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The effect of adhesive and adherend compliance on the failure of 3D-printed parts 胶粘剂和粘附体顺应性对3d打印零件失效的影响
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-17 DOI: 10.1007/s40194-025-02048-9
Özkan Öz, Fatih Huzeyfe Öztürk

The present study deals with the adhesive selection for extrusion-based 3D-printed parts. The compatibility of acrylate (AC), polyurethane (PU), methyl methacrylate (MM) and epoxy (EP) adhesives with polylactic acid (PLA), polyethylene terephthalate glycol (PETG), acrylonitrile butadiene styrene (ABS), and acrylonitrile styrene acrylate (ASA) adherends was investigated. Tensile tests were conducted to provide enhanced knowledge on the failure behavior of these joints. Taguchi L16 orthogonal array and analysis of variance (ANOVA) were used to the design of experiment (DOE) and to identify the contribution of each parameter on the response, respectively. In addition, a closed-form solution of critical stress (peel and shear stresses) distributions along the bondline was used to gain a better insight into the failure mechanism of joints considered in this study. The ANOVA results showed that the effect of adhesive type is clearly the most important factor influencing the joint strength, followed by the adherend type. Statistically, the contribution of the adherend type (5.28%) is also important, but it is smaller than the contribution of the adhesive type (91.60%). The highest joint strength was obtained for PETG bonded with MM adhesive. In the case of PU, EP, and AC adhesives, the maximum load-carrying capacity was reached using PLA adherends. ASA showed the lowest joint strength for all adhesive types. This research provides comprehensive knowledge, allowing designers to select an appropriate adhesive for custom or industrial bonding applications without time-consuming surface treatments.

本研究涉及基于挤压的3d打印部件的粘合剂选择。研究了丙烯酸酯(AC)、聚氨酯(PU)、甲基丙烯酸甲酯(MM)和环氧树脂(EP)胶粘剂与聚乳酸(PLA)、聚对苯二甲酸乙二醇酯(PETG)、丙烯腈-丁二烯-苯乙烯(ABS)和丙烯腈-苯乙烯-丙烯酸酯(ASA)胶粘剂的相容性。进行拉伸试验是为了更好地了解这些接头的破坏行为。采用田口L16正交试验设计(DOE)和方差分析(ANOVA)分别确定各参数对响应的贡献。此外,为了更好地了解本研究中所考虑的接头的破坏机制,采用了沿结合线的临界应力(剥离应力和剪切应力)分布的封闭解。方差分析结果表明,粘结剂类型是影响接头强度的最重要因素,其次是粘结剂类型。统计上,粘附型的贡献(5.28%)也很重要,但小于粘附型的贡献(91.60%)。PETG与MM胶粘剂的结合强度最高。在PU, EP和AC胶粘剂的情况下,使用PLA胶粘剂达到最大承载能力。ASA显示所有胶粘剂类型的接头强度最低。这项研究提供了全面的知识,允许设计人员为定制或工业粘合应用选择合适的粘合剂,而无需耗时的表面处理。
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引用次数: 0
Impact of beam oscillation and power modulation on the intermixing behavior of dissimilar titanium/niobium/nitinol joints during micro electron beam welding 电子束振荡和功率调制对微细电子束焊接中不同钛/铌/镍钛诺接头混合行为的影响
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-16 DOI: 10.1007/s40194-025-02039-w
Michael Wiegand, Johannes-Seneca Loose, Martin Kahlmeyer, Wenwen Song, Stefan Böhm

The present study seeks to expand the knowledge on dissimilar fusion welding of the material combination NiTi/Nb/Ti by investigating micro electron beam welding in a butt-joint configuration. In addition to adapted power modulation, a novel approach of utilizing the process-inherent fast beam oscillation is applied to improve the melting and intermixing behavior of the comparatively high-melting Nb filler material. Two different Nb thicknesses, measuring 0.2 and 0.4 mm, are implemented and compared with regard to weldability and microstructural evolution in the weld metal. It is demonstrated that the welding experiments are associated with major challenges due to the considerable differences in melting temperature and thermal conductivity of the base and filler materials, resulting in inhomogeneous elemental distribution and welding defects. Nevertheless, the welded joints exhibit excellent mechanical properties under quasi-static tensile load, which can be attributed to a reduced formation of Ti2Ni intermetallic compounds due to the intermixing of Nb. Ultimate tensile strengths of up to 673 MPa and elongations at break of 6.9% are achieved, demonstrating that micro electron beam welding is a promising process to produce high-strength dissimilar NiTi/Nb/Ti joints.

本研究旨在通过对接结构的微电子束焊接研究,扩大对NiTi/Nb/Ti材料组合异种熔焊的认识。除了自适应功率调制外,还采用了一种利用过程固有快束振荡的新方法来改善高熔点铌填充材料的熔化和混合行为。采用0.2和0.4 mm两种不同的Nb厚度,对焊缝金属的可焊性和显微组织演变进行了比较。结果表明,由于基体和填充材料的熔化温度和导热系数存在较大差异,导致元素分布不均匀和焊接缺陷,导致焊接实验面临重大挑战。然而,焊接接头在准静态拉伸载荷下表现出优异的力学性能,这可归因于Nb的混合减少了Ti2Ni金属间化合物的形成。实验结果表明,微电子束焊接是制备高强度异种NiTi/Nb/Ti接头的理想工艺,其抗拉强度高达673 MPa,断裂伸长率达6.9%。
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引用次数: 0
Transvarestraint testing of high-strength steel filler metal 高强度钢填充金属的横向应变试验
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-16 DOI: 10.1007/s40194-025-02042-1
Philipp Liepold, Arne Kromm, Thomas Kannengiesser

High-strength steel welds are typically not known to be susceptible to Solidification Cracking (SC). However, modern light-weight constructions may force welding in highly restrained conditions, which are known to increase the probability of Solidification Crack (SC) emergence. In this article, the Modified Varestraint-Transvarestraint (MVT) test was used to evaluate the hot cracking susceptibility of welds made from high-strength, low-alloyed filler material. The materials tested include solid wires and a metal-cored wire. All wires are typically used in the Gas Metal Arc Welding (GMAW) process. Susceptibility to SC was measured over a wide range of welding parameters and bending speeds. Results show little affinity of the tested materials to SC. However, crack length increases in most cases with arc energy ((text{U}bullet text{I}/text{welding speed})) and welding speed. The length of the longest crack in one test specimen follows a similar trend until high welding speeds, where stagnation of crack length with changing arc energy was observed.

高强度钢焊缝通常不容易发生凝固开裂(SC)。然而,现代轻量化结构可能会在高度受限的条件下强制焊接,这增加了凝固裂纹(SC)出现的可能性。本文采用修正变应变-横变应变(MVT)试验方法对高强低合金填充材料焊接件的热裂敏感性进行了评价。测试的材料包括实心导线和金属芯导线。所有电线通常用于气体金属电弧焊(GMAW)工艺。在广泛的焊接参数和弯曲速度范围内测量了对SC的敏感性。结果表明,被试材料对SC的亲和力很小,但裂纹长度在大多数情况下随着电弧能量((text{U}bullet text{I}/text{welding speed}))和焊接速度的增加而增加。在一个试样中最长裂纹的长度遵循类似的趋势,直到高焊接速度,在那里观察到裂纹长度随着电弧能量的变化而停滞。
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引用次数: 0
Effects of vacuum brazing on microstructure and pseudoelasticity of NiTi shape memory alloy brazements 真空钎焊对NiTi形状记忆合金钎焊显微组织和准弹性的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-16 DOI: 10.1007/s40194-025-02044-z
Lukas Wojarski, Alexa Nebel, Wolfgang Tillmann

NiTi shape memory alloys exhibit pseudoelasticity, allowing them to fully recover from prior deformations under varying thermal or mechanical loads. Unlike conventional materials like steels, these alloys can endure elastic strain rates up to ten times higher, owing to a diffusion-free transformation between the austenite and martensite phases in their crystal lattice induced by temperature or stress. Given their material properties, NiTi shape memory alloys find applications as actuators, implants, and stents, demanding high reliability and biocompatibility standards. To maintain maximum pseudoelasticity when joining NiTi components, any microstructural changes have to be kept to a minimum. In this regard, vacuum brazing is a promising joining technique, as it is capable to produce joints at comparatively low joining temperatures without melting the base material. Hence, this paper is aimed at evaluating the influence of different holding times and brazing temperatures on the deformation behavior of NiTi alloys in vacuum brazing applying AgCuTi braze alloy. For this purpose, microstructural analyses by means of SEM and EDS as well as tensile tests were conducted. Furthermore, the fracture surfaces were analyzed by SEM. It could be observed that a stress plateau was present in the brazed samples leading to the assumption that brazing with AgCuTi is a suitable joining technique to preserve the properties of NiTi. Nevertheless, the brazed samples fractured in the stress plateau. 

NiTi形状记忆合金表现出假弹性,允许它们在不同的热载荷或机械载荷下从先前的变形中完全恢复。与钢等传统材料不同,这些合金可以承受高达十倍的弹性应变率,这是由于温度或应力引起的晶格中奥氏体和马氏体相之间的无扩散转变。鉴于其材料特性,NiTi形状记忆合金可以应用于执行器、植入物和支架,要求高可靠性和生物相容性标准。为了在连接NiTi组件时保持最大的伪弹性,必须将任何微观结构变化保持在最低限度。在这方面,真空钎焊是一种很有前途的连接技术,因为它能够在相对较低的连接温度下产生连接,而不会熔化基材。因此,本文旨在评估不同保温时间和钎焊温度对AgCuTi钎焊合金真空钎焊中NiTi合金变形行为的影响。为此,采用扫描电镜和能谱仪进行了显微组织分析,并进行了拉伸试验。此外,还对断口进行了扫描电镜分析。可以观察到,在钎焊样品中存在应力平台,从而假设用AgCuTi钎焊是一种合适的连接技术,以保持NiTi的性能。然而,钎焊试样在应力平台上发生断裂。
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引用次数: 0
Detection of molten pool state using ResNet50 and control of molten pool penetration in CO2 gas shielded arc welding 利用ResNet50检测CO2气体保护弧焊熔池状态及熔池熔透控制
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-16 DOI: 10.1007/s40194-025-02020-7
Satoshi Yamane, ChuanZhi Wang, Takahito Nakamura, Takuya Nagai, Keito Ishizaki

In V groove butt welding with a ceramic backing material, the molten pool should penetrate well. Regardless of the gap fluctuations, the molten pool must maintain a good penetration shape. For this purpose, the molten pool state is detected using ResNet50 as one of the deep learning. The molten pool using a CMOS camera is taken. Fundamental experiments are performed, and images are collected for learning of ResNet50. Good estimation results are obtained for untraining data. The gap and its center are detected processing the molten pool images. The seam tracking is carried out using PI controller, with inputs being the difference between the wire tip and the gap center, and the output is Y axis position. The weaving width is adjusted to fit the gap. The molten pool state is controlled adjusting the travel speed of the welding torch, to keep constant the arc position, because the state of the molten pool depends on the arc position. If there is gap fluctuation as the disturbance and the reference of the arc position is same, it is difficult to get the same penetration of the molten pool. Therefore, the reference according to the output of ResNet50 is adjusted. Molten pool control is based on PI controller with the input is the difference between the arc position and its reference, and the output is the travel speed. The control performance is verified in a case where the gap varies from 7 to 3 mm, and good results are obtained.

用陶瓷衬底材料进行V型坡口对接焊时,熔池应渗透良好。无论间隙波动如何,熔池都必须保持良好的渗透形状。为此,使用ResNet50作为深度学习之一来检测熔池状态。用CMOS相机拍摄熔池。进行基础实验,采集图像进行ResNet50的学习。对未训练数据进行了较好的估计。通过对熔池图像的处理,检测出熔池间隙及其中心。采用PI控制器进行焊缝跟踪,输入为线尖与间隙中心的差值,输出为Y轴位置。调整织造宽度以适应间隙。控制熔池状态是通过调整焊枪的移动速度,保持电弧位置不变,因为熔池的状态取决于电弧位置。如果存在间隙波动作为扰动,且电弧位置的参考点相同,则很难获得相同的熔池穿透。因此,参照ResNet50的输出进行调整。熔池控制基于PI控制器,输入为电弧位置与其参考点的差值,输出为运动速度。在间隙为7 ~ 3mm的情况下验证了控制性能,取得了良好的效果。
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引用次数: 0
Influence of activated flux on the mechanical and microstructural response of cold metal transfer welded AA6063-MgAZ31B dissimilar alloy 活性助焊剂对AA6063-MgAZ31B异种合金冷态转移焊接力学和显微组织响应的影响
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-15 DOI: 10.1007/s40194-025-02038-x
Abhi Bansal, S. C. Vettivel, Mukesh Kumar

Welding of dissimilar alloys is challenging due to differences in their physical and chemical properties. The main problem while joining dissimilar alloys is intermetallic compound (IMC) formation, which affects the weld quality. Controlling the heat input is necessary to minimize the formation of IMC. This work uses cold metal transfer (CMT) welding with low heat input. However, the application of CMT welding is limited to thin sheets due to low depth of penetration (DOP). Activated flux can improve the performance of CMT welding, thus improving the DOP and minimizing the weld width (WW) by arc constrict mechanism. In this investigation, the SiO2 was used as an activated flux. The process parameters used in this study are welding current and welding speed, which were used to optimize tensile strength, hardness, DOP/WW ratio, and heat input. Numerous experiments were conducted as per the design of experiment using response surface methodology. The optimal input parameters from various experiments are a welding current of 150 A and a welding speed of 8.295 mm/s. The scanning electron microscope was used to analyze the microstructure of weld specimens. Energy dispersive spectroscopy and X-ray diffraction were used for elements and phase analysis.

由于不同合金的物理和化学性质的差异,焊接是具有挑战性的。异种合金连接的主要问题是金属间化合物(IMC)的形成,影响焊接质量。控制热输入是必要的,以尽量减少内压的形成。这项工作使用冷金属转移(CMT)焊接与低热量输入。然而,由于渗透深度(DOP)低,CMT焊接的应用仅限于薄板。激活助焊剂可以改善CMT焊接的性能,从而通过电弧收缩机制提高DOP并使焊缝宽度(WW)最小化。在本研究中,SiO2被用作活性助熔剂。本研究采用的工艺参数为焊接电流和焊接速度,用于优化拉伸强度、硬度、DOP/WW比和热输入。采用响应面法,按照实验设计进行了大量实验。各种实验的最佳输入参数为焊接电流为150 a,焊接速度为8.295 mm/s。采用扫描电镜对焊缝试样的显微组织进行了分析。采用能量色散光谱和x射线衍射进行元素和物相分析。
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引用次数: 0
Round-robin study on the determination of weld geometry parameters—part B: analysis of welded specimen 焊接几何参数确定的循环研究- B部分:焊接试样的分析
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-15 DOI: 10.1007/s40194-025-02033-2
Finn Renken, Jan Schubnell, Matthias Jung, Moritz Braun, Heikki Remes

The local geometry of the weld toe or the weld seam has a high influence on the fatigue strength of welded joints. Two main parameters for the geometrical description of the weld toe are the weld toe radius and the weld toe angle. Currently, there is no uniform definition or standardized measurement approach for the assessment of these parameters. For this reason, the presented extensive round-robin (RR) study focusses on the influence of different evaluation techniques and measurement systems regarding the mentioned parameters based on 3D surface scans. In total, 20 participants take part in this two stage RR (19 participants in the second part). In this work, the results of the second part (part B) of the RR, namely the evaluation of weld toe radius and weld toe angle on real welded joints, are presented, where the actual weld toe geometry is not known a priori. For this, 22 data sets were evaluated. The data sets consist of measured values for the radius and angle of the weld toe in relation to the position along the weld seam. In general, significant variations are determined for the evaluated weld geometry parameters, especially for the weld toe radius. It is also shown that the condition of the weld toe transition has a high influence on the parameter. Particularly for weld seams with a low weld toe angle, the measurement results for the radius of the individual participants show high variations. For small weld toe radii, the results are quite comparable between the participants. The results for the weld toe angle are comparable for flat welds, but a wide range of results is observed for sharp weld toes. The degree of automation of the measurement method also has a high influence on the results. The most accurate results are expected from manual measurements, while the fully automatic and semi-automatic methods show larger deviations.

焊趾或焊缝的局部几何形状对焊接接头的疲劳强度影响很大。焊缝脚趾几何描述的两个主要参数是焊缝脚趾半径和焊缝脚趾角。目前,这些参数的评估没有统一的定义或标准化的测量方法。因此,目前广泛的循环(RR)研究侧重于基于3D表面扫描的不同评估技术和测量系统对上述参数的影响。两阶段RR共20人(第二阶段19人)。在这项工作中,提出了RR的第二部分(B部分)的结果,即对实际焊接接头的焊缝脚趾半径和焊缝脚趾角的评估,其中实际的焊缝脚趾几何形状是未知的。为此,评估了22个数据集。这些数据集包括与焊缝位置相关的焊缝脚趾的半径和角度的测量值。一般来说,对于评估的焊缝几何参数,特别是焊缝脚趾半径,确定了显著的变化。结果还表明,焊趾过渡条件对该参数影响较大。特别是对于焊缝焊缝与低焊趾角,测量结果为个别参与者的半径显示出很大的变化。对于小焊接脚趾半径,结果是相当可比的参与者之间。焊接脚趾角的结果与平焊相当,但对尖锐的焊接脚趾观察到的结果范围很广。测量方法的自动化程度对结果也有很大的影响。人工测量结果最准确,而全自动和半自动测量结果偏差较大。
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引用次数: 0
TIG braze welding of rod-type art structures 棒状艺术结构的TIG钎焊
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-15 DOI: 10.1007/s40194-025-02045-y
Serhii Minakov, Yevgenia Chvertko, Nataliya Strelenko, Anton Minakov, Denys Stepanov, Anatoliy Zavdoveev, Dmytro Vdovychenko, Ivan Vdovychenko, Ievgen Byba

The paper presents the results of research on artwork joints of considerable thickness (10 mm). Butt welds in artworks are always difficult to perform because access to the joint is often one-sided. Traditional arc welding technologies are of limited use for such one-off production tasks, as full access to the joint is required and after welding the bulge must be cleaned from all sides of the bar, which is often unacceptable. Existing brazing technologies require a controlled gap between the joining surfaces, which is impossible to achieve for a wide variety of joints in art designs. Increasing the gap results in a decrease in the mechanical properties of the structure. A synergistic combination of welding and brazing using TIG technology can ensure a high-quality joint for thick bars of art structures. For such joints and conditions, the technology of high-temperature arc (TIG) brazing with partial melting of the parts to be joined and subsequent introduction of brazing alloy (CuSi3) into the metal pools of the parts to mix the liquid metal of the parts and the brazing alloy was developed. The developed technology makes it possible to fill the gap between the surfaces of bar-type parts with one-way access in the flat position, with minimal need to clean up solder that has protruded beyond the part.

本文介绍了相当厚度(10mm)艺术品接缝的研究结果。艺术品中的对焊总是很难进行,因为接合处通常是单向的。传统的弧焊技术对于这种一次性生产任务的应用是有限的,因为需要完全进入接头,并且焊接后必须从杆的所有侧面清除凸起,这通常是不可接受的。现有的钎焊技术需要在连接表面之间控制间隙,这对于艺术设计中的各种连接是不可能实现的。间隙的增大导致结构力学性能的降低。采用TIG技术将焊接与钎焊协同结合,可确保艺术结构粗棒的高质量连接。针对这种接头和条件,开发了高温电弧(TIG)钎焊技术,将待连接部件部分熔化,然后将钎焊合金(CuSi3)引入部件的金属池中,使部件的液态金属与钎焊合金混合。开发的技术使得有可能填补在平面位置单向通道的棒状零件的表面之间的差距,以最小的需要清理的焊料已经超出了部分。
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引用次数: 0
Effect of heat control on mechanical properties and residual stresses at the transition zone of component and substrate in hybrid DED-arc manufacturing 热控制对复合电弧制造中构件和衬底过渡区力学性能和残余应力的影响
IF 2.4 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-15 DOI: 10.1007/s40194-025-02036-z
R. Scharf-Wildenhain, L. Engelking, A. Haelsig, D. Schroepfer, T. Kannengiesser, J. Hensel

In hybrid additive manufacturing, components or semi-finished products manufactured by conventional primary forming are enhanced or modified by additive manufactured structures. However, systematic investigations focusing on the critical transition area between the specific properties of the substrate (like high-strength) and the additively manufactured component, made of specific filler material, are still lacking. The focus of the present study was to determine the influence of heat control on the ∆t8/5 cooling time, the distortion, the mechanical properties, and the residual stresses in the transition area of hybrid-additive components. This contributed to the knowledge regarding the safe avoidance of cold cracking, excessive distortion, a reduction in yield stress, and the implementation of hybrid DED-arc manufacturing. The heat control was varied by means of heat input and working temperature such that the ∆t8/5 cooling times corresponded to the recommended processing range. The heat input has a greater influence on the cooling time in the transition area than the working temperature. Working temperature and the total energy applied per layer have a significant effect on component distortion. The lowest working temperature of 100 °C in combination with the highest total energy per layer leads to significantly greater distortion compared to manufacturing with a high working temperature of 300 °C and low total energy per layer. In addition, the longitudinal residual compressive stresses in the sensitive transition area are reduced from − 500 MPa to approx. − 200 MPa by adjusting the working temperature from 100 to 300 °C. Such complex interactions must be clarified comprehensively to provide users with easily applicable processing recommendations and standard specifications for an economical hybrid additive manufacturing of components made, for example, of high-strength steels in the transition area.

在混合增材制造中,通过常规初级成形制造的部件或半成品通过增材制造结构得到增强或改性。然而,对基材的特定性能(如高强度)和由特定填充材料制成的增材制造部件之间的关键过渡区域的系统研究仍然缺乏。本研究的重点是确定热控制对混合添加剂部件的∆t1 /5冷却时间、变形、力学性能和过渡区残余应力的影响。这有助于安全避免冷裂、过度变形、降低屈服应力以及实现混合ded电弧制造。热量控制通过热量输入和工作温度的变化而变化,使∆t1 /5冷却时间对应于推荐的加工范围。热输入比工作温度对过渡区冷却时间的影响更大。工作温度和每层施加的总能量对元件畸变有显著影响。与300°C的高工作温度和低每层总能量的制造相比,最低工作温度为100°C,每层总能量最高,导致畸变明显更大。此外,敏感过渡区的纵向残余压应力从- 500 MPa降至约。−200mpa,工作温度在100 ~ 300℃范围内调节。这种复杂的相互作用必须全面澄清,以便为用户提供易于适用的加工建议和标准规格,用于经济混合增材制造部件,例如在过渡区域使用高强度钢。
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引用次数: 0
Effect of Zn interlayer on joint characteristics of dissimilar friction stir welding of Mg and Cu alloy 锌中间层对镁铜合金异种搅拌摩擦焊接头特性的影响
IF 2.5 4区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2025-04-14 DOI: 10.1007/s40194-025-02041-2
Abhijeet Bhowmik, Satya Kumar Dewangan, Pragya Nandan Banjare, Manoranjan Kumar Manoj

Joining of dissimilar AZ31 Mg alloy and Cu- 8Zn alloy by using zinc interlayer through Friction Stir Welding (FSW) has been studied for the first time. The process parameters include 1200 rpm rotational speed and 20 mm/min traverse speed. Microstructural characterizations were performed to study material flow behavior, grain refinement and IMCs formation whereas, mechanical characterization includes hardness and tensile tests. SEM EDS and XRD were used for identification of phases and fracture behavior. The study revealed that for direct joining of Mg/Cu, the stir zone (SZ) mainly consisted of two-phase region containing δ-Mg and Mg2Cu along with fragments of Cu particles. Small amount of MgCu2 was also observed in the form of intercalated layer along with Cu. Voids and tunnelling defects were also observed. On the other hand, the application of Zn interlayer has completely modified the structure of SZ which contains well distributed mixture of δ-Mg and MgZn. A very thin layer of MgZn2 and MgO was observed in the SZ. Average tensile strength of Mg/Cu with Zn interlayer has improved to 93 MPa which is the highest joint strength as compared to the previously reported joint strength of Mg/Cu weld.

本文首次研究了异种AZ31镁合金与Cu- 8Zn合金采用搅拌摩擦焊(FSW)连接锌中间层的方法。工艺参数包括1200转/分的转速和20毫米/分钟的导线速度。显微组织表征研究材料的流动行为,晶粒细化和IMCs形成,而力学表征包括硬度和拉伸测试。采用SEM、EDS、XRD等方法对试样的物相及断裂行为进行了表征。研究表明,Mg/Cu直接连接时,搅拌区(SZ)主要由δ-Mg和Mg2Cu两相区以及Cu颗粒碎片组成。微量的MgCu2与Cu一起以插层形式存在。还观察到空洞和隧道缺陷。另一方面,Zn中间层的应用完全改变了SZ的结构,使其含有δ-Mg和MgZn的均匀混合物。在SZ中观察到一层很薄的MgZn2和MgO。与之前报道的Mg/Cu焊缝的接头强度相比,添加Zn中间层的Mg/Cu焊缝的平均抗拉强度提高到93 MPa,是最高的接头强度。
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引用次数: 0
期刊
Welding in the World
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