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The Effect of Different Mn/Fe Ratio on Microstructure Alloy Based on Al-Si-Mg 不同Mn/Fe比对Al-Si-Mg基微结构合金的影响
IF 0.6 Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/AFE.2019.127129
D. Bolibruchová, R. Podprocká
This article deals with the effect of manganese that is the most applied element to eliminate the negative effect of iron in the investigated alloy AlSi7Mg0.3. In this time are several methods that are used for elimination harmful effect of iron. The most used method is elimination by applying the additive elements, so-called iron correctors. The influence of manganese on the morphology of excluded ironbased intermetallic phases was analysed at various iron contents (0.4; 0.8 and 1.2 wt. %). The effect of manganese was assessed in additions of 0.1; 0.2; 0.4 and 0.6 wt. % Mn. The morphology of iron intermetallic phases was assessed using electron microscopy (SEM) and EDX analysis. The increase of iron content in investigated alloys caused the formation of more intermetallic phases and this effect has been more significant with higher concentrations of manganese. The measurements carried out also showed that alloys with the same Mn/Fe ratio can manifest different structures and characteristics of excluded iron-based intermetallic phases, which might, at the same time, be related to different resulting mechanical properties.
本文研究了在AlSi7Mg0.3合金中应用最多的锰元素对消除铁的负面影响的作用。在这个时候,有几种方法被用来消除铁的有害影响。最常用的方法是通过添加元素,即所谓的铁校正器来消除。分析了不同铁含量(0.4;0.8和1.2 wt %)。评价锰在添加量为0.1时的效果;0.2;0.4和0.6 wt. % Mn。利用电子显微镜(SEM)和EDX分析对铁金属间相的形貌进行了评价。合金中铁含量的增加导致了更多金属间相的形成,这种影响随着锰浓度的增加而更加显著。测量结果还表明,相同Mn/Fe比的合金可以表现出不同的组织和不含铁基金属间相的特征,这可能与不同的力学性能有关。
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引用次数: 2
Primary Microstructure Characterization of As-Casted Co-20Ni-7Al-7W Superalloy 铸态Co-20Ni-7Al-7W高温合金的初次组织表征
IF 0.6 Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/AFE.2019.127143
A. Tomaszewska, G. Moskal, T. Mikuszewski, G. Junak, A. Płachta
The primary microstructure of new Co-based superalloy of Co-20Ni-7Al-7W (at.%) type was showed in this article. The alloy was manufactured by induction melting in vacuum furnaces. This alloy is a part of new group of high-temperature materials based on Co solid solution and strengthened by coherent L1 2 phase similar to Ni-based superalloys with γʹ phase. The final form of Co ss /L1 2 microstructure is obtained after fully heat treatment included homogenization, solutionizing and aging processes. But first step of heat treatment thermal parameters determination is characterization of primary microstructure of alloys after casting process with special attentions on segregations of alloying elements in solid solution and presences of structural elements such as eutectic areas, and other phases precipitations. In analysed case the relatively high homogeneity of chemical composition was expected especially in the case of W distribution, what was confirmed be SEM/EDS analysis in dendritic and interdendritic areas.
研究了Co-20Ni-7Al-7W (at.%)型新型co基高温合金的初次显微组织。该合金是在真空炉中感应熔炼而成的。该合金是一类以Co固溶体为基体,以L1 - 2相强化的新型高温材料,类似于含γ - α相的ni基高温合金。经过均匀化、固溶和时效等充分热处理,得到最终的Co ss /L1微观组织。但热处理热参数确定的第一步是合金铸造后初级组织的表征,特别关注合金元素在固溶体中的偏析和共晶区等组织元素的存在,以及其他相的析出。在分析的情况下,化学成分的均匀性相对较高,特别是在W分布的情况下,这在枝晶和枝晶间区域的SEM/EDS分析中得到了证实。
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引用次数: 2
Experimental and Numerical Comparison of Lead-Free and Lead-Containing Brasses for Fixture Application 夹具用无铅与含铅黄铜的实验与数值比较
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2023.146672
A comparative analysis of brasses alloys, namely lead-free CuZn (CB771) and lead containing CuZn (CB770), was conducted in this article. The results of the comparative analysis and experimental investigations aimed to provide comprehensive knowledge about the thermophysical properties and solidification characteristics of these alloys. Thermodynamic simulations using Thermo-Calc software and modifications in the chemical composition of the CB771 alloy were employed to approximate its characteristics to those of the lead containing CuZn alloy. Thermal-derivative analysis of the alloys and a technological trial were carried out to determine their solidification characteristics, fluidity, and reproducibility. The casting trials were conducted under identical conditions
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引用次数: 0
Compacted Graphite Iron with the Addition of Tin 添加锡的压实石墨铁
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2020.133323
The paper presents the effect of tin on the crystallization process, microstructure and hardness of cast iron with compacted (vermicular) graphite. The compacted graphite was obtained with the use of magnesium treatment process (Inmold technology). The lack of significant effect of tin on the temperature of the eutectic transformation has been demonstrated. On the other hand, a significant decrease in the eutectoid transformation temperature with increasing tin concentration has been shown. It was demonstrated that tin narrows the temperature range of the austenite transformation. The effect of tin on the microstructure of cast iron with compacted graphite considering casting wall thickness has been investigated and described. The carbide-forming effect of tin in thin-walled (3 mm) castings has been demonstrated. The nomograms describing the microstructure of compacted graphite iron versus tin concentration have been developed. The effect of tin on the hardness of cast iron was given.
{"title":"Compacted Graphite Iron with the Addition of Tin","authors":"","doi":"10.24425/afe.2020.133323","DOIUrl":"https://doi.org/10.24425/afe.2020.133323","url":null,"abstract":"The paper presents the effect of tin on the crystallization process, microstructure and hardness of cast iron with compacted (vermicular) graphite. The compacted graphite was obtained with the use of magnesium treatment process (Inmold technology). The lack of significant effect of tin on the temperature of the eutectic transformation has been demonstrated. On the other hand, a significant decrease in the eutectoid transformation temperature with increasing tin concentration has been shown. It was demonstrated that tin narrows the temperature range of the austenite transformation. The effect of tin on the microstructure of cast iron with compacted graphite considering casting wall thickness has been investigated and described. The carbide-forming effect of tin in thin-walled (3 mm) castings has been demonstrated. The nomograms describing the microstructure of compacted graphite iron versus tin concentration have been developed. The effect of tin on the hardness of cast iron was given.","PeriodicalId":8301,"journal":{"name":"Archives of Foundry Engineering","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-11-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135634293","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
The Use of Phosphate Binder for Ablation Casting of AlSi7Mg Modified TiB Alloy 磷酸盐粘结剂在AlSi7Mg改性TiB合金烧蚀铸造中的应用
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2022.140218
The possibilities of using an inorganic phosphate binder for the ablation casting technology are discussed in this paper. This kind of binder was selected for the process due to its inorganic character and water-solubility. Test castings were made in the sand mixture containing this binder. Each time during the pouring liquid alloy into the molds and solidification process of castings, the temperature in the mold was examined. Then the properties of the obtained castings were compared to the properties of the castings solidifying at ambient temperature in similar sand and metal molds. Post-process materials were also examined - quartz matrix and water. It has been demonstrated that ablation casting technology promotes refining of the microstructure, and thus upgrades the mechanical properties of castings (R m was raised about approx. 20%). Properties of these castings are comparable to the castings poured in metal moulds. However, the post-process water does not meet the requirements of ecology, which significantly reduces the possibility of its cheap disposal.
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引用次数: 0
Plasma Coatings on Aluminium-Silicon Alloy Surfaces 铝硅合金表面的等离子涂层
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2021.138671
Plasma oxidation, similarly to anodic oxidation (anodizing), are classified as electrochemical surface treatment of metals such as Al, Mg, Ti and their alloys. This type of treatment is used to make surface of castings, plastically processed products, shaped with incremental methods to suitable for certain requirements. The most important role of the micro plasma coating is to protect the metal surface against corrosion. It is well known that coating of aluminium alloys containing silicon using anodic oxidation causes significant difficulties. They are linked to the eutectic nature of this alloy and result in a lack of coverage in silicon-related areas. The coating structure in these areas is discontinuous. In order to eliminate this phenomenon, it is required to apply oxidation coatings using the PEO (Plasma Electrolytic Oxidation) method. It allows a consistent, crystalline coating to be formed. This study presents the mechanical properties of the coatings applied to Al-Si alloy using the PEO method. As part of the testing, the coating thickness, microhardness and scratch resistance were determined. On the basis of the results obtained, it was concluded that the thickness of the coatings complies with the requirements of conventional anodizing. Additionally, microhardness values exceeded the results obtained with standard methods.
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引用次数: 1
A New Laser-Registered View of the Shrinkage Kinetics of Foundry Alloys 铸造合金收缩动力学的激光记录新观点
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2020.133328
This paper presents a new stand for studying the linear shrinkage kinetics of foundry alloys. The stand is equipped with a laser displacement sensor. Thanks to this arrangement, the measurement is of a contactless nature. This solution allows for the elimination of errors which occur in measurements made using intermediary elements (steel rods). The supposition of the expansion (shrinkage) of the sample and the expansion of the heated rod lead to the distortion of the image of the actual dimensional changes of the studied sample. A series of studies of foundry alloys conducted using the new stand allowed a new image of shrinkage kinetics to be obtained, in particular regarding cast iron. The authors introduce in the study methodology a real-time measurement of two linked quantities; shrinkage (the displacement of the free end of the sample) and temperature in the surface layer of the sample casting. This generates not only a classic image of shrinkage (S) understood as S = f (t), but also the view S = f (T). The latter correlation, developed based on results obtained using the contactless method, provide a new, so far poorly known image of the course of shrinkage in foundry alloys, especially cast iron with graphite in the structure. The study made use of hypo- and hypereutectic cast iron in order to generate an image of the differences which occur in the kinetics of shrinkage (as well as in pre-shrinkage expansion - expansion occurs during solidification).
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引用次数: 1
Impact of Ti and Fe on the Microstructure and Properties of Copper and Copper Alloys Ti和Fe对铜及铜合金组织和性能的影响
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2020.133352
The paper discusses issues related to the technology of melting and processing of copper alloys. An assessment was made of the impact of titanium and iron introduced in the form of pre-alloy - Ti73Fe master alloy on the microstructure and selected properties of pure copper and copper-silicon alloy. There are known examples of the use of titanium and iron additive to the copper alloy. Titanium as an additive introduced to copper alloys to improve their properties is sometimes also applicable. In the first stage of the study, a series of experimental castings were conducted with variable content of Ti73Fe master alloy entering copper in quantities of 5 %, 15 %, 25 % in relation to the mass of the metal charge. In the second stage, a silicon additive was introduced into copper in the amount of about 4 % by weight and 0.5 % and 1 % respectively of the initial Ti73Fe alloy. Thermodynamic phase parameters were modelled using CALPHAD method and Thermo-Calc software, thus obtaining the crystallization characteristics of the test alloys and the percentage of structural components at ambient temperature. Experiments confirmed the validity of the use of Ti73Fe master alloy as an additive. The pre-alloy used showed a favourable performance, both in terms of addition solubility and in the area of improvement of strength properties. Changes were achieved in the microstructure, mainly within the grain, but also in the developed dendrites of the solid solution. Changes occur with the introduction of titanium with iron into copper as well as to two-component silicon bronze.
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引用次数: 0
Comparison of Methods for Determining the Ferrite Content in Duplex Cast Steels 双相铸钢中铁素体含量测定方法的比较
Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/afe.2019.127121
V. Kaňa, V. Pernica, A. Zadera, V. Krutiš
The paper is concerned with comparing the methods for determining the ferrite content in castings from duplex stainless steels. It uses Schaeffler diagram, empirical formula based calculation, image analysis of metallographic sample, X-ray diffraction and measurement with a feritscope. The influence of wall thickness of the casting on the ferrite content was tested too. The results of the experiments show that the casting thickness of 25 or 60 mm does not have a significant effect on the measured amount of ferrite. The image analysis of metallographic sample and the measurement with the feritscope appear to be the most suitable methods. On the contrary, predictive methods, such as Schaeffler diagram or empirical formula based calculation are only indicative and cannot replace the real measurements. X-ray diffraction seems to be the least suitable measuring method. Values of ferrite content measured in such a way often deviated from the values measured by image analysis and with feritscope.
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引用次数: 8
Gas Blowing Ultrasonic Aluminium Degassing Assessment with the Reduced Pressure Test (RPT) Method 用减压试验(RPT)方法评价气吹超声铝脱气
IF 0.6 Q3 Materials Science Pub Date : 2023-11-06 DOI: 10.24425/AFE.2020.131312
H. Galarraga, M. G. Cortázar, E. Arregi, A. Artola, J. L. Oncala, Mikel Merchán-Zubieta
This work has been done within the AL-STRUC project supported by the ELKARTEK program of the Basque Government under Grant KK-2017/00020.
这项工作是在巴斯克政府ELKARTEK计划(KK-2017/00020赠款)支持的AL-STRUC项目中完成的。
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引用次数: 2
期刊
Archives of Foundry Engineering
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