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LNG density measurement by gravimetric method 用重量法测定液化天然气密度
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-16 DOI: 10.1016/j.cryogenics.2024.103925

Density is a critical parameter in the liquefied natural gas (LNG) industry, which necessitates the study of measurement methods. Standard methods for calculating LNG density are employed in downstream LNG custody transfer, but it still faces challenges in density measurement in the upstream, such as in LNG plants and LNG refueling station. In this paper, a gravimetric density measurement method was established for LNG plants, which is SI-traceable as it relies on volume and mass. A home-made sampling device was developed and employed to obtain the LNG volume and mass. The principle involves trapping LNG in a known-volume quantitative tube within the sampling device. The LNG is then transferred to a vacuum sampling cylinder and weighed using a mass compactor. This approach not only provides representative samples but also enables compositional analysis while performing density calculations according to ISO 6578. Feasibility and practicality tests of this novel method were conducted in an LNG plant. The test results indicate that the reproducibility is 0.6 %(RSD), and the relative expanded uncertainty is 2.0 % (k = 2). Compared to the revised Klosek and McKinley method (RKM), it shows a relative difference of −0.3 % to 1.5 %, demonstrating the applicability to LNG plants.

密度是液化天然气(LNG)行业的一个关键参数,因此有必要对测量方法进行研究。液化天然气密度的标准计算方法被应用于下游的液化天然气监管转移,但在上游的密度测量中,如液化天然气工厂和液化天然气加气站,仍然面临着挑战。本文为液化天然气工厂建立了一种重力密度测量方法,由于该方法依赖于体积和质量,因此具有 SI 可追溯性。为获得液化天然气的体积和质量,开发并使用了一种自制的采样装置。其原理是在取样装置内的已知体积定量管中捕获液化天然气。然后,将液化天然气转移到真空采样瓶中,并使用质量压缩器进行称重。这种方法不仅能提供具有代表性的样品,还能进行成分分析,同时根据 ISO 6578 标准进行密度计算。在液化天然气工厂对这种新方法进行了可行性和实用性测试。测试结果表明,重现性为 0.6%(RSD),相对扩展不确定性为 2.0%(k = 2)。与修订后的 Klosek 和 McKinley 方法 (RKM) 相比,其相对差值在 -0.3 % 到 1.5 % 之间,这表明该方法适用于液化天然气工厂。
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引用次数: 0
Measurement of thermal contact resistance and the design of thermal contacts at cryogenic temperatures 测量低温条件下的热接触电阻和热接触设计
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-14 DOI: 10.1016/j.cryogenics.2024.103922

The prevalence of technologies that operate at cryogenic temperatures requires that the cooling systems used to maintain these systems be carefully designed. This research focuses on understanding the thermal performance of the heat path between the heat source (the technology being cooled) and the cooling source (the cryocooler). Specifically, this work characterizes through measurement the thermal properties of common heat path materials, with a focus on bulk thermal conductivity and thermal contact resistance of pressed contacts. A framework for using these measurements to optimize a bolted contact is proposed and demonstrated.

在低温下运行的技术非常普遍,这就要求对用于维护这些系统的冷却系统进行精心设计。这项研究的重点是了解热源(被冷却的技术)和冷却源(低温冷却器)之间热路径的热性能。具体来说,这项工作通过测量常见热路径材料的热性能,重点是冲压触头的体积热导率和热接触电阻。提出并演示了利用这些测量结果优化螺栓连接触头的框架。
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引用次数: 0
Review of the design and optimization of BOG re-liquefaction process for LNG carriers 审查液化天然气运输船 BOG 再液化工艺的设计和优化
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-12 DOI: 10.1016/j.cryogenics.2024.103924

Over the past few years, liquefied natural gas (LNG) evaporated gas re-liquefaction technology has rapidly developed. This technology is particularly useful in trans-oceanic LNG trade, which has grown to be a hot sector in the world’s energy trade. And there are several limitations on board. Reducing energy consumption, improving efficiency, and lowering costs are crucial factors in the BOG re-liquefaction process. This review provides a comprehensive review of the recent advancements in the design and optimization of BOG re-liquefaction processes. It includes a detailed analysis and comparison of existing BOG re-liquefaction technologies, and specifically discusses two types of re-liquefaction processes: dynamic and steady-state. Furthermore, this review examines different perspectives and directions for improving these two re-liquefaction technologies. Finally, the challenges faced by the BOG re-liquefaction process for LNG carriers are presented, along with future directions for addressing these challenges.

过去几年来,液化天然气(LNG)蒸发气再液化技术发展迅速。这种技术在跨洋液化天然气贸易中特别有用,已发展成为世界能源贸易的热门领域。而船上有几个限制条件。减少能耗、提高效率和降低成本是 BOG 再液化过程中的关键因素。本综述全面回顾了近期在设计和优化 BOG 再液化工艺方面取得的进展。其中包括对现有 BOG 再液化技术的详细分析和比较,并特别讨论了两种类型的再液化工艺:动态和稳态。此外,本综述还探讨了改进这两种再液化技术的不同视角和方向。最后,介绍了液化天然气运输船 BOG 再液化工艺面临的挑战,以及应对这些挑战的未来方向。
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引用次数: 0
Thermal expansion calculation using FBGS in cryogenic applications 在低温应用中使用 FBGS 进行热膨胀计算
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-06 DOI: 10.1016/j.cryogenics.2024.103918

This study presents the measurement of the thermal expansion of aluminum alloy 6061 at cryogenic temperatures using Helium as the cooling medium. Three distinct tests were conducted to evaluate thermal expansion: two with gradual and natural heating of the material, and a third with temperature stabilization at key points. Measurements were carried out using Fiber Bragg Grating Sensors (FBGS), which provided precise and reliable data on the material's thermal behavior. The obtained results were compared with reference curves from the National Institute of Standards and Technology (NIST), showing good agreement and validation of the employed methods. This research highlights the effectiveness of using FBGS in measuring thermal expansion under cryogenic conditions and the importance of heating procedures in obtaining accurate data.

本研究介绍了使用氦气作为冷却介质测量铝合金 6061 在低温下的热膨胀。对热膨胀进行了三次不同的测试:两次是材料逐渐自然加热,第三次是关键点温度稳定。使用光纤布拉格光栅传感器(FBGS)进行了测量,为材料的热行为提供了精确可靠的数据。获得的结果与美国国家标准与技术研究院(NIST)的参考曲线进行了比较,结果表明所采用的方法具有良好的一致性和有效性。这项研究强调了在低温条件下使用 FBGS 测量热膨胀的有效性,以及加热程序对获得精确数据的重要性。
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引用次数: 0
Enhancing the cryogenic performance of superconducting magnet encapsulation resins with hyperbranched polymers: A molecular dynamics simulation and experimental study 利用超支化聚合物提高超导磁体封装树脂的低温性能:分子动力学模拟和实验研究
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-05 DOI: 10.1016/j.cryogenics.2024.103919

Epoxy resin (EP) plays a crucial role in safeguarding superconducting magnets. One of the major concerns related to its usage is its inherent susceptibility to cracking under cryogenic temperatures and the strong electromagnetic forces experienced during the operation of superconducting magnets. In this study, we utilize molecular dynamics (MD)simulation and cryogenic experiments to conduct a comprehensive investigation aimed at gaining a profound understanding of the cryogenic toughening mechanism in hyperbranched polymers-toughened (HBPs) EPs. Five different crosslinking models of EP composites were established by MD simulations. The performance parameters obtained from the MD simulation calculations are highly consistent with the experimental results, which included the glass transition temperature, coefficient of thermal expansion, mechanical properties, free volume and atomic mean square displacement. Moreover, the relationship between structural changes and properties of the MD models was investigated. This research method provides a new avenue of exploration for superconducting magnet encapsulation resin materials.

环氧树脂(EP)在保护超导磁体方面起着至关重要的作用。与使用环氧树脂有关的一个主要问题是,环氧树脂在低温条件下和超导磁体运行过程中的强电磁力作用下容易开裂。在本研究中,我们利用分子动力学(MD)模拟和低温实验进行了全面研究,旨在深刻理解超支化聚合物增韧 EPs 的低温增韧机制。通过 MD 模拟建立了五种不同的 EP 复合材料交联模型。MD 模拟计算得到的性能参数与实验结果高度一致,包括玻璃化转变温度、热膨胀系数、力学性能、自由体积和原子均方位移。此外,还研究了 MD 模型的结构变化与性能之间的关系。该研究方法为超导磁体封装树脂材料提供了一条新的探索途径。
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引用次数: 0
Thermal propagation analysis of 2G HTS stacked wires based on a dimensional coupling method 基于尺寸耦合方法的 2G HTS 叠层导线热传播分析
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-05 DOI: 10.1016/j.cryogenics.2024.103921

Stacked structures of high-temperature superconducting (HTS) tapes are usually employed to enhance current-carrying capacity in cable or magnet applications, but their multilayer characteristics may result in local hot spots due to uneven cooling. Besides, the inconsistencies along the length of tapes introduced during manufacturing process and the significant transverse Lorentz forces experienced in magnet operations can lead to weak parts, bringing uncertainties to thermal stability. Finite-element methods are widely used to predict thermal propagations, but 3D models encounter challenges such as distorted mesh elements and convergence issues, particularly when combining electromagnetic and heat transfer modules for long-distance wires. In this work, we have developed a Dimensional Coupling Method (DCM) to assess the thermal impact of weak parts in stacked wires applying coupled 1D and 2D models. The 2D model analyzes the electromagnetic and heat characteristics of stacked surfaces, and provides an initial heat source for the 1D model, which evaluates thermal propagation longitudinally. Simulation results of the 1D module are then transferred back to update the 2D outcomes. Models of distinct dimensions are coupled sequentially in physical steps but simultaneously in the time domain. Our approach is verified by 3D model benchmarks and offers a computational cost reduction of approximately 60 % compared to the benchmarks, making it more suitable for applications with large Iop/Ic ratios. Specially, multi-layer stacked wires under low ratios cases are also been analyzed. What’s more, two influencing factors of heat propagation, the weak-part length and position, are also investigated.

高温超导 (HTS) 磁带的堆叠结构通常用于提高电缆或磁体应用中的载流能力,但其多层特性可能会因冷却不均而导致局部热点。此外,制造过程中引入的磁带长度不一致以及磁体运行过程中产生的巨大横向洛伦兹力都可能导致部件薄弱,给热稳定性带来不确定性。有限元方法被广泛用于预测热传播,但三维模型会遇到网格元素扭曲和收敛问题等挑战,尤其是在结合长距离导线的电磁和热传导模块时。在这项工作中,我们开发了一种尺寸耦合方法(DCM),利用耦合的一维和二维模型来评估堆叠导线中薄弱部分的热影响。二维模型分析堆叠表面的电磁和热特性,并为一维模型提供初始热源,一维模型评估热的纵向传播。然后将一维模块的模拟结果传回,更新二维结果。不同维度的模型在物理步骤中依次耦合,但在时域中同时耦合。我们的方法得到了三维模型基准的验证,与基准相比,计算成本降低了约 60%,因此更适用于大/比的应用。我们还特别分析了低比率情况下的多层堆叠导线。此外,还研究了热传播的两个影响因素,即薄弱部分的长度和位置。
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引用次数: 0
Genetic algorithm based optimization of nozzle profiles for a hydrogen turbo-expander 基于遗传算法的氢气涡轮膨胀机喷嘴轮廓优化设计
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-08-03 DOI: 10.1016/j.cryogenics.2024.103920

Liquid hydrogen plays an important role in the large scale storage and long-distance transportation. The development of hydrogen turbo-expander is the key to increase the efficiency of hydrogen liquefaction, reducing the cost of liquid hydrogen production, storage and transportation. In this paper, a numerical model of hydrogen nozzle is established and validated against experimental data. The performance of four traditional nozzle profiles in hydrogen turbo-expanders is simulated and analyzed. The poor uniformity of outlet flow angle is generally found in these nozzle profiles, leading to nozzle passage and impeller incidence losses in turbo-expanders. A genetic algorithm based method is proposed to optimize the nozzle profiles. The optimization objectives involve the nozzle efficiency, the uniformity of the nozzle outlet angle and the uniformity of the outlet Mach number. The deviations in the outlet angle and Mach number of the optimized nozzle are reduced by 50.26 % and 14.03 %, respectively, while the nozzle efficiency reaches 98.64 %. The matching characteristics of the optimized nozzle with the impeller are obtained via simulation of a hydrogen turbo-expander, and the results indicate the expansion efficiency can be increased by 1.53 %.

液氢在大规模储存和长距离运输中发挥着重要作用。氢气涡轮膨胀机的开发是提高氢气液化效率、降低液氢生产、储存和运输成本的关键。本文建立了氢气喷嘴的数值模型,并根据实验数据进行了验证。模拟并分析了氢气涡轮膨胀机中四种传统喷嘴剖面的性能。这些喷嘴剖面普遍存在出口流角均匀性差的问题,导致涡轮膨胀机中喷嘴通道和叶轮入射损失。本文提出了一种基于遗传算法的喷嘴剖面优化方法。优化目标包括喷嘴效率、喷嘴出口角的均匀性和出口马赫数的均匀性。优化后喷嘴的出口角和马赫数偏差分别减少了 50.26 % 和 14.03 %,喷嘴效率达到 98.64 %。通过模拟氢气涡轮膨胀机,获得了优化喷嘴与叶轮的匹配特性,结果表明膨胀效率可提高 1.53%。
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引用次数: 0
Experimental study on vibration reduction of a cryogen-free dilution refrigerator system pre-cooled by a GM cryocooler 通过 GM 低温冷却器预冷的无低温稀释制冷系统减震实验研究
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-07-31 DOI: 10.1016/j.cryogenics.2024.103911

In order to carry out vibration reduction work on a cryogen-free dilution refrigerator system pre-cooled by a GM cryocooler, this paper first introduces the method of vibration measurement, particularly presenting the results and verification of displacement measurement obtained through acceleration integration. Subsequently, based on the construction of our dilution refrigerator, the paper reports experimental evidence of the direct impact of vibration on temperature and provides an effective vibration reduction scheme for the system. The study finds that vibrations transmitted through the path of “low-temperature part of GM- copper braid − support structure − various cold plates” have the most significant impact, hence making good internal soft connections is key. The influence of vibrations from the room-temperature part of GM can be mitigated to some extent by suspending the cold head, either by a separate frame or using the dilution refrigerator’s own frame. The use of a structure composed of air springs and honeycomb rubber in the suspension system has proven to be effective. Our final experimental results have demonstrated that with adequate vibration damping, the impact of vibrations from the GM on temperature can be essentially eliminated, allowing the dilution refrigerator to achieve a temperature level close to that when pre-cooled by a PT. The research in this paper has certain reference value for the construction and vibration mitigation of ultra-low temperature refrigeration systems.

为了在由 GM 低温冷却器预冷的无低温稀释制冷系统上开展减振工作,本文首先介绍了振动测量方法,特别是介绍了通过加速度积分获得的位移测量结果和验证。随后,根据稀释制冷器的构造,本文报告了振动对温度直接影响的实验证据,并为系统提供了有效的减振方案。研究发现,通过 "GM 的低温部分-铜编织物-支撑结构-各种冷板 "路径传播的振动影响最大,因此做好内部软连接是关键。通过单独的框架或稀释制冷机本身的框架来悬挂冷头,可以在一定程度上减轻来自 GM 常温部分的振动影响。事实证明,在悬挂系统中使用由空气弹簧和蜂窝橡胶组成的结构是有效的。我们最终的实验结果表明,在充分减震的情况下,可以基本消除来自通用汽车的振动对温度的影响,使稀释制冷机的温度水平接近由 PT 预冷时的温度水平。本文的研究对超低温制冷系统的建造和减震具有一定的参考价值。
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引用次数: 0
Towards scalable cryogenic quantum dot biasing using memristor-based DC sources 利用基于忆阻器的直流电源实现可扩展的低温量子点偏压
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-07-29 DOI: 10.1016/j.cryogenics.2024.103910

Cryogenic memristor-based DC sources offer a promising avenue for in situ biasing of quantum dot arrays. In this study, we present experimental results and discuss the scaling potential for such DC sources. We first demonstrate the operation of a commercial discrete operational amplifier down to

which is used on the DC source prototype. Then, the tunability of the memristor-based DC source is validated by performing several
-DC sweeps with a resolution of
at room temperature and at
. Additionally, the DC source prototype exhibits a limited output drift of
at
. This showcases the potential of memristor-based DC sources for quantum dot biasing. Limitations in power consumption and voltage resolution using discrete components highlight the need for a fully integrated and scalable complementary metal–oxide–semiconductor-based (CMOS-based) approach. To address this, we propose to monolithically co-integrate emerging non-volatile memories (eNVMs) and
CMOS circuitry. Simulations reveal a reduction in power consumption, down to
per DC source and in footprint. This allows for the integration of up to one million eNVM-based DC sources at the
stage of a dilution fridge, paving the way for near term large-scale quantum computing applications.

基于低温忆阻器的直流电源为量子点阵列的原位偏压提供了一个前景广阔的途径。在本研究中,我们展示了实验结果,并讨论了此类直流源的扩展潜力。我们首先演示了直流源原型上使用的商用分立运算放大器在低至▪的条件下的运行情况。然后,通过在室温和 ▪ 条件下以 ▪ 的分辨率进行几次 ▪-DC 扫频,验证了基于忆阻器的直流源的可调谐性。此外,直流电源原型在 ▪ 时显示出有限的 ▪ 输出漂移。这展示了基于忆阻器的直流源在量子点偏压方面的潜力。使用分立元件在功耗和电压分辨率方面的局限性突出表明,需要一种完全集成且可扩展的基于互补金属氧化物半导体(CMOS)的方法。为了解决这个问题,我们建议将新兴的非易失性存储器(eNVM)和 ▪ CMOS 电路进行单片共同集成。仿真结果表明,每个直流电源的功耗和占地面积都降低了 ▪。这样就可以在稀释冰箱的 ▪ 阶段集成多达一百万个基于 eNVM 的直流源,为近期大规模量子计算应用铺平道路。
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引用次数: 0
Design, construction and testing of the prototype cryogenic circulation centrifugal pump for the high energy photon source 高能光子源低温循环离心泵原型的设计、建造和测试
IF 1.8 3区 工程技术 Q3 PHYSICS, APPLIED Pub Date : 2024-07-26 DOI: 10.1016/j.cryogenics.2024.103900

A cryogenic circulation pump (CCP) with the small flow rate and low heat leakage, which is the key equipment of the cooling system for the cryogenic permanent magnet undulator (CPMU) and synchrotron monochromator in High Energy Photon Source(HEPS), is developed according to the design parameters and operation experiences. The mechanic structure of the CCP including a motor at room temperature, an impeller and a volute in the cryogenic environment is designed, and numerical simulation on the rotating shaft and internal flows are performed to predict the mechanical and hydrodynamic performances of the pump. Meanwhile, the experimental investigation of the CCP is carried out in the liquid nitrogen (LN2) cryogenic system, and the hydrodynamic performances of the CCP are verified experimentally. The results are shown that the calculated performances of the CCP are in reasonable agreement with the experimental results, which indicates that the numerical calculation model of the CCP is more effective. Moreover, the deviations of pressure drop and efficiency between the calculation and measurement are analyzed in this paper.

高能光子源(HEPS)中的低温永磁起电机(CPMU)和同步加速器单色仪冷却系统的关键设备--小流量、低漏热的低温循环泵(CCP),根据设计参数和运行经验研制了CCP。设计了 CCP 的机械结构,包括室温下的电机、叶轮和低温环境下的涡壳,并对旋转轴和内部流动进行了数值模拟,预测了泵的机械和流体力学性能。同时,在液氮(LN2)低温系统中对 CCP 进行了实验研究,并通过实验验证了 CCP 的流体力学性能。结果表明,CCP 的计算性能与实验结果基本一致,这表明 CCP 的数值计算模型更加有效。此外,本文还分析了计算结果与测量结果在压降和效率方面的偏差。
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引用次数: 0
期刊
Cryogenics
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