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Experimental investigation on performance of bubble-bursting atomization methods for minimum quantity lubrication in face milling tool steel 面铣工具钢最小量润滑的爆泡雾化方法性能实验研究
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-15 DOI: 10.1016/j.rineng.2024.102903
Muhammad Rizal , Amir Zaki Mubarak , Jaharah A. Ghani

The metal cutting industry faces challenges in machining hard materials due to high forces and temperatures. This paper introduces bubble-bursting atomization minimum quantity lubrication (BBA-MQL), a novel MQL technique that generates fine biodegradable oil mists for cooling and lubrication. Although the initial results of BBA-MQL are promising, there has not been a comprehensive investigation into its use in machining hard materials, specifically tool steels. Therefore, this study focused on the applicability of BBA-MQL in face milling of AISI P20 + Ni tool steel in comparison with dry cutting and conventional MQL using commercial and vegetable oil. The machining tests were performed at three cutting speeds (50, 80, and 110 m/min), fixed cutting depth (0.2 mm), and feed rate (0.15 mm/tooth). The performance is evaluated by measuring the cutting force, surface quality, cutting temperature, and tool wear. It was found that BBA-MQL decreased cutting force and surface roughness considerably, with the average reductions being 23.2 % and 49.8 % compared with the conventional minimum quantity lubrication. The highest cutting speed of 110 m/min was preferred for achieving the lowest roughness value and cutting force when milling tool steel P20 + Ni. Furthermore, BBA-MQL with castor oil proved more effective compared to conventional MQL in reducing cutting force, showing improved surface finish, reduced cutting temperature, and delayed tool wear.

金属切削行业在加工硬质材料时面临着高力和高温的挑战。本文介绍了气泡爆破雾化最小量润滑(BBA-MQL),这是一种新型 MQL 技术,可产生用于冷却和润滑的生物可降解油雾。虽然 BBA-MQL 的初步结果令人鼓舞,但尚未对其在加工硬质材料(特别是工具钢)中的应用进行全面调查。因此,本研究将重点放在 BBA-MQL 在 AISI P20 + Ni 工具钢端面铣削中的适用性上,并与干切削和使用商业油和植物油的传统 MQL 进行了比较。加工测试在三种切削速度(50、80 和 110 米/分钟)、固定切削深度(0.2 毫米)和进给率(0.15 毫米/齿)下进行。通过测量切削力、表面质量、切削温度和刀具磨损来评估其性能。结果发现,BBA-MQL 大大降低了切削力和表面粗糙度,与传统的最小量润滑相比,平均降低了 23.2 % 和 49.8 %。在铣削工具钢 P20 + Ni 时,110 米/分钟的最高切削速度可获得最低的粗糙度值和切削力。此外,与传统的 MQL 相比,使用蓖麻油的 BBA-MQL 在降低切削力、改善表面光洁度、降低切削温度和延迟刀具磨损方面更为有效。
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引用次数: 0
Numerical investigation of synergistic effects of magnetic fields and bluff bodies on heat transfer enhancement and pressure drop reduction in microchannels 磁场和崖体对微通道传热增强和压降降低的协同效应的数值研究
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102894
Shohreh Jalali, Ebrahim Barati, Mahdi Farkhondeh Kalat

Efficient thermal management is essential for designing compact and high-performance heat sinks and heat exchangers. This study addresses the challenge of optimizing heat transfer while minimizing pressure losses in systems exposed to concentrated heat flux by proposing a novel approach that employs both active and passive vortex generators. Specifically, a uniform magnetic field generated by permanent magnets and a bluff body are utilized within a microchannel containing a 2 vol% ferrofluid. Numerical simulations were performed across Reynolds numbers ranging from 100 to 500 and magnetic field intensities up to 0.5 T to evaluate the system's performance. The results demonstrate that the combination of magnetic fields and a bluff body induces vortex generation, alters velocity distribution, and enhances flow mixing, resulting in a 30 % increase in heat transfer efficiency and an 11 % reduction in pressure drop under optimal conditions. Although the introduction of barriers led to a 3 % rise in pressure drop, the uniform magnetic field effectively mitigated friction by reducing flow separation and limiting surface contact. These findings highlight the potential of this method for improving the design of advanced thermal management systems.

高效的热管理对于设计紧凑型高性能散热器和热交换器至关重要。本研究通过提出一种同时采用主动和被动涡流发生器的新方法,解决了在暴露于集中热流的系统中优化传热同时尽量减少压力损失的难题。具体来说,就是在含有 2 Vol% 铁流体的微通道内利用永磁体和崖体产生的均匀磁场。在雷诺数为 100 到 500、磁场强度为 0.5 T 的范围内进行了数值模拟,以评估系统的性能。结果表明,磁场和栅栏体的结合可诱导涡流产生、改变速度分布并增强流动混合,从而在最佳条件下将传热效率提高 30%,压降降低 11%。虽然屏障的引入导致压降增加了 3%,但均匀磁场通过减少流动分离和限制表面接触,有效地减轻了摩擦。这些发现凸显了这种方法在改进先进热管理系统设计方面的潜力。
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引用次数: 0
Strategic load management: Enhancing eco-efficiency in mining operations through automated technologies 战略性负荷管理:通过自动化技术提高采矿作业的生态效益
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102890
Ali Akbar Firoozi , Magdeline Tshambane , Ali Asghar Firoozi , Sajid Mubashir Sheikh

In the face of escalating global demands for sustainable practices within the construction and mining sectors, this paper investigates the transformative impact of automated load analysis technologies. Focused on bridging the gap between traditional operational methodologies and the forefront of automation technology, the study provides an in-depth examination of the integration of onboard weighing systems, the Internet of Things (IoT), and machine learning into mining operations. Through a series of detailed case studies, the research showcases how these technological innovations contribute to substantial improvements in operational efficiency, notably through enhanced load management, reduced fuel consumption, and optimized resource allocation, thereby fostering a decrease in the environmental footprint of mining activities. Furthermore, the paper addresses critical sustainability issues, including workforce transformation, stakeholder engagement, and the broader environmental implications of adopting automated technologies in mining processes. Concluding with strategic policy recommendations, the study advocates for widespread adoption of automated systems within the construction sector to achieve improved environmental and economic outcomes. By emphasizing a multidisciplinary approach, this research highlights the essential role of technological innovation in aligning mining operations with sustainable development goals, positioning automated load analysis as a pivotal strategy for advancing eco-efficiency in the construction and mining industries.

面对全球对建筑和采矿业可持续发展实践不断升级的要求,本文研究了自动化载荷分析技术的变革性影响。该研究侧重于缩小传统操作方法与自动化技术前沿之间的差距,深入探讨了将车载称重系统、物联网(IoT)和机器学习整合到采矿操作中的问题。通过一系列详细的案例研究,该研究展示了这些技术创新如何有助于大幅提高运营效率,特别是通过加强负载管理、降低燃料消耗和优化资源配置,从而减少采矿活动对环境的影响。此外,本文还探讨了关键的可持续发展问题,包括劳动力转型、利益相关者参与以及在采矿过程中采用自动化技术对环境的广泛影响。研究报告最后提出了战略性政策建议,主张在建筑行业广泛采用自动化系统,以实现更好的环境和经济效益。通过强调多学科方法,本研究强调了技术创新在使采矿作业符合可持续发展目标方面的重要作用,并将自动化载荷分析定位为推进建筑业和采矿业生态效益的关键战略。
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引用次数: 0
Enhancing CO2 conversion in a temperature-controlled DBD plasma reactor with HKUST-1 catalyst: Water removal and CuO/Cu2O-derived approach 使用 HKUST-1 催化剂提高温控 DBD 等离子反应器中的二氧化碳转化率:脱水和 CuO/Cu2O 衍生方法
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102884
Hadi Hatami , Mohammadreza Khani , Babak Shokri

Due to a synergy effect, using dielectric barrier discharge (DBD) plasma technology combined with catalysts for CO2 decomposition, a major contributor to global warming, is recognized as an effective approach to transforming CO2 into valuable products such as CO, which is a crucial feedstock for chemical synthesis. Herein, HKUST-1 was synthesized using the hydrothermal method for CO2 conversion in the DBD reactor. To enhance catalyst performance in the plasma region, HKUST-1 was treated with O2 plasma to increase its specific surface area. Additionally, HKUST-1 was calcined at 300 °C to produce the CuO/Cu2O catalyst. Since the recombination reaction in the CO2 conversion is increased at higher temperatures, the reactor heat is removed using fan cooling and a water circulation system. In the presence of the HKUST-1 catalyst, the CO2 conversion rate significantly increased by 132 %, 82 %, and 12 % in reactors operating without cooling, with fan cooling, and with water cooling circulation, respectively compared to the reactors without catalyst, at a flow rate of 50 ml/min and maximum input power. The catalysts have been characterized using a comprehensive suite of analytical techniques, including FTIR, XRD,TEM, SEM, EDS, and BET analysis. The BET analysis indicates that the specific surface area of HKUST-1 after O2 plasma treatment is increased by 52 %, which causes an increasing conversion rate of up to 18 %. The CuO/Cu2O catalyst demonstrated maximum CO2 conversion of 21 % at an input power of 140 W and achieved energy efficiency of 8.6 % at 40 W. The presence of oxygen vacancies within this catalyst enhances the process of CO2 decomposition.

由于协同效应,使用介质阻挡放电(DBD)等离子体技术与催化剂结合进行二氧化碳分解(导致全球变暖的主要因素)被认为是将二氧化碳转化为有价值产品(如作为化学合成重要原料的一氧化碳)的有效方法。本文采用水热法合成了 HKUST-1,用于在 DBD 反应器中进行二氧化碳转化。为了提高等离子体区域的催化剂性能,HKUST-1 经过了 O2 等离子体处理,以增加其比表面积。此外,HKUST-1 经 300 °C 煅烧后生成 CuO/Cu2O 催化剂。由于二氧化碳转化过程中的重组反应在较高温度下会加剧,因此使用风扇冷却和水循环系统去除反应器的热量。与不使用催化剂的反应器相比,在 50 毫升/分钟的流量和最大输入功率条件下,使用 HKUST-1 催化剂的反应器在无冷却、风扇冷却和水冷循环条件下的二氧化碳转化率分别显著提高了 132%、82% 和 12%。催化剂的表征采用了一整套分析技术,包括傅立叶变换红外光谱、XRD、TEM、SEM、EDS 和 BET 分析。BET 分析表明,经过 O2 等离子处理后,HKUST-1 的比表面积增加了 52%,从而使转化率提高了 18%。在输入功率为 140 W 时,CuO/Cu2O 催化剂的二氧化碳最大转化率为 21%,在输入功率为 40 W 时,能量效率为 8.6%。
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引用次数: 0
The effect of nanocellulose and silica filler on the mechanical properties of natural fiber polymer matrix composites 纳米纤维素和二氧化硅填料对天然纤维聚合物基复合材料机械性能的影响
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102898
Endalkachew Gashawtena , Addis Kidane , Belete Sirahbizu

Natural fiber-reinforced polymer matrix composites recently got great attention in biomedical applications due to their inherent characteristics such as biocompatibility, lightweight, and biodegradability. However, natural fiber composites suffer from poor mechanical properties and weak interfacial adhesion. It is well documented that the addition of nanofiller has improved the mechanical properties of different synthetic fibers such as glass and carbon composites. The main objective of this paper is to study nanofillers' effect on the mechanical properties of unidirectional false banana fibers reinforced polymer composites. The filler materials, crystalline nanocellulose fibrils, and crystalline nanosilica particles were extracted from sugarcane bagasse and its byproducts. The composite samples were fabricated by adding the nanofillers in unidirectional natural fibers arranged in four fiber orientations (0°, 0o/90o ±45o, and quasi-isotropic), and their tensile, flexural, compression strength, thermal stability, and void content were measured following ASTM standards. The results revealed that adding nanofillers increased the tensile, flexural, and compressive strengths by 16 % (98.83 Mpa), 11 % (161.60 Mpa), and 23 % (114.62 Mpa), respectively. Similarly, at 0° orientation, the addition of nanoparticles enhances the tensile, bending, and compressive modulus by 30 % (15.43 Gpa), 12 % (13.52 Gpa), and 60 % (42.6 Gpa), respectively. On the other hand, the void content was reduced with the addition of nanofillers. The results also revealed that composites with crystalline nanosilica particle fillers had superior thermal stability compared to crystalline nanocellulose fibril fillers. The overall results of this research give the confidence that nano particle-filled natural fiber composites can be used for bio-based engineering applications, such as prosthetic sockets.

天然纤维增强聚合物基复合材料因其固有的生物相容性、轻质和生物降解性等特点,最近在生物医学应用中受到极大关注。然而,天然纤维复合材料存在机械性能差、界面粘附性弱等问题。有资料表明,添加纳米填料可改善不同合成纤维(如玻璃纤维和碳纤维复合材料)的机械性能。本文的主要目的是研究纳米填料对单向假香蕉纤维增强聚合物复合材料机械性能的影响。填充材料、结晶纳米纤维素纤维和结晶纳米二氧化硅颗粒是从甘蔗渣及其副产品中提取的。按照 ASTM 标准测量了复合材料样品的拉伸、弯曲、压缩强度、热稳定性和空隙率。结果表明,添加纳米填料后,拉伸强度、弯曲强度和压缩强度分别提高了 16%(98.83 兆帕)、11%(161.60 兆帕)和 23%(114.62 兆帕)。同样,在 0° 取向时,添加纳米颗粒可使拉伸模量、弯曲模量和压缩模量分别提高 30 %(15.43 Gpa)、12 %(13.52 Gpa)和 60 %(42.6 Gpa)。另一方面,纳米填料的加入降低了空隙含量。研究结果还显示,与结晶纳米纤维素纤维填料相比,使用结晶纳米二氧化硅颗粒填料的复合材料具有更高的热稳定性。这项研究的总体结果使人们相信,纳米颗粒填充的天然纤维复合材料可用于生物基工程应用,如假体插座。
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引用次数: 0
Recent advancements in indirect solar dryer performance and the associated thermal energy storage 间接太阳能干燥器性能和相关热能储存的最新进展
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102877
Gadisa Desa Shekata , Getachew Shunki Tibba , Aklilu Tesfamichael Baheta

Drying is a fundamental process for preserving agricultural products, involving heat and mass exchanges. As a sustainable selection, researchers are focusing on solar dryers to improve drying efficiency, shorten drying times, and maintain product quality. Indirect type solar dryers (ITSD) have shown promise in post-harvest preservation. However, there is a lack of detailed investigation in their unique features, types, and performance-enhancement techniques. Thermal energy storage methods, which store excess energy for times when there is no solar irradiance, can improve the dependability of solar drying. Expensive experimental setups have led to the use of computer simulation techniques like computational fluid dynamics (CFD) to optimize drying conditions and dryer design while maintaining product quality. The review aims to provide an overview of different ITSD designs, techniques of thermal energy storage, and explore the use of CFD in analyzing heat and mass transfer phenomena in indirect solar drying systems. Additionally, this review study inspires researchers to explore the development of indirect solar dryers suitable for various drying environments, diverse product drying capacities, and different drying durations. Further research and development in these areas will continue to enhance the performance, energy efficiency, and scalability of indirect solar dryers, contributing to sustainable agriculture and energy conservation.

干燥是保存农产品的基本过程,涉及热量和质量交换。作为一种可持续的选择,研究人员正在重点研究太阳能干燥器,以提高干燥效率、缩短干燥时间并保持产品质量。间接式太阳能干燥器(ITSD)在收获后保鲜方面已显示出前景。然而,对其独特功能、类型和性能提升技术还缺乏详细研究。热能储存方法可在没有太阳辐照时储存多余能量,从而提高太阳能干燥的可靠性。昂贵的实验装置促使人们使用计算流体动力学(CFD)等计算机模拟技术来优化干燥条件和干燥机设计,同时保持产品质量。本综述旨在概述不同的 ITSD 设计和热能储存技术,并探讨如何使用 CFD 分析间接太阳能干燥系统中的传热和传质现象。此外,本综述研究还激励研究人员探索开发适合各种干燥环境、不同产品干燥能力和不同干燥持续时间的间接太阳能干燥器。在这些领域的进一步研究和开发将继续提高间接太阳能干燥器的性能、能效和可扩展性,为可持续农业和节能做出贡献。
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引用次数: 0
Elevated effect of hydrothermal treatment on phosphorus transition between solid-liquid phase in swine manure 水热处理对猪粪中磷在固液相之间转变的增强效应
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102887
Shiyu Xie , Xinyue He , Mohammed Ali Alshehri , Salah F. Abou-Elwafa , Tao Zhang

The morphology and composition of phosphorus in biomass wastes are key factors in determining its potential for utilization. However, the morphological distribution and evolutionary mechanism of phosphorus during the hydrothermal conversion of biomass wastes are still unclear. In this study, swine manure was investigated as the research subject, and the changes in its solid-phase organic components, such as lignocellulose, and inorganic constituents, including metals and phosphorus, during the hydrothermal carbonization (HTC) processes were analyzed in relation to hydrothermal reaction severity (LnR0). A significant linear correlation in Phase II was observed between the solid-phase yield of swine manure and the LnR0. The rapid decline in the solid-phase yield during the initial phase (LnR0 < 9.72) was primarily attributed to the hydrolysis of hemicellulose and similar components. Similarly, solid phase phosphorus showed a very significant phase II with the decrease of solid phase yield. In the first stage, inorganic phosphorus and metal ions (calcium ions, magnesium ions) transferred to the liquid phase (LnR0<9.41). When LnR0 > 9.41, and the driving force of inorganic phosphorus and metal ions into solid phase is enhanced. As the LnR0 was further increased, the HTC could fix over 90 % of the total phosphorus content. XANES analysis indicated that hydroxyapatite emerged as the predominant phosphorus fraction in the solid-phase products, comprising more than 60 %, while magnesium ammonium phosphate components also appeared. This research elucidates the underlying mechanisms of component interaction and phosphorus transformation, providing a solid foundation for enhancing the reuse efficiency of phosphorus in wastes.

生物质废物中磷的形态和组成是决定其利用潜力的关键因素。然而,磷在生物质废物水热转化过程中的形态分布和演化机理尚不清楚。本研究以猪粪为研究对象,分析了其在水热碳化(HTC)过程中固相有机成分(如木质纤维素)和无机成分(包括金属和磷)的变化与水热反应严重程度(LnR0)的关系。在第二阶段,猪粪的固相产量与 LnR0 呈明显的线性相关。初始阶段固相产率的快速下降(LnR0 <9.72)主要归因于半纤维素和类似成分的水解。同样,随着固相产率的降低,固相磷也出现了非常显著的第二阶段。在第一阶段,无机磷和金属离子(钙离子、镁离子)转移到液相(LnR0<9.41)。当 LnR0 为 9.41 时,无机磷和金属离子进入固相的动力增强。随着 LnR0 的进一步增加,HTC 可以固定 90% 以上的总磷含量。XANES 分析表明,羟基磷灰石是固相产物中最主要的磷组分,占 60% 以上,同时还出现了磷酸铵镁组分。这项研究阐明了组分相互作用和磷转化的基本机制,为提高废物中磷的再利用效率奠定了坚实的基础。
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引用次数: 0
Rate expression model from thermodynamics application and optimal kinetic parameters determination for urea synthesis and production process 尿素合成和生产过程中热力学应用的速率表达模型和最佳动力学参数的确定
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102885
O.E. Ojong , J.G. Akpa , K.K. Dagde , D. Amadi

Urea, an essential organic fertilizer, enhances soil fertility by providing 0.466 nitrogen for maximum crop yield. In this study, urea is synthesized from NH3 and CO2 in an equilibrium reaction process adhering to Le Chatelier's principle, maintained under process conditions: flow rate of 63.5 kg/s, temperature of 184 °C, and pressure of 160 kg/cm2. A new rate expression model, formulated in terms of extent of reaction and mole fraction, was developed based on mass action relations and thermodynamic models. Two industrial reactors were considered: a plug flow reactor (PFR) at Notore and a continuous stirred tank reactor (CSTR) at Indorama plants. Transient reactor models, based on material and energy balance conservation principles, were numerically resolved using MATLAB version 2020 with specified input conditions. A non-linear regression statistical optimization model was employed to refine kinetic parameter values, ensuring optimal and high-quality urea yield. Model validations were conducted using literature data, revealing higher urea yields of 0.726 and 0.7032 for the CSTR and PFR, respectively. Deviations (0.134, 0.10 to 1.135 and 0.635, 0.326 to 0.850) and root mean square errors (RMSE) (0.043, 0.033 to 0.193 and 0.137, 0.087 to 0.162) were observed when validated against plant and literature values for the CSTR and PFR respectively. The refined kinetic parameters (activation energies, Arrhenius constants, and rate constants) exhibited negligible deviations (0.0004–0.0466 and 0.0004 to 0.0491) and RMSE (0.0228, 0.0055, and 0.0256 and 0.0241, 0.0096, and 0.0269) when validated against plant data, significantly enhancing urea yield in CSTR and PFR reactors respectively.

尿素是一种重要的有机肥料,可提供 0.466% 的氮,从而提高土壤肥力,使作物获得最高产量。在本研究中,尿素由 NH3 和 CO2 按照勒夏特列原理在平衡反应过程中合成,工艺条件为:流速 63.5 kg/s、温度 184 °C 和压力 160 kg/cm2。在质量作用关系和热力学模型的基础上,根据反应程度和分子分数建立了一个新的速率表达模型。考虑了两个工业反应器:Notore 工厂的塞流反应器(PFR)和 Indorama 工厂的连续搅拌罐反应器(CSTR)。瞬态反应器模型以物料和能量平衡守恒原理为基础,使用 MATLAB 2020 版本在指定输入条件下进行数值解析。采用非线性回归统计优化模型来完善动力学参数值,确保获得最佳和高质量的尿素产量。利用文献数据对模型进行了验证,结果显示,CSTR 和 PFR 的尿素产量分别为 0.726 和 0.7032。在对 CSTR 和 PFR 的工厂值和文献值进行验证时,分别观察到了偏差(0.134,0.10 至 1.135 和 0.635,0.326 至 0.850)和均方根误差(RMSE)(0.043,0.033 至 0.193 和 0.137,0.087 至 0.162)。在与工厂数据进行验证时,改进后的动力学参数(活化能、阿伦尼斯常数和速率常数)的偏差(0.0004-0.0466 和 0.0004 至 0.0491)和均方根误差(0.0228、0.0055 和 0.0256 以及 0.0241、0.0096 和 0.0269)均可忽略不计,分别显著提高了 CSTR 和 PFR 反应器中的尿素产量。
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引用次数: 0
Trajectory and spreading of falling circular dense jets in shallow stagnant ambient water 浅层死水中圆形致密射流的下落轨迹和扩散
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-14 DOI: 10.1016/j.rineng.2024.102897
Hossein Azizi Nadian , Nima Shahni Karamzadeh , Javad Ahadiyan , Morteza Bakhtiari

This study investigates the trajectory and spreading of a horizontal circular dense jet flow discharged above the water surface, the flow of which falls into shallow stagnant ambient water. For this purpose, 27 experiments were performed using three diameters, flow rates, and falling heights to investigate jet trajectory. In addition, nine experiments with constant falling height were conducted to study jet spreading. The densimetric Froude number of the jet flow at the nozzle outlet and water surface of the present study ranged from 0.72 to 4.22 and 36.96 to 86.10, respectively. The data pertaining to this study were extracted and analyzed through image processing. The results of the experiments showed that by increasing both the momentum and falling height, the trajectory of the jet flow reached a farther distance from the discharge nozzle. The spreading of the outer boundaries of the dense circular falling jet flow tended to extend downstream of the impact point and had an elliptical motion on the bed. The relationship between radial distance from the impingement point to the outer boundary of flow and time was determined to have a power of 0.67 for flow along the flume and 0.59 for flow along the flume's width.

本研究调查了水平圆形密集射流的轨迹和扩散情况,射流从水面上方排出,落入浅层死水环境中。为此,使用三种直径、流速和下落高度进行了 27 次实验,以研究射流轨迹。此外,还进行了 9 次恒定下落高度的实验,以研究射流的扩散情况。在本研究中,喷嘴出口和水面上的射流密度计弗劳德数分别为 0.72 至 4.22 和 36.96 至 86.10。本研究的相关数据通过图像处理进行提取和分析。实验结果表明,通过增加动量和下降高度,射流的轨迹到达了离排放喷嘴更远的距离。密集的圆形下降射流的外边界扩散趋向于向冲击点下游延伸,并在床面上呈椭圆形运动。经测定,从撞击点到流动外边界的径向距离与时间之间的关系为:沿水槽流动的幂为 0.67,沿水槽宽度流动的幂为 0.59。
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引用次数: 0
Microwave-assisted extraction of phenolic compounds from Commiphora gileadensis leaf and their characterization 微波辅助萃取金银花叶中的酚类化合物及其特性分析
IF 6 Q1 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2024-09-13 DOI: 10.1016/j.rineng.2024.102892
Aiman A. Bin Mokaizh , Abdurahman Hamid Nour , Chinonso Ishmael Ukaegbu

Commiphora gileadensis (C. gileadensis) is a plant traditionally used in many parts of the world for medicinal purposes. However, the benefits of this plant are yet to be uncovered due to the use of conventional extraction methods during its extraction. Hence, there is a need for more efficient and environment-friendly extraction methods for optimum recovery of the bioactive components of C. gileadensis. This study aims to evaluate the impact of microwave-assisted extraction (MAE) process parameters (individually and in combination) on the recovery of phenolic compounds from C. gileadensis leaf. One-Factor-At-a-Time (OFAT) optimization method was used in this work to study the impact of varying the MAE process parameters (sample: solvent ratio, microwave power, ethanol concentration, and extraction temperature) on the optimum yield of phenolic compounds. The obtained phenolic compounds were characterized using Gas chromatography-mass spectrometry (GC–MS) for tentative identification of the component phytochemicals of the extract. The results showed that the optimal process condition of microwave power at 300 W, solvent/sample ratio of 1:10 g/mL, solvent concentration of 40 % v/v, and extraction temperature of 40 °C gave the maximum extraction yield of 33.20 ± 0.42 % w/w, total phenolic content (TPC) of 114.65 ± 3.14 mg GAE/g d.w., and total flavonoids content (TFC) of 37.56 mg QE/g d.w.). Furthermore, the GC-MS analysis identified 25 phenolic compounds with good antioxidant activities from the extracts. Therefore, MAE is considered a non-conventional green method for improved extraction of phenolic compounds from C. gileadensis leaf compared to the existing conventional extraction methods.

吉列当归(Commiphora gileadensis)是世界许多地区传统的药用植物。然而,由于在提取过程中使用了传统的提取方法,这种植物的功效尚未被发掘出来。因此,有必要采用更高效、更环保的萃取方法,以优化 C. gileadensis 生物活性成分的回收。本研究旨在评估微波辅助萃取(MAE)工艺参数(单独和组合)对吉利莲叶中酚类化合物回收率的影响。本研究采用单因素-时间(OFAT)优化法研究了改变微波辅助萃取工艺参数(样品:溶剂比、微波功率、乙醇浓度和萃取温度)对酚类化合物最佳产量的影响。利用气相色谱-质谱法(GC-MS)对所获得的酚类化合物进行表征,以初步鉴定提取物中的植物化学成分。结果表明,在微波功率为 300 W、溶剂/样品比为 1:10 g/mL、溶剂浓度为 40 % v/v、萃取温度为 40 °C 的最佳工艺条件下,萃取率最高(33.20 ± 0.42 % w/w),总酚含量(TPC)最高(114.65 ± 3.14 mg GAE/g d.w.),总黄酮含量(TFC)最高(37.56 mg QE/g d.w.)。此外,气相色谱-质谱分析还从提取物中鉴定出 25 种具有良好抗氧化活性的酚类化合物。因此,与现有的传统提取方法相比,MAE 被认为是一种非常规的绿色提取方法,可提高 C. gileadensis 叶中酚类化合物的提取率。
{"title":"Microwave-assisted extraction of phenolic compounds from Commiphora gileadensis leaf and their characterization","authors":"Aiman A. Bin Mokaizh ,&nbsp;Abdurahman Hamid Nour ,&nbsp;Chinonso Ishmael Ukaegbu","doi":"10.1016/j.rineng.2024.102892","DOIUrl":"10.1016/j.rineng.2024.102892","url":null,"abstract":"<div><p><em>Commiphora gileadensis</em> (<em>C. gileadensis</em>) is a plant traditionally used in many parts of the world for medicinal purposes. However, the benefits of this plant are yet to be uncovered due to the use of conventional extraction methods during its extraction. Hence, there is a need for more efficient and environment-friendly extraction methods for optimum recovery of the bioactive components of <em>C. gileadensis.</em> This study aims to evaluate the impact of microwave-assisted extraction (MAE) process parameters (individually and in combination) on the recovery of phenolic compounds from <em>C. gileadensis</em> leaf. One-Factor-At-a-Time (OFAT) optimization method was used in this work to study the impact of varying the MAE process parameters (sample: solvent ratio, microwave power, ethanol concentration, and extraction temperature) on the optimum yield of phenolic compounds. The obtained phenolic compounds were characterized using Gas chromatography-mass spectrometry (GC–MS) for tentative identification of the component phytochemicals of the extract. The results showed that the optimal process condition of microwave power at 300 W, solvent/sample ratio of 1:10 g/mL, solvent concentration of 40 % v/v, and extraction temperature of 40 °C gave the maximum extraction yield of 33.20 ± 0.42 % w/w, total phenolic content (TPC) of 114.65 ± 3.14 mg GAE/g d.w., and total flavonoids content (TFC) of 37.56 mg QE/g d.w.). Furthermore, the GC-MS analysis identified 25 phenolic compounds with good antioxidant activities from the extracts. Therefore, MAE is considered a non-conventional green method for improved extraction of phenolic compounds from <em>C. gileadensis</em> leaf compared to the existing conventional extraction methods.</p></div>","PeriodicalId":36919,"journal":{"name":"Results in Engineering","volume":"24 ","pages":"Article 102892"},"PeriodicalIF":6.0,"publicationDate":"2024-09-13","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S2590123024011472/pdfft?md5=4f0125335bddaf98462bdc6916160c12&pid=1-s2.0-S2590123024011472-main.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142229577","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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Results in Engineering
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