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Microstructure and hydrogen embrittlement of Q690 bainitic steel welded using electron beam 使用电子束焊接 Q690 贝氏体钢的微观结构和氢脆现象
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-23 DOI: 10.1007/s40194-024-01770-0
Pengcong Yang, Kuijun Fu, Yumin Wu, Jiaji Wang, Fengya Hu, Yulai Song

This investigation focused on the welding of Q690 bainitic steel using vacuum electron beam welding with currents of 350 and 500 mA, yielding samples with diverse microstructures and distinct fusion and heat-affected zones. Additionally, H2S immersion tests were conducted to evaluate the susceptibility of the welded microstructure to hydrogen embrittlement. The results indicated different fracture sites in the samples welded under currents of 350 and 500 mA. Under the 350-mA welding current, fracture occurred in the coarse-grain heat-affected zone (CGHAZ) because of the high dislocation density in the bainitic ferrite plates and the low concentration of retained austenite in the CGHAZ. Under the 500-mA current, hydrogen embrittlement and fracture occurred in the upper bainite of the fusion zone because of the high welding-induced heat input that led to coarse precipitation and micro-void coalescence.

这项研究的重点是使用电流分别为 350 mA 和 500 mA 的真空电子束焊接 Q690 贝氏体钢,焊接出的样品具有不同的微观结构以及明显的熔合区和热影响区。此外,还进行了 H2S 浸入试验,以评估焊接微观结构对氢脆的敏感性。结果表明,在 350 mA 和 500 mA 电流下焊接的样品具有不同的断裂部位。在 350 毫安的焊接电流下,断裂发生在粗晶粒热影响区(CGHAZ),这是因为贝氏体铁素体板中的位错密度高,而 CGHAZ 中保留奥氏体的浓度低。在 500 mA 电流下,熔合区上部贝氏体发生氢脆和断裂,原因是高焊接诱导热输入导致粗大析出和微空洞凝聚。
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引用次数: 0
Fatigue and failure behaviour of friction welded steel joints under normal and shear stresses 摩擦焊接钢接头在法向应力和剪切应力作用下的疲劳和失效行为
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-22 DOI: 10.1007/s40194-024-01774-w
Jörg Baumgartner, Lorenz Uhlenberg, Frank Trommer, Ann-Christin Hesse, Markus Köhler, Klaus Dilger

Rotary friction welding is a fast and efficient joining process with the possibility to join materials that are not weldable by conventional GMAW-processes. If done properly, the welds have a static and fatigue strength higher than the base material. However, in literature, there exists only sparse information on the design and assessment of these joints in terms of fatigue. The fatigue strength of two material combinations, S355-S355 and S355-1.4301, is investigated based on two specimen conditions, (1) with flash and (2) with flash mechanically removed. In the majority of tests, failure occurred outside the weld zone, in the base material. The derived endurable nominal stresses are compared to the design S-N curve of conventionally welded specimens and show a more than 50% higher fatigue strength.

旋转摩擦焊是一种快速高效的焊接工艺,可以焊接传统 GMAW 工艺无法焊接的材料。如果操作得当,焊缝的静态强度和疲劳强度均高于母材。然而,在文献中,关于这些接头的疲劳设计和评估的信息很少。本文基于两种试样条件(1)带闪光和(2)机械去除闪光,对 S355-S355 和 S355-1.4301 这两种材料组合的疲劳强度进行了研究。在大多数试验中,失效发生在焊接区之外的母材中。得出的耐久名义应力与传统焊接试样的设计 S-N 曲线进行了比较,结果表明疲劳强度提高了 50%以上。
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引用次数: 0
Fatigue life evaluation of welded joints under multiaxial loading for different stress concepts using an extended Gough-Pollard criterion 使用扩展的戈夫-波拉德准则评估不同应力概念下多轴载荷焊接接头的疲劳寿命
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-17 DOI: 10.1007/s40194-024-01716-6
N. M. Bauer, J. Baumgartner, M. Fass

Fatigue life evaluation of welded joints under multiaxial loading usually refers to stresses normal to the weld and shear stresses. Stresses parallel to the weld are not considered in most experiments or the well-known Gough-Pollard criterion. Hence, the Gough-Pollard criterion has recently been extended to include all stress components at the weld surface. In this paper, both the original and, for the first time, the extended Gough-Pollard criterion are applied to different welded specimens under multiaxial loading that includes stresses parallel to the weld. As shown, the original criterion is insufficient to evaluate such stress states. This is because the calculated fatigue life becomes less conservative as the stresses parallel to the weld become more significant. The extended criterion, on the other hand, shows greatly improved accuracy while significantly reducing the likelihood of non-conservative results. In conclusion, the extended Gough-Pollard criterion can describe fatigue life under multiaxial loading better than the original version and provides reliable and conservative results for welded joints. The main findings are valid for the nominal, the hot spot, and the notch stress concept.

多轴载荷下焊接接头的疲劳寿命评估通常是指焊缝的法向应力和剪切应力。大多数实验或著名的 Gough-Pollard 准则都没有考虑平行于焊缝的应力。因此,最近对 Gough-Pollard 准则进行了扩展,以包括焊缝表面的所有应力成分。在本文中,原始的 Gough-Pollard 准则和扩展的 Gough-Pollard 准则首次被应用于多轴载荷(包括平行于焊缝的应力)下的不同焊接试样。结果表明,原始准则不足以评估这种应力状态。这是因为当平行于焊缝的应力变得越来越大时,计算出的疲劳寿命就会变得不那么保守。而扩展准则则大大提高了准确性,同时显著降低了出现非保守结果的可能性。总之,扩展的 Gough-Pollard 准则能比原始版本更好地描述多轴载荷下的疲劳寿命,并为焊接接头提供可靠而保守的结果。主要结论适用于标称应力、热点应力和缺口应力概念。
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引用次数: 0
Effect of copper interlayer in dissimilar TA6V/AU4G rotary friction weld joints 铜夹层对异种 TA6V/AU4G 旋转摩擦焊焊点的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-12 DOI: 10.1007/s40194-024-01771-z
Houssem Eddine Lakache, Abdelghani May, Riad Badji, Nathalie Poirot, Slimane Nasre Eddine Reguieg Yssaad

Welding titanium to aluminum alloys is difficult and challenging due to the differences in their chemical and physical properties. The aim of this research is to investigate the effect of integrating a pure copper (Cu) interlayer on the mechanical behavior and the microstructure of the dissimilar TA6V/AU4G Rotary Friction Weld (RFW) joints. Tensile tests and microhardness measurements were conducted to demonstrate the mechanical behavior of the RFW joints. Microscopic observations were carried out to identify the structural nuances and quality of the weld joint. Energy Dispersive X-Ray (EDX) analysis was performed to reveal the interdiffusion phenomenon at the weld interfaces, and the present phases were identified through X-Ray Diffraction (XRD) analysis. The results suggest that adding a Cu-interlayer changes the flow direction of thermoplastically deformed material, leading to an increase in the Ultimate Tensile Strength (UTS) value up to 393.34 MPa. The microhardness profile of the TA6V/Cu/AU4G RFW joint is similar to that of the TA6V/AU4G joint, except for noticeable difference at the interface. In addition, the use of a Cu-interlayer has been shown to be more effective in preventing the formation of brittle TiAl3 intermetallic compounds (IMCs) compared to direct TA6V/AU4G welds. The inclusion of a Cu-interlayer results in a significant improvement in joint efficiency by 105.32%, demonstrating the effectiveness of the Cu-interlayer in enhancing the mechanical properties of the dissimilar TA6V/AU4G RFW joints.

由于钛和铝合金的化学和物理性质不同,因此将它们焊接在一起是一件困难而又具有挑战性的事情。本研究的目的是探讨加入纯铜 (Cu) 中间膜对异种 TA6V/AU4G 旋转摩擦焊 (RFW) 接头的机械性能和微观结构的影响。为证明 RFW 接头的机械性能,进行了拉伸试验和显微硬度测量。还进行了显微观察,以确定焊点的结构细微差别和质量。进行了能量色散 X 射线 (EDX) 分析,以揭示焊接界面的相互扩散现象,并通过 X 射线衍射 (XRD) 分析确定了存在的相。结果表明,添加铜夹层改变了热塑性变形材料的流动方向,导致极限拉伸强度 (UTS) 值增加到 393.34 兆帕。TA6V/Cu/AU4G RFW 接头的显微硬度曲线与 TA6V/AU4G 接头相似,只是在界面处有明显差异。此外,与 TA6V/AU4G 直接焊接相比,使用 Cu 夹层能更有效地防止形成脆性的 TiAl3 金属间化合物 (IMC)。加入铜中间膜后,接头效率显著提高了 105.32%,证明了铜中间膜在提高异种 TA6V/AU4G 射频焊接接头机械性能方面的有效性。
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引用次数: 0
Effect of filler paste’s mixing ratio on the properties of Al-64430 dip-brazed joints 填充膏混合比对 Al-64430 浸辫接头性能的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-11 DOI: 10.1007/s40194-024-01772-y
Siddharth Garg, Qasim Murtaza

This study compares the paste/slurry formed by different filler mixing ratios (filler metal powder: DM water [wt.%/wt.%]) used to fabricate dip-brazed joints for Al-64430. Eight different filler ratios were selected, namely 1:5, 1:4, 1:3, 1:2, 1:1, 5:4, 2:1 and 3:1. The fabricated samples were tested for bump test, microhardness, tensile strength and surface deformation. Maximum microhardness and tensile strength were observed at a 5:4 mixing ratio. Both the values increased until the 5:4 mixing ratio (450% increase in microhardness and a 5400% increase in tensile strength compared to a 1:4 mixing ratio sample), after which they declined (3% decrease in microhardness and a 35% decrease in tensile strength). Surface deformation of the samples remained almost constant throughout, although these values were 10–20 times less than those of samples produced by conventional welding operations. Microstructural analysis revealed dendrite formation at the brazed joints. Voids and cracks were also detected in some samples. Al-Si eutectic matrix and (alpha)-aluminium were visible at the joint. SEM analysis was carried out to determine the silicon state in the matrix, which displayed the presence of both primary and eutectic silicon. EDX analysis showed that the silicon concentration at the joint increased as the filler ratio increased, and this silicon concentration played a major role in determining the strength and hardness of the joints.

本研究比较了不同填料混合比(填料金属粉末:DM 水 [重量百分比/重量百分比])形成的浆料/泥浆,用于制造 Al-64430 的浸钎焊接点。选择了八种不同的填料比例,即 1:5、1:4、1:3、1:2、1:1、5:4、2:1 和 3:1。对制作的样品进行了凹凸测试、显微硬度、拉伸强度和表面变形测试。在混合比例为 5:4 时,微硬度和拉伸强度达到最大值。与混合比为 1:4 的样品相比,这两个值在混合比为 5:4 之前一直在增加(显微硬度增加了 450%,拉伸强度增加了 5400%),之后则有所下降(显微硬度下降了 3%,拉伸强度下降了 35%)。样品的表面变形在整个过程中几乎保持不变,尽管这些数值比传统焊接工艺生产的样品小 10-20 倍。微观结构分析表明,钎焊接头处形成了枝晶。在一些样品中还发现了空洞和裂缝。接合处可见铝硅共晶基体和铝(α)。为确定基体中的硅状态,进行了扫描电镜分析,结果显示存在原生硅和共晶硅。EDX 分析表明,接头处的硅浓度随着填料比率的增加而增加,这种硅浓度在决定接头的强度和硬度方面起着重要作用。
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引用次数: 0
Microstructure and mechanical properties of laser-MIG hybrid multi-layer welded joints for 20-mm thick aluminum alloy plates 20 毫米厚铝合金板激光-MIG 混合多层焊接接头的微观结构和力学性能
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-11 DOI: 10.1007/s40194-024-01773-x
Zhibin Yang, Likang Sheng, Yanqi Xie

Laser-MIG hybrid multi-layer welding was performed upon the 20-mm thick 6082-T6 aluminum alloy butt-joints. The weld formation, microstructure, and mechanical properties of the welded joints were studied in details. The results indicated that the well-formed weld without obvious incomplete fusion and cracks could be obtained by using the optimal welding parameters, only very few porosities appeared in the filling layer and covering layer. The equiaxed crystals and columnar crystals were respectively observed in the weld center and near the fusion in the weld metal; their sizes and widths of each layer were different. The microhardness values of the weld metal and heat-affected zone are lower than those of the base metal; the lowest microhardness value appeared in the heat affected zone. The order of microhardness values in the weld center from high to low was filling layer, backing layer, and covering layer; their microhardness values were 74 HV, 70 HV, and 67 HV, respectively. The average tensile strength of the joints reached up to 235.2 MPa, which was 79.7% of the base metal. The tensile specimen fractured near the fusion line in the heat affected zone and the fracture propagated approximately parallel to the fusion line, and the tensile fracture showed a typical plastic fracture mode. The median fatigue limit and safety fatigue limit of the welded joints were 99 MPa and 93 MPa, respectively. The fatigue specimen fractured in the weld metal, and the crack initiated in the backing layer.

对 20 毫米厚的 6082-T6 铝合金对接接头进行了激光-MIG 混合多层焊接。详细研究了焊接接头的焊缝成形、显微组织和机械性能。结果表明,采用最佳焊接参数可获得成形良好的焊缝,无明显的不完全熔合和裂纹,只有极少数气孔出现在填充层和覆盖层中。在焊缝中心和焊缝金属熔合处附近分别观察到等轴晶粒和柱状晶粒,各层晶粒的大小和宽度不同。焊缝金属和热影响区的显微硬度值均低于母材;热影响区的显微硬度值最低。焊缝中心的显微硬度值从高到低的顺序为填充层、背衬层和覆盖层,其显微硬度值分别为 74 HV、70 HV 和 67 HV。接头的平均抗拉强度达到 235.2 兆帕,是母材的 79.7%。拉伸试样在热影响区熔合线附近断裂,断口大致平行于熔合线扩展,拉伸断口呈现典型的塑性断裂模式。焊接接头的中值疲劳极限和安全疲劳极限分别为 99 兆帕和 93 兆帕。疲劳试样在焊接金属中断裂,裂纹从背衬层开始。
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引用次数: 0
Correction: Multi-objective optimization of laser welding parameters for steel/Al based on Kriging-MSSA 更正:基于 Kriging-MSSA 的钢/铝激光焊接参数的多目标优化
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-11 DOI: 10.1007/s40194-024-01768-8
Zhi-wei Zhu, Yong-huan Guo, Xin-ran Zhang, Xiang-ning Lu, Jun-yi Hua
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引用次数: 0
Influence of magnetic head structure and parameters on the axial magnetic field hybrid TIG welding 磁头结构和参数对轴向磁场混合氩弧焊的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-09 DOI: 10.1007/s40194-024-01763-z
H. Wu, Y. L. Chang, C. H. Chang

Through the analysis of the magnetic field around the arc, the feasibility of controlling the arc shape and performance by the external axial magnetic field is clarified. Combined with the derived mathematical expression of the alternating axial magnetic field generated by the energized solenoid, the magnetic field and its distribution were simulated with COMSOL Multiphysics and MATLAB software, and the effects of the magnetic head structure and parameters on the magnetic field and its distribution were determined. A magnetic head was designed and manufactured according to the simulation results, and the welding process experiments were carried out. The experimental results show that the high-frequency axial magnetic field can significantly compress the arc and improve the welding penetration.

通过对电弧周围磁场的分析,阐明了通过外部轴向磁场控制电弧形状和性能的可行性。结合通电螺线管产生的交变轴向磁场的数学表达式,利用 COMSOL Multiphysics 和 MATLAB 软件对磁场及其分布进行了仿真,确定了磁头结构和参数对磁场及其分布的影响。根据仿真结果设计并制造了磁头,并进行了焊接工艺实验。实验结果表明,高频轴向磁场能显著压缩电弧,提高焊接穿透力。
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引用次数: 0
Effect of appropriate vibration frequency on microstructure and properties of laser cladding Co-based self-lubricating composite coatings 适当的振动频率对激光熔覆钴基自润滑复合涂层微观结构和性能的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-09 DOI: 10.1007/s40194-024-01767-9
Lianjie Bi, Hua Yan, Peilei Zhang, Qinghua Lu, Haichuan Shi, Zhiyuan Li

CrS/NbC reinforced Co-based self-lubricating composite coatings were successfully prepared on the surface of Cr12MoV steel by high-frequency micro-vibration (HFMV) assisted laser cladding technology. The microstructure, phase composition, microhardness, and wear resistance of the composite coatings were studied by means of X-ray diffractometer (XRD), scanning electron microscope (SEM), energy dispersive spectrometer (EDS), microhardness tester, and friction-wear tester. The results show that there were excellent metallurgical bonding and free of pores and cracks in the CrS/NbC Co-based self-lubricating composite coating with 10% WS2 prepared by laser cladding at 552 Hz vibration frequency. The appropriate vibration frequency could cause strong convection in the molten pool and refine the microstructure, which made NbC hard particulates and CrS lubricants to be evenly distributed in the composite coating. In particular, the refined CrS and NbC in the upper area of the coating were combined with each other to form a dense network microstructure. Moreover, the hardness of the coating prepared at the vibration frequency of 552 Hz was significantly improved due to its excellent microstructure compared with the without vibration and 985 Hz vibration frequencies and the maximum hardness reached 652.8 HV0.5. Its wear resistance was also significantly improved, and the friction coefficient of the coating was reduced to 0.451. Only abrasive wear and slight adhesive wear were observed on the coatings surface, and the tearing layer and wear loss of grinding defects were significantly reduced.

通过高频微振动(HFMV)辅助激光熔覆技术在 Cr12MoV 钢表面成功制备了 CrS/NbC 增强 Co 基自润滑复合镀层。通过 X 射线衍射仪 (XRD)、扫描电子显微镜 (SEM)、能量色散光谱仪 (EDS)、显微硬度计和摩擦磨损试验机研究了复合涂层的微观结构、相组成、显微硬度和耐磨性。结果表明,在 552 Hz 振动频率下,通过激光熔覆制备的含 10% WS2 的 CrS/NbC Co 基自润滑复合涂层具有良好的冶金结合力,且无孔隙和裂纹。适当的振动频率能使熔池中产生强烈对流,细化微观结构,从而使 NbC 硬颗粒和 CrS 润滑剂均匀分布在复合涂层中。特别是在涂层上部区域,细化的 CrS 和 NbC 相互结合,形成了致密的网状微结构。此外,与无振动和 985 Hz 振动频率相比,在 552 Hz 振动频率下制备的涂层因其优异的微观结构而显著提高了硬度,最大硬度达到 652.8 HV0.5。涂层的耐磨性也得到明显改善,摩擦系数降至 0.451。涂层表面只出现了磨料磨损和轻微的粘着磨损,磨削缺陷的撕裂层和磨损损耗明显减少。
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引用次数: 0
Enabling magnetic pulse welding for dissimilar tubular arrester cable joints 为异种管状避雷器电缆接头实现磁脉冲焊接
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-04-08 DOI: 10.1007/s40194-024-01760-2
M. Graß, N. Sommer, S. Böhm

Climate change exacerbates the need for resource-efficient and cost-effective production processes across manifold industries, including the field of electrical connections. This specific field is characterized by a conflict of objectives, i.e., weight reductions while maintaining joint strength and electrical conductivity. From a material point of view, the use of aluminum as a conductor material is suitable for this application, as it is lighter than copper, a classical conductor material. Electrical conductors are often used in the form of flexible cables, so-called stranded wires. This type of conductor as well as the fact that the sole use of aluminum in electrical systems is not feasible, e.g., because the predetermined connection terminals of power electronic components are made of copper, creates a substantial demand for dissimilar aluminum-copper cable arrester joints. However, traditional fusion-based welding processes have proved incapable of reliably producing these dissimilar aluminum-copper joints because of thermophysical effects and chemical incompatibilities, the latter eventually leading to the formation of intermetallic phases. These phases adversely affect the quality of the joint in terms of both mechanical and electrical performance. Yet, magnetic pulse welding, a pressure welding process, is ideally suited for producing dissimilar metal joints on the basis of a low energy input during the welding process. Consequently, the formation of intermetallic phases is restrained. However, magnetic pulse welding has not been sufficiently investigated for the reliable contacting of stranded cables to tubular arresters. As a result, this paper focuses on the fabrication of tubular stranded cable arrester joints using magnetic pulse welding. To shed light on possible material combinations, aluminum-to-aluminum and copper-to-copper joints as well as their dissimilar counterparts are welded. Subsequently, the joints are characterized with regard to their microstructure and quasi-static material strength. Electrical characterization comprises the four-wire Kelvin measurement method to evaluate the resistance of the electrical joints. The results demonstrate that magnetic pulse welding is ideally suited to join the aforementioned material combination and joint configuration due to its process characteristics eventually leading to material continuity. As a result, the stranded wires are welded to the tubular arresters rather than crimped. Consequently, a comparative analysis of the joint properties with those of the joining partners shows that the measured electrical resistances and mechanical tensile forces may be considered very good.

气候变化加剧了各行各业对资源节约型和成本效益型生产工艺的需求,其中包括电气连接领域。这一特定领域的特点是目标冲突,即在保持连接强度和导电性的同时减轻重量。从材料的角度来看,使用铝作为导体材料非常适合这一应用,因为铝比传统导体材料铜更轻。导体通常以柔性电缆的形式使用,即所谓的绞合导线。这种导体类型以及在电气系统中仅使用铝是不可行的,例如,由于电力电子元件的预定连接端子是由铜制成的,因此对异种铝铜电缆避雷器接头的需求量很大。然而,由于热物理效应和化学不相容性(后者最终会导致金属间相的形成),传统的熔融焊接工艺已被证明无法可靠地生产这些异种铝铜接头。这些金属相会对接头的机械和电气性能产生不利影响。然而,磁脉冲焊接是一种压力焊接工艺,在焊接过程中能量输入低,非常适合生产异种金属接头。因此,金属间相的形成受到限制。然而,对于将绞合电缆与管状避雷器可靠连接的问题,磁脉冲焊接尚未得到充分研究。因此,本文重点讨论了利用磁脉冲焊接制造管状绞合电缆避雷器接头的问题。为了揭示可能的材料组合,我们焊接了铝对铝、铜对铜以及它们的异种材料。随后,对接头的微观结构和准静态材料强度进行表征。电气特性分析包括采用四线开尔文测量法评估电气接头的电阻。结果表明,磁脉冲焊接由于其工艺特点,非常适合连接上述材料组合和接头结构,最终实现材料的连续性。因此,绞线是焊接到管状避雷器上的,而不是压接。因此,对接头特性和连接伙伴的特性进行比较分析后发现,测量到的电阻和机械拉力都非常好。
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引用次数: 0
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Welding in the World
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