing high wear resistance of parts. It is shown that one of the adverse phenomena during wear of the nitrided layer is the formation of abrasive particles as a result of spalling; these particles promote surface scoring of the bushing and, consequently, accelerate the wear process. The aim of the work was to investigate the wear resistance of steel that was glow‑discharge nitrided following preliminary processing by surface plastic deformation, medium‑energy ion implantation, magnetic‑pulse processing, and combined activation methods. The following surface activation regimes were used prior to ion nitriding: shot‑peening with steel microspheres 50–100 µm in diameter at speeds of 30–70 m/s; implanted ions—nitrogen; dose—1.3 × 1017 ions/cm2; dose rate—1 × 1015 ions/s; ion implantation energy – 25 keV. Magnetic‑pulse processing (MPP) was carried out with pulse energies from 2 to 8 kJ, pulse durations from 5 to 40 µs, and number of pulses from 2 to 5. It was shown that the most efficient preliminary surface‑activation method before nitriding is medium‑energy ion implantation, which allows increasing the wear resistance of the nitrided layer of 40Kh steel by a factor of 5.7 and of 40KhN steel by a factor of 4.5 compared with conventional ion nitriding.
{"title":"Wear Resistance of 40Kh and 40KhN Structural Steels with a Nitrided Layer after Modifying Processing","authors":"N. K. Krioni, A. A. Mingazheva, A. Dzh. Mingazhev","doi":"10.3103/S106836662570059X","DOIUrl":"10.3103/S106836662570059X","url":null,"abstract":"<p>The article presents results of studies on the wear resistance of structural steels used to manufacture shafts for rotary positive‑displacement pumps. A characteristic feature of these pumps is the extremely small clearances between their working elements, on the order of about 10–25 µm, which depend on the amount of wear of the shafts at the bearing interfaces. Glow‑discharge nitriding (plasma nitriding) is the most efficient method for providing high wear resistance of parts. It is shown that one of the adverse phenomena during wear of the nitrided layer is the formation of abrasive particles as a result of spalling; these particles promote surface scoring of the bushing and, consequently, accelerate the wear process. The aim of the work was to investigate the wear resistance of steel that was glow‑discharge nitrided following preliminary processing by surface plastic deformation, medium‑energy ion implantation, magnetic‑pulse processing, and combined activation methods. The following surface activation regimes were used prior to ion nitriding: shot‑peening with steel microspheres 50–100 µm in diameter at speeds of 30–70 m/s; implanted ions—nitrogen; dose—1.3 × 10<sup>17</sup> ions/cm<sup>2</sup>; dose rate—1 × 10<sup>15</sup> ions/s; ion implantation energy – 25 keV. Magnetic‑pulse processing (MPP) was carried out with pulse energies from 2 to 8 kJ, pulse durations from 5 to 40 µs, and number of pulses from 2 to 5. It was shown that the most efficient preliminary surface‑activation method before nitriding is medium‑energy ion implantation, which allows increasing the wear resistance of the nitrided layer of 40Kh steel by a factor of 5.7 and of 40KhN steel by a factor of 4.5 compared with conventional ion nitriding.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"252 - 256"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027223","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700539
M. I. Aleutdinova, V. V. Fadin
The aim of the work is to study the distribution of oxygen in the contact layer of C45 steel during pin-on-ring dry friction against St3 steel under high-density electric current (>100 A/cm2). The formation of a transfer layer on the contact surface of the counterbody and the formation of a melt on the contact surface of the transfer layer were shown by the electron microscopy method. The melt has weak signs of adhesive interaction, which is an indicator of high melt viscosity. X-ray spectral microanalysis of the contact surface of the transfer layer showed an oxygen content of 30 at %, which serves as an indicator of FeO formation. The oxygen corresponds to a concentration of about 60 vol % FeO. The oxygen concentration in the cross-section of the transfer layer at a distance of 3 μm from the contact surface was about 10 at % that corresponds to about 20 vol % FeO. The X-ray phase analysis method established the predominance of FeO and α-Fe in the contact surface of the transfer layer of C45 steel, i.e., about 90 vol % FeO. These data indirectly prove the existence of a FeO concentration gradient directed into the depth of the transfer layer and allow us to state that the melt consists of neutral atoms or ions of iron and oxygen. An increase in the current density in the contact leads to an increase in the electrical conductivity of the contact and to a decrease in the friction coefficient. This allows us to assume an increase in the amount of melt in the contact space with an increase in the current density. An increase in the current density also leads to an increase in the sliding stage (“slip”) during sliding in the stick–slip mode and to a decrease in the friction coefficient. The obtained data can serve as a guideline in the design of current-collecting friction units for powerful electric motors and generators.
本研究的目的是研究高密度电流(100 A/cm2)下C45钢与St3钢销环干摩擦过程中C45钢接触层中氧的分布。用电镜法观察了在对偶体接触面上形成转移层和在转移层接触面上形成熔体的过程。熔体有粘接相互作用的微弱迹象,这是熔体高粘度的一个指标。传递层接触面的x射线光谱微分析显示,氧含量为30 at %,这是FeO形成的标志。氧对应于约60 vol % FeO的浓度。在距离接触面3 μm处传递层横截面上的氧浓度约为10 at %,对应于约20 vol %的FeO。x射线相分析方法确定了C45钢传递层接触面中FeO和α-Fe的优势,即FeO含量约为90 vol %。这些数据间接证明了转移层深处存在FeO浓度梯度,并允许我们声明熔体由铁和氧的中性原子或离子组成。接触中电流密度的增加导致接触电导率的增加和摩擦系数的降低。这允许我们假设接触空间中的熔体量随着电流密度的增加而增加。在粘滑模式下,电流密度的增加还会导致滑动阶段(“滑移”)的增加,并导致摩擦系数的降低。所得数据可为大功率电动机和发电机集流摩擦单元的设计提供指导。
{"title":"Distribution of Oxygen in the Surface Layer of a Steel Counterbody from C45 Steel under Friction Conditions without Lubricant under Action of High-Density Electric Current","authors":"M. I. Aleutdinova, V. V. Fadin","doi":"10.3103/S1068366625700539","DOIUrl":"10.3103/S1068366625700539","url":null,"abstract":"<p>The aim of the work is to study the distribution of oxygen in the contact layer of C45 steel during pin-on-ring dry friction against St3 steel under high-density electric current (>100 A/cm<sup>2</sup>). The formation of a transfer layer on the contact surface of the counterbody and the formation of a melt on the contact surface of the transfer layer were shown by the electron microscopy method. The melt has weak signs of adhesive interaction, which is an indicator of high melt viscosity. X-ray spectral microanalysis of the contact surface of the transfer layer showed an oxygen content of 30 at %, which serves as an indicator of FeO formation. The oxygen corresponds to a concentration of about 60 vol % FeO. The oxygen concentration in the cross-section of the transfer layer at a distance of 3 μm from the contact surface was about 10 at % that corresponds to about 20 vol % FeO. The X-ray phase analysis method established the predominance of FeO and α-Fe in the contact surface of the transfer layer of C45 steel, i.e., about 90 vol % FeO. These data indirectly prove the existence of a FeO concentration gradient directed into the depth of the transfer layer and allow us to state that the melt consists of neutral atoms or ions of iron and oxygen. An increase in the current density in the contact leads to an increase in the electrical conductivity of the contact and to a decrease in the friction coefficient. This allows us to assume an increase in the amount of melt in the contact space with an increase in the current density. An increase in the current density also leads to an increase in the sliding stage (“slip”) during sliding in the stick–slip mode and to a decrease in the friction coefficient. The obtained data can serve as a guideline in the design of current-collecting friction units for powerful electric motors and generators.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"205 - 212"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027200","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700618
A. S. Shirobokova, E. V. Kharanzhevskiy, A. G. Ipatov, A. V. Makarov
This work investigates the tribological characteristics of the surface of carbon steel alloyed with bismuth oxide with the addition of an oxidizer or a reducing agent, specifically lithium nitrate or highly dispersed graphite powder, respectively. Tribological tests were performed in contact with an aluminum alloy AZh1 under boundary lubrication conditions. It was established that carbon interacts with bismuth oxide during the alloying process under high temperature laser treatment, leading to the formation of metallic bismuth, which negatively affects the performance of the tribological pair under high contact load. Furthermore, a higher carbon content in the powder mixture results in a greater amount of reduced bismuth oxide in the steel surface and a lower load-carrying capacity of the pair at a constant speed of 9.0 m/s. Conversely, the decomposition of lithium nitrate with the release of oxygen during high-intensity laser processing leads to an increased proportion of oxidized bismuth in the alloyed surface. The addition of the oxidizer significantly improves the tribological characteristics of the pair under boundary lubrication friction conditions. A possible mechanism for the occurrence of ultra-low friction and wear coefficients during sliding friction under boundary lubrication for the bismuth–oxide–alloyed steel vs. aluminum alloy friction pair is proposed.
{"title":"The Effect of Redox Reactions during Laser Alloying of Steel with Bismuth Oxide on Tribological Characteristics under Boundary Friction Conditions","authors":"A. S. Shirobokova, E. V. Kharanzhevskiy, A. G. Ipatov, A. V. Makarov","doi":"10.3103/S1068366625700618","DOIUrl":"10.3103/S1068366625700618","url":null,"abstract":"<p>This work investigates the tribological characteristics of the surface of carbon steel alloyed with bismuth oxide with the addition of an oxidizer or a reducing agent, specifically lithium nitrate or highly dispersed graphite powder, respectively. Tribological tests were performed in contact with an aluminum alloy AZh1 under boundary lubrication conditions. It was established that carbon interacts with bismuth oxide during the alloying process under high temperature laser treatment, leading to the formation of metallic bismuth, which negatively affects the performance of the tribological pair under high contact load. Furthermore, a higher carbon content in the powder mixture results in a greater amount of reduced bismuth oxide in the steel surface and a lower load-carrying capacity of the pair at a constant speed of 9.0 m/s. Conversely, the decomposition of lithium nitrate with the release of oxygen during high-intensity laser processing leads to an increased proportion of oxidized bismuth in the alloyed surface. The addition of the oxidizer significantly improves the tribological characteristics of the pair under boundary lubrication friction conditions. A possible mechanism for the occurrence of ultra-low friction and wear coefficients during sliding friction under boundary lubrication for the bismuth–oxide–alloyed steel vs. aluminum alloy friction pair is proposed.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"262 - 267"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027219","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700540
A. V. Ivakhnik, V. I. Zhornik
The article is devoted to the study of the possibility of reducing the cost of complex calcium sulfonate grease (CCSG) through the use of by-products of the production of ultra-alkaline calcium sulfonate (UCS). The purpose of the work is to evaluate the prospects for the use of calcium compound concentrate (CCC), a by-product of the production of UCS, to reduce the cost of CCC production while ensuring a given level of their operational characteristics. The article proposes a variant for the manufacturing of CCSG based on sulfonated compounds of various origins and describes a method for monitoring the synthesis using infrared (IR) spectrometry. The synthesis of CCSG samples based on UCS and a concentrate of calcium compounds is described, with control of the lubricant manufacturing process using IR spectroscopy and assessment of its rheological properties and tribological characteristics (penetration, drop point, colloidal stability, welding load, and critical load). It has been established that samples of lubricants based on UCS and CCS demonstrate high performance characteristics comparable to their foreign counterparts. It is shown that the use of by-products of UCS production is acceptable and advisable, while it opens up the possibility of reducing the cost and improving the environmental conditions of CCSG production.
{"title":"Complex Calcium Sulfonate Lubricant Based on a By-Product of Chemical Production","authors":"A. V. Ivakhnik, V. I. Zhornik","doi":"10.3103/S1068366625700540","DOIUrl":"10.3103/S1068366625700540","url":null,"abstract":"<p>The article is devoted to the study of the possibility of reducing the cost of complex calcium sulfonate grease (CCSG) through the use of by-products of the production of ultra-alkaline calcium sulfonate (UCS). The purpose of the work is to evaluate the prospects for the use of calcium compound concentrate (CCC), a by-product of the production of UCS, to reduce the cost of CCC production while ensuring a given level of their operational characteristics. The article proposes a variant for the manufacturing of CCSG based on sulfonated compounds of various origins and describes a method for monitoring the synthesis using infrared (IR) spectrometry. The synthesis of CCSG samples based on UCS and a concentrate of calcium compounds is described, with control of the lubricant manufacturing process using IR spectroscopy and assessment of its rheological properties and tribological characteristics (penetration, drop point, colloidal stability, welding load, and critical load). It has been established that samples of lubricants based on UCS and CCS demonstrate high performance characteristics comparable to their foreign counterparts. It is shown that the use of by-products of UCS production is acceptable and advisable, while it opens up the possibility of reducing the cost and improving the environmental conditions of CCSG production.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"213 - 220"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027220","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S106836662570062X
Fulan Liu, Yanqing Tan, Yinming Jiang, Tian Fang
Ultrasonic impact treatment is a surface strengthening technique that utilizes ultrasonic vibrations to enhance the topography, stress, hardness, and other surface characteristics of materials, thereby improving their resistance to wear, corrosion, and similar performance attributes. This paper focuses on the application of ultrasonic impact treatment on 1045 steel, which underwent this process subsequent to quenching. Experimental analysis of the surface hardness and roughness of untreated, quenched, and ultrasonic impact-treated 1045 steel specimens demonstrates that the quenching process results in a 37.4% increase in surface hardness and a 32.9% reduction in surface roughness. In comparison, the ultrasonic impact treatment leads to a more substantial improvement, with a 47.2% increase in surface hardness and a 56.4% decrease in surface roughness. To evaluate the friction and wear characteristics of the different specimens, a series of ball–disk tests were conducted under both dry friction and oil lubrication conditions. The results indicate that the surface subjected to ultrasonic impact treatment exhibited the lowest coefficient of friction, minimal surface wear, and a relatively moderate surface wear development rate under dry friction conditions. Specifically, the quenching process reduced the surface wear rate by 10.8%, while the ultrasonic impact treatment led to a substantial reduction of 52.60%. Under oil lubrication conditions, ultrasonic impact treatment decreased the surface wear rate by 18.26%. Additionally, this research delves into the microscopic wear mechanisms and observed wear behaviors of the 1045 steel specimens under different lubrication conditions. It particularly examines how lubricating oils may adversely affect the tribological performance of ultrasonically treated steel surfaces. By providing a comparative analysis of the specimens subjected to ultrasonic impact treatment and those processed through traditional quenching, this paper aims to enhance the understanding of the effects of ultrasonic impact treatment on the performance of metal materials and to offer a reference framework for optimizing the tribological applications of such materials.
{"title":"Study on Microscopic Characteristics and Wear Testing of Steel Surface after Ultrasonic Impact Treatment","authors":"Fulan Liu, Yanqing Tan, Yinming Jiang, Tian Fang","doi":"10.3103/S106836662570062X","DOIUrl":"10.3103/S106836662570062X","url":null,"abstract":"<p>Ultrasonic impact treatment is a surface strengthening technique that utilizes ultrasonic vibrations to enhance the topography, stress, hardness, and other surface characteristics of materials, thereby improving their resistance to wear, corrosion, and similar performance attributes. This paper focuses on the application of ultrasonic impact treatment on 1045 steel, which underwent this process subsequent to quenching. Experimental analysis of the surface hardness and roughness of untreated, quenched, and ultrasonic impact-treated 1045 steel specimens demonstrates that the quenching process results in a 37.4% increase in surface hardness and a 32.9% reduction in surface roughness. In comparison, the ultrasonic impact treatment leads to a more substantial improvement, with a 47.2% increase in surface hardness and a 56.4% decrease in surface roughness. To evaluate the friction and wear characteristics of the different specimens, a series of ball–disk tests were conducted under both dry friction and oil lubrication conditions. The results indicate that the surface subjected to ultrasonic impact treatment exhibited the lowest coefficient of friction, minimal surface wear, and a relatively moderate surface wear development rate under dry friction conditions. Specifically, the quenching process reduced the surface wear rate by 10.8%, while the ultrasonic impact treatment led to a substantial reduction of 52.60%. Under oil lubrication conditions, ultrasonic impact treatment decreased the surface wear rate by 18.26%. Additionally, this research delves into the microscopic wear mechanisms and observed wear behaviors of the 1045 steel specimens under different lubrication conditions. It particularly examines how lubricating oils may adversely affect the tribological performance of ultrasonically treated steel surfaces. By providing a comparative analysis of the specimens subjected to ultrasonic impact treatment and those processed through traditional quenching, this paper aims to enhance the understanding of the effects of ultrasonic impact treatment on the performance of metal materials and to offer a reference framework for optimizing the tribological applications of such materials.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"268 - 277"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027197","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700564
M. Sh. Migranov, M. P. Kozochkin, A. S. Gusev, A. A. Maslov, Yu. O. Pristinskii
This study aims at enhancing the efficiency of high-speed edge cutting of heat-resistant alloys. The enhancement is based on improving the tribotechnical characteristics of wear-resistant coatings by using multicomponent target cathodes made from sintered high-entropy alloys deposited by the magnetron method. Technologies for producing high-entropy target cathodes (with a diameter of 20 and 70 mm) obtained by high-temperature spark plasma sintering with various content of Al, Cr, Hf, Mo, Nb, Ni, Ta, Ti, V, W, and Zr have been developed; control of their parameters, density, grain-size composition, electrical conductivity, hardness, and crack resistance is provided. The morphology of the sintered samples was examined by scanning electron microscopy and non-dispersive analysis. Production equipment for magnetron coating systems in various gas media is manufactured. Tribotechnical tests were carried out using tribometers and during edge cutting of various grades of steels and alloys. The test results were used to determine the most effective compositions of multilayer composite nanostructured high-entropy wear-resistant coatings, in particular, Al20Ti20Zr15V15Cr15Nb15 and Al20Hf10Ni15Ti25W10Zr20, which provide improved cutting performance of EI654 and EI698VD chromium-nickel alloys. Comparative tests of commercially used wear-resistant coatings and coatings made of high-entropy target cathodes: Al20Hf10Ni15Ti25W10Zr20, Al20Ti20Zr15V15Cr15Nb15, Al20Hf15V15Cr15Ti15Ta10W10, Ti15Zr15Cr15Ni10W10V10Nb15Al10, Ti20Hf15Mo15W10V10Nb15Al15, Ti40Zr10Cr10Ni10W10Mo10Nb10, etc., were carried out. Studies in the longitudinal turning of EI-654 and EI‑698VD chromium-nickel alloys confirmed that the efficiency of using high-entropy coatings on a cutting tool increases on average by 20–25%.
{"title":"Studies of Innovative Wear-Resistant Coatings for High-Speed Machining","authors":"M. Sh. Migranov, M. P. Kozochkin, A. S. Gusev, A. A. Maslov, Yu. O. Pristinskii","doi":"10.3103/S1068366625700564","DOIUrl":"10.3103/S1068366625700564","url":null,"abstract":"<p>This study aims at enhancing the efficiency of high-speed edge cutting of heat-resistant alloys. The enhancement is based on improving the tribotechnical characteristics of wear-resistant coatings by using multicomponent target cathodes made from sintered high-entropy alloys deposited by the magnetron method. Technologies for producing high-entropy target cathodes (with a diameter of 20 and 70 mm) obtained by high-temperature spark plasma sintering with various content of Al, Cr, Hf, Mo, Nb, Ni, Ta, Ti, V, W, and Zr have been developed; control of their parameters, density, grain-size composition, electrical conductivity, hardness, and crack resistance is provided. The morphology of the sintered samples was examined by scanning electron microscopy and non-dispersive analysis. Production equipment for magnetron coating systems in various gas media is manufactured. Tribotechnical tests were carried out using tribometers and during edge cutting of various grades of steels and alloys. The test results were used to determine the most effective compositions of multilayer composite nanostructured high-entropy wear-resistant coatings, in particular, Al<sub>20</sub>Ti<sub>20</sub>Zr<sub>15</sub>V<sub>15</sub>Cr<sub>15</sub>Nb<sub>15</sub> and Al<sub>20</sub>Hf<sub>10</sub>Ni<sub>15</sub>Ti<sub>25</sub>W<sub>10</sub>Zr<sub>20</sub>, which provide improved cutting performance of EI654 and EI698VD chromium-nickel alloys. Comparative tests of commercially used wear-resistant coatings and coatings made of high-entropy target cathodes: Al<sub>20</sub>Hf<sub>10</sub>Ni<sub>15</sub>Ti<sub>25</sub>W<sub>10</sub>Zr<sub>20</sub>, Al<sub>20</sub>Ti<sub>20</sub>Zr<sub>15</sub>V<sub>15</sub>Cr<sub>15</sub>Nb<sub>15</sub>, Al<sub>20</sub>Hf<sub>15</sub>V<sub>15</sub>Cr<sub>15</sub>Ti<sub>15</sub>Ta<sub>10</sub>W<sub>10</sub>, Ti<sub>15</sub>Zr<sub>15</sub>Cr<sub>15</sub>Ni<sub>10</sub>W<sub>10</sub>V<sub>10</sub>Nb<sub>15</sub>Al<sub>10</sub>, Ti<sub>20</sub>Hf<sub>15</sub>Mo<sub>15</sub>W<sub>10</sub>V<sub>10</sub>Nb<sub>15</sub>Al<sub>15</sub>, Ti<sub>40</sub>Zr<sub>10</sub>Cr<sub>10</sub>Ni<sub>10</sub>W<sub>10</sub>Mo<sub>10</sub>Nb<sub>10</sub>, etc., were carried out. Studies in the longitudinal turning of EI-654 and EI‑698VD chromium-nickel alloys confirmed that the efficiency of using high-entropy coatings on a cutting tool increases on average by 20–25%.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"227 - 235"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027199","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700606
D. G. Tyulenev, V. V. Maistrenko, A. N. Abramov, T. I. Gilmanov
The paper discusses the development and application of domestic hardening oil during the heat treatment of elastic terminals for rail fasteners. The paper presents the results of laboratory comparative tests of the developed oil and its imported counterpart. The study of the effect of the cooling properties of hardening oils on the hardness and structure was conducted during the heat treatment of samples made of 38Si7 steel, which is used for the production of elastic terminals. The cooling properties of hardening oils were evaluated using the UZS-2 device for determining the cooling characteristics of technological and hardening media. It has been shown that the developed prototype of the quenching oil provides a maximum cooling rate of 94.2°C/s, a maximum cooling rate temperature of 615.8°C, a cooling time of 7.03 s to 600°C, a cooling time of 10.3 s to 400°C, a cooling time of 39.3 s to 200°C, and a cooling rate of 7.84°C/s at 300°C. At the same time, the hardness of the 38Si7 steel blanks after hardening is 53.2–54.6 HRC. As a result of the industrial tests, it was found that the developed hardening oil meets the requirements of the technological process of heat treatment of elastic terminals for rail fasteners made of 38SI7 steel and allows one to reduce the cost of purchasing an imported analog.
{"title":"Development and Implementation of a New Import-Substituting Tempering Oil for Steel Heat Treatment","authors":"D. G. Tyulenev, V. V. Maistrenko, A. N. Abramov, T. I. Gilmanov","doi":"10.3103/S1068366625700606","DOIUrl":"10.3103/S1068366625700606","url":null,"abstract":"<p>The paper discusses the development and application of domestic hardening oil during the heat treatment of elastic terminals for rail fasteners. The paper presents the results of laboratory comparative tests of the developed oil and its imported counterpart. The study of the effect of the cooling properties of hardening oils on the hardness and structure was conducted during the heat treatment of samples made of 38Si7 steel, which is used for the production of elastic terminals. The cooling properties of hardening oils were evaluated using the UZS-2 device for determining the cooling characteristics of technological and hardening media. It has been shown that the developed prototype of the quenching oil provides a maximum cooling rate of 94.2°C/s, a maximum cooling rate temperature of 615.8°C, a cooling time of 7.03 s to 600°C, a cooling time of 10.3 s to 400°C, a cooling time of 39.3 s to 200°C, and a cooling rate of 7.84°C/s at 300°C. At the same time, the hardness of the 38Si7 steel blanks after hardening is 53.2–54.6 HRC. As a result of the industrial tests, it was found that the developed hardening oil meets the requirements of the technological process of heat treatment of elastic terminals for rail fasteners made of 38SI7 steel and allows one to reduce the cost of purchasing an imported analog.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"257 - 261"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027176","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700576
E. N. Moskvichev, N. N. Shamarin, N. L. Savchenko
This work presents a study on the development and evaluation of the tribological characteristics of metal matrix composites (MMCs) based on CuAl7 aluminum bronze, reinforced with tungsten (W) and tungsten carbide (WC) particles, produced using electron beam additive manufacturing (EBAM). The aim of the study is to obtain wear-resistant materials based on aluminum bronze with a surface-engineered composite layer of CuAl7–W–WC and to investigate their tribological performance under dry sliding conditions at room and elevated temperatures in air. The authors employed a combined wire–powder feed method, which enabled the fabrication of composite coatings with a uniform distribution of the reinforcing phase. Samples were produced from pure bronze (CuAl7), as well as composites containing 10 vol % (CuAl7–W5–WC5) and 20 vol % (CuAl7–W10–WC10) of reinforcing particles. It was established that the addition of W and WC significantly reduces the wear rate compared to pure bronze, while the friction coefficients of the composites remain comparable to those of the base material. The wear mechanisms of the obtained MMCs were identified as predominantly oxidative, with the formation of a multilayered tribofilm containing copper and iron oxides, acting as a solid lubricant. The presence of reinforcing particles limits direct contact with the counterbody and suppresses plastic deformation of the matrix, thereby enhancing wear resistance. This study demonstrates the potential of EBAM technology for precise surface modification and provides new insights into the wear mechanisms of MMCs under high-temperature sliding conditions. The developed materials can be used in the manufacturing of components with enhanced wear resistance, such as those used in mechanical engineering and aerospace applications.
{"title":"Tribotechnical Characteristics of CuAl7–W–WC Composites Fabricated by Electron Beam Additive Manufacturing","authors":"E. N. Moskvichev, N. N. Shamarin, N. L. Savchenko","doi":"10.3103/S1068366625700576","DOIUrl":"10.3103/S1068366625700576","url":null,"abstract":"<p>This work presents a study on the development and evaluation of the tribological characteristics of metal matrix composites (MMCs) based on CuAl7 aluminum bronze, reinforced with tungsten (W) and tungsten carbide (WC) particles, produced using electron beam additive manufacturing (EBAM). The aim of the study is to obtain wear-resistant materials based on aluminum bronze with a surface-engineered composite layer of CuAl7–W–WC and to investigate their tribological performance under dry sliding conditions at room and elevated temperatures in air. The authors employed a combined wire–powder feed method, which enabled the fabrication of composite coatings with a uniform distribution of the reinforcing phase. Samples were produced from pure bronze (CuAl7), as well as composites containing 10 vol % (CuAl7–W5–WC5) and 20 vol % (CuAl7–W10–WC10) of reinforcing particles. It was established that the addition of W and WC significantly reduces the wear rate compared to pure bronze, while the friction coefficients of the composites remain comparable to those of the base material. The wear mechanisms of the obtained MMCs were identified as predominantly oxidative, with the formation of a multilayered tribofilm containing copper and iron oxides, acting as a solid lubricant. The presence of reinforcing particles limits direct contact with the counterbody and suppresses plastic deformation of the matrix, thereby enhancing wear resistance. This study demonstrates the potential of EBAM technology for precise surface modification and provides new insights into the wear mechanisms of MMCs under high-temperature sliding conditions. The developed materials can be used in the manufacturing of components with enhanced wear resistance, such as those used in mechanical engineering and aerospace applications.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"236 - 241"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027221","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-23DOI: 10.3103/S1068366625700588
A. L. Skorentsev, N. M. Rusin
The structure and tribological properties of sintered Al–40Sn alloy reinforced with Al3Ti particles of different volume concentrations were studied. The composite samples were sintered at 710°C for 1 h and then compacted in a closed die at a temperature of 250°C and a pressure of about 300 MPa. Wear resistance tests were carried out using a Tribotechnic tribotester (France) in the absence of lubrication according to the pin-on-disk scheme at a constant sliding speed of 0.6 m/s, increasing the load every 1000 m of the friction path. A steel disk made of hardened grade 40X steel with a hardness of 48–50 HRC was used as a counterbody. It was found that the concentration of hard particles of ~32% by volume ensures maximum wear resistance of the sintered Al–Al3Ti–Sn samples. A further increase in the content of aluminides up to ~40% by volume leads to the formation of a significant number of brittle contacts between the hard particles, which negatively affects the wear resistance of the studied materials. It was concluded that in order to increase the wear resistance of composites of this system, it is necessary to achieve uniform distribution of hard phase particles around the perimeter of matrix grains. It was found that the wear intensity of Al–Al3Ti–Sn composites increases with increasing pressure on the friction surface, while the value of the friction coefficient decreases and is practically independent of the composition of the studied materials. The wear mechanism of the composite samples of hybrid phase composition under dry friction against a steel disk is considered. The wear process of the composites of this system is carried out by two main mechanisms: deformation-oxidative wear through plastic deformation of a thin surface layer and its embrittlement by small oxide particles, as well as fatigue wear through involvement in deformation by shear of grains of the upper layer of the sample with their subsequent delamination along tin interlayers that have exhausted their plasticity resource.
{"title":"Effect of Titanium Aluminide Particles on Tribological Properties of Al–40Sn Alloy under Dry Friction Against Steel","authors":"A. L. Skorentsev, N. M. Rusin","doi":"10.3103/S1068366625700588","DOIUrl":"10.3103/S1068366625700588","url":null,"abstract":"<p>The structure and tribological properties of sintered Al–40Sn alloy reinforced with Al<sub>3</sub>Ti particles of different volume concentrations were studied. The composite samples were sintered at 710°C for 1 h and then compacted in a closed die at a temperature of 250°C and a pressure of about 300 MPa. Wear resistance tests were carried out using a Tribotechnic tribotester (France) in the absence of lubrication according to the pin-on-disk scheme at a constant sliding speed of 0.6 m/s, increasing the load every 1000 m of the friction path. A steel disk made of hardened grade 40X steel with a hardness of 48–50 HRC was used as a counterbody. It was found that the concentration of hard particles of ~32% by volume ensures maximum wear resistance of the sintered Al–Al<sub>3</sub>Ti–Sn samples. A further increase in the content of aluminides up to ~40% by volume leads to the formation of a significant number of brittle contacts between the hard particles, which negatively affects the wear resistance of the studied materials. It was concluded that in order to increase the wear resistance of composites of this system, it is necessary to achieve uniform distribution of hard phase particles around the perimeter of matrix grains. It was found that the wear intensity of Al–Al<sub>3</sub>Ti–Sn composites increases with increasing pressure on the friction surface, while the value of the friction coefficient decreases and is practically independent of the composition of the studied materials. The wear mechanism of the composite samples of hybrid phase composition under dry friction against a steel disk is considered. The wear process of the composites of this system is carried out by two main mechanisms: deformation-oxidative wear through plastic deformation of a thin surface layer and its embrittlement by small oxide particles, as well as fatigue wear through involvement in deformation by shear of grains of the upper layer of the sample with their subsequent delamination along tin interlayers that have exhausted their plasticity resource.</p>","PeriodicalId":633,"journal":{"name":"Journal of Friction and Wear","volume":"46 4","pages":"242 - 251"},"PeriodicalIF":0.5,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146027222","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}