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Correction: Study on precise weld diameter validations by comparing destructive testing methods in resistance spot welding 更正:通过比较电阻点焊中的破坏性测试方法验证精确焊缝直径的研究
IF 2.1 4区 材料科学 Q2 Materials Science Pub Date : 2024-04-24 DOI: 10.1007/s40194-024-01778-6
Christian Mathiszik, Johannes Koal, Jörg Zschetzsche, Uwe Füssel, Hans Christian Schmale
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引用次数: 0
The microstructure and wear behavior of WC-reinforced diamond composite coating WC 增强金刚石复合涂层的微观结构和磨损行为
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-24 DOI: 10.1007/s40194-024-01769-7
Qilong Wu, Weimin Long, Lei Zhang, Chenying Zhu

Herein, diamond and diamond/WC composite coating were deposited on the surface of 45 steel by induction brazing. The microstructures of the composite coating were studied by scanning electron microscope, energy dispersive spectrometer, and X-ray diffractometer, and the wear resistance of the composite coating was assessed by rubber wheel abrasion test. The microstructure investigation indicates that both Cr3C2 and Cr7C3 carbides are formed at the interface between the diamond and BNi-2 alloy matrix, and Ni2W4C and NiW was formed at the interface between WC and BNi-2 alloy matrix. When WC is added to the diamond coating, the microhardness of the BNi-2 alloy matrix increases, and the microhardness of the BNi-2 alloy matrix reaches 583 HV0.2, which is 7.6% higher than that of the coating without WC. In addition, after 120 min wear test, the wear loss of the diamond WC composite coating is 0.337g, which is reduced by 31.5%. In the wear tests, abrasive wear was the main wear mechanism for composite coating. WC particles in diamond/WC composite coating improved the wear resistance and hardness of the alloy matrix.

Graphical Abstract

本文通过感应钎焊在 45 钢表面沉积了金刚石和金刚石/WC 复合涂层。通过扫描电子显微镜、能量色散光谱仪和 X 射线衍射仪研究了复合涂层的微观结构,并通过橡胶轮磨损试验评估了复合涂层的耐磨性。微观结构研究表明,在金刚石和 BNi-2 合金基体的界面上形成了 Cr3C2 和 Cr7C3 碳化物,在 WC 和 BNi-2 合金基体的界面上形成了 Ni2W4C 和 NiW。在金刚石涂层中加入 WC 后,BNi-2 合金基体的显微硬度增加,BNi-2 合金基体的显微硬度达到 583 HV0.2,比未加入 WC 的涂层高 7.6%。此外,经过 120 分钟的磨损试验后,金刚石 WC 复合涂层的磨损损耗为 0.337g,降低了 31.5%。在磨损试验中,磨料磨损是复合涂层的主要磨损机制。金刚石/WC 复合涂层中的 WC 颗粒提高了合金基体的耐磨性和硬度。
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引用次数: 0
Ti–Zr–Cu–Co–Fe amorphous/nanocrystalline brazing filler metals for joining Ti-6Al-4V alloy 用于连接 Ti-6Al-4V 合金的 Ti-Zr-Cu-Co-Fe 非晶/纳米晶钎焊填充金属
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-23 DOI: 10.1007/s40194-024-01776-8
Rao Peng, Yan Si, Huyang Li, Xueyin Bai, Shujie Pang, Huaping Xiong, Tao Zhang

A novel Ti50Zr30Cu8Co7Fe5 (at.%) amorphous/nanocrystalline brazing filler metal (BFM) with low Cu content and low liquidus temperature (1154 K) was developed and prepared into a flexible ribbon by melt-spinning for brazing Ti-6Al-4V (Ti64) alloy. The effects of vacuum brazing temperature and holding time on the microstructure and mechanical properties of the joints were investigated. For the joint brazed at a low brazing temperature of 1173 K for 15 min, a messy segregated layer consisted of α-Ti, β-Ti, and Ti2Cu intermetallic compound was formed in the center of the braze zone, resulting in relatively low tensile shear strength (~ 310 MPa) of the joint. With the brazing temperature increasing up to 1233 K, the joints exhibited uniform Widmanstätten structure mainly consisting of acicular α-Ti, β-Ti, and sporadic Ti2Cu intermetallic compound without segregated layer. The Ti64 joint brazed at 1233 K for 15 min possesses an improved tensile shear strength of ~ 400 MPa. By extending the holding time to 30 min and 45 min at the brazing temperature of 1233 K, the amount of Ti2Cu intermetallic compound in the braze zone decreased, leading to the high strength of the joints up to ~ 446 and ~ 491 MPa, respectively.

开发了一种新型 Ti50Zr30Cu8Co7Fe5 (at.%)非晶/纳米晶钎焊填充金属 (BFM),具有低铜含量和低液相温度 (1154 K),并通过熔融纺丝制备成柔性带状,用于钎焊 Ti-6Al-4V (Ti64)合金。研究了真空钎焊温度和保温时间对接头微观结构和机械性能的影响。对于在 1173 K 低钎焊温度下钎焊 15 分钟的接头,钎焊区中心形成了由α-Ti、β-Ti 和 Ti2Cu 金属间化合物组成的杂乱偏析层,导致接头的拉伸剪切强度相对较低(~ 310 MPa)。随着钎焊温度升高至 1233 K,接头呈现出均匀的 Widmanstätten 结构,主要由针状的 α-Ti、β-Ti 和零星的 Ti2Cu 金属间化合物组成,没有偏析层。在 1233 K 下钎焊 15 分钟的 Ti64 接头的拉伸剪切强度提高了约 400 兆帕。在 1233 K 的钎焊温度下将保温时间延长至 30 分钟和 45 分钟后,钎焊区中 Ti2Cu 金属间化合物的数量减少,从而使接头的强度分别达到 ~ 446 MPa 和 ~ 491 MPa。
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引用次数: 0
Microstructure and hydrogen embrittlement of Q690 bainitic steel welded using electron beam 使用电子束焊接 Q690 贝氏体钢的微观结构和氢脆现象
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-23 DOI: 10.1007/s40194-024-01770-0
Pengcong Yang, Kuijun Fu, Yumin Wu, Jiaji Wang, Fengya Hu, Yulai Song

This investigation focused on the welding of Q690 bainitic steel using vacuum electron beam welding with currents of 350 and 500 mA, yielding samples with diverse microstructures and distinct fusion and heat-affected zones. Additionally, H2S immersion tests were conducted to evaluate the susceptibility of the welded microstructure to hydrogen embrittlement. The results indicated different fracture sites in the samples welded under currents of 350 and 500 mA. Under the 350-mA welding current, fracture occurred in the coarse-grain heat-affected zone (CGHAZ) because of the high dislocation density in the bainitic ferrite plates and the low concentration of retained austenite in the CGHAZ. Under the 500-mA current, hydrogen embrittlement and fracture occurred in the upper bainite of the fusion zone because of the high welding-induced heat input that led to coarse precipitation and micro-void coalescence.

这项研究的重点是使用电流分别为 350 mA 和 500 mA 的真空电子束焊接 Q690 贝氏体钢,焊接出的样品具有不同的微观结构以及明显的熔合区和热影响区。此外,还进行了 H2S 浸入试验,以评估焊接微观结构对氢脆的敏感性。结果表明,在 350 mA 和 500 mA 电流下焊接的样品具有不同的断裂部位。在 350 毫安的焊接电流下,断裂发生在粗晶粒热影响区(CGHAZ),这是因为贝氏体铁素体板中的位错密度高,而 CGHAZ 中保留奥氏体的浓度低。在 500 mA 电流下,熔合区上部贝氏体发生氢脆和断裂,原因是高焊接诱导热输入导致粗大析出和微空洞凝聚。
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引用次数: 0
Fatigue and failure behaviour of friction welded steel joints under normal and shear stresses 摩擦焊接钢接头在法向应力和剪切应力作用下的疲劳和失效行为
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-22 DOI: 10.1007/s40194-024-01774-w
Jörg Baumgartner, Lorenz Uhlenberg, Frank Trommer, Ann-Christin Hesse, Markus Köhler, Klaus Dilger

Rotary friction welding is a fast and efficient joining process with the possibility to join materials that are not weldable by conventional GMAW-processes. If done properly, the welds have a static and fatigue strength higher than the base material. However, in literature, there exists only sparse information on the design and assessment of these joints in terms of fatigue. The fatigue strength of two material combinations, S355-S355 and S355-1.4301, is investigated based on two specimen conditions, (1) with flash and (2) with flash mechanically removed. In the majority of tests, failure occurred outside the weld zone, in the base material. The derived endurable nominal stresses are compared to the design S-N curve of conventionally welded specimens and show a more than 50% higher fatigue strength.

旋转摩擦焊是一种快速高效的焊接工艺,可以焊接传统 GMAW 工艺无法焊接的材料。如果操作得当,焊缝的静态强度和疲劳强度均高于母材。然而,在文献中,关于这些接头的疲劳设计和评估的信息很少。本文基于两种试样条件(1)带闪光和(2)机械去除闪光,对 S355-S355 和 S355-1.4301 这两种材料组合的疲劳强度进行了研究。在大多数试验中,失效发生在焊接区之外的母材中。得出的耐久名义应力与传统焊接试样的设计 S-N 曲线进行了比较,结果表明疲劳强度提高了 50%以上。
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引用次数: 0
Fatigue life evaluation of welded joints under multiaxial loading for different stress concepts using an extended Gough-Pollard criterion 使用扩展的戈夫-波拉德准则评估不同应力概念下多轴载荷焊接接头的疲劳寿命
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-17 DOI: 10.1007/s40194-024-01716-6
N. M. Bauer, J. Baumgartner, M. Fass

Fatigue life evaluation of welded joints under multiaxial loading usually refers to stresses normal to the weld and shear stresses. Stresses parallel to the weld are not considered in most experiments or the well-known Gough-Pollard criterion. Hence, the Gough-Pollard criterion has recently been extended to include all stress components at the weld surface. In this paper, both the original and, for the first time, the extended Gough-Pollard criterion are applied to different welded specimens under multiaxial loading that includes stresses parallel to the weld. As shown, the original criterion is insufficient to evaluate such stress states. This is because the calculated fatigue life becomes less conservative as the stresses parallel to the weld become more significant. The extended criterion, on the other hand, shows greatly improved accuracy while significantly reducing the likelihood of non-conservative results. In conclusion, the extended Gough-Pollard criterion can describe fatigue life under multiaxial loading better than the original version and provides reliable and conservative results for welded joints. The main findings are valid for the nominal, the hot spot, and the notch stress concept.

多轴载荷下焊接接头的疲劳寿命评估通常是指焊缝的法向应力和剪切应力。大多数实验或著名的 Gough-Pollard 准则都没有考虑平行于焊缝的应力。因此,最近对 Gough-Pollard 准则进行了扩展,以包括焊缝表面的所有应力成分。在本文中,原始的 Gough-Pollard 准则和扩展的 Gough-Pollard 准则首次被应用于多轴载荷(包括平行于焊缝的应力)下的不同焊接试样。结果表明,原始准则不足以评估这种应力状态。这是因为当平行于焊缝的应力变得越来越大时,计算出的疲劳寿命就会变得不那么保守。而扩展准则则大大提高了准确性,同时显著降低了出现非保守结果的可能性。总之,扩展的 Gough-Pollard 准则能比原始版本更好地描述多轴载荷下的疲劳寿命,并为焊接接头提供可靠而保守的结果。主要结论适用于标称应力、热点应力和缺口应力概念。
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引用次数: 0
Effect of copper interlayer in dissimilar TA6V/AU4G rotary friction weld joints 铜夹层对异种 TA6V/AU4G 旋转摩擦焊焊点的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-12 DOI: 10.1007/s40194-024-01771-z
Houssem Eddine Lakache, Abdelghani May, Riad Badji, Nathalie Poirot, Slimane Nasre Eddine Reguieg Yssaad

Welding titanium to aluminum alloys is difficult and challenging due to the differences in their chemical and physical properties. The aim of this research is to investigate the effect of integrating a pure copper (Cu) interlayer on the mechanical behavior and the microstructure of the dissimilar TA6V/AU4G Rotary Friction Weld (RFW) joints. Tensile tests and microhardness measurements were conducted to demonstrate the mechanical behavior of the RFW joints. Microscopic observations were carried out to identify the structural nuances and quality of the weld joint. Energy Dispersive X-Ray (EDX) analysis was performed to reveal the interdiffusion phenomenon at the weld interfaces, and the present phases were identified through X-Ray Diffraction (XRD) analysis. The results suggest that adding a Cu-interlayer changes the flow direction of thermoplastically deformed material, leading to an increase in the Ultimate Tensile Strength (UTS) value up to 393.34 MPa. The microhardness profile of the TA6V/Cu/AU4G RFW joint is similar to that of the TA6V/AU4G joint, except for noticeable difference at the interface. In addition, the use of a Cu-interlayer has been shown to be more effective in preventing the formation of brittle TiAl3 intermetallic compounds (IMCs) compared to direct TA6V/AU4G welds. The inclusion of a Cu-interlayer results in a significant improvement in joint efficiency by 105.32%, demonstrating the effectiveness of the Cu-interlayer in enhancing the mechanical properties of the dissimilar TA6V/AU4G RFW joints.

由于钛和铝合金的化学和物理性质不同,因此将它们焊接在一起是一件困难而又具有挑战性的事情。本研究的目的是探讨加入纯铜 (Cu) 中间膜对异种 TA6V/AU4G 旋转摩擦焊 (RFW) 接头的机械性能和微观结构的影响。为证明 RFW 接头的机械性能,进行了拉伸试验和显微硬度测量。还进行了显微观察,以确定焊点的结构细微差别和质量。进行了能量色散 X 射线 (EDX) 分析,以揭示焊接界面的相互扩散现象,并通过 X 射线衍射 (XRD) 分析确定了存在的相。结果表明,添加铜夹层改变了热塑性变形材料的流动方向,导致极限拉伸强度 (UTS) 值增加到 393.34 兆帕。TA6V/Cu/AU4G RFW 接头的显微硬度曲线与 TA6V/AU4G 接头相似,只是在界面处有明显差异。此外,与 TA6V/AU4G 直接焊接相比,使用 Cu 夹层能更有效地防止形成脆性的 TiAl3 金属间化合物 (IMC)。加入铜中间膜后,接头效率显著提高了 105.32%,证明了铜中间膜在提高异种 TA6V/AU4G 射频焊接接头机械性能方面的有效性。
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引用次数: 0
Effect of filler paste’s mixing ratio on the properties of Al-64430 dip-brazed joints 填充膏混合比对 Al-64430 浸辫接头性能的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-11 DOI: 10.1007/s40194-024-01772-y
Siddharth Garg, Qasim Murtaza

This study compares the paste/slurry formed by different filler mixing ratios (filler metal powder: DM water [wt.%/wt.%]) used to fabricate dip-brazed joints for Al-64430. Eight different filler ratios were selected, namely 1:5, 1:4, 1:3, 1:2, 1:1, 5:4, 2:1 and 3:1. The fabricated samples were tested for bump test, microhardness, tensile strength and surface deformation. Maximum microhardness and tensile strength were observed at a 5:4 mixing ratio. Both the values increased until the 5:4 mixing ratio (450% increase in microhardness and a 5400% increase in tensile strength compared to a 1:4 mixing ratio sample), after which they declined (3% decrease in microhardness and a 35% decrease in tensile strength). Surface deformation of the samples remained almost constant throughout, although these values were 10–20 times less than those of samples produced by conventional welding operations. Microstructural analysis revealed dendrite formation at the brazed joints. Voids and cracks were also detected in some samples. Al-Si eutectic matrix and (alpha)-aluminium were visible at the joint. SEM analysis was carried out to determine the silicon state in the matrix, which displayed the presence of both primary and eutectic silicon. EDX analysis showed that the silicon concentration at the joint increased as the filler ratio increased, and this silicon concentration played a major role in determining the strength and hardness of the joints.

本研究比较了不同填料混合比(填料金属粉末:DM 水 [重量百分比/重量百分比])形成的浆料/泥浆,用于制造 Al-64430 的浸钎焊接点。选择了八种不同的填料比例,即 1:5、1:4、1:3、1:2、1:1、5:4、2:1 和 3:1。对制作的样品进行了凹凸测试、显微硬度、拉伸强度和表面变形测试。在混合比例为 5:4 时,微硬度和拉伸强度达到最大值。与混合比为 1:4 的样品相比,这两个值在混合比为 5:4 之前一直在增加(显微硬度增加了 450%,拉伸强度增加了 5400%),之后则有所下降(显微硬度下降了 3%,拉伸强度下降了 35%)。样品的表面变形在整个过程中几乎保持不变,尽管这些数值比传统焊接工艺生产的样品小 10-20 倍。微观结构分析表明,钎焊接头处形成了枝晶。在一些样品中还发现了空洞和裂缝。接合处可见铝硅共晶基体和铝(α)。为确定基体中的硅状态,进行了扫描电镜分析,结果显示存在原生硅和共晶硅。EDX 分析表明,接头处的硅浓度随着填料比率的增加而增加,这种硅浓度在决定接头的强度和硬度方面起着重要作用。
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引用次数: 0
Microstructure and mechanical properties of laser-MIG hybrid multi-layer welded joints for 20-mm thick aluminum alloy plates 20 毫米厚铝合金板激光-MIG 混合多层焊接接头的微观结构和力学性能
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-11 DOI: 10.1007/s40194-024-01773-x
Zhibin Yang, Likang Sheng, Yanqi Xie

Laser-MIG hybrid multi-layer welding was performed upon the 20-mm thick 6082-T6 aluminum alloy butt-joints. The weld formation, microstructure, and mechanical properties of the welded joints were studied in details. The results indicated that the well-formed weld without obvious incomplete fusion and cracks could be obtained by using the optimal welding parameters, only very few porosities appeared in the filling layer and covering layer. The equiaxed crystals and columnar crystals were respectively observed in the weld center and near the fusion in the weld metal; their sizes and widths of each layer were different. The microhardness values of the weld metal and heat-affected zone are lower than those of the base metal; the lowest microhardness value appeared in the heat affected zone. The order of microhardness values in the weld center from high to low was filling layer, backing layer, and covering layer; their microhardness values were 74 HV, 70 HV, and 67 HV, respectively. The average tensile strength of the joints reached up to 235.2 MPa, which was 79.7% of the base metal. The tensile specimen fractured near the fusion line in the heat affected zone and the fracture propagated approximately parallel to the fusion line, and the tensile fracture showed a typical plastic fracture mode. The median fatigue limit and safety fatigue limit of the welded joints were 99 MPa and 93 MPa, respectively. The fatigue specimen fractured in the weld metal, and the crack initiated in the backing layer.

对 20 毫米厚的 6082-T6 铝合金对接接头进行了激光-MIG 混合多层焊接。详细研究了焊接接头的焊缝成形、显微组织和机械性能。结果表明,采用最佳焊接参数可获得成形良好的焊缝,无明显的不完全熔合和裂纹,只有极少数气孔出现在填充层和覆盖层中。在焊缝中心和焊缝金属熔合处附近分别观察到等轴晶粒和柱状晶粒,各层晶粒的大小和宽度不同。焊缝金属和热影响区的显微硬度值均低于母材;热影响区的显微硬度值最低。焊缝中心的显微硬度值从高到低的顺序为填充层、背衬层和覆盖层,其显微硬度值分别为 74 HV、70 HV 和 67 HV。接头的平均抗拉强度达到 235.2 兆帕,是母材的 79.7%。拉伸试样在热影响区熔合线附近断裂,断口大致平行于熔合线扩展,拉伸断口呈现典型的塑性断裂模式。焊接接头的中值疲劳极限和安全疲劳极限分别为 99 兆帕和 93 兆帕。疲劳试样在焊接金属中断裂,裂纹从背衬层开始。
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引用次数: 0
Correction: Multi-objective optimization of laser welding parameters for steel/Al based on Kriging-MSSA 更正:基于 Kriging-MSSA 的钢/铝激光焊接参数的多目标优化
IF 2.1 4区 材料科学 Q2 Materials Science Pub Date : 2024-04-11 DOI: 10.1007/s40194-024-01768-8
Zhi-wei Zhu, Yong-huan Guo, Xin-ran Zhang, Xiang-ning Lu, Jun-yi Hua
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引用次数: 0
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Welding in the World
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