Pub Date : 2024-09-12DOI: 10.1007/s10762-024-01011-x
Masaya Nagai, Sou Watanabe, Ryosuke Imamura, Masaaki Ashida, Kohei Shimoyama, Haobo Li, Azusa N. Hattori, Hidekazu Tanaka
We present two ideas to simplify the measurement and analysis of terahertz time-domain spectroscopic ellipsometry data of ultrathin films. The measurement is simplified by using a specially designed sample holder with mirrors, which can be mounted on a cryostat. It allows us to perform spectroscopic ellipsometry by simply inserting the holder into a conventional terahertz spectroscopy system for measurements in transmission geometry. The analysis of the obtained data is simplified by considering a single interface with a certain sheet conductivity ({sigma }_{s}) (since the film thickness is significantly smaller than the wavelength of the terahertz light). We demonstrate the application of these ideas by evaluating the sheet conductivities of two perovskite rare-earth nickelate thin films in the temperature range 78–478 K. The use of this particular analytical method and the sample holder design will help to establish terahertz time-domain spectroscopic ellipsometry as a characterization technique for ultrathin films.
我们提出了两个简化超薄薄膜太赫兹时域光谱椭偏仪数据测量和分析的想法。通过使用专门设计的带反射镜的样品支架来简化测量,该支架可安装在低温恒温器上。只需将样品架插入传统的太赫兹光谱系统中,即可进行透射几何测量,从而实现光谱椭偏测量。考虑到单个界面具有一定的片状电导率 ({sigma}_{s})(因为薄膜厚度明显小于太赫兹光的波长),可以简化对所获数据的分析。我们通过评估 78-478 K 温度范围内两种过氧化物稀土镍酸盐薄膜的片状电导率来演示这些想法的应用。使用这种特殊的分析方法和样品支架设计将有助于建立太赫兹时域光谱椭偏仪作为超薄薄膜的表征技术。
{"title":"Characterization of Ultrathin Conductive Films Using a Simplified Approach for Terahertz Time-Domain Spectroscopic Ellipsometry","authors":"Masaya Nagai, Sou Watanabe, Ryosuke Imamura, Masaaki Ashida, Kohei Shimoyama, Haobo Li, Azusa N. Hattori, Hidekazu Tanaka","doi":"10.1007/s10762-024-01011-x","DOIUrl":"https://doi.org/10.1007/s10762-024-01011-x","url":null,"abstract":"<p>We present two ideas to simplify the measurement and analysis of terahertz time-domain spectroscopic ellipsometry data of ultrathin films. The measurement is simplified by using a specially designed sample holder with mirrors, which can be mounted on a cryostat. It allows us to perform spectroscopic ellipsometry by simply inserting the holder into a conventional terahertz spectroscopy system for measurements in transmission geometry. The analysis of the obtained data is simplified by considering a single interface with a certain sheet conductivity <span>({sigma }_{s})</span> (since the film thickness is significantly smaller than the wavelength of the terahertz light). We demonstrate the application of these ideas by evaluating the sheet conductivities of two perovskite rare-earth nickelate thin films in the temperature range 78–478 K. The use of this particular analytical method and the sample holder design will help to establish terahertz time-domain spectroscopic ellipsometry as a characterization technique for ultrathin films.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"38 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-09-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142220813","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-09-11DOI: 10.1007/s10762-024-01010-y
Haitham Hamada, Mohamed Mamdouh M. Ali, Shoukry I. Shams, Mahmoud Elsaadany, Ashraf A. M. Khalaf, A. M. M. A. Allam, A. Kishk
Recent developments in communication networks are catering to dynamic requirements as well as providing facilities for future potential applications that are significantly expanded. This necessitates the emergence of mm-wave components that exhibit desirable electrical characteristics, such as compactness, cost efficiency, and minimal manufacturing complexity. Gap waveguide (GW) technology is being considered a potential solution since it provides a promising guiding structure for millimetre-wave applications. This paper presents a novel out-of-phase power divider using the standard waveguide WR-15 interface. The presented power divider is based on a trapped printed gap waveguide (TPGW), which is designed to employ aperture coupling to achieve a stable (180^{circ }) phase imbalance. The power divider and transition have been designed and optimised to minimise the reflection coefficient at the input WR-15 port within the desired frequency range of 50-65 GHz. A deep matching level of beyond (-)20 dB is sufficient to obtain a relative bandwidth of 29% at 60 GHz. A back-to-back model is developed to validate the performance of the proposed power divider configuration and a standard WR-15 waveguide. Furthermore, mathematical analyses are performed to investigate the relationship between the back-to-back model and the individual power divider. A prototype for the proposed power divider through a back-to-back structure is fabricated to validate its performance, and good agreement is achieved between the simulated and measured results.
{"title":"A 60-GHz Out-of-Phase Power Divider with WR-15 Standard Interface Based on Trapped Printed Gap Waveguide Technology","authors":"Haitham Hamada, Mohamed Mamdouh M. Ali, Shoukry I. Shams, Mahmoud Elsaadany, Ashraf A. M. Khalaf, A. M. M. A. Allam, A. Kishk","doi":"10.1007/s10762-024-01010-y","DOIUrl":"https://doi.org/10.1007/s10762-024-01010-y","url":null,"abstract":"<p>Recent developments in communication networks are catering to dynamic requirements as well as providing facilities for future potential applications that are significantly expanded. This necessitates the emergence of mm-wave components that exhibit desirable electrical characteristics, such as compactness, cost efficiency, and minimal manufacturing complexity. Gap waveguide (GW) technology is being considered a potential solution since it provides a promising guiding structure for millimetre-wave applications. This paper presents a novel out-of-phase power divider using the standard waveguide WR-15 interface. The presented power divider is based on a trapped printed gap waveguide (TPGW), which is designed to employ aperture coupling to achieve a stable <span>(180^{circ })</span> phase imbalance. The power divider and transition have been designed and optimised to minimise the reflection coefficient at the input WR-15 port within the desired frequency range of 50-65 GHz. A deep matching level of beyond <span>(-)</span>20 dB is sufficient to obtain a relative bandwidth of 29% at 60 GHz. A back-to-back model is developed to validate the performance of the proposed power divider configuration and a standard WR-15 waveguide. Furthermore, mathematical analyses are performed to investigate the relationship between the back-to-back model and the individual power divider. A prototype for the proposed power divider through a back-to-back structure is fabricated to validate its performance, and good agreement is achieved between the simulated and measured results.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"114 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-09-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142227318","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-09-07DOI: 10.1007/s10762-024-01012-w
Tim Vogel, Clara J. Saraceno
We provide a comprehensive technical analysis of the data acquisition process with oscillating delay lines for Terahertz-time domain spectroscopy. The utilization of these rapid stages, particularly in high-repetition-rate systems, is known to enable an effective reduction of noise content through averaging. However, caution must be exercised to optimize the data averaging process, with the goal of significantly optimizing the dynamic range (DR) and signal-to-noise ratio (SNR). Here we discuss some pitfalls to avoid and the effect of improper data handling on the dynamic range obtainable. A free and open-source program, called parrot (Processing All Rapidly & Reliably Obtained THz-traces), is provided alongside this publication to overcome the discussed pitfalls and facilitate the acceleration of experimental setups and data analysis, thereby enhancing signal fidelity and reproducibility.
我们对太赫兹时域光谱中使用振荡延迟线的数据采集过程进行了全面的技术分析。众所周知,利用这些快速阶段,特别是在高重复率系统中,可以通过平均有效减少噪声含量。然而,必须谨慎优化数据平均过程,以显著优化动态范围(DR)和信噪比(SNR)。在此,我们将讨论一些需要避免的误区,以及数据处理不当对可获得动态范围的影响。本刊物还提供了一个名为 parrot(Processing All Rapidly & Reliably Obtained THz-traces)的免费开放源码程序,以克服所讨论的陷阱,促进实验设置和数据分析的加速,从而提高信号的保真度和可重复性。
{"title":"Advanced Data Processing of THz-Time Domain Spectroscopy Data with Sinusoidally Moving Delay Lines","authors":"Tim Vogel, Clara J. Saraceno","doi":"10.1007/s10762-024-01012-w","DOIUrl":"https://doi.org/10.1007/s10762-024-01012-w","url":null,"abstract":"<p>We provide a comprehensive technical analysis of the data acquisition process with oscillating delay lines for Terahertz-time domain spectroscopy. The utilization of these rapid stages, particularly in high-repetition-rate systems, is known to enable an effective reduction of noise content through averaging. However, caution must be exercised to optimize the data averaging process, with the goal of significantly optimizing the dynamic range (DR) and signal-to-noise ratio (SNR). Here we discuss some pitfalls to avoid and the effect of improper data handling on the dynamic range obtainable. A free and open-source program, called <i>parrot</i> (Processing All Rapidly & Reliably Obtained THz-traces), is provided alongside this publication to overcome the discussed pitfalls and facilitate the acceleration of experimental setups and data analysis, thereby enhancing signal fidelity and reproducibility.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"60 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-09-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142220811","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-08-31DOI: 10.1007/s10762-024-00998-7
Alex Shteinman, Yaakov Anker, Moshe Einat
Deep geothermal drilling is a necessary technological stage to produce renewable energy by “enhanced geothermal systems” everywhere. However, the high cost and complexity of deep drilling through hard rock formations is a major barrier to its commercialization. One approach to reach affordability and reduce the cost of deep drilling is to use millimeter-wave (mmw) gyrotron radiation to melt or vaporize rocks. In this paper, the results of an experimental study of mmw radiation absorption by hard rocks are presented. Electromagnetic attenuation and reflection were measured in W-band at frequencies from 75 to 110 GHz in eight rock samples from six different geological formations originated in Israel. The results show that the mmw radiation absorption in hard rocks ranges from 90 to 99% per centimeter. The absorption varies slightly with rock type and is relatively independent of frequency but has reached higher values at the upper W band for all samples. The study suggests that high-power mmw radiation is a promising technology for deep geothermal drilling. The results of this experiment, attenuation, and reflection of W-band radiation in hard rocks provide valuable information for the design and optimization of mmw-based drilling systems, and will support the design and optimization of gyrotron based hard rock drilling equipment for geothermal applications.
深层地热钻探是各地通过 "强化地热系统 "生产可再生能源的必要技术阶段。然而,在坚硬岩层中进行深层钻探的高成本和复杂性是其商业化的主要障碍。要达到可负担性并降低深层钻探成本,一种方法是使用毫米波(mmw)陀螺辐射来熔化或汽化岩石。本文介绍了硬质岩石对毫米波辐射吸收的实验研究结果。在 W 波段 75 至 110 千兆赫频率范围内,对来自以色列六种不同地质构造的八个岩石样本进行了电磁衰减和反射测量。结果表明,硬质岩石对毫米波辐射的吸收率为每厘米 90% 至 99%。吸收率随岩石类型的不同而略有差异,与频率也相对无关,但所有样本在高 W 波段的吸收率都较高。这项研究表明,大功率毫米波辐射是一种很有前途的深层地热钻探技术。该实验的结果、W 波段辐射在坚硬岩石中的衰减和反射为基于毫米波的钻探系统的设计和优化提供了有价值的信息,并将为地热应用中基于陀螺仪的坚硬岩石钻探设备的设计和优化提供支持。
{"title":"Hard Rock Absorption Measurements in the W-Band","authors":"Alex Shteinman, Yaakov Anker, Moshe Einat","doi":"10.1007/s10762-024-00998-7","DOIUrl":"https://doi.org/10.1007/s10762-024-00998-7","url":null,"abstract":"<p>Deep geothermal drilling is a necessary technological stage to produce renewable energy by “enhanced geothermal systems” everywhere. However, the high cost and complexity of deep drilling through hard rock formations is a major barrier to its commercialization. One approach to reach affordability and reduce the cost of deep drilling is to use millimeter-wave (mmw) gyrotron radiation to melt or vaporize rocks. In this paper, the results of an experimental study of mmw radiation absorption by hard rocks are presented. Electromagnetic attenuation and reflection were measured in W-band at frequencies from 75 to 110 GHz in eight rock samples from six different geological formations originated in Israel. The results show that the mmw radiation absorption in hard rocks ranges from 90 to 99% per centimeter. The absorption varies slightly with rock type and is relatively independent of frequency but has reached higher values at the upper W band for all samples. The study suggests that high-power mmw radiation is a promising technology for deep geothermal drilling. The results of this experiment, attenuation, and reflection of W-band radiation in hard rocks provide valuable information for the design and optimization of mmw-based drilling systems, and will support the design and optimization of gyrotron based hard rock drilling equipment for geothermal applications.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"8 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-08-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142220775","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
This work reports an ultra-low noise, multi-stage stagger-tuned low-noise amplifier (MS-ST-LNA) over the D-band performance and achieves a best trade-off between noise, bandwidth, and gain parameters. The ultra-low-noise is achieved in three ways: First, the high-gain 3-stage stagger tuned amplifier (STA) realizes a 3X gain compared to the conventional single-stage amplifier, which sets a low floor noise. Second, the stagger-tuned amplifier achieves 1.6 times lower noise than the traditional single-stage amplifier. Finally, the stagger tune realizes a high-order transfer function, which mitigates the high-frequency noise. The full LNA is implemented and fabricated using a commercial nano-manufacturing 9-nm graphene film FET on a silicon wafer using a 0.065-μm commercial process, occupying an area of 0.21 mm2. The proposed design achieves an optimum performance: a maximum measured gain of 20.5 dB and a minimum noise figure (NF) of 4.2 dB over 123.7 to 162.5 GHz. The proposed LNA consumes ultra-low power consumption of 21.3 mW under the power supply of 1.2 V.
{"title":"Performance Analysis of Novel Graphene Process Low-Noise Amplifier with Multi-stage Stagger-Tuned Approach over D-band","authors":"Porika Nandini, Deepak Naik Jatoth, Pradeep Gorre, Manishankar Prasad Gupta, Sandeep Kumar, AlaaDdin Al-Shidaifat, Hanjung Song","doi":"10.1007/s10762-024-01009-5","DOIUrl":"https://doi.org/10.1007/s10762-024-01009-5","url":null,"abstract":"<p>This work reports an ultra-low noise, multi-stage stagger-tuned low-noise amplifier (MS-ST-LNA) over the D-band performance and achieves a best trade-off between noise, bandwidth, and gain parameters. The ultra-low-noise is achieved in three ways: First, the high-gain 3-stage stagger tuned amplifier (STA) realizes a 3X gain compared to the conventional single-stage amplifier, which sets a low floor noise. Second, the stagger-tuned amplifier achieves 1.6 times lower noise than the traditional single-stage amplifier. Finally, the stagger tune realizes a high-order transfer function, which mitigates the high-frequency noise. The full LNA is implemented and fabricated using a commercial nano-manufacturing 9-nm graphene film FET on a silicon wafer using a 0.065-μm commercial process, occupying an area of 0.21 mm<sup>2</sup>. The proposed design achieves an optimum performance: a maximum measured gain of 20.5 dB and a minimum noise figure (NF) of 4.2 dB over 123.7 to 162.5 GHz. The proposed LNA consumes ultra-low power consumption of 21.3 mW under the power supply of 1.2 V.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"68 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-08-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142220779","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Conventional baseband processing techniques for communication must be adapted to the specificities of terahertz channels. Currently, there is limited research on channel coding applicable to terahertz bands, particularly in terms of performing real-time tests that differentiate them from offline processing. This paper presents a test platform for a 300 GHz wireless communication system based on the PXIe platform. The experiment utilizes a high-performance, low-complexity serial scheduling approach with the Minimum Sum-Log Likelihood Ratio Belief Propagation (MS-LLR-BP) soft decision decoding algorithm to test point-to-point real-time line-of-sight communication for low-density parity-check (LDPC) code communication systems. The results indicate that the implementation of LDPC coding in QPSK terahertz wireless transmission systems results in a performance enhancement of approximately 25–55% in bit error rate (BER), demonstrating the excellent performance of LDPC codes against terahertz channel fading. This highlights their potential in future ultra-high-speed communication systems.
{"title":"Experiment and Performance Analysis on PXIe-Based Real-Time Terahertz Wireless Communication with LDPC Code","authors":"Zhuoyu Zhang, Jiahui Wang, Yunchuan Liu, Zhe Yang, Cunlin Zhang, Jingsuo He","doi":"10.1007/s10762-024-01007-7","DOIUrl":"https://doi.org/10.1007/s10762-024-01007-7","url":null,"abstract":"<p>Conventional baseband processing techniques for communication must be adapted to the specificities of terahertz channels. Currently, there is limited research on channel coding applicable to terahertz bands, particularly in terms of performing real-time tests that differentiate them from offline processing. This paper presents a test platform for a 300 GHz wireless communication system based on the PXIe platform. The experiment utilizes a high-performance, low-complexity serial scheduling approach with the Minimum Sum-Log Likelihood Ratio Belief Propagation (MS-LLR-BP) soft decision decoding algorithm to test point-to-point real-time line-of-sight communication for low-density parity-check (LDPC) code communication systems. The results indicate that the implementation of LDPC coding in QPSK terahertz wireless transmission systems results in a performance enhancement of approximately 25–55% in bit error rate (BER), demonstrating the excellent performance of LDPC codes against terahertz channel fading. This highlights their potential in future ultra-high-speed communication systems.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"295 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-08-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142220812","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-08-17DOI: 10.1007/s10762-024-01008-6
Jacqueline Damas, Niels Neumann, Abdi T. Abdalla, Dirk Plettemeier
Indoor wireless systems at 60 GHz provide much higher throughput than today’s solutions but need more closely spaced access points. Radio-over-Fiber advancements are a promising solution for the signal distribution. We propose a broadband IF-over-Fiber architecture comprised of miniaturized electronic components for quadrature modulation and upconversion. The 60 GHz wireless generation is realized by transmitting at intermediate frequency (IF) at 10 GHz over single mode fiber (SMF) and upconversion at the base station (BS) front-end with low-cost electronic components on printed circuit board (PCB). The central station (CS) includes an electronic IQ modulator for the provision of multi-Gbps quadrature data modulation formats and successively increase the spectral efficiency of the wirelessly transmitted data. The BS front-end comprises of the 60 GHz upconverter and a 60 GHz planar 2(times )2 microstrip antenna array. The 10 GHz IF carrier allows an optical transmission with higher spectral efficiency in optical domain, as well as it is less susceptible to dispersion induced power fading inherent in optical fiber. The optical fronthaul link of the 10 GHz IF signal modulated with up to 2 Gbps payload data over SMF lengths of 2 km, 12.8 km and 25.6 km has been studied. The system analysis is made with respect to error vector magnitude (EVM), eye and constellation diagrams. The recovered QPSK data has signal-to-noise of 14 dB corresponding to EVM of 20% for transmission over 25.6 km SMF.
{"title":"Measurement of Broadband IF-over-Fiber Link for 60 GHz Wireless Applications","authors":"Jacqueline Damas, Niels Neumann, Abdi T. Abdalla, Dirk Plettemeier","doi":"10.1007/s10762-024-01008-6","DOIUrl":"https://doi.org/10.1007/s10762-024-01008-6","url":null,"abstract":"<p>Indoor wireless systems at 60 GHz provide much higher throughput than today’s solutions but need more closely spaced access points. Radio-over-Fiber advancements are a promising solution for the signal distribution. We propose a broadband IF-over-Fiber architecture comprised of miniaturized electronic components for quadrature modulation and upconversion. The 60 GHz wireless generation is realized by transmitting at intermediate frequency (IF) at 10 GHz over single mode fiber (SMF) and upconversion at the base station (BS) front-end with low-cost electronic components on printed circuit board (PCB). The central station (CS) includes an electronic IQ modulator for the provision of multi-Gbps quadrature data modulation formats and successively increase the spectral efficiency of the wirelessly transmitted data. The BS front-end comprises of the 60 GHz upconverter and a 60 GHz planar 2<span>(times )</span>2 microstrip antenna array. The 10 GHz IF carrier allows an optical transmission with higher spectral efficiency in optical domain, as well as it is less susceptible to dispersion induced power fading inherent in optical fiber. The optical fronthaul link of the 10 GHz IF signal modulated with up to 2 Gbps payload data over SMF lengths of 2 km, 12.8 km and 25.6 km has been studied. The system analysis is made with respect to error vector magnitude (EVM), eye and constellation diagrams. The recovered QPSK data has signal-to-noise of 14 dB corresponding to EVM of 20% for transmission over 25.6 km SMF.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"5 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-08-17","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142220814","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Measurements of terahertz absorption spectra of pharmaceutical hydrate samples are achieved under a normal humidity condition by combining terahertz frequency-domain spectroscopy with a newly proposed method for suppressing absorption peaks caused by water vapor. In this method, only simple mathematical operations such as subtraction, thresholding, interpolation, and smoothing are applied to extinction (or absorbance) data obtained by locating samples under a normal humidity condition. By considering the difference in spectral line width between narrow absorption peaks caused by water vapor and the relatively wide absorption peaks caused by active pharmaceutical ingredients (APIs) in solid forms, the absorption peaks caused by water vapor can be effectively suppressed without affecting the absorption peaks of the APIs in the samples. In the present study, levofloxacin hydrates were used as samples to investigate the performance of the proposed method. Spectra were obtained under both dry and normal humidity conditions. The temperature of the samples was raised from 300 to 363 K to dehydrate them and brought back to 313 K to observe hydration under the normal humidity condition. Spectra obtained under the normal humidity condition were processed with the proposed method. The spectra of the hydrates obtained under the dry condition were slightly different from those obtained under the normal humidity condition and processed by our method. Dehydration during the measurements under the dry condition was suggested. Stable and reliable results are expected by measuring spectra under normal humidity conditions and applying the proposed method to suppress absorption peaks by water vapor.
通过将太赫兹频域光谱与新提出的抑制水蒸气引起的吸收峰的方法相结合,在正常湿度条件下测量了药物水合物样品的太赫兹吸收光谱。在这种方法中,只需对正常湿度条件下通过定位样品获得的消光(或吸光度)数据进行简单的数学运算,如减法、阈值、插值和平滑。考虑到水蒸气引起的窄吸收峰与固体形式的活性药物成分(API)引起的相对较宽的吸收峰之间光谱线宽的差异,可以有效抑制水蒸气引起的吸收峰,而不影响样品中 API 的吸收峰。本研究以左氧氟沙星水合物为样品,考察了该方法的性能。光谱是在干燥和正常湿度条件下获得的。将样品温度从 300 K 升至 363 K 以使其脱水,然后将其温度降至 313 K 以观察正常湿度条件下的水合情况。在正常湿度条件下获得的光谱采用建议的方法进行处理。在干燥条件下获得的水合物光谱与在正常湿度条件下获得并用我们的方法处理的光谱略有不同。这表明在干燥条件下进行测量时出现了脱水现象。通过在正常湿度条件下测量光谱,并采用建议的方法抑制水蒸气的吸收峰,有望获得稳定可靠的结果。
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Pub Date : 2024-08-06DOI: 10.1007/s10762-024-01005-9
A. Ünal
Passive millimeter-wave (MMW) and TeraHertz (THz) imaging systems have become increasingly popular in recent years due to their cost-effectiveness and non-invasive characteristics compared to active systems, prompting a surge in research interest. Evaluating the quality of reconstructed images used in these systems is essential for revealing the fine details. General image quality metrics such as the structural similarity index (SSIM) and the peak signal-to-noise ratio (PSNR) require a reference image in order to compare the reconstructed image. However, there is a notable gap in the literature regarding the evaluation of reconstruction or deconvolution algorithms with a reference image in the passive MMW/THz bands. This study proposes a reference image generation technique for passive MMW/THz imaging systems using an infrared imaging system that shares a similar physical background. Then, passive MMW/THz images were evaluated using the reference images at varying target distances and spatial resolutions. Besides these, the assessment of passive MMW/THz images with the SSIM and PSNR metrics after the reconstruction algorithms were performed. The metrics SSIM and PSNR, are inadequate in the evaluation of reconstruction algorithms alone in terms of concealed object (CO) detection. Because of this reason, the contrast level (CL) method was proposed to address the application-based shortcomings of PSNR and SSIM metrics. Hence, the image quality metric, CL, indicates that the Richardson–Lucy (RL) algorithm yielded superior results in variable optical configurations and target distances with the aid of CL metric. Finally, contrast enhancement techniques were developed in order to increase the contrast level of the CO. As a result, the introduction of these novel methods—the reference image generation technique using an infrared imaging system in passive MMW/THz bands, the evaluation of the reconstructed images with the application-based CL metric, and contrast enhancement techniques for single-band or multi-band imaging methods—holds the potential for the development of innovative techniques. These advancements may contribute to the creation of new applications within the passive MMW/THz bands, particularly focusing on the improvement of detection methods in the future.
{"title":"New Assessment Methods in Passive MMW/THz Imaging Systems","authors":"A. Ünal","doi":"10.1007/s10762-024-01005-9","DOIUrl":"https://doi.org/10.1007/s10762-024-01005-9","url":null,"abstract":"<p>Passive millimeter-wave (MMW) and TeraHertz (THz) imaging systems have become increasingly popular in recent years due to their cost-effectiveness and non-invasive characteristics compared to active systems, prompting a surge in research interest. Evaluating the quality of reconstructed images used in these systems is essential for revealing the fine details. General image quality metrics such as the structural similarity index (SSIM) and the peak signal-to-noise ratio (PSNR) require a reference image in order to compare the reconstructed image. However, there is a notable gap in the literature regarding the evaluation of reconstruction or deconvolution algorithms with a reference image in the passive MMW/THz bands. This study proposes a reference image generation technique for passive MMW/THz imaging systems using an infrared imaging system that shares a similar physical background. Then, passive MMW/THz images were evaluated using the reference images at varying target distances and spatial resolutions. Besides these, the assessment of passive MMW/THz images with the SSIM and PSNR metrics after the reconstruction algorithms were performed. The metrics SSIM and PSNR, are inadequate in the evaluation of reconstruction algorithms alone in terms of concealed object (CO) detection. Because of this reason, the contrast level (CL) method was proposed to address the application-based shortcomings of PSNR and SSIM metrics. Hence, the image quality metric, CL, indicates that the Richardson–Lucy (RL) algorithm yielded superior results in variable optical configurations and target distances with the aid of CL metric. Finally, contrast enhancement techniques were developed in order to increase the contrast level of the CO. As a result, the introduction of these novel methods—the reference image generation technique using an infrared imaging system in passive MMW/THz bands, the evaluation of the reconstructed images with the application-based CL metric, and contrast enhancement techniques for single-band or multi-band imaging methods—holds the potential for the development of innovative techniques. These advancements may contribute to the creation of new applications within the passive MMW/THz bands, particularly focusing on the improvement of detection methods in the future.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"58 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-08-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141938288","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-08-05DOI: 10.1007/s10762-024-01006-8
V. V. Balandin, Vl. Vl. Balandin, D. A. Mansfeld, K. V. Mineev, V. V. Parkhachev, R. M. Rozental, A. V. Vodopyanov
A millimeter wave interferometer based on a Ka-band CW signal generator and a high-speed oscilloscope has been implemented, which makes it possible to carry out measurements without frequency conversion. The experimental measurements of the amplitude of transverse deformations of a metal rod caused by impact loading have been carried out. A good agreement between the calculated and measured data was revealed, demonstrating the possibility to measure microsecond-duration surface deviations with an accuracy of about 1 μm and a relative error of about 8%.
基于 Ka 波段 CW 信号发生器和高速示波器的毫米波干涉仪已经实现,这使得无需频率转换即可进行测量成为可能。对金属棒在冲击载荷作用下产生的横向变形幅度进行了实验测量。结果表明,计算数据和测量数据之间的一致性很好,证明可以测量微秒持续时间的表面偏差,精度约为 1 μm,相对误差约为 8%。
{"title":"Measuring Fast Mechanical Deformation with Micrometer Precision Based on Millimeter Wave Interferometry","authors":"V. V. Balandin, Vl. Vl. Balandin, D. A. Mansfeld, K. V. Mineev, V. V. Parkhachev, R. M. Rozental, A. V. Vodopyanov","doi":"10.1007/s10762-024-01006-8","DOIUrl":"https://doi.org/10.1007/s10762-024-01006-8","url":null,"abstract":"<p>A millimeter wave interferometer based on a Ka-band CW signal generator and a high-speed oscilloscope has been implemented, which makes it possible to carry out measurements without frequency conversion. The experimental measurements of the amplitude of transverse deformations of a metal rod caused by impact loading have been carried out. A good agreement between the calculated and measured data was revealed, demonstrating the possibility to measure microsecond-duration surface deviations with an accuracy of about 1 μm and a relative error of about 8%.</p>","PeriodicalId":16181,"journal":{"name":"Journal of Infrared, Millimeter, and Terahertz Waves","volume":"2 1","pages":""},"PeriodicalIF":2.9,"publicationDate":"2024-08-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141938289","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}