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Experimental Analysis of Autoclave Airflow Patterns and the Implementation of Active Flow Manipulation to Improve Manufacturing Efficiency 高压灭菌器气流模式的实验分析及主动流动控制的实施以提高制造效率
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-07-16 DOI: 10.1007/s10443-025-10357-x
Markus Englhard, Tobias A. Weber, Raphael Strecker, Benjamin Hailer, Jan-Christoph Arent, Peter Middendorf

This study is dedicated to enhance the efficiency of autoclave curing processes for composite components in the aerospace industry, focusing on reducing time and energy consumption along with improving part quality. Comprehensive flow field analyses were conducted in a large autoclave under industrial loading conditions. Lumped mass calorimeter were incorporated to measure the distribution of heat transfer coefficients and variations in the temperature field during the process. Additionaly, tuft flow visualization was employed to reveal airflow patterns. The results indicated significant spatial variations in heat transfer conditions due to a highly complex flow field, emphasizing the necessity for sophisticated optimization strategies. In this regard, a novel approach using supplementary fans in the loading chamber was introduced to actively manipulate the flow field and address the previously identified process limitations. An experimental proof of concept demonstrated that the fans offer significant potential for enhancing heat transfer and improving local gas mixing capability in areas with minimal airflow, especially during ambient pressure heating stages. A subsequent hypothetical performance estimate demonstrated that for a given test configuration (five-meter-long, 2200 kg test tool), the employment of three fans could reduce the lead-time by 106 min and decrease the temperature spread within the composite part by 48%. Consequently, this study provides fundamental insights into flow dynamics and heat transfer in an industrial scale autoclave, and it highlights a promising method to improve both process efficiency and part quality for mixed loading batches as well as for batches of large, integrated components.

本研究致力于提高航空航天工业中复合材料部件的蒸压釜固化工艺的效率,重点是减少时间和能源消耗,提高零件质量。在工业负荷条件下,对大型高压灭菌器进行了全面的流场分析。采用集总质量量热仪测量了传热系数的分布和温度场的变化。此外,采用簇状流动可视化来显示气流模式。结果表明,由于高度复杂的流场,传热条件在空间上存在显著差异,强调了采用复杂优化策略的必要性。在这方面,引入了一种新颖的方法,在加载室中使用辅助风扇来主动操纵流场,并解决了先前确定的工艺限制。一项概念实验证明,在气流最小的区域,特别是在环境压力加热阶段,风扇提供了增强传热和改善局部气体混合能力的巨大潜力。随后的假设性能评估表明,对于给定的测试配置(5米长,2200公斤的测试工具),使用三个风扇可以减少106分钟的交货时间,并将复合材料部件内的温度扩散降低48%。因此,本研究为工业规模高压灭菌器的流动动力学和传热提供了基本的见解,并强调了一种有前途的方法,可以提高混合装载批次以及大型集成组件批次的工艺效率和零件质量。
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引用次数: 0
Effect of Triangular Defect Geometry and Distribution in Automated Fiber Placement on the Mechanical Properties of Composite Structures 自动铺布过程中三角形缺陷的几何形状和分布对复合材料结构力学性能的影响
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-07-12 DOI: 10.1007/s10443-025-10361-1
W. A. Ren, X. H. Chen, J. D. Hu

Triangular defects generated during the Automated Fiber Placement (AFP) process in double-curvature composite structures are a common flaw that significantly affects structural mechanical properties. This study systematically investigates the formation mechanisms of triangular defects, examines their various geometries, and analyzes their stacking behavior across different plies in relation to mechanical performance. The goal is to determine the AFP trajectory design strategy to balance the processability of layup and the performance of the structure for the engineering products. The findings indicate that defect geometry has a relatively minor effect on specimen performance. However, the number of defects and their overlap considerably influence structural behavior. Specifically, a 0° triangular defect in the first ply reduces tensile properties by 13.5%, whereas a 3° defect in the same ply decreases tensile performance by 17.5%. Notably, the presence of two overlapping 3° defects results in a 33.5% reduction in tensile properties, and three overlapping 3° defects lead to a 41.3% decline. Consequently, the design of AFP trajectories for composite structures should aim to minimize the occurrence of triangular defects. Moreover, defects in the same orientation across different plies should be staggered to avoid overlap in the thickness direction, thereby reducing the risk of structural failure. In addition, finite element (FE) simulation analysis demonstrates that the deviation between the triangular defect model and experimental results remains within ± 8%, with deviations for single-ply defects below 5%. This simple FE model and test method are considered reliable and can be utilized for trajectory design, triangular defect analysis, and the control of triangular defects in large size composite structures, thereby enhancing defect management in AFP, and promote the engineering project forward.

双曲率复合材料在自动铺放纤维(AFP)过程中产生的三角形缺陷是影响结构力学性能的常见缺陷。本研究系统地研究了三角形缺陷的形成机制,考察了它们的各种几何形状,并分析了它们在不同层间的堆积行为与力学性能的关系。目标是确定在工程产品的铺层工艺性和结构性能之间取得平衡的AFP轨迹设计策略。研究结果表明,缺陷几何形状对试样性能的影响相对较小。然而,缺陷的数量和它们的重叠对结构行为有很大的影响。具体来说,第一层中0°三角形缺陷会使拉伸性能降低13.5%,而同一层中3°缺陷会使拉伸性能降低17.5%。值得注意的是,两个重叠的3°缺陷导致拉伸性能下降33.5%,三个重叠的3°缺陷导致拉伸性能下降41.3%。因此,复合材料结构的AFP轨迹设计应以最小化三角形缺陷的发生为目标。不同层间相同方向的缺陷应错开,避免厚度方向上的重叠,从而降低结构破坏的风险。此外,有限元模拟分析表明,三角缺陷模型与实验结果的偏差在±8%以内,单层缺陷的偏差在5%以下。这种简单的有限元模型和试验方法被认为是可靠的,可用于大尺寸复合材料结构的轨迹设计、三角缺陷分析和三角缺陷控制,从而加强AFP中的缺陷管理,推动工程项目向前发展。
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引用次数: 0
Damage Tolerance of CFRP with Wrinkle Defect Under Different Impact Energies 含褶皱缺陷CFRP在不同冲击能量下的损伤容限
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-07-03 DOI: 10.1007/s10443-025-10359-9
Huiming Ding, Jian Wang, Shidi Zhang

Evaluating the damage tolerance of CFRP structures with wrinkle defects under impact loading is crucial for safe service of the composite structures. In this study, the impact tests and compression tests after impact on CFRP specimens with two different wrinkle sizes under three different impact energies are conducted. The damage tolerance of CFRP specimens under varying impact energies and wrinkle defects is evaluated through impact response and compression response. The results indicate that, corresponding to the theory, the maximum contact force exhibits significant stepwise increase with the increase of impact energy no matter what kind of wrinkle size. However, it should be emphasized that, under the same impact energy, the effect of the wrinkle size on the impact performance is not significant with the variation rate of the maximum contact force less than 10%. In terms of impact damage, the specimens subjected to higher impact energy exhibit severe delamination, and the effect of wrinkle size on impact delamination under the same impact energy is more significant at higher impact energy. As for the compression response, due to the effect of the impact damage and wrinkle fibers, the impact energy and wrinkle size both have significant effect on the residual compressive strength. Moreover, the wrinkle fibers play a dominant role in the compression failure mode of the specimen, while the impact damage caused by impact energy influences the extent of the compression failure of the specimen.

具有褶皱缺陷的CFRP结构在冲击载荷作用下的损伤容限评价对复合材料结构的安全使用至关重要。本研究对两种不同褶皱尺寸的CFRP试件在三种不同冲击能量下进行了冲击试验和冲击后压缩试验。通过冲击响应和压缩响应来评价CFRP试件在不同冲击能和褶皱缺陷下的损伤容限。结果表明,与理论相对应的是,无论何种皱折尺寸,最大接触力都随着冲击能量的增加呈显著的逐步增大。但需要强调的是,在相同的冲击能量下,当最大接触力变化率小于10%时,起皱尺寸对冲击性能的影响不显著。在冲击损伤方面,高冲击能的试件表现出严重的分层现象,相同冲击能下褶皱尺寸对冲击分层的影响在高冲击能下更为显著。在压缩响应方面,由于冲击损伤和起皱纤维的影响,冲击能量和起皱尺寸对残余抗压强度均有显著影响。褶皱纤维在试件的压缩破坏模式中起主导作用,而冲击能量造成的冲击损伤影响试件的压缩破坏程度。
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引用次数: 0
High-Precision Parametric Modeling and Needling Process Mechanism of Carbon Fiber Needled Preforms 碳纤维针刺预制件的高精度参数化建模及针刺工艺机理
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-30 DOI: 10.1007/s10443-025-10358-w
Zhiping Ying, Xueyan Sun, Zhenyu Wu, Laihu Peng, Xiaoying Cheng, Fangyong Zhu, Feiyu Chen

The carbon fiber needled composite material uses the needled preform as the reinforcing phase and has extremely excellent properties. Current research has revealed the basic relationships among the needling process parameters, porosity, and the properties of carbon fibers. However, these studies have not made in-depth observations of the sliding tendency of fibers between the composites during the needling process, as well as the generation and variation trends of pores. Especially, the research on the needled preform is still far from adequate. The internal structure of the carbon fiber preform is extremely complex. Structural characteristics such as diverse fiber morphologies and random fiber distributions have not been fully studied. In the research on the key structural characteristics inside the preform, there is a lack of an effective means to comprehensively, deeply, and accurately parameterize and characterize the internal structure. This defect prevents us from having an in-depth understanding of the preparation and performance optimization processes of the carbon fiber preform, and also makes it impossible to provide accurate predictions and guidance for its performance in practical applications. In view of this, this study conducts parametric modeling of the needled carbon fiber preform, analyzes the internal structure of the preform and performs parameter characterization, constructs a finite element model to study its needling behavior, studies the dynamic behavior of the fibers inside the preform, and analyzes the influence of density on the needling behavior.

碳纤维针刺复合材料采用针刺预制体作为增强相,具有极为优异的性能。目前的研究已经揭示了针刺工艺参数、孔隙率和碳纤维性能之间的基本关系。然而,这些研究并没有深入观察针刺过程中纤维在复合材料之间的滑动趋势,以及孔隙的产生和变化趋势。特别是对针状预制棒的研究还很不充分。碳纤维预制体的内部结构极为复杂。纤维形态的多样性和纤维分布的随机性等结构特征尚未得到充分研究。在对预制件内部关键结构特性的研究中,缺乏一种全面、深入、准确地参数化和表征内部结构的有效手段。这一缺陷使我们无法深入了解碳纤维预制棒的制备和性能优化工艺,也无法对其在实际应用中的性能提供准确的预测和指导。鉴于此,本研究对针刺碳纤维预成型件进行参数化建模,分析预成型件内部结构并进行参数表征,构建有限元模型研究其针刺行为,研究预成型件内部纤维的动态行为,分析密度对针刺行为的影响。
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引用次数: 0
Extending the Double-Double Concept for Woven GFRP Laminates 扩展GFRP复合编织板的双重理念
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-30 DOI: 10.1007/s10443-025-10356-y
Lucas L. Vignoli, Heraldo S. C. Mattos, João M. L. Reis

The influence of the stacking sequence on the mechanical behavior of composite laminates is unquestionable, being one of the most important definitions for structural design. Recently, a novel stacking sequence was proposed in the literature, named Double-Double (DD), demonstrating a great homogenization capability and suitability for optimization procedures due to its double-helix characteristic. However, most DD studies are dedicated to unidirectional carbon fiber reinforced polymers (CFRP). The goal of the present investigation is to extend the DD application to woven glass fiber reinforced polymers (GFRP) for the first time. The stiffness equivalence between DD and quadriaxial (QUAD) is derived based on the classical laminate theory, indicating that it is possible to obtain DD and QUAD woven laminates with the same in-plane stiffness. Tensile tests are carried out to demonstrate experimentally the equivalence between DD and QUAD not only considering the stiffness, but also the laminate strengths. An analytical modeling is implemented to evaluate the laminate failure by applying the Hashin criterion, which is compared with the experimental results and achieved reliable estimations. The influence of multiaxial stress states is also discussed in this study, and the results show that the difference between DD and QUAD strengths is not greater than 10%. At last, a parametric analysis of the strengths of DD laminates is performed. The results highlight that, despite it is theoretically possible to define an equivalent QUAD for the DD with the highest strength, it is not applicable in practice because it would require a large number of plies.

叠层顺序对复合材料层合板力学性能的影响是不容置疑的,是结构设计中最重要的定义之一。最近,在文献中提出了一种新的堆叠序列,称为Double-Double (DD),由于其双螺旋特性,它具有很强的均匀化能力和优化程序的适用性。然而,大多数DD研究都致力于单向碳纤维增强聚合物(CFRP)。本研究的目的是首次将DD应用于编织玻璃纤维增强聚合物(GFRP)。基于经典层压板理论,推导了四轴复合材料(QUAD)与DD复合材料的刚度等效性,表明可以得到具有相同面内刚度的DD复合材料与QUAD复合材料。通过拉伸试验验证了DD和QUAD的等效性,不仅考虑了层合材料的刚度,而且考虑了层合材料的强度。应用Hashin准则建立了层合板破坏分析模型,并与实验结果进行了比较,得到了可靠的估计。本研究还讨论了多轴应力状态的影响,结果表明,DD与QUAD强度的差异不大于10%。最后,对DD层压板的强度进行了参数化分析。结果强调,尽管理论上可以为具有最高强度的DD定义等效QUAD,但在实践中并不适用,因为它需要大量的层。
{"title":"Extending the Double-Double Concept for Woven GFRP Laminates","authors":"Lucas L. Vignoli,&nbsp;Heraldo S. C. Mattos,&nbsp;João M. L. Reis","doi":"10.1007/s10443-025-10356-y","DOIUrl":"10.1007/s10443-025-10356-y","url":null,"abstract":"<div><p>The influence of the stacking sequence on the mechanical behavior of composite laminates is unquestionable, being one of the most important definitions for structural design. Recently, a novel stacking sequence was proposed in the literature, named Double-Double (DD), demonstrating a great homogenization capability and suitability for optimization procedures due to its double-helix characteristic. However, most DD studies are dedicated to unidirectional carbon fiber reinforced polymers (CFRP). The goal of the present investigation is to extend the DD application to woven glass fiber reinforced polymers (GFRP) for the first time. The stiffness equivalence between DD and quadriaxial (QUAD) is derived based on the classical laminate theory, indicating that it is possible to obtain DD and QUAD woven laminates with the same in-plane stiffness. Tensile tests are carried out to demonstrate experimentally the equivalence between DD and QUAD not only considering the stiffness, but also the laminate strengths. An analytical modeling is implemented to evaluate the laminate failure by applying the Hashin criterion, which is compared with the experimental results and achieved reliable estimations. The influence of multiaxial stress states is also discussed in this study, and the results show that the difference between DD and QUAD strengths is not greater than 10%. At last, a parametric analysis of the strengths of DD laminates is performed. The results highlight that, despite it is theoretically possible to define an equivalent QUAD for the DD with the highest strength, it is not applicable in practice because it would require a large number of plies.</p></div>","PeriodicalId":468,"journal":{"name":"Applied Composite Materials","volume":"32 6","pages":"2671 - 2686"},"PeriodicalIF":2.9,"publicationDate":"2025-06-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145341345","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Design and Static Strength Evaluation of SiC/SiC Turbine Blades Considering Manufacturing Constraints 考虑制造约束的SiC/SiC涡轮叶片设计与静强度评价
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-24 DOI: 10.1007/s10443-025-10355-z
Chenyang Liu, Sheng Zhang, Xu Zhang, Chengqian Dong, Fang Wang, Xiguang Gao, Yingdong Song

The use of ceramic matrix composite (CMC) in blades is crucial for improving aero-engine performance. However, designing complex fiber architectures while considering manufacturing constraints poses significant challenges for blade design and evaluation. Manufacturing constraints specifically refer to fiber continuity constraints and fiber path curvature constraints. Here, a cross-scale design methodology and a static strength evaluation system for CMC blades were established and subsequently applied to the design of shrouded blades. The cross-scale design method adequately considered the variety and differences in fiber-architecture molding methods. Weaving parameters were optimized through a cost-effective, simulation-driven design. The blade performance and structural integrity were balanced under manufacturing constraints. The developed static strength evaluation system was used to compare the performance of different designs through simulation analysis and critical tests. No defect was found in the CMC blade prototypes after holding a load for 2 min at 1.15 times their maximum rotational speed. This demonstrated sufficient static strength and confirmed the effectiveness of the design methodology and evaluation system.

陶瓷基复合材料(CMC)在叶片中的应用对于提高航空发动机的性能至关重要。然而,在考虑制造限制的情况下设计复杂的光纤架构对叶片的设计和评估提出了重大挑战。制造约束具体指纤维连续性约束和纤维路径曲率约束。本文建立了CMC叶片的跨尺度设计方法和静强度评估体系,并将其应用于冠状叶的设计。跨尺度设计方法充分考虑了纤维结构成型方法的多样性和差异性。通过经济高效的仿真驱动设计优化织造参数。在制造约束下,平衡了叶片的性能和结构完整性。利用所开发的静强度评价系统,通过仿真分析和关键试验对不同设计方案的性能进行了比较。CMC叶片原型在1.15倍最大转速下保持负载2分钟后未发现缺陷。这证明了足够的静强度,证实了设计方法和评价体系的有效性。
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引用次数: 0
Robust Electrical Contact with Low Interface Resistance Using Embedded Co-cured Electrodes in Carbon Fibre Composites 在碳纤维复合材料中采用嵌入式共固化电极实现低界面电阻的稳健电接触
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-19 DOI: 10.1007/s10443-025-10345-1
Sheik Abdul Malik, Meisam Jalalvand, Matthew D. Wadge, J. D. Acosta, Reda M. Felfel

Achieving robust low-resistance electrical contact with carbon fibres embedded in polymeric matrices is a challenge, and different electrode fabrication methods mostly post-curing the composite have been examined in the literature. This paper investigates the use of metallic foils co-cured on the top surface of carbon fibre reinforced polymer (CFRP) composites to form stable electrodes. The effects of different electrode materials and their geometric variations on the interface resistance (IR) between CFRP and electrodes are studied experimentally. Finite element (FE) analysis is used to estimate the spread resistance (SR), providing a reliable measure of IR for various electrode–CFRP configurations. Copper is found to be the optimal electrode material and has a low IR per unit electrode area ranging from 2.5 × 10−4 Ωmm−2 to 1 × 10−3 Ωmm−2 independent of geometric parameters. Pull-off tests demonstrate that the co-cured electrodes exhibit acceptable mechanical bonding with the composite layer. Compared to other electrode fabrication methods, the co-curing technique is significantly easier, less invasive and more cost-effective, as it eliminates the need to alter or induce surface damage in CFRP specimens.

Graphical Abstract

Co-cured metal foils simplify electrode fabrication in CFRP and achieves stable, low interface resistance

与嵌入在聚合物基体中的碳纤维实现坚固的低电阻电接触是一个挑战,文献中研究了不同的电极制造方法,大多数是在复合材料固化后。本文研究了利用金属箔在碳纤维增强聚合物(CFRP)复合材料的表面共固化形成稳定电极的方法。实验研究了不同电极材料及其几何变化对CFRP与电极界面电阻的影响。有限元(FE)分析用于估计扩散电阻(SR),为各种电极- cfrp配置提供可靠的IR测量。铜是最理想的电极材料,其单位电极面积的红外光谱在2.5 × 10−4 Ωmm−2到1 × 10−3 Ωmm−2之间,与几何参数无关。拉脱试验表明,共固化电极与复合层表现出可接受的机械结合。与其他电极制造方法相比,共固化技术明显更容易,侵入性更小,成本效益更高,因为它不需要改变或诱导CFRP样品的表面损伤。共固化金属箔简化了CFRP电极的制作,实现了稳定、低界面电阻
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引用次数: 0
Response of Structurally Integrated Antenna Subjected to Low Velocity Impacts 结构集成天线在低速冲击下的响应
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-13 DOI: 10.1007/s10443-025-10354-0
Jianqiang Hu, Zhiyuan Zhang, Zewei Lian, Zhehan Lin

In this study, an integrated composite antenna structure was designed and fabricated to investigate its behavior under low-velocity impacts with energy levels ranging from 10 J to 100 J. The specimens were positioned and supported in accordance with ASTM D7136 standards, while post-impact compression tests followed ASTM D7137 protocols. Numerical models were developed using ABAQUS finite element (FE) software to validate experimental results, including impact response curves, damage morphologies, and compression failure modes. Both experimental and simulation results demonstrated strong agreement, confirming the accuracy of the constitutive model. Additionally, electromagnetic performance evaluations through experiments and simulations verified the structural integrity and functional reliability of the antenna under varying impact conditions.

本研究设计并制作了一种集成复合材料天线结构,研究了其在10 J ~ 100 J低速冲击下的性能。试件的定位和支撑按照ASTM D7136标准进行,冲击后压缩试验按照ASTM D7137标准进行。利用ABAQUS有限元软件建立数值模型,验证试验结果,包括冲击响应曲线、损伤形态和压缩破坏模式。实验结果与仿真结果吻合较好,验证了本构模型的准确性。此外,通过实验和仿真进行电磁性能评估,验证了天线在不同冲击条件下的结构完整性和功能可靠性。
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引用次数: 0
Production, Microstructure, and Tensile Properties of Copper-Coated Short Carbon Fiber Reinforced Al-Matrix Composite Sheets via Accumulative Roll-Bonding 累积滚接镀铜短碳纤维增强铝基复合材料板的生产、微观结构和拉伸性能
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-12 DOI: 10.1007/s10443-025-10336-2
Wenchuang Liu, Xingang Liu, Ying Guo, Wenquan Li, Kenjiro Sugio, Yujiao Ke, Gen Sasaki

Metal matrix composite (MMC) sheets with well-dispersed reinforcements can be continuously produced using the accumulative roll-bonding (ARB) method. However, carbon fibers (CFs), an ideal reinforcement for MMCs, have not been extensively utilized due to the poor wettability of carbon/aluminum system. This study addresses this issue by modifying the fiber surface with copper (Cu) coating and applying this new reinforcement to Aluminum matrix composites (AMCs) produced via the ARB method. The results demonstrate that copper coated CFs (Cu-CFs) were well-dispersed throughout the matrix with appropriate ARB cycles. The surface treatment improved the spatial uniformity of the reinforcement, enhanced interfacial bonding, and refined the matrix grains. Consequently, the Cu-CF/Al composites exhibited the highest tensile strength (187.8 MPa) compared to composites reinforced with uncoated CFs (131.9 MPa) and monolithic Al without CFs (122.7 MPa). These findings suggest that combining ARB with electroless copper coating holds broad prospects in materials engineering, providing a valuable area of study for enhancing composite material performance.

采用累积滚接(ARB)方法可以连续生产具有良好分散增强的金属基复合材料(MMC)板材。然而,碳纤维作为mmc的理想增强材料,由于碳/铝体系的润湿性较差,一直没有得到广泛的应用。本研究通过在纤维表面涂覆铜(Cu)涂层,并将这种新型增强材料应用于ARB法生产的铝基复合材料(amc),解决了这一问题。结果表明,铜包覆碳纤维(cu -碳纤维)在适当的ARB循环下分散在基体中。表面处理改善了增强体的空间均匀性,增强了界面结合,细化了基体晶粒。结果表明,Cu-CF/Al复合材料的抗拉强度为187.8 MPa,高于未包覆碳纤维的复合材料(131.9 MPa)和未包覆碳纤维的单片铝复合材料(122.7 MPa)。这些发现表明,ARB与化学镀铜相结合在材料工程中具有广阔的应用前景,为提高复合材料的性能提供了一个有价值的研究领域。
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引用次数: 0
The Effect of PA66 Nanofibrous Interlayers on Mode II Delamination Behavior of Filament-wound CFRP Laminates at Room and Cryogenic Temperatures PA66纳米纤维夹层对常温和低温下缠绕CFRP复合材料II型分层行为的影响
IF 2.9 4区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2025-06-12 DOI: 10.1007/s10443-025-10353-1
Recep Ufuk, Baris Emre Kiral, Melih Papila, Kaan Bilge

This work aims to assess the potential of commercially available PA 6,6 nanofibrous mats when incorporated to large scale filament winding process. The conventional wet winding process was employed on a specially designed flat mandrel to manufacture uni-directional composite laminates. A49-12 K carbon fibers and cryogenic-compatible CTD 7.1 epoxy resin was employed. The winding process was temporarily paused at the mid-plane thickness to introduce a pre-crack using a 12 μm non-adherent film and to place PA66 nanofibers with an aerial weight of 3 g/m². The winding process then resumed. Laminate curing was performed in an autoclave oven for 3 h at 80oC under nitrogen environment. Flat wound laminates were then cut into end notched flexure (ENF) test samples in accordance with ASTM D7905/D7905M-19. ENF tests were performed at room temperature (RT) and cryogenic conditions in a liquid nitrogen bath. Test results suggested that mode II strain energy (GIIc) of interlayered laminates were 35% higher than the one of neat laminates when tested at room temperature. On the contrary, addition of polymeric nanofibrous interlayers reduced GIIc by 40% in cryogenic conditions. Fractographic analysis suggested that the improvement at RT was primarily due to (i) toughening at the resin rich pockets inherent by the tow-undulation effect in wet winding (ii) crack deflection in irregular tow-tow interfaces. The reduction in GIIc was attributed to synchrony of several factors, namely dominance of fiber/matrix debonding due to thermal contraction at fiber/resin interfaces, elevated brittleness of the polymeric nanofibers and pre-mature cracking due to nanofiber/resin debonding.

这项工作旨在评估商用pa6,6纳米纤维垫在大规模长丝缠绕工艺中的潜力。在特殊设计的平面芯轴上采用传统湿缠绕工艺制备单向复合材料层合板。采用a49 - 12k碳纤维和低温兼容CTD 7.1环氧树脂。缠绕过程暂时停止在中间平面厚度,使用12 μm的非粘附膜引入预裂缝,并放置航空重量为3 g/m²的PA66纳米纤维。接着,上卷过程又开始了。层压板在氮气环境下,在80℃的高压蒸箱中固化3小时。然后按照ASTM D7905/D7905M-19将平面缠绕层压板切割成端缺口弯曲(ENF)测试样品。ENF测试在室温(RT)和液氮浴低温条件下进行。实验结果表明,在室温下,层间层合板的II型应变能(GIIc)比整齐层合板的应变能高35%。相反,在低温条件下,聚合物纳米纤维夹层的加入使GIIc降低了40%。断口分析表明,热应力的改善主要是由于(i)湿缠绕中的拖-波动效应所固有的富树脂袋的增韧(ii)不规则拖-拖界面的裂纹挠曲。GIIc的降低归因于几个因素的同步,即纤维/树脂界面的热收缩导致纤维/基体脱粘,聚合物纳米纤维的脆性升高以及纳米纤维/树脂脱粘导致的过早开裂。
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引用次数: 0
期刊
Applied Composite Materials
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