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2006 15th ieee international symposium on the applications of ferroelectrics最新文献

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A Micro Ultrasonic Scalpel Using Hydrothermal PZT Thin Film 热液PZT薄膜微超声手术刀
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387901
Y. Umehara, M. Kurosawa
A transducer for a micro ultrasonic scalpel has been fabricated. The micro ultrasonic scalpel can be used with an endoscope for a non-abdominal operation or micro surgery, for example, through a microscope. The ultrasonic transducer was 9.8 mm long and 2.7 mm wide and has stepped horn to amplify vibration velocity; tip of the horn is 0.6 mm wide. The scalpel vibrated in longitudinal mode at about 278 kHz resonance frequency. The piezoelectric material was lead zirconate titanate (PZT) that was deposited by the hydrothermal method. This is because the hydrothermal deposition film transducer has superior performance in vibration velocity. The vibration velocity at the tip of the horn in longitudinal direction was 4.0 m/s with 40 Vp-p driving voltage in both side electrodes. To demonstrate a beneficial effect of the scalpel, a cutting test that the transducer was stuck into pork fat was carried out. Efficient cutting performance was demonstrated using the transducer sized for an endoscope.
研制了一种微型超声手术刀的换能器。微型超声手术刀可以与内窥镜一起用于非腹部手术或显微手术,例如,通过显微镜。超声波换能器长9.8 mm,宽2.7 mm,阶梯式喇叭放大振动速度;喇叭的尖端是0.6毫米宽。手术刀以278千赫左右的共振频率纵向振动。压电材料为锆钛酸铅(PZT),采用水热法制备。这是因为热液沉积薄膜换能器在振动速度上具有优越的性能。喇叭尖端纵向振动速度为4.0 m/s,两侧电极驱动电压为40 Vp-p。为了证明手术刀的有益效果,进行了将换能器插入猪油中的切割试验。使用内窥镜尺寸的换能器证明了有效的切割性能。
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引用次数: 2
Application of Acoustical Activity in Lithium Niobate Crystals for Control of Light Intensity 声活性在铌酸锂晶体光强控制中的应用
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387845
F. Akhmedzhanov
New technology is offered for measuring and control of light intensity. In the proposed method the phenomenon of acoustical activity and Bragg light diffraction on hypersonic waves in ferroelectric crystal LiNbO3 is used. Control of light intensity can be realized by transference of crystal or by modification of generator frequency by which the transverse acoustic wave is excited. The change of light intensity is provided electronically, fluently and with high accuracy. Using previously the standard calibration, it is possible to measure and change the light intensity to the necessary value.
提出了光强测量与控制的新技术。该方法利用了铁电晶体LiNbO3中高超声速波的声活动和布拉格光衍射现象。光强的控制可以通过晶体的转移或通过改变激发横声波的发生器频率来实现。光强的变化是电子提供,流畅和高精度。使用先前的标准校准,可以测量和改变光强到必要的值。
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引用次数: 0
Comparison of Surface and Bulk Crystal Structure in the xBiFeO3-(1-x)PbTiO3 Solid Solution System
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387852
S. Turner, T. Comyn, A. Bell
Sintered high density compacts from the BiFeQ3- PbTiO3 solid solution series were fabricated using conventional mixed-oxide techniques. The compacts were then prepared and examined using conventional X-ray diffraction. This surface measurement showed a large region of co-existence of two crystallographic phases, rhombohedral and tetragonal. Examination of the bulk material using transmission of synchrotron generated x-rays shows there to be a large difference between the surface and bulk structures. However, upon heat treatment, the structure at the surface transforms into a phase assemblage more closely resembling that of the bulk.
采用传统的混合氧化物技术制备了BiFeQ3- PbTiO3固溶体系列烧结高密度致密体。然后用常规的x射线衍射法制备和检查压片。这种表面测量表明,两种晶体相,菱形和四边形共存的大区域。使用同步加速器产生的x射线透射检查块状材料,表明表面和块状结构之间存在很大差异。然而,经过热处理后,表面的结构转变为更接近于体的相组合。
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引用次数: 0
Direct-Write Deposition of PZT Thick Films Derived from Modified Sol-Gel Process 溶胶-凝胶法制备PZT厚膜的直接写入沉积
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387832
J. Sun, M. Vittadello, E. K. Akdoğan, A. Hall, N. M. Hagh, A. Safari
Lead zirconate titanate (PZT) thick films (6-70 mum) have been deposited on platinum coated alumina and silicon substrates using Micropentrade direct-write technique. Feedstock materials for Micropen deposition have been prepared by a modified sol-gel process in which different amounts of commercial PZT powder (15, 20, 25, 30 vol%) were dispersed in a stable PZT sol to achieve low temperature heat treatment conditions (700degC). The effects of the substrate, intermediate sol layer, film thickness, PZT content, and Micropen parameters on the resulting multi-layer PZT films have been investigated. The films using 15 vol% paste on Pt/Si substrate showed dielectric constant in the range 540-870, dielectric loss between 4.1 and 4.5 % at 1 kHz, remanent polarization (Pr) of 7-12 muC/cm2, and coercive field (Ec) of 24-30 kV/cm.
采用Micropentrade直接写入技术在铂涂层氧化铝和硅衬底上制备了锆钛酸铅(PZT)厚膜(6-70 μ m)。采用改进的溶胶-凝胶工艺制备了Micropen沉积的原料,其中不同量的PZT粉末(15、20、25、30 vol%)分散在稳定的PZT溶胶中,以达到低温热处理条件(700℃)。研究了衬底、中间溶胶层、薄膜厚度、PZT含量和Micropen参数对多层PZT薄膜的影响。在Pt/Si衬底上使用15 vol%浆料制备的薄膜介电常数在540 ~ 870之间,1 kHz时介电损耗在4.1 ~ 4.5%之间,剩余极化(Pr)为7 ~ 12 muC/cm2,矫顽力场(Ec)为24 ~ 30 kV/cm。
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引用次数: 2
Epitaxial Growth of Ferroelectric Thin Films by Combustion Chemical Vapor Deposition and Their Electrical Properties 燃烧化学气相沉积法外延生长铁电薄膜及其电学性能
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387905
Zhiyong Zhao, Yongdong Jiang, Xiaoyan Wang, Kwang Choi, A. Hunt
Combustion chemical vapor deposition (CCVD) has been used to grow a wide variety of ferroelectric thin films such as Ba1-xSrxTiO3 (BST) and PbZrxTi1-xO3 (PZT) on single crystal substrates. This paper presents the growth and characterization of epitaxial BST films on sapphire. Surface morphology, phase, and composition of the as -grown films were characterized. Planar gap capacitors were fabricated, and their capacitance, quality factor (Q) and tunability were investigated as a function of film thickness and DC bias. A 2:1 tunability was achieved for BST thin films under a DC bias of 10 V, and low-frequency Q can be as high as 100. Coplanar waveguide (CPW) structures were also designed and fabricated onto BST coated sapphire substrates. S-parameters of the CPW were tested using a vector network analyzer, and dielectric constant and loss tangent were then derived by comparing the measured data with electromagnetic (EM) simulation results. The dielectric constant was found to be in the range of 300-800, and a loss tangent of 0.05 at 40 GHz was achieved for a 300 nm thick BST film. The epitaxial BST films have been used to fabricate low-loss tunable filters and phase shifters with operation frequencies up to 40 GHz.
燃烧化学气相沉积(CCVD)已被用于在单晶衬底上生长各种铁电薄膜,如Ba1-xSrxTiO3 (BST)和PbZrxTi1-xO3 (PZT)。本文介绍了蓝宝石外延BST薄膜的生长和表征。表征了生长膜的表面形貌、物相和组成。制作了平面间隙电容器,研究了其电容、品质因子Q和可调性随薄膜厚度和直流偏置的变化规律。BST薄膜在直流偏置10v下可调谐达到2:1,低频Q可高达100。在BST涂层蓝宝石衬底上设计并制备了共面波导(CPW)结构。利用矢量网络分析仪测试了CPW的s参数,并将测量数据与电磁仿真结果进行比较,得到了CPW的介电常数和损耗正切。发现300 nm厚BST薄膜的介电常数在300 ~ 800之间,损耗正切在40 GHz时为0.05。外延BST薄膜已被用于制造工作频率高达40ghz的低损耗可调谐滤波器和移相器。
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引用次数: 6
Piezoelectric and Ferroelectric Properties of (1-x)Pb(Sc0.5Ta0.5)O3-xPb(Zr0.52Ti0.48)O3 Relaxor Ferroelectric Ceramics (1-x)Pb(Sc0.5Ta0.5)O3- xpb (Zr0.52Ti0.48)O3弛豫铁电陶瓷的压电和铁电性能
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387862
Wei Shi, Qiang Chen, D. Lan, Lin Chen, Wei Huang, D. Xiao, Jianguo Zhu
(1-x)Pb(Sc0.5Ta0.5)O3-xPb(Zr0.52Ti0.48)O3 (PSTZT-100x) ceramics were prepared by using conventional oxide processing, and their piezoelectric and ferroelectric properties studied. The results of X-ray diffraction (XRD) suggest that PSTZT-100x ceramics formed a single-phase perovskite structure when 0.1lesxles0.8. The ceramics exhibit relatively good piezoelectric and ferroelectric properties: piezoelectric constant, d33=117 pC/N; planar electromechanical coupling factor, kp=45%, remnant polarization, Pr=14 muC/cm2, coercive field, Ec=0.65 kV/mm. The morphotropic phase boundary (MPB) of PSTZT-100x maybe located at x=0.75 because of the maximum piezoelectric constant d33 achieved at x=0.75. The pinched hysteresis loops were founded for PSTZT-100x ceramics when x>0.7, and it was suggested that the pinched ferroelectric loops due to the pinning effect of the dipolar defects formed in PSTZT-100x ceramics.
采用常规氧化物工艺制备了(1-x)Pb(Sc0.5Ta0.5)O3- xpb (Zr0.52Ti0.48)O3 (PSTZT-100x)陶瓷,并对其压电和铁电性能进行了研究。x射线衍射(XRD)结果表明,PSTZT-100x陶瓷在0.1lesxles0.8时形成了单相钙钛矿结构。陶瓷具有较好的压电和铁电性能:压电常数d33=117 pC/N;平面机电耦合系数kp=45%,残余极化,Pr=14 muC/cm2,矫顽力场,Ec=0.65 kV/mm。由于压电常数d33在x=0.75处达到最大值,因此PSTZT-100x的致形相边界(MPB)可能位于x=0.75处。当x>0.7时,PSTZT-100x陶瓷出现了缩紧磁滞回线,认为缩紧磁滞回线是由于PSTZT-100x陶瓷中偶极缺陷的钉住效应造成的。
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引用次数: 0
Sol-gel derived lead-free piezoelectric Bi1/2Na1/2TiO3 thin film for MEMS applications 用于MEMS应用的溶胶-凝胶衍生无铅压电Bi1/2Na1/2TiO3薄膜
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4349274
Ting Yu, K. Kwok, H. Chan
Bi1/2Na1/2TiO3 (abreviated as BNT) is considered as a promising lead-free piezoelectric material for sensor and actuator applications. In this study, we demonstrate an improved sol-gel process using rapid thermal annealing (RTA). Our results indicate that thermal annealing in an oxygen atmosphere after each layer of coating is effective in promoting crystallization of the BNT film at a low temperature of 650degC. The resulting film is dense and well crystallized in the perovskite phase. The piezoelectric properties of the sol-gel derived BNT films are characterized with the help of a laser interferometer. The BNT based film is expected to be a new and promising candidate for lead-free piezoelectric MEMS applications.
Bi1/2Na1/2TiO3(简称BNT)被认为是一种很有前途的无铅压电材料,可用于传感器和执行器。在这项研究中,我们展示了一种改进的使用快速热退火(RTA)的溶胶-凝胶工艺。结果表明,在650℃的低温下,每层涂层后在氧气气氛中进行热处理,可以有效地促进BNT薄膜的结晶。所得薄膜致密且在钙钛矿相中结晶良好。利用激光干涉仪对溶胶-凝胶衍生BNT薄膜的压电特性进行了表征。BNT基薄膜有望成为无铅压电MEMS应用的新候选材料。
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引用次数: 5
Aging in Ferroelectrics, a Drift Approach 铁电体的老化,一种漂移方法
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387888
Y. Genenko, N. Balke, D. Lupascu
Point defect migration is considered as a mechanism to yield aging in ferroelectrics. Different from magnetic systems, ferroelectric domains can be pinned by free charges at the perimeter of otherwise homogeneous grains or crystals. This clamping is shown to be stronger due to the reorientation of defect dipoles. Clamping stresses are calculated to be in the range of 106 to 107 Pa in a uniaxial model corresponding to experimental values in the model material BaTiO3. Their time dependence is given in a uniaxial model case. An extension to three dimensions is discussed. The values are independent of the type of mobile defect charge carrier, electronic or ionic.
点缺陷迁移被认为是铁电体屈服老化的一种机制。与磁性系统不同,铁电畴可以由均匀颗粒或晶体周围的自由电荷固定。由于缺陷偶极子的重定向,这种夹持被证明是更强的。在单轴模型中计算出的夹紧应力范围为106 ~ 107 Pa,与模型材料BaTiO3的实验值相对应。在单轴模型情况下给出了它们的时间依赖关系。讨论了对三维空间的扩展。这些值与移动缺陷电荷载体的类型无关,是电子的还是离子的。
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引用次数: 0
Effect of Sintering Temperature on Thermal Expansion and Dielectric Properties of Pb TiO3 Ceramics Prepared under various sintering conditions 烧结温度对不同烧结条件下制备的pbtio3陶瓷热膨胀和介电性能的影响
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387834
R. Wongmaneerung, R. Yimnirun, S. Ananta, R. Guo, A. Bhalla
In this work, the effect of two stage sintering and sintering temperature on dielectric properties of perovskite PbTiO3 ceramics are reported. High density lead titanate (PbTiO3) ceramics were prepared by a solid solution method. Several sintering temperatures were selected to prepare the samples. The dielectric constant of these samples was measured in a frequency range from 100 Hz to 1 MHz. Thermal expansion measurements on pure and doped samples under various thermal cycling and poling conditions were also done in order to understand the stress behavior of PbTiO3.
本文报道了两段烧结和烧结温度对钙钛矿型PbTiO3陶瓷介电性能的影响。采用固溶法制备了高密度钛酸铅(PbTiO3)陶瓷。选择了几种烧结温度来制备样品。在100 Hz至1 MHz的频率范围内测量了这些样品的介电常数。为了了解PbTiO3的应力行为,还对不同热循环和极化条件下的纯样品和掺杂样品进行了热膨胀测量。
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引用次数: 0
Piezoelectric Micromachined Ultrasonic Transducers based on PZT films 基于PZT薄膜的压电微机械超声换能器
Pub Date : 2006-07-01 DOI: 10.1109/ISAF.2006.4387898
B. Belgacem, F. Calame, P. Muralt
Piezoelectric micro machined ultrasonic transducers (pMUT) are piezoelectric laminated plates operating at flexural modes. The pMUT's fabricated in this work contained a 4 mum thick lead zirconate titanate (PZT) thin film deposited by a sol-gel technique, and exhibiting a permittivity of epsivr=1200, and an effective transverse piezoelectric coefficient e31.f of 12 C/m2. A further optimization of the sol-gel process yielded larger grain diameters and consequently improved properties: epsivr=1600, e31.f of 16 C/m2. A design and micromachining concpet for easy scaling in frequency has been developed. The electromechanical coupling coefficient (k2) and the quality factor (Q) of rectangular clamped elements (with former PZT process) were measured as k2=4.4% and Q=145 in air for a low frequency transducer (@240 kHz). The 16.9 MHz transducer yielded values of Q=25 and k2 =3% in air. The effect of DC bias voltage on frequency and k2 has been studied.
压电微机械超声换能器(pMUT)是一种工作在弯曲模式下的压电层合板。采用溶胶-凝胶法制备的pMUT包含4 μ m厚的锆钛酸铅(PZT)薄膜,其介电常数epsivr=1200,有效横向压电系数e31。f (12c /m2)溶胶-凝胶工艺的进一步优化产生了更大的颗粒直径,从而改善了性能:epsivr=1600, e31。f (16c /m2)提出了一种易于缩放频率的设计和微加工概念。对低频换能器(@240 kHz)在空气中的机电耦合系数(k2)和品质因子(Q)(采用原PZT工艺)分别为k2=4.4%和Q=145。16.9 MHz换能器在空气中产生Q=25和k2 =3%的值。研究了直流偏置电压对频率和k2的影响。
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引用次数: 14
期刊
2006 15th ieee international symposium on the applications of ferroelectrics
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