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Resonance Enhancement of Atomic-Scale Friction: Nontrivial Role of Damping 原子尺度摩擦的共振增强:阻尼的重要作用
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-10-14 DOI: 10.1007/s11249-025-02078-w
S. Yu. Krylov

Autoparametric resonance in a combined contact (tip apex)–driving-spring (cantilever) system, that is responsible for the appearance of multiple peaks in friction as a function of scanning velocity, is investigated in a wide range of the possible system damping. The role of cantilever damping, being practically inessential in conventional stick–slip regime at lower velocities, is shown to be crucial for the appearance of friction force peaks at the resonant and quasi-resonant velocities. With changing damping, the evolution of different peaks turns out to be nontrivial, that is related with an unusual manifestation of double slips of the tip and memory effects. Relative value of the main force peaks as functions of damping factor are non-monotonous with maximum, which can reach several tens percent, depending on the system parameters and temperature. Such a strong resonance enhancement of energy dissipation is likely to occur in practical systems, where damping of driving spring can be significant, in contrast to nearly ideal cantilevers used in AFM experiments.

Graphical Abstract

结合接触(尖端)-驱动-弹簧(悬臂)系统的自参数共振,负责出现多峰的摩擦作为扫描速度的函数,研究了在广泛的可能的系统阻尼范围。悬臂阻尼的作用,实际上是不重要的传统粘滑制度在较低的速度,被证明是至关重要的摩擦力峰值的出现在共振和准共振速度。随着阻尼的变化,不同峰的演化变得不平凡,这与尖端双滑移和记忆效应的不寻常表现有关。随着系统参数和温度的变化,主力峰的相对值与阻尼因子的关系不单调,最大可达几十个百分点。与AFM实验中使用的近乎理想的悬臂梁相比,在实际系统中,驱动弹簧的阻尼可能是显著的,因此这种强烈的能量耗散共振增强很可能发生。图形抽象
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引用次数: 0
Analyzing and Predicting Interfacial Frictional States in Soft–Hard Contact via Tangential Displacement–Friction Force Relationships 基于切向位移-摩擦力关系的软硬接触界面摩擦态分析与预测
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-10-03 DOI: 10.1007/s11249-025-02074-0
Jianhua Tang, Zhenglun Wang, Wei Li

The friction behavior between soft and hard materials has long been a crucial research subject in diverse fields, such as artificial joints, human skin contact, and robotic grasping. This study combines theoretical analysis with experimental exploration. By analyzing the variation in friction force and the characteristics of the sliding traces of silicone rubber materials during the entire friction process, it aims to delve into the frictional characteristics of soft–hard material interfaces. The results show that the sliding behavior at the soft–hard interface occurs before the peak of static friction. Through the approximation of a frictional theoretical model, the relationship between the friction force and the relative sliding distance at the interface is verified. Moreover, a method for predicting the interface frictional contact state and the relative sliding distance at the interface based on the friction force–tangential displacement curve is proposed. This research enhances our understanding of the friction mechanism at soft–hard interfaces and offers both theoretical support and practical guidance for the development of fine tactile feedback and dexterous manipulation systems in robotic grasping.

软硬材料之间的摩擦行为一直是人工关节、人体皮肤接触和机器人抓取等多个领域的重要研究课题。本研究将理论分析与实验探索相结合。通过分析硅橡胶材料在整个摩擦过程中摩擦力的变化和滑动轨迹的特征,探讨软硬材料界面的摩擦特性。结果表明:软-硬界面的滑动行为发生在静摩擦峰值之前;通过摩擦理论模型的近似,验证了摩擦力与界面处相对滑动距离的关系。此外,提出了一种基于摩擦力-切向位移曲线预测界面摩擦接触状态和界面相对滑动距离的方法。本研究增强了我们对软硬界面摩擦机理的认识,为机器人抓取中精细触觉反馈和灵巧操作系统的开发提供了理论支持和实践指导。
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引用次数: 0
Effect of Surface Oxidation on Adsorption and Frictional Properties of Oiliness Additives Evaluated by Atomic Force Microscopy 原子力显微镜研究表面氧化对油性添加剂吸附和摩擦性能的影响
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-30 DOI: 10.1007/s11249-025-02069-x
Lin Sun, Naoki Yamashita, Tomoko Hirayama, Kento Mimura, Yoshihiro Ito, Hironobu Nakanishi

A novel methodology using atomic force microscopy (AFM) has been developed for assessing the effect of surface oxidation on the adsorption and frictional properties of oiliness additives. This study focused on comparing the tribological behaviors of ester-based oiliness additives on oxidized versus pure Ti surfaces. The substrates were patterned to facilitate precise AFM-based friction testing. The oxide layer thickness was characterized by X-ray photoelectron spectroscopy and subsequently abraded using a diamond-coated AFM probe to expose the pure Ti surface. Tribological performance under atmospheric conditions was evaluated by comparing frictional properties using ester-based additives of varying ester functionalities, ranging from monoester to tetraester. Adsorption properties were characterized through neutron reflectometry and contact angle measurements. The results demonstrated a clear correlation between adsorption density and friction reduction, with tetraester showing superior performance, especially on pure Ti surfaces. These findings highlight the critical effect of oxidation states and additive molecular structures on frictional properties and adsorption behaviors at nanoscale resolution, providing valuable insights into boundary lubrication mechanisms and lubricant optimization.

本文提出了一种利用原子力显微镜(AFM)评价表面氧化对油性添加剂吸附和摩擦性能影响的新方法。本研究的重点是比较酯基油性添加剂在氧化钛和纯钛表面的摩擦学行为。为了便于精确的afm摩擦测试,对衬底进行了图案化处理。利用x射线光电子能谱对氧化层厚度进行表征,随后使用金刚石涂层AFM探针进行研磨,以暴露纯Ti表面。通过比较不同酯功能的酯基添加剂(从单酯到四酯)的摩擦性能,评估了常压条件下的摩擦学性能。通过中子反射和接触角测量对吸附性能进行了表征。结果表明,吸附密度与摩擦减少之间存在明显的相关性,四酯表现出优异的性能,特别是在纯钛表面上。这些发现强调了氧化态和添加剂分子结构对纳米级摩擦性能和吸附行为的关键影响,为边界润滑机制和润滑剂优化提供了有价值的见解。
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引用次数: 0
In Situ and Ex Situ Analysis of the Reciprocating Sliding Wear Behavior of Cold Sprayed CrMnCoFeNi Cantor HEA Coatings in Dry Air and Ambient Air Conditions 冷喷涂CrMnCoFeNi Cantor HEA涂层在干燥空气和环境空气条件下往复滑动磨损行为的原位和非原位分析
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-30 DOI: 10.1007/s11249-025-02072-2
Maya M. Harfouche, Sima A. Alidokht, Richard R. Chromik

This study examined and compared the tribological properties of a cold-sprayed CrMnCoFeNi high entropy alloy (Cantor alloy) coating under ambient and dry air conditions. Tribological testing was conducted using an in situ tribometer equipped with video microscopy, allowing real-time monitoring of the evolution of the sliding interfaces through a transparent sapphire counterface. This experimental setup provided the opportunity to observe phenomena that would otherwise remain concealed between the contacting bodies. The wear rate was 1.8 ± 0.5 × 10⁻4 mm3/Nm in ambient air and 7.5 ± 0.7 × 10⁻4 mm3/Nm in dry air. In dry air, the velocity accommodation mode was characterized by interfacial sliding of a static transfer film against the wear track, resulting in a stable steady-state coefficient of friction (CoF) of 0.5. In contrast, ambient air conditions led to an average CoF of 0.8, with fluctuations attributed to plastic shearing of the transfer film observed in situ. The higher humidity in ambient air inhibited cold welding of wear particles, resulting in a less stable transfer film that underwent removal or extrusion events, which were associated with sudden drops in CoF. Additionally, a “metal debris” oxide formation mechanism was observed in ambient air, contributing to the formation of a protective tribofilm and a reduction in the wear rate. In dry air, the “oxidation-scrape-reoxidation” mechanism dominated, facilitated by the absence of adsorbed water droplets. This resulted in an increased wear rate under dry conditions.

Graphical Abstract

研究并比较了常温和干燥空气条件下冷喷涂CrMnCoFeNi高熵合金(康托合金)涂层的摩擦学性能。使用配备视频显微镜的原位摩擦计进行摩擦学测试,可以通过透明蓝宝石台面实时监测滑动界面的演变。这个实验装置提供了观察现象的机会,否则将保持隐藏在接触体之间。磨耗率在环境空气中为1.8±0.5 × 10 - 3毫米/毫米,在干燥空气中为7.5±0.7 × 10 - 3毫米/毫米。在干燥空气中,速度调节模式的特征是静态传递膜在磨损轨迹上的界面滑动,导致稳定的稳态摩擦系数(CoF)为0.5。相比之下,环境空气条件导致的平均CoF为0.8,其中波动归因于原位观察到的转移膜的塑性剪切。环境空气中较高的湿度抑制了磨损颗粒的冷焊,导致传递膜不稳定,发生了移除或挤压事件,这与CoF的突然下降有关。此外,在环境空气中观察到“金属碎片”氧化物形成机制,有助于形成保护性摩擦膜并降低磨损率。在干燥空气中,由于没有吸附的水滴,“氧化-刮擦-再氧化”机制占主导地位。这增加了干燥条件下的磨损率。图形抽象
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引用次数: 0
Defining Scuffing Phases via Friction Evolution and Surface Analysis Through Experiments Using Castor Oil Biolubricant 用蓖麻油生物润滑剂通过摩擦演化和表面分析来确定磨损阶段
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-26 DOI: 10.1007/s11249-025-02073-1
R. H. S. Souza, G. Lasch, A. A. Rodrigues, G. S. Gehlen, L. Y. Barros, J. C. Poletto, P. Stradolini, C. L. Petzhold, N. F. Ferreira, P. D. Neis

Scuffing is a severe wear mode that occurs under boundary lubrication. This wear mode remains challenging to predict, and no objective criteria have been established in the literature to characterize the evolution of the phenomenon across the distinct phases of frictional behavior. This study proposes a quantitative method to characterize the three typical scuffing phases (stable, incipient, and severe) based on friction force evolution. Block-on-ring tests were conducted using SAE 52100 steel and two biolubricants: pure castor oil (CO) and aminolyzed castor oil (ACO). A mathematical approach was developed by analyzing the variation of friction force (delta friction) across discretized time intervals. Real-time imaging enabled direct correlation between friction behavior and surface damage. SEM/EDS analyses revealed that the material accumulated during severe scuffing consisted of oxidized oil and steel particles. The dynamic of formation and destruction of these accumulated material explains the observed friction instabilities. The proposed method successfully identified all scuffing phases across tests and was validated by consistent morphological and chemical evidence. ACO significantly increased the time to reach severe scuffing compared to CO, with results confirmed by Weibull statistical analysis. The approach presented herein provides a robust and replicable framework for scuffing characterization and supports the application of chemically modified biolubricants as sustainable alternatives with enhanced tribological performance.

磨损是在边界润滑下发生的一种严重磨损模式。这种磨损模式的预测仍然具有挑战性,并且在文献中没有建立客观的标准来描述这种现象在摩擦行为的不同阶段的演变。本研究提出了一种基于摩擦力演化的定量方法来表征三个典型磨损阶段(稳定阶段、初期阶段和严重阶段)。采用SAE 52100钢和两种生物润滑剂(纯蓖麻油(CO)和氨基水解蓖麻油(ACO))进行了环块试验。通过分析摩擦力(δ摩擦力)在离散时间间隔上的变化,提出了一种数学方法。实时成像可以将摩擦行为与表面损伤直接联系起来。SEM/EDS分析表明,在严重磨损过程中积累的物质由氧化油和钢颗粒组成。这些累积物质的形成和破坏的动力学解释了观察到的摩擦不稳定性。该方法成功地识别了所有磨损阶段,并通过一致的形态和化学证据进行了验证。与CO相比,ACO显著增加了达到严重磨损的时间,Weibull统计分析证实了这一结果。本文提出的方法为磨损表征提供了一个可靠且可复制的框架,并支持化学改性生物润滑剂作为具有增强摩擦学性能的可持续替代品的应用。
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引用次数: 0
Research on Fractal Modeling of Hard-Coated Rough Surface Contact Considering the Mechanism of Elastic–Plastic Deformation 考虑弹塑性变形机理的硬质涂层粗糙表面接触分形建模研究
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-25 DOI: 10.1007/s11249-025-02071-3
Yizhang Lian, Xueliang Zhang, Nanshan Wang, Yonghui Chen, Shanjun Liao

This study develops an elastoplastic fractal contact model for rough hard-coated surfaces along, with a corresponding contact stiffness model based, on a coated asperity contact model and a statistical rough surface contact model. To establish the contact stiffness model for the coated surface asperities, seven fundamental postulates were developed. Numerical simulations were conducted to systematically analyze the influence of the ratio between the coating thickness and the asperity radius, the material properties of the coating and the substrate, and the substrate surface roughness on the contact behavior and stiffness of the coated surfaces. The results demonstrate that under a given load, hard-coated rough surfaces exhibit a smaller real contact area but higher stiffness compared to uncoated surfaces. Thicker and stiffer coatings further reduce the contact area while increasing stiffness. Smoother substrate surfaces lead to a larger contact area and higher stiffness in the coated systems. These findings align with the existing statistical contact models for hard-coated rough surfaces, and the predicted contact area closely matches the prior simulation results. To validate the model, experimental tests were conducted on the TiN-coated specimens. The theoretically predicted contact stiffness showed strong agreement with the experimental measurements, confirming the accuracy and applicability of the proposed fractal-based stiffness model.

本研究建立了粗糙硬涂层表面的弹塑性分形接触模型,并在此基础上建立了相应的接触刚度模型。为了建立涂层表面凹凸不平的接触刚度模型,提出了7个基本假设。通过数值模拟,系统分析了涂层厚度与粗糙度半径之比、涂层与基体的材料性能、基体表面粗糙度对涂层表面接触行为和刚度的影响。结果表明,在给定载荷下,硬涂层粗糙表面的实际接触面积比未涂层表面小,但刚度更高。更厚和更硬的涂层进一步减少了接触面积,同时增加了刚度。更光滑的基材表面导致涂层系统中更大的接触面积和更高的刚度。这些发现与现有硬涂层粗糙表面的统计接触模型一致,预测的接触面积与先前的模拟结果非常吻合。为了验证模型的有效性,对镀锡试样进行了实验测试。理论预测的接触刚度与实验测量结果吻合较好,验证了分形刚度模型的准确性和适用性。
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引用次数: 0
Sliding Friction of Hard Sliders on Rubber: Theory and Experiment 硬滑块在橡胶上的滑动摩擦:理论与实验
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-17 DOI: 10.1007/s11249-025-02064-2
R. Xu, B. N. J. Persson

We present a study of sliding friction for rigid triangular steel sliders on soft rubber substrates under both lubricated and dry conditions. For rubber surfaces lubricated with a thin film of silicone oil, the measured sliding friction at room temperature agrees well with theoretical predictions obtained from a viscoelastic model originally developed for rolling friction. On the lubricated surface, the sliding friction is primarily due to bulk viscoelastic energy dissipation in the rubber. The model, which includes strain-dependent softening of the rubber modulus, accurately predicts the experimental friction curves. At lower temperatures ((T = -20^circ textrm{C}) and (-40^circ textrm{C})), the measured friction exceeds the theoretical prediction. We attribute this increase to penetration of the lubricant film by surface asperities, leading to a larger adhesive contribution. For dry surfaces, the adhesive contribution becomes dominant. By subtracting the viscoelastic component inferred from the lubricated case, we estimate the interfacial frictional shear stress. This shear stress increases approximately linearly with the logarithm of the sliding speed, consistent with stress-augmented thermal activation mechanisms.

我们提出了在润滑和干燥条件下软橡胶基板上的刚性三角形钢滑块滑动摩擦的研究。对于用硅油薄膜润滑的橡胶表面,在室温下测量的滑动摩擦与最初为滚动摩擦开发的粘弹性模型的理论预测吻合得很好。在润滑表面,滑动摩擦主要是由于橡胶中的大块粘弹性能量耗散。该模型考虑了橡胶模量随应变的软化,能够准确地预测实验摩擦曲线。在较低的温度下((T = -20^circ textrm{C})和(-40^circ textrm{C})),测量的摩擦超过理论预测。我们将这种增加归因于表面凸起对润滑膜的渗透,从而导致更大的粘合剂贡献。对于干燥的表面,粘合剂的贡献成为主导。通过减去从润滑情况推断的粘弹性分量,我们估计了界面摩擦剪应力。剪切应力随滑动速度的对数近似线性增加,与应力增强热激活机制一致。
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引用次数: 0
Achieving Ultra-Low Friction in Ti-6Al-4 V Alloy: Hydration Lubrication Mechanisms of HEC-Glycerol Composite 在ti - 6al - 4v合金中实现超低摩擦:hec -甘油复合材料的水化润滑机制
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-17 DOI: 10.1007/s11249-025-02068-y
Dezun Sheng, Hongliang Yu, Xiao Zhang, Xin Zhou

Reducing alloy friction to achieve ultra-low friction is a valuable approach to save energy and reduce pollution from oil use, which is a major challenge for researchers. This study introduces a successful method to achieve ultra-low friction in Ti-6Al-4 V using a hydrated lubricant composed of hydroxyethyl cellulose (HEC). And the effects of speed and concentration on lubricating were investigated. It was found that excessive sliding speeds may lead to lubricant detachment and consequent friction increase, indicating that the adsorption ability of HEC needs to be enhanced in future studies. In addition, when the concentration exceeds 5 wt%, wear loss tends to stabilize across tests with different concentrations, while the friction force increases with rising concentrations. Based on these findings, microscopic studies were conducted to investigate the mechanism of friction reduction. Notably, distinct topographic features resembling ‘valleys’ and ‘plateaus’ were identified on the wear scars in a nanoscale scope. The movement of the surfaces induces the hydrated HEC lubricant to flow from the lower valleys to the higher plateaus, suggesting elastohydrodynamic lubrication mechanisms to form robust films. The valleys serve as lubricant reservoirs, while the plateau tops support the lubricant films to prevent contacts between Ti-6Al-4 V and Si3N4. The schematic illustrations depict the microscopic mechanisms for achieving of ultra-low friction on Ti-6Al-4 V alloy.

降低合金摩擦以实现超低摩擦是一种有价值的节能和减少石油污染的方法,也是研究人员面临的主要挑战。本研究介绍了一种利用由羟乙基纤维素(HEC)组成的水合润滑剂在ti - 6al - 4v中实现超低摩擦的成功方法。考察了转速和浓度对润滑性能的影响。研究发现,过大的滑动速度可能导致润滑油脱离,从而导致摩擦增加,这表明HEC的吸附能力需要在未来的研究中得到加强。此外,当浓度超过5wt %时,不同浓度下的磨损量趋于稳定,而摩擦力随浓度的增加而增加。基于这些发现,进行了微观研究,以探讨摩擦减少的机制。值得注意的是,在纳米尺度范围内,在磨损痕上发现了类似“山谷”和“高原”的独特地形特征。表面的运动诱导水合HEC润滑剂从较低的山谷流向较高的高原,表明弹性流体动力润滑机制形成坚固的膜。山谷作为润滑剂储层,而高原顶部支撑润滑膜,防止ti - 6al - 4v和Si3N4接触。原理图描述了ti - 6al - 4v合金实现超低摩擦的微观机理。
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引用次数: 0
Laser-Induced Fluorescence (LIF) Method-Based Research on the Influence of Textured Water-Lubricated UHMWPE Bearing Tribological Performance 基于激光诱导荧光(LIF)方法的织构水润滑超高分子量聚乙烯轴承摩擦学性能影响研究
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-12 DOI: 10.1007/s11249-025-02070-4
Haixian Song, Haideng Mu, Dequan Zhu, Quan Zheng, Fuming Kuang

The surface texturing of water-lubricated ultra-high molecular weight polyethylene (UHMWPE) bearing has the advantages of enhancing the hydrodynamic effect, capturing wear debris, reducing secondary friction, and storing water, and is one of the research hotspots in tribology. However, the influence of the surface texture of water-lubricated UHMWPE bearing on the friction performance of bearing is still unclear. Based on the laser induced fluorescence (LIF) method, this study developed an in situ-visualization observation system for water film on the friction interface of non-metallic bearing with the help of transparent glass friction pair. The typical textures with different area ratios, aspect ratios and distribution angles were used as the research objects. The water film thickness, friction coefficient and surface morphology of the friction interface of UHMWPE bearing with different textures under low-speed and heavy-load conditions were analyzed. The results show that elongated textures with a reasonable area ratio and length-to-width ratio, arranged along the direction of friction, are more likely to form hydrodynamic effects and create strong support points at the friction interface. Additionally, the divergent and convergent spaces formed at the inlet and outlet of the textured units cause the lubrication pressure at the inlet to be lower than that at the outlet, resulting in severer wear at the inlet compared to the outlet. The overall trends and the mechanism discussed in this research may be considered as a guideline for the design and optimization of surface texture of water-lubricated UHMWPE bearing.

水润滑超高分子量聚乙烯(UHMWPE)轴承的表面织构具有增强流体动力效应、捕获磨损碎屑、减少二次摩擦、储水等优点,是摩擦学领域的研究热点之一。然而,水润滑UHMWPE轴承表面织构对轴承摩擦性能的影响尚不清楚。基于激光诱导荧光(LIF)方法,研制了一种基于透明玻璃摩擦副的非金属轴承摩擦界面水膜的现场可视化观测系统。以不同面积比、纵横比和分布角度的典型纹理为研究对象。分析了低速和重载条件下不同质地超高分子量聚乙烯轴承摩擦界面的水膜厚度、摩擦系数和表面形貌。结果表明:沿摩擦方向排列具有合理面积比和长宽比的细长织构更容易形成水动力效应,并在摩擦界面处形成强支撑点;此外,在织构单元的进出口处形成发散和收敛的空间,导致进口处的润滑压力低于出口处的润滑压力,导致进口处的磨损比出口处严重。本文研究的总体趋势和机理可为水润滑超高分子量聚乙烯轴承表面织构的设计和优化提供指导。
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引用次数: 0
Effects of High-Temperature Annealing on the Frictional Properties of Graphene 高温退火对石墨烯摩擦性能的影响
IF 3.3 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2025-09-11 DOI: 10.1007/s11249-025-02065-1
Wenjie He, Yu Zhang, Qiang He, Wen Wang

Due to the high surface-to-volume ratio, micro/nano-electromechanical systems (MEMS/NEMS) undergo severe wear during the relative sliding. Graphene, possessing excellent mechanical, physical, and chemical properties, can achieve an ultralow friction and wear state, making it highly promising for significantly minimizing friction and wear in MEMS/NEMS. However, graphene films used in MEMS/NEMS are typically subjected to thermal annealing pretreatment during the fabrication process. To maintain optimal performance, it is particularly necessary to investigate the evolution of graphene tribological properties after high-temperature annealing. In this article, by performing nanoscale atomic force microscopy (AFM) measurements on mechanically exfoliated graphene, we reveal that the friction force on graphene decreases slightly upon annealing to approximately 200 °C, then gradually increases before rising rapidly once the annealing temperature exceeds 500 °C. Raman spectroscopy identifies that the changes in friction result from the annealing-induced compressive stress accumulation and defects creation. Our results provide deep insights for the application of graphene in sliding MEMS/NEMS.

Graphical Abstract

由于高表面体积比,微/纳米机电系统(MEMS/NEMS)在相对滑动过程中会遭受严重的磨损。石墨烯具有优异的机械、物理和化学性能,可以实现超低摩擦和磨损状态,在MEMS/NEMS中具有极大的应用前景。然而,用于MEMS/NEMS的石墨烯薄膜通常在制造过程中进行热退火预处理。为了保持最佳性能,研究石墨烯高温退火后摩擦学性能的演变尤为必要。在本文中,通过对机械剥离的石墨烯进行纳米尺度原子力显微镜(AFM)测量,我们发现石墨烯上的摩擦力在退火至约200℃时略有下降,然后逐渐增加,一旦退火温度超过500℃时迅速上升。拉曼光谱分析表明,摩擦的变化是由退火引起的压应力积累和缺陷产生引起的。我们的研究结果为石墨烯在滑动MEMS/NEMS中的应用提供了深刻的见解。图形抽象
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引用次数: 0
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