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2017 IEEE International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale (3M-NANO)最新文献

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Controlled manipulation of TRAIL into single human colon cancer cells using atomic force microscope 利用原子力显微镜控制TRAIL进入单个人结肠癌细胞
Yingmin Qu, Jinyun Liu, Guoliang Wang, Zhengxun Song, Zuobin Wang
In this study, an AFM tip was used to penetrate the human colon cancer cells (SW480) in the culture medium containing pEGFP-N1-TRAIL plasmids. The trail plasmids encoded with the enhanced green fluorescent protein (EGFP) were moved into the SW480 cells through membrane holes created by the AFM probe. Following the penetration, the culture medium was changed into the RPMI1640 medium supplemented with 10% of fetal bovine serum and incubated for 24h. The expression of PEGFP-N1-TRAIL in SW480 cells was then observed by inverted fluorescence microscope. The experiment results indicate that the AFM tip can be used to penetrate the membranes of targeted cells individually.
本研究使用AFM尖端在含有pEGFP-N1-TRAIL质粒的培养基中穿透人结肠癌细胞(SW480)。用增强的绿色荧光蛋白(EGFP)编码的trail质粒通过AFM探针形成的膜孔进入SW480细胞。穿透后,将培养基改为添加10%胎牛血清的RPMI1640培养基,孵育24h。倒置荧光显微镜观察PEGFP-N1-TRAIL在SW480细胞中的表达。实验结果表明,AFM尖端可以单独穿透目标细胞的膜。
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引用次数: 1
Study on wear resistance of micro-pits texture on turning surface 车削表面微坑织构的耐磨性研究
Qianqian Cai, Yiquan Li, Umair Ayub, Zhanjiang Yu, Jinkai Xu, Huadong Yu
Cutting tools with surface micro-textures can effectively improve the wear resistance of the tool and improve cutting conditions. The effects of average output power on the morphology and quality of the micro-textures were analyzed by laser processing technology. The micro-pit diameter was 35μm, 30μm, 25μm, 20μm and non-woven tool on the wear resistance of tool was evaluated. The micro-texture performance was evaluated from tool wear length, width and machined surface roughness. The results show that micro-pore diameter and pit depth increase with increase of laser power. The diameter of the micro-pit has a certain influence on the wear resistance of tool. With decrease of the diameter, the surface roughness of Ti6Al4V alloy is decreasing. When the diameter is less than 25μm, the wear resistance of the tool is weakened and the surface roughness of Ti6Al4V alloy is increasing. Micro-pit texture plays an active role in the friction contact state between blade and chip, adhesion resistance, wear resistance, resistance reduction, storage chip and so on.
具有表面微织构的刀具能有效提高刀具的耐磨性,改善切削条件。采用激光加工技术,分析了平均输出功率对微织构形貌和质量的影响。微坑直径分别为35μm、30μm、25μm、20μm和无纺布刀具对刀具耐磨性的影响进行了评价。从刀具磨损长度、宽度和加工表面粗糙度等方面评价了微织构性能。结果表明:微孔直径和坑深随激光功率的增大而增大;微坑的直径对刀具的耐磨性有一定的影响。随着直径的减小,Ti6Al4V合金的表面粗糙度减小。当直径小于25μm时,刀具的耐磨性减弱,Ti6Al4V合金的表面粗糙度增大。微坑织构在叶片与切屑的摩擦接触状态、抗粘着性、耐磨性、减阻性、储屑性等方面起着积极的作用。
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引用次数: 1
A novel nanokaolinite photocatalyst for degradation of P-nitrophenol 一种新型纳米高岭石光催化剂降解对硝基苯酚
S. El-Sheikh, A. Shawky, Sabrin M. Abdo, Thanaa I. El-Dosoqy, Mohamed Nageeb Rashad
Nanokaolinite photocatalyst was successfully prepared from bulk kaolinite by using simple intercalation-delamination method. The obtained nanokaolinite photocatalysts have been characterized by X-ray diffraction (XRD), FTIR analysis, transmission electron microscope (TEM), and UV-VIS diffuse reflectance spectroscopy (DRS). The XRD revealed that the layers of bulk kaolinite were exfoliated to form nanokaolinite with crystallite size ∼26–32 nm. FTIR spectra showed the presence of nitrogen species between nanokaolinite layers, which lead to decrease of band gap of as-prepared samples as estimated from DRS. The photocatalytic degradation of P-Nitrophenol (PNP) was investigated using the as-prepared nanokaolinite photocatalysts under UV irradiation. The optimum nanokaolinite sample using urea as intercalating agent shows a complete photodegradation of PNP within 30 minutes. This novel nanokaolinite photocatalyst represents an extraordinary alternate for oxide-based photocatalysts.
以大块高岭石为原料,采用简单的插层-分层法制备了纳米高岭石光催化剂。采用x射线衍射(XRD)、红外光谱(FTIR)、透射电子显微镜(TEM)和紫外-可见漫反射光谱(DRS)对制备的纳米高岭石光催化剂进行了表征。XRD分析表明,块状高岭石被剥离形成纳米高岭石,晶粒尺寸为~ 26 ~ 32 nm。FTIR光谱显示,纳米高岭石层间存在氮物质,使得制备样品的带隙减小。研究了制备的纳米高岭石光催化剂在紫外照射下对硝基苯酚(PNP)的光催化降解。以尿素为插层剂的最佳纳米高岭土样品在30分钟内可完全光降解PNP。这种新型纳米高岭石光催化剂代表了氧化物基光催化剂的非凡替代品。
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引用次数: 0
Orthogonal experiment on the preparation of hydrophobic Ti6Al4V surface by WEDM 电火花切割制备疏水Ti6Al4V表面的正交实验
Jinkai Xu, Xuefeng Li, Jingjing Liu, Huadong Yu
The surface roughness of the hydrophobic titanium alloy was obtained by using the electric spark wire cutting (Ti6Al4V) technology. The surface of the titanium alloy was measured and characterized by means of ultra depth of field microscopy, scanning electron microscopy and contact angle measurement. The pulse width, the number of power transistors (peak current) and feed speed parameters were optimized by orthogonal experiment, and the influence of these parameters on the wettability of Ti6Al4V surface was discussed. The results show that when the pulse width is 32μs, the number of the power tube is 4, the feed rate is 50 μm/s, the contact angle of Ti6Al4V is preferably 142 degrees.
采用电火花线切割(Ti6Al4V)技术获得疏水钛合金的表面粗糙度。采用超景深显微镜、扫描电镜和接触角测量等方法对钛合金表面进行了测量和表征。通过正交实验优化了脉冲宽度、功率晶体管数(峰值电流)和馈电速度等参数,并讨论了这些参数对Ti6Al4V表面润湿性的影响。结果表明:当脉冲宽度为32μs,功率管数为4根,进给速率为50 μm/s时,Ti6Al4V的接触角为142°。
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引用次数: 1
Laser micro structuring of composite Li(Ni0.6Mn0.2Co0.2)O2 cathode layersfor lithium-ion batteries 锂离子电池用复合材料Li(Ni0.6Mn0.2Co0.2)O2正极层的激光微结构研究
J. Rakebrandt, Y. Zheng, H. Seifert, P. Smyrek, Wilhelm Pfleging
Lithium-ion batteries (LIB) using lithium nickel manganese cobalt oxide (Li(Nu/3Mn1/3Co1/3)O2, NMC-111) as cathode material have already become one of the most important types of mobile power sources due to their high gravimetric and volumetric capacity. Nevertheless, the automotive industry needs batteries with a further improved energy density to develop electric vehicles (EV) with comparable or even higher range than automobiles with ICE (Internal combustion engine). One approach to enhance the energy density is to increase the nickel content of the NMC cathode material. Therefore, NMC-622 cathodes were produced via tape casting containing 80 wt% of active material with a film thickness of 54 μm. The specific capacities were measured using galvanostatic measurements at different charging/discharging currents for cells with structured and unstructured electrodes. An improved lithium-ion diffusion kinetic due to an increased active surface area could be achieved by laser-assisted generation of three-dimensional architectures. Ultrafast laser ablation was used in order to avoid a thermal-induced damage of the active material. It could be shown that laser structuring of electrode material leads to a significant improvement of the electrochemical performance, especially at high charging and discharging currents.
以锂镍锰钴氧化物(Li(Nu/3Mn1/3Co1/3)O2, NMC-111)为正极材料的锂离子电池(LIB)由于具有较高的重量容量和体积容量,已成为最重要的移动电源类型之一。然而,汽车行业需要进一步提高能量密度的电池来开发与内燃机汽车相当甚至更高续航里程的电动汽车(EV)。提高能量密度的方法之一是提高NMC正极材料的镍含量。因此,NMC-622阴极是通过含有80 wt%活性物质的带铸造生产的,膜厚度为54 μm。在不同的充电/放电电流下,对结构电极和非结构电极的电池进行了恒流测量。由于活性表面积的增加,锂离子扩散动力学的改善可以通过激光辅助生成三维结构来实现。为了避免活性材料的热致损伤,采用了超快激光烧蚀。结果表明,电极材料的激光结构导致电化学性能的显著提高,特别是在高充放电电流下。
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引用次数: 1
Computational simulations of solvation force of water under different hydrophobic interactions 不同疏水相互作用下水溶剂化力的计算模拟
Zhongwu Li, Kun Li, Pinyao He, Kabin Lin, Jingjie Sha, Yunfei Chen
Surfaces in water would bear hydration repulsion or hydrophobic attraction when separation is small. However, the interaction mechanism of hydrophobic surfaces is still unclear though they are very important when the surfaces are in nanometer separation. With molecular dynamics simulations, the solvation force of water molecules between graphene surfaces of different hydrophobicity is analyzed. Important features of the step-like solvation force oscillatory behavior during the compression within a distance of ∼ 1.5 nm indicate that water is squeezed out layer-by-layer. The hydrophobicity of the graphene surfaces is shown to be an important parameter that influences the solvation force of water molecules. We find that the solvation force decreases when the hydrophobicity of the graphene surfaces increases. Detailed analysis of the water density distributions and the water molecule orientation between graphene surfaces show that changing hydrophobicity would influence the water structure. As the graphene surface becomes more hydrophobic, the water molecules become less ordered and the concentration will also decrease to some extent, which can account for the attenuation of the solvation force.
当分离很小时,水中的表面会受到水合排斥或疏水吸引。疏水表面在纳米分离中起着重要作用,但其相互作用机理尚不清楚。通过分子动力学模拟,分析了水分子在不同疏水性石墨烯表面之间的溶剂化力。在约1.5 nm的压缩距离内,阶梯状溶剂化力振荡行为的重要特征表明水被逐层挤出。石墨烯表面的疏水性是影响水分子溶剂化力的重要参数。我们发现,随着石墨烯表面疏水性的增加,溶剂化力减小。对石墨烯表面水密度分布和水分子取向的详细分析表明,改变疏水性会影响水的结构。随着石墨烯表面的疏水性增强,水分子的有序度降低,浓度也会在一定程度上降低,这可以解释溶剂化力的衰减。
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引用次数: 0
Design and test of MEMS gyroscope control system based on LMSD 基于LMSD的MEMS陀螺仪控制系统的设计与测试
Shuai Guo, Xudong Zheng, Yiyu Lin, Wei Ma, Zhong-he Jin
In order to improve the performance of MEMS gyroscopes, the least mean square demodulation (LMSD) algorithm is utilized in MEMS gyroscope control system. By using Matlab tool, the simulation result shows that the LMSD algorithm has better noise suppression performance than multiplicative demodulation (MD). LMSD algorithm is carried out in field-programmed-gate-array (FPGA) and experimental results are in good agreement with the simulation. Combining with automatic gain control (AGC) and phase-locked loop (PLL) technology, the amplitude variance and phase variance of drive mode are respectively 62ppm and 0.001°. The nonlinearity of scale factor based on LMSD algorithm is 0.068%. Moreover, the gyroscope using LMSD exhibits a bias stability (BS) of 1.8°/h and an angle random walk (ARW) of 0.031°/Vh, better than the BS 6.7°/h and ARW 0.114°/Vh using MD. The experiment proves the feasibility and effectiveness of LMSD algorithm in the digital control system of MEMS gyroscope.
为了提高MEMS陀螺仪的性能,将最小均方解调(LMSD)算法应用于MEMS陀螺仪控制系统中。利用Matlab仿真工具,仿真结果表明LMSD算法比乘解调(MD)具有更好的噪声抑制性能。LMSD算法在现场可编程门阵列(FPGA)上实现,实验结果与仿真结果吻合较好。结合自动增益控制(AGC)和锁相环(PLL)技术,驱动模式的幅度方差和相位方差分别为62ppm和0.001°。基于LMSD算法的尺度因子非线性为0.068%。采用LMSD的陀螺仪的偏置稳定性(BS)为1.8°/h,角度随机游走(ARW)为0.031°/Vh,优于采用MD的BS 6.7°/h和ARW 0.114°/Vh,实验证明了LMSD算法在MEMS陀螺仪数字控制系统中的可行性和有效性。
{"title":"Design and test of MEMS gyroscope control system based on LMSD","authors":"Shuai Guo, Xudong Zheng, Yiyu Lin, Wei Ma, Zhong-he Jin","doi":"10.1109/3M-NANO.2017.8286267","DOIUrl":"https://doi.org/10.1109/3M-NANO.2017.8286267","url":null,"abstract":"In order to improve the performance of MEMS gyroscopes, the least mean square demodulation (LMSD) algorithm is utilized in MEMS gyroscope control system. By using Matlab tool, the simulation result shows that the LMSD algorithm has better noise suppression performance than multiplicative demodulation (MD). LMSD algorithm is carried out in field-programmed-gate-array (FPGA) and experimental results are in good agreement with the simulation. Combining with automatic gain control (AGC) and phase-locked loop (PLL) technology, the amplitude variance and phase variance of drive mode are respectively 62ppm and 0.001°. The nonlinearity of scale factor based on LMSD algorithm is 0.068%. Moreover, the gyroscope using LMSD exhibits a bias stability (BS) of 1.8°/h and an angle random walk (ARW) of 0.031°/Vh, better than the BS 6.7°/h and ARW 0.114°/Vh using MD. The experiment proves the feasibility and effectiveness of LMSD algorithm in the digital control system of MEMS gyroscope.","PeriodicalId":6582,"journal":{"name":"2017 IEEE International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale (3M-NANO)","volume":"301 1","pages":"260-263"},"PeriodicalIF":0.0,"publicationDate":"2017-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"79728167","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Automated manipulation of flexible nanowires with an atomic force microscope 用原子力显微镜自动操纵柔性纳米线
Sen Wu, Huitian Bai, Fan Jin
Precise placement of individual nano scale objects is an essential requirement of nanodevices fabrication. Although the recently developed nanomanipulation technology based on Atomic force microscope (AFM) has realized automatic movement of rigid nanoparticles, it was not applicable to nanowires due to the complicated behaviors of flexible one-dimensional material. To improve the efficiency of nanowires manipulation, this work proposes a highly automated manipulation method. The new method allows automatic sample identification and manipulating vectors generation. Image processing techniques such as edge detection, filling and skeleton extraction are performed to identify the nanowires from the AFM images. Once a target position is assigned for the selected nanowire, a series of parallel pushing vectors (PPVs) are generated according to the translation and rotation strategies, which are simulated and optimized using the finite element method. Then the PPVs are continuously executed to transfer the nanowire to the target and make it in a straight shape. For multiple nanowires manipulation, a graph theory method is proposed to sort the movements of the objects. Because no intermediate scanning is needed, the time consumption of complex manipulation is greatly reduced. Experiments are carried out to verify the efficiency of the new method. The translating-rotating combined manipulation of a single silver nanowire proves the high accuracy of the proposed strategies. The successful assembly of two patterns, which are respectively formed by 12 carbon nanofibers and 50 silver nanowires, implies the reliability of the manipulation. Since the present method doesn't require additional hardware, it can be easily integrated to common AFMs.
精确放置单个纳米尺度物体是纳米器件制造的基本要求。近年来发展起来的基于原子力显微镜(AFM)的纳米操作技术虽然实现了刚性纳米粒子的自动运动,但由于柔性一维材料的复杂行为,使其不适用于纳米线。为了提高纳米线的操作效率,本工作提出了一种高度自动化的操作方法。新方法允许自动样本识别和操纵向量生成。采用边缘检测、填充和骨架提取等图像处理技术从原子力显微镜图像中识别纳米线。选定纳米线的目标位置后,根据平移和旋转策略生成一系列平行推进矢量(ppv),并利用有限元法对其进行仿真和优化。然后连续执行ppv以将纳米线转移到目标上并使其呈直线形状。针对多纳米线操作,提出了一种图论方法对物体的运动进行排序。由于不需要中间扫描,因此大大减少了复杂操作的时间消耗。通过实验验证了该方法的有效性。通过对单根银纳米线的平移-旋转组合操作,验证了所提策略的高精度。分别由12根碳纳米纤维和50根银纳米线组成的两种图案的成功组装表明了操作的可靠性。由于目前的方法不需要额外的硬件,它可以很容易地集成到常见的afm中。
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引用次数: 3
A study of functional micro/nano structural surfaces in bionic applications 功能微纳结构表面在仿生中的应用研究
Zhenzhen Xu, L. Kong
Increasing research attentions have been paid to the bionic structures and functional materials in recent years. In order to gain the insights into functional micro/nano-structures and hence form the theoretical basis for design and fabrication of such micro/nano-structural surfaces, this paper conducts a preliminary research study on functional micro/nano structural surfaces. A short review is firstly undertaken for the existing functional micro/nano structures in bionics, and then an analytical model for the Nepenthes Alata's peristome surface is proposed, as an example, which is applicable for production by ultra-precision machining technology. In the short review, existing functional structural surfaces are classified into three categories: structural surfaces with anti-adhesive properties, environmental adaptability structural surfaces, and biological structures with other specific functions. Research work for the above three categories are reviewed: (a) The structural surface with anti-adhesive properties. Super-hydrophobic self-cleaning surface inspired by lotus effect, low friction surface inspired by shark skin, as examples, are introduced and explained. Such structural surfaces have wide and promising applications in the fields of transportation, self-cleaning materials, biomedicine and so on. This has gained intensive interest from research and industry; (b) Environmental adaptability structural surface. The formation mechanism and its application of biological colors with broad military application prospects are reviewed and introduced; (c) Biological structure with specific functions. The latest research progress of insect compound eyes, desert beetle back surface, spider silk, peristome surface of Nepenthes alata and other structures are reviewed in this part. After that, the mechanism of unidirectional liquid spreading without extra energy input on the peristome surface of Nepenthes alata was further investigated, and the structures are also designed to improve the functions based on the existing research which is on the structures of the Nepenthes with one of the typical structures having the function of directional transport without extra power supply. Furthermore, a bionic design model was proposed and the model parameters were analyzed and optimized to achieve better functional performance. Future study for functional micro/nano structural surfaces is also suggested in the end of the paper.
近年来,仿生结构和功能材料的研究受到越来越多的关注。为了深入了解功能性微纳米结构,从而为设计和制造此类微纳米结构表面提供理论基础,本文对功能性微纳米结构表面进行了初步的研究。首先对仿生学中已有的功能微纳结构进行了简要的综述,然后以蜈蚣草(Nepenthes Alata)为例,提出了一种适用于超精密加工技术生产的蜈蚣草(Nepenthes Alata)表面的解析模型。在简要综述中,现有的功能性结构表面可分为三大类:具有抗粘接性能的结构表面、具有环境适应性的结构表面和具有其他特定功能的生物结构表面。对以上三类的研究工作进行了综述:(a)具有抗粘接性能的结构表面。以莲花效应启发的超疏水自洁表面、鲨鱼皮启发的低摩擦表面为例进行了介绍和说明。这种结构表面在交通运输、自洁材料、生物医药等领域有着广阔的应用前景。这引起了研究和工业界的强烈兴趣;(b)环境适应性结构面。综述并介绍了具有广阔军事应用前景的生物色素的形成机理及其应用;(c)具有特定功能的生物结构。综述了昆虫复眼、沙漠甲虫背表面、蜘蛛丝、蜈蚣胃壁表面等结构的最新研究进展。然后,在现有研究的基础上,进一步研究了无额外能量输入的液体在豚草胃壁表面单向扩散的机理,并设计了具有定向输送功能的典型结构,其中一种结构具有无额外能量输入的定向输送功能。在此基础上,提出了仿生设计模型,并对模型参数进行了分析和优化,以获得更好的功能性能。最后对功能性微纳结构表面的未来研究进行了展望。
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引用次数: 1
Experimental characterization of helical propulsion in Newtonian and viscoelastic mediums 牛顿和粘弹性介质中螺旋推进的实验表征
Dalia Mahdy, Abdallah Mohamed, A. Klingner, Ashraf Tammam, A. Wahdan, M. Serry, I. Khalil
This work in vestigates the locomotion of helical robots in a low Reynolds number environment with two different rheological properties. We study the swimming characteristics of the robot during its transition from a Newtonian fluid to a viscoelastic environment. Our experimental results show that the helical robot causes shear thinning in gelatin with intermediate concentration. Therefore, its speed in gelatin is greater than that in silicone oil. The helical robot swims at maximum speed of 0.36 mm/s in silicone oil with viscosity of 5 Pa.s, and 0.22 mm/s, 0.71 mm/s, and 0.94 mm/s in gelatin with concentration of 2%, 3% and 4%, respectively, under the influence of two rotating dipole fields.
本文研究了具有两种不同流变性能的螺旋机器人在低雷诺数环境下的运动。研究了机器人从牛顿流体过渡到粘弹性环境时的游动特性。实验结果表明,在中等浓度的明胶中,螺旋机器人可以引起剪切变薄。因此,其在明胶中的速度大于在硅油中的速度。螺旋机器人在粘度为5 Pa的硅油中以0.36 mm/s的最大速度游动。在两个旋转偶极子场的影响下,在浓度为2%、3%和4%时,凝胶的分子量分别为0.22 mm/ S、0.71 mm/ S和0.94 mm/ S。
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引用次数: 0
期刊
2017 IEEE International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale (3M-NANO)
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