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A simplified mathematical model for total temperature rise calculation in non-oriented silicon steel cold rolling deformation zone 无取向硅钢冷轧变形区总温升计算的简化数学模型
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-20 DOI: 10.1051/metal/2021095
Guomin Han, Hongbo Li, Yujin Liu, J. Zhang, N. Kong, Zhiyuan Hu, Lei Liu
In tandem cold rolling, the control of the temperature of high-grade non-oriented silicon steel is a difficult problem for its large deformation resistance and the preheating procedure before rolling. And it is complicated to calculate the total temperature rise of rolling deformation zone due to the comprehensive influence of the plastic deformation heat, the friction heat and the contact heat loss. So, to precisely calculate the total temperature rise, firstly, based on the four classical cold rolling force formulas, the initial total temperature rise calculation models are established correspondingly by theoretically analyzing the temperature rise of deformation heat, the temperature rise of friction heat and the temperature drop of contact heat loss; then, the model based on the improved Lian rolling force formula is adopted, which leads to calculated best matching the measured temperature; finally, considering the complex formula calculation of the initial model, based on the influences of different rolling parameters on the total temperature rise, a simplified model for convenient calculation is proposed by the nonlinear regression analysis of the initial model calculation results and main rolling parameters, which is convenient for the actual application by the field technicians.
高档无取向硅钢因其抗变形能力大,且轧制前需预热,因此在冷轧连轧过程中,温度的控制是一个难题。由于塑性变形热、摩擦热和接触热损失的综合影响,轧制变形区总温升的计算比较复杂。因此,为了精确计算总温升,首先,在四种经典冷轧力公式的基础上,通过理论分析变形热温升、摩擦热温升和接触热损失温降,建立了相应的初始总温升计算模型;然后,采用基于改进的连轧力公式的模型,使计算结果与实测温度最匹配;最后,考虑到初始模型公式计算复杂,基于不同轧制参数对总温升的影响,通过对初始模型计算结果与主要轧制参数的非线性回归分析,提出了简化模型,便于计算,便于现场技术人员的实际应用。
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引用次数: 2
Effect of niobium and austenitizing temperature on the microstructures and properties of spray-deposited AISI M3:2 high speed steel 铌和奥氏体化温度对喷镀AISI M3:2高速钢组织和性能的影响
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-20 DOI: 10.1051/metal/2021097
Hebin Wang, D. Hong, L. Hou, Li Shen, P. Ou, LiFang Qiu, Zhi-gang Wang, Hong-jin Zhao
The microstructure and properties of niobium-containing AISI M3:2 high speed steels (HSSs) fabricated by spray forming and traditional casting have been investigated. The results show that fine and uniformly-distributed grains without macrosegregation appeared in the as-deposited HSSs that differ from those of as-cast HSSs. Nb mostly appears in primary MC carbides, whereas it contributes less to the formation of M6C carbides. The high stabilization of Nb-rich MC carbides can pin the grain boundaries during high-temperature austenitizing process, thus conferring a fine grains and raising the content of dissolved alloying elements. Enhanced precipitation strengthening and fine dispersion of NbC carbides throughout the matrix contribute to the high hardness and red hardness of Nb-containing HSS.
研究了喷射成形和传统铸造制备含铌AISI M3:2高速钢的组织和性能。结果表明:与铸态合金相比,沉积态合金的晶粒细小、分布均匀,无宏观偏析;Nb主要出现在初生MC碳化物中,而对M6C碳化物的形成贡献较小。在高温奥氏体化过程中,高稳定度的富铌碳化物能够固定晶界,从而获得细小的晶粒,提高合金中溶解元素的含量。NbC碳化物的析出强化和在基体中的精细分散,使含nb高速钢具有较高的硬度和红硬度。
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引用次数: 0
Significant impact of intercritical annealing temperature on microstructure and mechanical properties of Al substituted Si dual phase steel under ultra-rapid heating 临界间退火温度对Al取代Si双相钢超快速加热组织和力学性能的影响
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-07-01 DOI: 10.1051/metal/2021051
Y. Deng, R. Misra
The significant impact of ultra-rapid heating continuous annealing on microstructure and mechanical properties of Al substituted Si dual phase steel under hot-dip galvanized process was studied. The heating rate of 300 °C/s, and different annealing temperatures in the range of 750 °C to 810 °C were explored. The study indicated that the yield and tensile strengths are increased with the increase of intercritical annealing temperature during rapid heating continuous annealing. When the annealing temperature was 780 °C, the steel exhibited good comprehensive properties with yield strength of 574.9 MPa, tensile strength up to 1009 MPa, total elongation of 18.5%. This is attributed to refined microstructure, appropriate proportion of phases, high density of dislocations and finely distributed NbC precipitates. Furthermore, the variations in strength, elongation and strain-hardening behavior of the steel with thermomechanical parameters and the inherent mechanism for strengthening were further discussed in relation to the microstructural features.
研究了超快加热连续退火对热浸镀锌Al取代Si双相钢组织和力学性能的显著影响。研究了300℃/s的升温速率和750 ~ 810℃的不同退火温度。研究表明,在快速加热连续退火过程中,屈服强度和抗拉强度随着临界间退火温度的升高而提高。当退火温度为780℃时,钢的屈服强度为574.9 MPa,抗拉强度为1009 MPa,总伸长率为18.5%,综合性能良好。这主要是由于合金组织精细、相比例适宜、位错密度高、碳化硅析出物分布精细所致。进一步讨论了钢的强度、伸长率和应变硬化性能随热力学参数的变化规律以及强化的内在机理。
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引用次数: 1
Cyclic annealing versus continuous annealing of 20 wt.% chromium white cast iron 循环退火与20 wt连续退火。%铬白口铸铁
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-06-18 DOI: 10.1051/metal/2021044
S. S. Mandal, D. Mondal, K. Ghosh
To destabilize as-cast microstructure of 20 wt.% chromium white iron, cyclic annealing involving repeated austenitization for short duration of 0.6 h at 900, 950, 1000, 1050 and 1100 °C followed by forced air cooling is conducted as an alternative to continuous annealing requiring austenitization for longer period of 4–6 h at the said temperatures followed by furnace cooling. Continuous austenitization destabilizes the austenite matrix through precipitation of secondary carbides and transforms the alloy depleted austenite to pearlite on furnace cooling, thereby reducing the as-cast hardness from HV 669 to HV466. In contrast, repeated austenitization not only destabilizes the austenite matrix through precipitation of secondary carbides followed by its transformation to martensite on forced air cooling, but also causes disintegration of longer eutectic carbides to shorter segments with subsequent increase in hardness to as high as HV 890. Notched impact toughness after both continuous and cyclic annealing remains uniformly at 12.0 J as compared to as-cast value of 6.0 J. Besides, an unexpected rise in abrasive wear resistance after cyclic annealing treatment makes the alloy superior than that obtained by continuous annealing treatment as practiced in industries.
使20wt的铸态组织失稳。%铬白口铁,在900、950、1000、1050和1100℃下重复奥氏体化0.6 h的短时间循环退火,然后进行强制风冷,作为在上述温度下需要奥氏体化4-6 h的长时间连续退火,然后进行炉冷。连续奥氏体化通过次生碳化物的析出破坏奥氏体基体的稳定性,使合金贫奥氏体在炉内冷却时转变为珠光体,从而使铸态硬度从hv669降低到HV466。相反,反复奥氏体化不仅使奥氏体基体析出次生碳化物,并在强制空冷条件下转变为马氏体,使基体不稳定,而且使较长的共晶碳化物崩解成较短的段,硬度随之提高到HV 890。连续退火和循环退火后的缺口冲击韧性均保持在12.0 J,而铸态时的缺口冲击韧性为6.0 J。此外,循环退火处理后的磨料耐磨性意外提高,使合金优于工业上使用的连续退火处理。
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引用次数: 1
Analyses of multi-size particle mixing behavior in an ore pre-reduction rotary kiln by discrete element method 用离散元法分析矿石预还原回转窑中多粒径颗粒混合行为
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-06-17 DOI: 10.1051/metal/2021038
Chenghong Liu, Xueyong Ding
The particle distribution in pre-reduction rotary kiln directly affects the reduction process of iron ore, and in-depth understanding of the mixing behavior is helpful to improve the product quality and productivity. The present work focused on the mixed dynamics of multi-component and multi-size systems in rotary kiln using discrete element method (DEM). We first confirmed that the final particle distribution and mixing degree are independent of the initial particle distribution, and then further discussed the influence of the key operating parameters such as rotating speed, average size ratio and filling degree on mixing behavior. The size segregation pattern of three components shows that the large particles segregated to the outer region, while the small particles were concentrated in the core region, forming an annular distribution with different particle sizes. Furthermore, the results also indicate that the rotational speed and fill degree show strong influence on the mixing time and have little influence on the mixing quality. Conversely, the average size ratio significantly affects on the mixing quality. The particle segregation is suppressed and the coal and iron ore particles are well mixed together for the whole bed when the average size of coal particles is smaller than that of iron ore particle. The findings of this work provide a reference for controlling and optimizing the particle mixing process in pre-reduction rotary kiln.
预还原回转窑中的颗粒分布直接影响铁矿石的还原过程,深入了解其混合行为有助于提高产品质量和生产率。本文采用离散元法研究了回转窑多部件、多尺寸系统的混合动力学问题。首先确定了最终颗粒分布和混合程度与初始颗粒分布无关,然后进一步讨论了转速、平均粒度比和填充度等关键操作参数对混合行为的影响。三组分的粒径偏析规律表明,大颗粒向外区偏析,小颗粒向核心区集中,形成不同粒径的环形分布。转速和填充度对搅拌时间影响较大,对搅拌质量影响较小。相反,平均粒度比对混合质量有显著影响。当煤颗粒的平均粒径小于铁矿颗粒的平均粒径时,颗粒偏析被抑制,煤与铁矿颗粒在整个床层内混合良好。研究结果可为预还原回转窑颗粒混合过程的控制和优化提供参考。
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引用次数: 0
Study on the separation of silicon from refining slag of industrial silicon 工业硅精炼渣中硅的分离研究
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-01-01 DOI: 10.1051/metal/2021036
Yong Hou, Guo-hua Zhang, K. Chou
During the process of production and refining of industrial silicon, the discharged slag usually contains more than 15 mass% of metallic silicon. However, the separation of silicon from slag is very difficult due to the close density of silicon and slag as well as the high viscosity of slag, which results in the waste of resources. In the present work, the effect of Na2O addition on the separation of silicon from slag is investigated in detail. It is found that the optimum separation condition of slag and silicon is 1723 K reacting for 60 min by adding 10 mass% Na2O to the slag. Viscosity and density are two important factors affecting the separation effect of silicon from slag. The addition of Na2O reduces the viscosity of slag and promotes the separation of silicon from slag. Even if the addition of Na2O will decrease the density of slag which is detrimental to the separation of silicon, the density variation is not the determining factor affecting the separation relative to viscosity. The separation and extraction of metallic silicon from silicon slag is of great significance for improving utilization of resources and reducing environmental pollution.
在工业硅的生产和精炼过程中,排放的炉渣中金属硅的质量分数通常在15%以上。但由于硅与渣的密度较密,渣的粘度较高,硅与渣的分离非常困难,造成了资源的浪费。本文详细研究了Na2O的加入对硅渣分离的影响。结果表明,炉渣与硅的最佳分离条件为1723 K,在炉渣中加入10质量%的Na2O,反应60 min。粘度和密度是影响硅渣分离效果的两个重要因素。Na2O的加入降低了炉渣的粘度,促进了硅与炉渣的分离。即使Na2O的加入会降低炉渣的密度,不利于硅的分离,但相对于粘度,密度的变化不是影响分离的决定因素。从硅渣中分离提取金属硅对提高资源利用率和减少环境污染具有重要意义。
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引用次数: 0
A comparison study of microstructure, texture and mechanical properties between two 6xxx aluminum alloys 两种6xxx铝合金组织、织构和力学性能的比较研究
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-01-01 DOI: 10.1051/METAL/2021013
Xiaofeng Wang, Hong Liu, Xiaobo Tang
This paper investigates a comparison study of microstructure, texture and mechanical properties between two 6xxx aluminum alloys through microstructure, texture characterization and tensile test. The results show that they exhibit different microstructure, texture and mechanical properties. In comparison with the alloy sheet with a low weight ratio of Mg to Si (Si-excess), the alloy sheet with a higher weight ratio of Mg to Si (Mg-excess) and additional Zn possesses the finer as-casting and solution treated equiaxed grain structure, less particles with larger size before solution treatment, weaker recrystallization texture mainly including Cube {001} orientation and weaker mechanical properties. The low weight ratio of Mg to Si corresponds to slightly higher yield strength and ultimate tensile strength, but much higher plastic strain ration r , work hardening exponent n values and elongation. Interestingly, Portevin-Le Chatelier (PLC) effect is very prevailed in the alloy sheet with a higher weight ratio of Mg to Si and additional Zn, which is responsible for the low elongation and r value. The alloy containing a low weight ratio of Mg to Si may be beneficial to improve comprehensive mechanical property.
通过组织、织构表征和拉伸试验,对两种6xxx铝合金的组织、织构和力学性能进行了对比研究。结果表明,它们具有不同的显微组织、织构和力学性能。与低镁硅比(Si-excess)合金板材相比,高镁硅比(Mg-excess)和添加Zn的合金板材在铸态和固溶处理时具有更细小的等轴组织,固溶处理前具有更大尺寸的颗粒较少,以Cube{001}取向为主的再结晶织构较弱,力学性能较弱。Mg / Si质量比小,屈服强度和极限抗拉强度略高,但塑性应变比r、加工硬化指数n值和伸长率高得多。有趣的是,在Mg / Si质量比较高且添加Zn的合金板材中,普遍存在Portevin-Le Chatelier (PLC)效应,这是导致延伸率和r值较低的原因。低镁硅质量比有利于提高合金的综合力学性能。
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引用次数: 5
The effect of microwave pretreatment on impact crushing of lead-zinc ore 微波预处理对铅锌矿冲击破碎的影响
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-01-01 DOI: 10.1051/metal/2021055
Yu-long Liu, D. Ding, Chen Wenguang, N. Hu, Lingling Wu, Lin Hu, Qiucai Zhang, Zhijun Zhang, Feng Li, Xue Xilong, Zhaopeng Li, Guicheng He, Qing Yu
The relationship between energy input and particle size of ore samples after crushing and effect of microwave pretreatment on impact crushing of lead-zinc ore were studied by drop weight impact test. The results showed that the lead-zinc ore became softer and had higher degree of crushing after microwave pretreatment. Compared with continuous microwave pretreatment, pulsed microwave pretreatment could improve the drop weight impact crushing efficiency of lead-zinc ore. When the specific comminution energy were 5 kW h/t, 10 kW h/t respectively, the crushing characteristic parameters t10 were 60.42% and 67.46% respectively by continuous microwave. But the values of t10 were increased to 68.64% and 75.88% respectively after pulsed microwave radiation under same microwave power and time. In addition, water quenching could more promote the impact crushing efficiency of lead-zinc ore after microwave irradiation.
通过落重冲击试验,研究了能量输入与破碎后矿石粒度的关系以及微波预处理对铅锌矿冲击破碎的影响。结果表明,微波预处理后的铅锌矿变得更软,破碎程度更高。与连续微波预处理相比,脉冲微波预处理可提高铅锌矿落重冲击破碎效率,在比粉碎能分别为5 kW h/t、10 kW h/t时,连续微波破碎特征参数t10分别为60.42%和67.46%。在相同的微波功率和时间下,脉冲微波辐照后,t10值分别提高到68.64%和75.88%。水淬更能提高微波辐照后铅锌矿的冲击破碎效率。
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引用次数: 0
Effect of tool offset on microstructure and mechanical properties of dissimilar copper-brass friction stir welding 刀具偏移对异种铜-黄铜搅拌摩擦焊组织和力学性能的影响
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-01-01 DOI: 10.1051/METAL/2021029
H. Sadeghi, K. Amini, F. Gharavi
This study has investigated the effect of tool offset on the mechanical behavior and microstructure of dissimilar copper and brass joints by friction stir welding (FSW). In this regard, the FSW method was used for joint with three different tool offset positions, namely center line (no offset), the copper side, and the brass alloy side. Microstructure and fracture surfaces of the specimens were examined by optical (OM) and scanning electron microscopies (SEM), respectively. Tensile, micro-hardness and bending tests were also utilized to evaluate the joints mechanical behavior. The results showed that an onion ring-shaped zone was formed with the tool offset towards the copper side, but this zone was not observed with the tool offset towards the brass alloy side. In addition, compared with the tool without offset, the tensile strength with the tool offset to copper side of 1 mm (Cu+1) increased by 33.33% and with the tool offset to brass alloy side of 1 mm (Brass+1) increased by 57.47%. The results of bending test showed that in the Brass+1 specimen, bending strength increased by approximately 5% compared with the specimen without offset. Finally, it was found that the best mechanical and microstructural properties were obtained by the tool offset of 1 mm towards the brass alloy side.
研究了刀具偏移量对异种铜黄铜搅拌摩擦焊接接头力学行为和组织的影响。为此,采用FSW方法对三种不同刀具偏移位置的连接进行了加工,即中心线(无偏移)、铜侧和黄铜合金侧。采用光学显微镜(OM)和扫描电镜(SEM)对试样的显微组织和断口形貌进行了观察。利用拉伸、显微硬度和弯曲试验对接头的力学性能进行了评价。结果表明:刀具向铜侧偏置时形成了一个洋葱环区,而刀具向黄铜合金侧偏置时则没有形成洋葱环区。此外,与未偏置刀具相比,刀具偏置铜侧1 mm (Cu+1)时抗拉强度提高了33.33%,刀具偏置黄铜合金侧1 mm (brass +1)时抗拉强度提高了57.47%。弯曲试验结果表明,在黄铜+1试样中,弯曲强度比没有偏移的试样提高了约5%。结果表明,当刀具向黄铜合金侧偏移1 mm时,合金的力学性能和显微组织性能最佳。
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引用次数: 1
Improvement of carbon segregation in cast bloom and heredity in hot-rolled bar 改进铸坯碳偏析及热轧棒材的遗传
IF 1.1 4区 材料科学 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-01-01 DOI: 10.1051/metal/2021072
Mengyun Zhang, Y. Bao, Li-hua Zhao, Xin Li
In this study, the effect of mechanical soft reduction on carbon segregation in the continuous casting of 300 × 400 mm 42CrMo alloy structural steel blooms was comparatively investigated by adjusting the casting speed, which was systematically optimized through numerical simulation. When the casting speed is 0.60 m · min−1, during the soft reduction process, the central solidification structure of the bloom becomes dense, and carbon segregation is improved. Moreover, the distribution of carbon in the samples before and after rolling was analyzed. Combined with the soft reduction process, the uniformity of carbon across the cross section of the bloom /bar distinctly improved for casting speeds of 0.50 m · min−1, 0.55 m · min−1 and 0.60 m · min−1, this was predominantly reflected in the core areas. The effective segregation length proportion of the bloom and rolled bar is approximately 40%. This phenomenon fully verifies the heredity characteristics of the elements in the rolling process.
本研究通过数值模拟系统优化了300 × 400 mm 42CrMo合金结构钢坯的铸造速度,比较研究了机械软还原对铸坯中碳偏析的影响。当浇注速度为0.60 m·min−1时,软还原过程中坯体中心凝固组织致密,碳偏析得到改善。并对轧制前后样品中的碳分布进行了分析。结合软还原工艺,浇注速度为0.50 m·min - 1、0.55 m·min - 1和0.60 m·min - 1时,坯棒截面上碳的均匀性明显改善,主要体现在芯区。坯与轧制棒材的有效偏析长度比例约为40%。这一现象充分验证了轧制过程中各元素的遗传特性。
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引用次数: 2
期刊
Metallurgical Research & Technology
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