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Горение частиц при взаимодействии излучения гиротрона со смесью порошков металл/диэлектрик 回旋加速器辐射与金属/电介质粉末混合燃烧
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.09.56214.127-23
З. А. Заклецкий, Н. Г. Гусейн-заде, Д. В. Малахов, Л.В. Бадьянова, Е. В. Воронова, В. Д. Степахин
As a result of interaction under normal conditions in an air atmosphere of a microwave pulse of a gyrotron with a mixture of Al/Al2O3 powders, ceramic particles of morphology microprocesses are synthesized. A variant of a multi-stage process for the development of physical and chemical processes in a reactor, taking into account ignition. After the end of the microwave pulse, a cloud is observed consisting of hot aluminum oxide particles and burning aluminum particles. A certain influence of the combustion process of aluminum particles on the products of plasma-chemical synthesis. The paper also determines the average velocity of particles from the powder mixture, the burning time of aluminum particles, the surface temperature of the particles of the powder mixture, and the temperature of the gaseous medium in the upper part of the plasma-chemical reactor.
在正常条件下,回旋管的微波脉冲与Al/Al2O3粉末混合物在空气气氛中相互作用,合成了具有形貌微过程的陶瓷颗粒。多阶段过程的一种变体,用于发展反应堆中的物理和化学过程,其中考虑了点火。在微波脉冲结束后,观察到由热的氧化铝颗粒和燃烧的铝颗粒组成的云。铝颗粒燃烧过程对等离子体化学合成产物的影响。本文还测定了粉末混合物中颗粒的平均速度、铝颗粒的燃烧时间、粉末混合物颗粒的表面温度以及等离子体化学反应器上部气体介质的温度。
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引用次数: 0
Теория квазистатического магнитоэлектрического взаимодействия в трехслойных асимметричных пьезомагнитострикционных структурах 三层不对称压强结构中的准静电相互作用理论
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.02.54497.193-22
Дмитрий Александрович Филиппов, Т. А. Галкина, И.Н. Маничева
The work is devoted to the theoretical investigation of the quasi-static magnetoelectric interaction in three-layer structures consisting of a piezoelectric and two magnetic layers with positive and negative magnetostriction. Using the system of elasto- and electrostatics equations for the piezoelectric and magnetostrictive phases, expressions for the electrical response of the structure in a magnetic field are obtained. The contributions from longitudinal and bending deformations are taken into account in value of ME interactions. It is shown that the use of an asymmetric three-layer asymmetric structure leads to an increase in the magnitude of the ME interaction by almost an order of magnitude compared to a two-layer structure. The dependences of the effect magnitude on the thickness of the third layer for the nickel/lead zirconate titanate/metglas structure are presented.
本文从理论上研究了具有正磁致伸缩和负磁致伸缩的压电层和磁层组成的三层结构中的准静态磁电相互作用。利用压电相和磁致伸缩相的弹性和静电方程组,得到了结构在磁场作用下的电响应表达式。在计算ME相互作用的值时考虑了纵向和弯曲变形的贡献。结果表明,与两层结构相比,使用不对称的三层不对称结构导致ME相互作用的幅度增加了几乎一个数量级。给出了镍/锆钛酸铅/ metglass结构的影响幅度与第三层厚度的关系。
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引用次数: 0
Исследование процесса гидрогенизации одностенных углеродных нанотрубок с помощью индукционно-связанной аргон-водородной плазмы 单链碳纳米管氢化过程研究
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.07.55741.71-23
Е.И. Преображенский, А В Водопьянов, А. В. Нежданов
In this article it was demonstrated the possibility of partial hydrogenation of single-walled carbon nanotubes using an inductively coupled argon-hydrogen plasma. It was studied the changes in the Raman spectrum of samples of single-walled carbon nanotubes during plasma hydrogen intercalation with depending on the treatment time, the discharge power, the substrate material on which the nanotubes were deposited, and the control external voltage. The predominant role of hydrogen ions in the hydrogenation of single-walled carbon nanotubes has been demonstrated.
本文证明了用电感耦合氩氢等离子体对单壁碳纳米管进行部分加氢的可能性。研究了等离子体插氢过程中单壁碳纳米管样品的拉曼光谱随处理时间、放电功率、衬底材料和控制外部电压的变化规律。氢离子在单壁碳纳米管加氢反应中的主导作用已得到证实。
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引用次数: 0
Особенности разрушения микроструи разбавленного полимерного раствора на основные и спутниковые микрокапли под действием внешнего вибрационного воздействия 外部振动影响下,稀释聚合物溶液对基本和卫星微滴的破坏特性
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.01.54061.198-22
Н.А. Хомутов, А. Е. Семенова, М. В. Белоногов, Антонио Ди Мартино, Е.А. Хан, Михаил Пискунов
An experimental study of the morphology of the laminar microjet flow of diluted aqueous solutions of sodium alginate without and with the addition of hydroxyethyl cellulose after a nozzle subject to external vibration stimulation by the action of the reverse piezoelectric effect was carried out. We studied the influence of the polymer concentration in the solution (0.5-5 mg/ml), the flow rate of the liquid (4-26 ml/min), and the frequency of the current of external perturbation (0-1.2 kHz) on the capillary crushing of the microjet with a diameter of about 210 um in the range of Ohnesorge numbers from 0.046 to 1.88 and Reynolds numbers 0.7 to 470. The modes of microjet flow and crushing on microdroplets with indication of boundaries of transitions between them are selected, and a general map of modes is built. Taking into account the polymer concentration in the solution, the dependence of the microjet fracture length on its velocity is shown. The conditions of monodisperse microjet destruction with equidistant arrangement of the main microdroplets in the flow are determined, which are related to an optimal balance between the molecular mass of the polymer in the solution, the intensity of external disturbance and the time of stress relaxation in polymer viscoelastic microjets. The role of formation of structures such as «beads-on-filament» in capillary destruction of microjet with identification of cases of absence of occurrence of «satellite» microdroplets from liquid threads between the main microdroplets has been studied. The results are applied to technologies based on in-air microfluidics (bioengineering and additive technologies), dealing with heterogeneous fluids with viscoelastic properties.
通过反向压电效应的作用,对不加和加羟乙基纤维素的稀海藻酸钠水溶液在喷嘴受外部振动刺激后的层流微射流形貌进行了实验研究。研究了溶液中聚合物浓度(0.5 ~ 5mg /ml)、液体流速(4 ~ 26ml /min)、外部扰动电流频率(0 ~ 1.2 kHz)对直径约为210 um的微射流在0.046 ~ 1.88、0.7 ~ 470雷诺数范围内的毛细管破碎性能的影响。选择了微射流流动和微液滴破碎的模式,并指出了两者之间的过渡边界,建立了总体模式图。考虑溶液中聚合物的浓度,给出了微射流破裂长度与速度的关系。确定了流中主要微滴等距排列的单分散微射流破坏条件,这与溶液中聚合物分子质量、外界干扰强度和聚合物粘弹性微射流应力松弛时间之间的最佳平衡有关。研究了微射流毛细管破坏中形成“丝上珠”等结构的作用,并确定了主微滴之间的液体螺纹中没有出现“卫星”微滴的情况。研究结果应用于基于空气微流体(生物工程和添加剂技术)的技术,处理具有粘弹性质的非均质流体。
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引用次数: 0
Особенности формирования нитевидной структуры микроволнового разряда в потоке аргона 氩流微波放电线状结构形成特性
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.01.54068.226-22
С.В. Синцов, А В Водопьянов, А. Н. Степанов, Д.А. Мансфельд, Н. В. Чекмарев, Е.И. Преображенский, А.А. Мурзанев, А.В. Ромашкин
This paper presents the results of an experimental study of the spatial structure of a microwave discharge maintained in an argon flow by gyrotron radiation in a continuous mode with a frequency of 24 GHz at atmospheric pressure. In the structure of the plasma plume, stationary filamentary channels are observed, elongated along the direction of the argon flow, regardless of the orientation of the external electric field of the wave, surrounded by a diffusion halo. Measurements of the electron density, vibrational and rotational temperatures of gas molecules in plasma filaments have been carried out. The role of gas-dynamic mechanisms responsible for the formation of the inhomogeneous static structure of the plasma torch and the maintenance of a substantially nonequilibrium distribution of temperature characteristics in the discharge is discussed.
本文介绍了在常压条件下,以24 GHz频率的回旋管辐射维持氩流中连续模式微波放电的空间结构的实验研究结果。在等离子体羽流的结构中,可以观察到固定的丝状通道,它们沿着氩流的方向被拉长,而与波的外电场的方向无关,并被扩散晕包围。测量了等离子体细丝中气体分子的电子密度、振动和旋转温度。讨论了气体动力学机制在等离子炬非均匀静态结构的形成和放电中温度特性基本不平衡分布的维持中所起的作用。
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引用次数: 0
Метод теплового баланса для расчета режимов охлаждения крупногабаритной оптики в вакуумных условиях 在真空条件下计算大型光学冷却模式的热平衡方法
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.05.55454.253-22
А.В. Завацкая, Ю А Резунков
The heat balance method is developed to optimize cooling modes of large-sized optics in a special cryogenic-vacuum system by considering a complicated heat transfer in the system to minimize the optics thermal deformations.
为了优化大型光学元件在特殊低温真空系统中的冷却方式,考虑了系统中复杂的传热过程,使光学元件的热变形最小化,提出了热平衡方法。
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引用次数: 0
Спектрофотометрический метод исследования устойчивости комплексов поздних лантаноидов 色谱光度测定法
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.04.55038.276-22
Ц.Б. Сумянова, В.Р. Прижилевская, Н. Е. Борисова
Представлены результаты исследования влияния центрального иона металла на устойчивость комплексов гадолиния и гольмия с диамидом 1,10'-фенантролин-2,9-дикарбоновой кислоты. Полученные значения констант устойчивости комплексов оказались на порядок ниже, чем известные ранее величины для комплексов этих элементов с диамидом 4,7-дихлор-1,10'-фенантролин-2,9-дикарбоновой кислоты. Ключевые слова: спектрофотометрия, гадолиний, гольмий, контрастные вещества.
研究中心金属离子对哈得那线抗拉强度的影响,以及1 - 10 -芬特洛林- 2.9 -野蛮酸的高原反应。产生的抗拉常数比以前已知的低了4.7 -二氯- 1.10 -费南特洛林- 2.9 -野蛮酸数。关键词:分光光度学,粗线,细线,对比材料。
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引用次数: 0
Влияние комбинированного ионного и электронного облучения на полосу люминесценции 2 eV в гексагональном нитриде бора 复合离子和电子辐射对六氮硼的发光带2 eV
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.07.55746.62-23
Юрий Владимирович Петров, О.А. Гогина, О.Ф. Вывенко, S. Kovalchuk, K. Bolotin
Point defects in wide-bandgap semiconductors, in particular in hexagonal boron nitride, are promising candidates for single-photon emitters, used in quantum informatics. We investigated cathodoluminescence of ion beam induced defects in hexagonal boron nitride, as well as the effect of prolonged electron irradiation on the intensity of the luminescence. It has been shown that the intensity of both band-to-band emission and defect related emission decreased after ion irradiation, and during subsequent electron irradiation the intensity of 2 eV luminescence band increased, whereas the intensity of other bands remained unchanged.
宽带隙半导体中的点缺陷,特别是六方氮化硼中的点缺陷,是量子信息学中使用的单光子发射器的有希望的候选者。研究了离子束诱导六方氮化硼缺陷的阴极发光,以及长时间电子辐照对阴极发光强度的影响。结果表明,离子辐照后,其带间发射强度和缺陷相关发射强度均有所降低,在随后的电子辐照过程中,2ev发光带强度增加,而其他波段强度保持不变。
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引用次数: 0
Визуализация магнитных полей в растровом электронном микроскопе 电子式显微镜内磁场可视化
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.07.55762.81-23
Д.А. Татарский, Е. В. Скороходов, Сергей Анатольевич Гусев
The fundamental possibility of measuring the stray fields distributions of magnetic objects in a scanning electron microscope is demonstrated. The main idea of the method is to use a sample holder for operation in the mode of a scanning transmission microscope, additionally equipped with a square diffraction grating. This grating, formed on the basis of a metal film, is placed at some distance under the magnetic sample. Reconstruction of the deflections of transmitted electrons by analyzing the geometric phase from visible distortions of the diffraction grating made it possible to reconstruct the distribution of the magnetic field created by the sample under study.
论证了用扫描电子显微镜测量磁性物体杂散场分布的基本可能性。该方法的主要思想是在扫描透射显微镜的模式下使用样品支架进行操作,另外配备方形衍射光栅。这种光栅是在金属膜的基础上形成的,放置在磁性样品下方一定距离处。通过分析衍射光栅可见畸变的几何相位来重建透射电子的偏转,可以重建所研究样品产生的磁场分布。
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引用次数: 0
Влияние радиационного воздействия на магнитные свойства пленок ферромагнетик/IrMn с обменным сдвигом 辐射影响铁磁/IrMn带交换位移的磁性
Pub Date : 2023-01-01 DOI: 10.21883/jtf.2023.07.55744.72-23
Д.О. Кривулин, И.Ю. Пашенькин, Р.В. Горев, П.А. Юнин, M.В. Сапожников, А. В. Грунин, Светлана Александровна Захарова, Виктор Николаевич Леонтьев
In this work, the effect of the action of gamma quanta and neutrons on the magnetic properties of Ta/feromagnet/IrMn/Ta bilayer films with an exchange bias of the hysteresis loop is studied. The samples were fabricated by magnetron sputtering, and their structure was studied by small-angle X-ray reflectometry and X-ray diffractometry. The measurement of the magnetic hysteresis loops of the irradiated and non-irradiated samples was carried out by the methods of magneto-optical Kerr magnetometry. As a result, the effect of broadening of the magnetic hysteresis loop after irradiation was found. The maximum broadening of the hysteresis loop was observed in the NiFe/IrMn film under neutron irradiation; in this case, the loop width increased by more than 2.5 times. No noticeable change in the field of the exchange bias of the hysteresis loops was observed in the entire range of radiation exposure.
本文研究了伽马量子和中子的作用对具有交换偏置磁滞回线的Ta/feromagnet/IrMn/Ta双层薄膜磁性能的影响。采用磁控溅射法制备了样品,并用小角x射线反射仪和x射线衍射仪研究了样品的结构。采用磁光克尔磁强计对辐照和未辐照样品的磁滞回线进行了测量。结果发现辐照后磁滞回线的展宽效应。中子辐照下,NiFe/IrMn薄膜的磁滞回线最大展宽;在这种情况下,环路宽度增加了2.5倍以上。在整个辐照范围内,磁滞回线的交换偏置场没有明显变化。
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引用次数: 0
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