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Microstructure evolution in a Fe-Ni-Si alloy during heat treatment and electron irradiation Fe-Ni-Si合金在热处理和电子辐照过程中的组织演变
Pub Date : 2021-10-01 DOI: 10.17804/2410-9908.2021.5.036-043
S. Danilov
Experiments have been made on studying structural and phase changes by the residual resistivity method in a Fe-Ni-Si alloy during annealing and electron irradiation. Thermal diffusion starts above 600 K and ensures decomposition of the solid solution up to 700 K; at higher temperatures it provides homogenization of the solid solution with the dissolution of intermetallic compounds in accordance with the equilibrium phase diagram. It is shown that, upon irradiation with electrons above 240 K, vacancy clusters are formed in both the aged and quenched alloys. Dissociation of clusters occurs at temperatures ranging between 350 and 500 K and leads to solid solution decomposition under the influence of diffusion caused by migrating vacancies with the formation of intermetallic precipitates. Irradiation at 423 K causes migration of vacancies and decomposition of the solid solution. In alloys irradiated at both temperatures above 700 K, as well as in unirradiated alloys, the precipitates dissolve in accordance with a single equilibrium dependence.
用残余电阻率法研究了Fe-Ni-Si合金在退火和电子辐照过程中的结构和相变化。热扩散从600 K以上开始,确保分解到700 K的固溶体;在较高的温度下,它使固溶体均匀化,金属间化合物的溶解符合平衡相图。结果表明,在240 K以上的电子辐照下,时效合金和淬火合金都形成了空位团簇。在350 ~ 500 K的温度范围内,团簇发生解离,并在迁移空位引起的扩散影响下导致固溶体分解,形成金属间析出物。423 K辐照引起空位迁移和固溶体分解。在700 K以上的温度下辐照的合金和未辐照的合金中,析出相都按照单一的平衡关系溶解。
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引用次数: 0
Mechanical properties and structure formation of aluminum-silicon alloys after friction stir processing 搅拌摩擦处理后铝硅合金的力学性能和组织形成
Pub Date : 2021-10-01 DOI: 10.17804/2410-9908.2021.5.044-059
А. V. Chumaevsky, D. V. Indoitu, А. V. Sudarikov, А. Zykova, А. R. Dobrovolsky, T. Kalashnikova, V. Е. Rubtsov, Е. А. Kolubaev
This study presents the results of experimental work on obtaining and investigating samples obtained by multipass friction stir processing of the Al-12 %Si and Al-9 %Si aluminum-silicon alloys. The results indicate a beneficial effect of friction stir processing on the strength properties of both alloys. The number of tool passes along the processing line has no effect on the mechanical properties and particle size of silicon in the aluminum matrix. The greatest influence on the mechanical properties is exerted by the first pass with the tool. The yield strength of the processed Al-9 %Si alloy increases by more than a factor of 1.5, whereas for the Al-12 %Si alloy there is no increase in yield strength. The tensile strength of the Al-12 %Si alloy increases by 17 %, while that of the Al-9 %Si alloy increases by 29 %. The most significant is the increase in relative elongation to failure, namely 77 % for Al-12 %Si and 113 % for Al-9 %Si.
本文介绍了对al - 12% Si和al - 9% Si铝硅合金进行多道次搅拌摩擦加工获得的样品的实验研究结果。结果表明,搅拌摩擦处理对两种合金的强度性能都有良好的影响。加工过程中刀具次数对铝基体中硅的力学性能和粒度没有影响。对机械性能影响最大的是刀具的第一次加工。加工后的al - 9% Si合金的屈服强度提高了1.5倍以上,而al - 12% Si合金的屈服强度没有提高。al - 12% Si合金的拉伸强度提高了17%,al - 9% Si合金的拉伸强度提高了29%。最显著的是相对延伸率的增加,al - 12% Si为77%,al - 9% Si为113%。
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引用次数: 1
Parallel technology for solving nonstationary heat conduction problems in axisymmetric domains 求解轴对称域非稳态热传导问题的并行技术
Pub Date : 2021-10-01 DOI: 10.17804/2410-9908.2021.6.60-71
L. Spevak, O. Nefedova
The paper develops a parallel algorithm and program for solving nonstationary heat conduction and diffusion problems in axisymmetric domains with axisymmetric boundary conditions. The numerical solution is based on the boundary element method. In order to optimize and enhance the effectiveness of the computer implementation of the algorithm, the computations are parallelized and the OpenMP application program interface is used. The program is tested by comparing the calculation results with the data of known exact solutions. The calculations confirm the correctness of the numerical solutions and the possibility of full scaling at different numbers of boundary elements according to the number of cores/processors available. The program is applicable to solving axisymmetric heat conduction and diffusion problems and, as a component of a software system, to solving nonlinear problems.
本文开发了一种求解轴对称边界条件下轴对称域非稳态热传导扩散问题的并行算法和程序。数值解基于边界元法。为了优化和提高算法的计算机实现效率,采用了并行计算和OpenMP应用程序接口。通过将计算结果与已知精确解的数据进行比较,对程序进行了验证。计算证实了数值解的正确性,以及根据可用的内核/处理器数量,在不同数量的边界元素上实现完全缩放的可能性。该程序适用于求解轴对称热传导和扩散问题,作为软件系统的组成部分,也可用于求解非线性问题。
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引用次数: 0
Features of magnetostriction in carbon steels 碳钢的磁致伸缩特性
Pub Date : 2021-10-01 DOI: 10.17804/2410-9908.2021.5.006-014
V. Novikov, K. Muratov, S. M. Kulak, A. Parakhin, R. Sokolov
Magnetostriction of the tempered 60G steel in the magnetic field of a solenoid is studied. A technique is proposed for dividing magnetostriction into components, namely those induced by the displacement of interdomain boundaries and those caused by the mechanism of rotation of spin magnetic moments. The dependences of the magnetostriction components on the tempering temperature of the hardened steel are constructed. This contributes to an increase in the effectiveness (accuracy) of evaluating elastic stresses in a steel structure by magnetoelastic methods. The essence of the technique lies in the application of the Langevin function to describing the experimental magnetostriction curves of the tempered 60G steel.
研究了回火60G钢在电磁阀磁场中的磁致伸缩特性。提出了一种将磁致伸缩分解为畴间边界位移引起的磁致伸缩分量和自旋磁矩旋转机制引起的磁致伸缩分量的方法。构造了磁致伸缩分量与淬火钢回火温度的关系。这有助于提高用磁弹性方法评估钢结构弹性应力的有效性(准确性)。该技术的实质在于应用朗之万函数来描述回火60G钢的实验磁致伸缩曲线。
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引用次数: 1
Analysis of specific kinetic energy for the Birikh–Ostroumov shear diffusion flow Birikh-Ostroumov剪切扩散流的比动能分析
Pub Date : 2021-06-01 DOI: 10.17804/2410-9908.2021.3.055-070
N. Burmasheva, E. Prosviryakov
The article presents a new exact solution for stratified steady-state shear diffusion flows of a viscous fluid in an infinite horizontal layer with impenetrable boundaries. The announced exact solution belongs to the Ostroumov–Birikh family. Two components of the velocity vector depend on the vertical (transverse) coordinate. The concentration field and the pressure field are described by linear forms relative to horizontal (longitudinal) coordinates, with coefficients depending on the third coordinate. The components of the velocity field and the shear stress field are analyzed in detail, and the behavior of the specific kinetic energy is studied. It is shown that this exact solution is capable of describing the stratification of the shear stress field and the nonmonotonic behavior of flow velocity. The relation of flow velocities and shear stresses to the distribution of specific kinetic energy is revealed.
本文给出了粘性流体在具有不可穿透边界的无限水平层中分层稳态剪切扩散流动的一种新的精确解。公布的确切解决方案属于奥斯特鲁莫夫-比克家族。速度矢量的两个分量依赖于垂直(横向)坐标。浓度场和压力场以相对于水平(纵向)坐标的线性形式描述,其系数取决于第三个坐标。详细分析了速度场和剪切应力场的组成,研究了比动能的变化规律。结果表明,该精确解能够描述剪切应力场的分层和流速的非单调特性。揭示了流速和剪应力与比动能分布的关系。
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引用次数: 0
In-situ nuclear reaction analysis 现场核反应分析
Pub Date : 2021-06-01 DOI: 10.17804/2410-9908.2021.4.006-014
V. Vykhodets, T. Kurennykh
The principles of in-situ nuclear reaction techniques and the need for them in various fields of scientific research are considered; several examples of the application of these techniques are given. It is shown that the techniques of in-situ nuclear reactions are effective in studying the diffusion of deuterium in metals at temperatures below room temperature, the diffusion of deuterium in proton-conducting oxides, the quantum diffusion of deuterium in metals at cryogenic temperatures, and the chemical composition of oxide nanopowders when they are heated in vacuum. Promising applications of nuclear reaction techniques in situ are formulated.
讨论了原位核反应技术的原理及其在各个科学研究领域的需要;给出了这些技术的几个应用实例。结果表明,原位核反应技术可以有效地研究氘在室温以下金属中的扩散、氘在质子导电氧化物中的扩散、低温下氘在金属中的量子扩散以及真空加热时氧化物纳米粉的化学组成。阐述了核反应技术在现场的应用前景。
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引用次数: 0
The influence of 2 at. % Si addition on the annealing of radiation-induced defects in the Fe-13Cr alloy 2 at的影响。添加% Si对Fe-13Cr合金辐射缺陷退火的影响
Pub Date : 2021-06-01 DOI: 10.17804/2410-9908.2021.4.023-033
A. Nikolaev
The paper presents data on electrical resistivity recovery in the Fe-13.4Cr and Fe13.6Cr-1.9Si alloys during isochronal annealing after 5 MeV electron irradiation below 77 K. Long-range migration of radiation-induced defects starts slightly above 200 K in Fe-13.4Cr. The silicon addition in Fe13.6Cr-1.9Si leads to immobilization of Frenkel pair defects thus making the peaks of the stages of the onset of long-range migration shift towards high temperatures up to 370 K and 420 K for self-interstitial atoms and vacancies, respectively. This finding confirms the data obtained earlier for Fe16Cr-Si alloys by means of positron annihilation technique (JNM 508(2018) 100–106) on trapping of radiation-induced defects on Si agglomerates (clusters consisting of several silicon atoms) formed during defect migration.
本文介绍了Fe-13.4Cr和Fe13.6Cr-1.9Si合金在77 K以下5 MeV电子辐照等时退火过程中的电阻率恢复数据。在Fe-13.4Cr中,辐射诱导缺陷的远程迁移开始于略高于200k的位置。在Fe13.6Cr-1.9Si中加入硅导致Frenkel对缺陷的固定化,从而使自间隙原子和空位的远程迁移起始阶段的峰值分别向高达370 K和420 K的高温移动。这一发现证实了之前通过正电子湮没技术(JNM 508(2018) 100-106)获得的Fe16Cr-Si合金在缺陷迁移过程中形成的Si团聚体(由几个硅原子组成的团簇)上捕获辐射诱导缺陷的数据。
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引用次数: 0
Elemental composition of calcium phosphate coatings modified with Fe-Cu nanoparticles 铁-铜纳米粒子修饰磷酸钙涂层的元素组成
Pub Date : 2021-06-01 DOI: 10.17804/2410-9908.2021.4.015-022
V. Chebodaeva, M. Sedelnikova, O. Bakina, Y. Sharkeev
The object of research is calcium-phosphate coatings doped with Fe-Cu nanoparticles. The elemental composition of the calcium-phosphate (CаP) coatings deposited by the microarc oxidation (MAO) method at a voltage of 250 V is studied. The quantitative content and distribution of Ca, P, O, Ti, Fe, and Cu over the coating surface prove to depend on the introduced additional electrolyte components. After modification with Fe-Cu nanoparticles, the Ca content increases from 4.5 at. % to 6.7 at. %. The amount of P and Ti after the introduction of nanoparticles increases from 11.7 to 22.3 at. % and from 7.9 to 15.8 at. %. Oxygen concentration, on the contrary, decreases from 75.9 to 55.0 at. %.
研究对象是掺杂Fe-Cu纳米颗粒的磷酸钙涂层。研究了在250 V电压下微弧氧化法制备的磷酸钙(c500p)涂层的元素组成。Ca、P、O、Ti、Fe和Cu在涂层表面的定量含量和分布取决于引入的附加电解质成分。Fe-Cu纳米粒子修饰后,Ca含量由4.5 at增加。%至6.7%。%。引入纳米粒子后,P和Ti的含量由11.7 at增加到22.3 at。%,从7.9%到15.8%。%。相反,氧浓度从75.9 at降低到55.0 at。%。
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引用次数: 0
Pressure dependence of shear stress during high-pressure torsion of the Au–Co alloys in liquid nitrogen 液氮中Au-Co合金高压扭转过程中剪切应力的压力依赖性
Pub Date : 2021-06-01 DOI: 10.17804/2410-9908.2021.3.006-016
T. Tolmachev, V. Pilyugin, A. M. Patselov, N. Nikolayeva, A. Vlasova
Measurements of the shear stress were carried out during mechanical alloying by high-pressure torsion of gold-cobalt powder mixing under cryogenic temperature at various pressures for the first time. The pressures were about 5, 8, 10 and 12 GPa. The Au–Co system is characterized by restricted solubility and difference in properties of the constituents. It was found that, in compari-son with the data obtained at room torsion temperature, the values of the shear stress are higher both at the stage of the initial intensive growth and subsequently, upon reaching saturation. With an in-crease in pressure of low-temperature mechanical alloying, a corresponding increase in the resistance to shear strain is observed at all stages of processing. In this case, the shape of the curves at each new pressure changes, as does the staging of the strain dependence. This reflects the extreme heter-ogeneity of the structure formation and phase composition processes of the non-equilibrium alloy. The most intense reflections in the X-ray diffractogram correspond to supersaturated fcc solid solu-tion of cobalt based on gold-base matrix. Also as a result of mechanical alloying, the components of the system are evenly distributed on the fracture surface of the alloy.
首次对金钴混合粉在不同压力下低温高压扭转机械合金化过程中的剪切应力进行了测量。压力分别为5、8、10和12 GPa。Au-Co体系的特点是溶解度有限,组分性质不同。结果表明,与室温下的数据相比,在初始强度生长阶段和随后达到饱和阶段,剪切应力值都更高。随着低温机械合金化压力的增加,在加工的各个阶段都观察到抗剪切应变的相应增加。在这种情况下,在每个新的压力下,曲线的形状会发生变化,应变依赖性的阶段也会发生变化。这反映了非平衡合金的组织形成和相组成过程的极端异质性。x射线衍射图中反射最强烈的是基于金基基体的钴的过饱和fcc固溶体。同样由于机械合金化,系统的成分均匀地分布在合金的断口表面。
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引用次数: 0
On the rational choice of the properties of structural elements constituting unidirectional compositions 论构成单向组合的结构要素性质的合理选择
Pub Date : 2021-06-01 DOI: 10.17804/2410-9908.2021.3.045-054
V. V. Struzhanov
A technique is proposed that makes it possible to implement a rational choice of fibers constituting a unidirectional tensile composite. The choice is made in such a way as to avoid catastrophic failure. The tensile properties of the fibers are characterized by complete deformation diagrams with falling branches. It is shown that the fibers must have different properties since it is impossible to avoid a catastrophe (dynamic fracture of the composite) if the properties are identical.
提出了一种技术,使合理选择构成单向拉伸复合材料的纤维成为可能。这样做是为了避免灾难性的失败。纤维的拉伸性能表现为带有落枝的完整变形图。结果表明,如果纤维的性能相同,则不可能避免复合材料的动态断裂,因此纤维的性能必然不同。
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引用次数: 0
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Diagnostics, Resource and Mechanics of materials and structures
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