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2017 IEEE International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale (3M-NANO)最新文献

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Study on wear resistance of micro-pits texture on turning surface 车削表面微坑织构的耐磨性研究
Qianqian Cai, Yiquan Li, Umair Ayub, Zhanjiang Yu, Jinkai Xu, Huadong Yu
Cutting tools with surface micro-textures can effectively improve the wear resistance of the tool and improve cutting conditions. The effects of average output power on the morphology and quality of the micro-textures were analyzed by laser processing technology. The micro-pit diameter was 35μm, 30μm, 25μm, 20μm and non-woven tool on the wear resistance of tool was evaluated. The micro-texture performance was evaluated from tool wear length, width and machined surface roughness. The results show that micro-pore diameter and pit depth increase with increase of laser power. The diameter of the micro-pit has a certain influence on the wear resistance of tool. With decrease of the diameter, the surface roughness of Ti6Al4V alloy is decreasing. When the diameter is less than 25μm, the wear resistance of the tool is weakened and the surface roughness of Ti6Al4V alloy is increasing. Micro-pit texture plays an active role in the friction contact state between blade and chip, adhesion resistance, wear resistance, resistance reduction, storage chip and so on.
具有表面微织构的刀具能有效提高刀具的耐磨性,改善切削条件。采用激光加工技术,分析了平均输出功率对微织构形貌和质量的影响。微坑直径分别为35μm、30μm、25μm、20μm和无纺布刀具对刀具耐磨性的影响进行了评价。从刀具磨损长度、宽度和加工表面粗糙度等方面评价了微织构性能。结果表明:微孔直径和坑深随激光功率的增大而增大;微坑的直径对刀具的耐磨性有一定的影响。随着直径的减小,Ti6Al4V合金的表面粗糙度减小。当直径小于25μm时,刀具的耐磨性减弱,Ti6Al4V合金的表面粗糙度增大。微坑织构在叶片与切屑的摩擦接触状态、抗粘着性、耐磨性、减阻性、储屑性等方面起着积极的作用。
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引用次数: 1
A novel nanokaolinite photocatalyst for degradation of P-nitrophenol 一种新型纳米高岭石光催化剂降解对硝基苯酚
S. El-Sheikh, A. Shawky, Sabrin M. Abdo, Thanaa I. El-Dosoqy, Mohamed Nageeb Rashad
Nanokaolinite photocatalyst was successfully prepared from bulk kaolinite by using simple intercalation-delamination method. The obtained nanokaolinite photocatalysts have been characterized by X-ray diffraction (XRD), FTIR analysis, transmission electron microscope (TEM), and UV-VIS diffuse reflectance spectroscopy (DRS). The XRD revealed that the layers of bulk kaolinite were exfoliated to form nanokaolinite with crystallite size ∼26–32 nm. FTIR spectra showed the presence of nitrogen species between nanokaolinite layers, which lead to decrease of band gap of as-prepared samples as estimated from DRS. The photocatalytic degradation of P-Nitrophenol (PNP) was investigated using the as-prepared nanokaolinite photocatalysts under UV irradiation. The optimum nanokaolinite sample using urea as intercalating agent shows a complete photodegradation of PNP within 30 minutes. This novel nanokaolinite photocatalyst represents an extraordinary alternate for oxide-based photocatalysts.
以大块高岭石为原料,采用简单的插层-分层法制备了纳米高岭石光催化剂。采用x射线衍射(XRD)、红外光谱(FTIR)、透射电子显微镜(TEM)和紫外-可见漫反射光谱(DRS)对制备的纳米高岭石光催化剂进行了表征。XRD分析表明,块状高岭石被剥离形成纳米高岭石,晶粒尺寸为~ 26 ~ 32 nm。FTIR光谱显示,纳米高岭石层间存在氮物质,使得制备样品的带隙减小。研究了制备的纳米高岭石光催化剂在紫外照射下对硝基苯酚(PNP)的光催化降解。以尿素为插层剂的最佳纳米高岭土样品在30分钟内可完全光降解PNP。这种新型纳米高岭石光催化剂代表了氧化物基光催化剂的非凡替代品。
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引用次数: 0
Computational simulations of solvation force of water under different hydrophobic interactions 不同疏水相互作用下水溶剂化力的计算模拟
Zhongwu Li, Kun Li, Pinyao He, Kabin Lin, Jingjie Sha, Yunfei Chen
Surfaces in water would bear hydration repulsion or hydrophobic attraction when separation is small. However, the interaction mechanism of hydrophobic surfaces is still unclear though they are very important when the surfaces are in nanometer separation. With molecular dynamics simulations, the solvation force of water molecules between graphene surfaces of different hydrophobicity is analyzed. Important features of the step-like solvation force oscillatory behavior during the compression within a distance of ∼ 1.5 nm indicate that water is squeezed out layer-by-layer. The hydrophobicity of the graphene surfaces is shown to be an important parameter that influences the solvation force of water molecules. We find that the solvation force decreases when the hydrophobicity of the graphene surfaces increases. Detailed analysis of the water density distributions and the water molecule orientation between graphene surfaces show that changing hydrophobicity would influence the water structure. As the graphene surface becomes more hydrophobic, the water molecules become less ordered and the concentration will also decrease to some extent, which can account for the attenuation of the solvation force.
当分离很小时,水中的表面会受到水合排斥或疏水吸引。疏水表面在纳米分离中起着重要作用,但其相互作用机理尚不清楚。通过分子动力学模拟,分析了水分子在不同疏水性石墨烯表面之间的溶剂化力。在约1.5 nm的压缩距离内,阶梯状溶剂化力振荡行为的重要特征表明水被逐层挤出。石墨烯表面的疏水性是影响水分子溶剂化力的重要参数。我们发现,随着石墨烯表面疏水性的增加,溶剂化力减小。对石墨烯表面水密度分布和水分子取向的详细分析表明,改变疏水性会影响水的结构。随着石墨烯表面的疏水性增强,水分子的有序度降低,浓度也会在一定程度上降低,这可以解释溶剂化力的衰减。
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引用次数: 0
Laser micro structuring of composite Li(Ni0.6Mn0.2Co0.2)O2 cathode layersfor lithium-ion batteries 锂离子电池用复合材料Li(Ni0.6Mn0.2Co0.2)O2正极层的激光微结构研究
J. Rakebrandt, Y. Zheng, H. Seifert, P. Smyrek, Wilhelm Pfleging
Lithium-ion batteries (LIB) using lithium nickel manganese cobalt oxide (Li(Nu/3Mn1/3Co1/3)O2, NMC-111) as cathode material have already become one of the most important types of mobile power sources due to their high gravimetric and volumetric capacity. Nevertheless, the automotive industry needs batteries with a further improved energy density to develop electric vehicles (EV) with comparable or even higher range than automobiles with ICE (Internal combustion engine). One approach to enhance the energy density is to increase the nickel content of the NMC cathode material. Therefore, NMC-622 cathodes were produced via tape casting containing 80 wt% of active material with a film thickness of 54 μm. The specific capacities were measured using galvanostatic measurements at different charging/discharging currents for cells with structured and unstructured electrodes. An improved lithium-ion diffusion kinetic due to an increased active surface area could be achieved by laser-assisted generation of three-dimensional architectures. Ultrafast laser ablation was used in order to avoid a thermal-induced damage of the active material. It could be shown that laser structuring of electrode material leads to a significant improvement of the electrochemical performance, especially at high charging and discharging currents.
以锂镍锰钴氧化物(Li(Nu/3Mn1/3Co1/3)O2, NMC-111)为正极材料的锂离子电池(LIB)由于具有较高的重量容量和体积容量,已成为最重要的移动电源类型之一。然而,汽车行业需要进一步提高能量密度的电池来开发与内燃机汽车相当甚至更高续航里程的电动汽车(EV)。提高能量密度的方法之一是提高NMC正极材料的镍含量。因此,NMC-622阴极是通过含有80 wt%活性物质的带铸造生产的,膜厚度为54 μm。在不同的充电/放电电流下,对结构电极和非结构电极的电池进行了恒流测量。由于活性表面积的增加,锂离子扩散动力学的改善可以通过激光辅助生成三维结构来实现。为了避免活性材料的热致损伤,采用了超快激光烧蚀。结果表明,电极材料的激光结构导致电化学性能的显著提高,特别是在高充放电电流下。
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引用次数: 1
An overview on design of homebuilt micro-contact transfer printing machine with easy access to one micron patterning resolution 易于获得1微米图案分辨率的自制微接触转移印花机的设计概述
Yongqiang Deng, Erwei Shang, Yu Liu, Weilian Gao, Yanqiu Chen, C. Bao, Peng Yan, Jin Jiang
A high-precision micro contact transfer printing machine, utilizing cantilever based force feedback control, is homebuilt for a general function in this work. It owns an agile access to control the contact force between the substrate and the printing stamp. The force is on-line processed by a micro controller unit carrying a P (proportional) — controller. The sample stage is installed on the horizontal axis so that the stamp could move from the ink position to the sample position. A real-time image of the press-down progress is shown on the operation interface, running on a personal computer. The printer could be implemented in printing electronics. With the resolution of 0.01N, the force between the stamp and the sample could be loaded precisely and the whole transfer printing process is visible thus it provides a way to take the force under consideration while investigating the mechanism of the transfer printer. Final demonstration on printing of a metallic array with resolution down to 1 micron has been in success.
利用悬臂式力反馈控制的高精度微接触转移印花机是为这项工作的一般功能而自制的。它有一个灵活的通道来控制承印物和印件之间的接触力。该力由带有P(比例)控制器的微控制器在线处理。样品台安装在水平轴上,使印章可以从墨水位置移动到样品位置。在个人电脑上运行的操作界面上显示了按下过程的实时图像。该打印机可应用于印刷电子领域。在0.01N的分辨率下,可以精确地加载邮票与样品之间的力,并且可以看到整个转移打印过程,从而为研究转移打印机的机理提供了一种考虑力的方法。打印分辨率低至1微米的金属阵列的最终演示已经成功。
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引用次数: 1
MEMS electrostatic energy harvesting device with spray coated electret 带有喷涂驻极体的MEMS静电能量收集装置
Anxin Luo, Yixin Xu, Siyan Chen, Hanning Dong, Yulong Zhang, Fei Wang
This paper presents the design and measurement of electrostatic energy harvesting. A spray coated electret based electrostatic energy harvester with out-of-plane gap closing scheme is fabricated using advanced MEMS technology. The size of this device is 13×18 mm2. With the matched resistance of 21 MΩ, an output power of 12 μW is harvested when the resonant frequency is 154 Hz under the acceleration of 28.5 m/s2. The thermal stability of this device is tested on 100 °C, decent power can be output after 34 hours.
本文介绍了静电能量收集的设计与测量。采用先进的微机电系统(MEMS)技术,研制了一种具有面外闭合方案的喷涂驻极体静电能量采集器。该设备的尺寸为13×18 mm2。匹配电阻为21 MΩ时,在28.5 m/s2加速度下,谐振频率为154 Hz,输出功率为12 μW。本装置在100℃的温度下进行热稳定性测试,34小时后可输出良好的功率。
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引用次数: 1
The micro hydrogen sensor chip with low power consumption 低功耗微型氢传感器芯片
Hairong Wang, M. Wang, Xiaowei Chen, B. Han
An integrated micro H2 sensor chip with low power consumption is presented. A pair of interdigitated sensing electrodes, sensing layer and heating electrodes surrounding them were designed on the same layer. To realize low power consumption, the silicon substrate with high thermal conduction was released by wet etching and the 1.3#x03BC;m thick membrane with excellent thermal insulation which consists of Si3N4/SiO2/Si3N4/SiO2 four films, was reserved to support the above structure. Annealing was carried out to reduce the stresses of the films. The stacked TiO2/SnO2 composite materials were used to detect H2 and they had six layers consisting of deposited SnO2 and TiO2 through RF magnetron sputtering in turn. The preparation process of the composite materials was combined with the conventional MEMS process to realize mass production of the wafer-level sensor chips with good consistency. The H2 sensor can work steadily for H2 detection (100–900ppm) at 244 °C with low power consumption as 36mW.
提出了一种集成式低功耗微型氢气传感器芯片。在同一层上设计了一对交错的感应电极、感应层和围绕它们的加热电极。为实现低功耗,采用湿法蚀刻法释放高导热硅衬底,并保留由Si3N4/SiO2/Si3N4/SiO2四层膜组成的1.3#x03BC;m厚、隔热性能优良的膜来支撑上述结构。退火是为了降低薄膜的应力。利用堆叠后的TiO2/SnO2复合材料对H2进行检测,通过射频磁控溅射,该复合材料由沉积的SnO2和TiO2依次组成6层。将复合材料的制备工艺与传统MEMS工艺相结合,实现了具有良好一致性的晶圆级传感器芯片的量产。H2传感器可在244°C下稳定工作(100-900ppm),功耗低至36mW。
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引用次数: 0
Design and test of MEMS gyroscope control system based on LMSD 基于LMSD的MEMS陀螺仪控制系统的设计与测试
Shuai Guo, Xudong Zheng, Yiyu Lin, Wei Ma, Zhong-he Jin
In order to improve the performance of MEMS gyroscopes, the least mean square demodulation (LMSD) algorithm is utilized in MEMS gyroscope control system. By using Matlab tool, the simulation result shows that the LMSD algorithm has better noise suppression performance than multiplicative demodulation (MD). LMSD algorithm is carried out in field-programmed-gate-array (FPGA) and experimental results are in good agreement with the simulation. Combining with automatic gain control (AGC) and phase-locked loop (PLL) technology, the amplitude variance and phase variance of drive mode are respectively 62ppm and 0.001°. The nonlinearity of scale factor based on LMSD algorithm is 0.068%. Moreover, the gyroscope using LMSD exhibits a bias stability (BS) of 1.8°/h and an angle random walk (ARW) of 0.031°/Vh, better than the BS 6.7°/h and ARW 0.114°/Vh using MD. The experiment proves the feasibility and effectiveness of LMSD algorithm in the digital control system of MEMS gyroscope.
为了提高MEMS陀螺仪的性能,将最小均方解调(LMSD)算法应用于MEMS陀螺仪控制系统中。利用Matlab仿真工具,仿真结果表明LMSD算法比乘解调(MD)具有更好的噪声抑制性能。LMSD算法在现场可编程门阵列(FPGA)上实现,实验结果与仿真结果吻合较好。结合自动增益控制(AGC)和锁相环(PLL)技术,驱动模式的幅度方差和相位方差分别为62ppm和0.001°。基于LMSD算法的尺度因子非线性为0.068%。采用LMSD的陀螺仪的偏置稳定性(BS)为1.8°/h,角度随机游走(ARW)为0.031°/Vh,优于采用MD的BS 6.7°/h和ARW 0.114°/Vh,实验证明了LMSD算法在MEMS陀螺仪数字控制系统中的可行性和有效性。
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引用次数: 0
A novel electromagnetic force method for micro/nano newton force measurement 一种用于微纳牛顿力测量的新型电磁力法
Chongkai Zhou, Yanling Tian, Fujun Wang, Zhiyong Guo, Dawei Zhang
Based on the electromagnetic actuator, a novel mechanical system is developed for the measurement of micro/nano newton force, as well as the deformation of the suspension mechanism. The system mainly includes the electromagnetic actuator, flexible suspension mechanism and displacement sensor. A null position measurement method for the suspension mechanism is introduced. The electromagnetic force is theoretically modeled and simulated in ANSYS Maxwell software to optimize the position of the magnet. And then, the suspension mechanism is simulated by Finite Element Analysis (FEA). According to the experimental results, the developed system has a current resolution 1mA, electromagnetic force conversion rate 400μN/mA, the stiffness 27.5N/m.
基于电磁作动器,设计了一种新型的微纳牛顿力测量系统,并对悬挂机构的变形进行了测量。该系统主要包括电磁执行机构、柔性悬架机构和位移传感器。介绍了一种悬架机构零位测量方法。在ANSYS Maxwell软件中对电磁力进行理论建模和仿真,优化磁体的位置。然后,通过有限元分析对悬架机构进行了仿真。实验结果表明,所研制的系统电流分辨率为1mA,电磁力转化率为400μN/mA,刚度27.5N/m。
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引用次数: 0
Growth of single crystal WS2 thin films via atmospheric pressure CVD 常压CVD法生长WS2单晶薄膜
Biao Zhou, Chen-Yi Su, Biao Shi, Yunjiao Wang, Leyong Yu, Shuanglong Feng, Deqiang Wang
Single crystal WS2 film has been paid much more attentions due to its special optical-electrical performance and potential application in the field of biosensor and photodetector in recent years. In this work, we focused on the growth of single crystal WS2 and explored the effect of the position of sulfur and carrier gas flow rate on the nucleation density systematically. The results indicated that the nucleation density of WS2 varies obviously correspond to sulfur position and gas flow, the reasons of the variety on the nucleation density was investigated. Meanwhile, granular and massive WS2 was characterized by an optical microscope, atomic force microscope and Raman spectra.
单晶WS2薄膜由于其特殊的光电性能和在生物传感器、光电探测器等领域的潜在应用,近年来受到了广泛的关注。本文以WS2单晶的生长为研究对象,系统地探讨了硫的位置和载气流速对WS2单晶成核密度的影响。结果表明,WS2的成核密度随硫的位置和气体流量的变化有明显的变化,并探讨了成核密度变化的原因。同时,利用光学显微镜、原子力显微镜和拉曼光谱对颗粒状和块状WS2进行了表征。
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引用次数: 0
期刊
2017 IEEE International Conference on Manipulation, Manufacturing and Measurement on the Nanoscale (3M-NANO)
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