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A review of the techniques used to characterize laser sintering of polymeric powders for use and re-use in additive manufacturing 综述了用于表征增材制造中使用和再利用的聚合物粉末的激光烧结技术
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/MFREVIEW/2021012
F. M. Mwania, M. Maringa, J. G. van der Walt
Additive manufacturing (AM), is one of the key components of the 4th industrial revolution. Polymer laser sintering (PLS) is a subset of AM that is commonly used to process polymers, and which achieves good surface finish, good mechanical properties of finished products and for which there is no need for support structures. However, the requirements for polymeric powder for PLS are strident. Moreover, PLS subjects polymeric feed powders to high temperatures that lead to degradation of their thermal, rheological, and physical properties and is thus an impediment to their recyclability. Therefore, it is imperative to investigate the degree of polymer degradation or aging before re-using the material. This paper reviews the common techniques that are employed to characterize the suitability of polymeric powders for use and re-use in the PLS process. These include, but are not limited to, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), laser diffraction analysis, gas pycnometry, scanning electron microscopy (SEM), and melt flow index (MFI) testing.
增材制造(AM)是第四次工业革命的关键组成部分之一。聚合物激光烧结(PLS)是AM的一个子集,通常用于加工聚合物,它可以实现良好的表面光洁度,成品的良好机械性能,并且不需要支撑结构。然而,对聚合物粉末的要求是苛刻的PLS。此外,PLS使聚合物饲料粉末处于高温下,导致其热、流变和物理性能退化,从而阻碍了其可回收性。因此,在材料再利用之前,必须对聚合物的降解或老化程度进行研究。本文回顾了用于表征聚合物粉末在PLS过程中使用和再利用的适用性的常用技术。这些包括但不限于,差示扫描量热法(DSC),热重分析(TGA),激光衍射分析,气体比重分析,扫描电子显微镜(SEM)和熔体流动指数(MFI)测试。
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引用次数: 6
Thermal behavior of lead silicate vitreous materials for sealants 密封胶用硅酸铅玻璃材料的热性能
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/MFREVIEW/2021002
A. Mocioiu, O. Mocioiu
The objective of our investigations consists in the thermal characterization of SiO2-PbO-Na2O vitreous materials in order to establish their properties for applications mainly as sealants. In order to evaluate the vitreous material − metal adherence, the thermal expansion coefficients (α) from experimental and theoretic data were determined. The differential thermal analysis of studied materials give the information about temperatures characteristic to glass transition, crystallization and melting. Dilatometer measurements were performed in air atmosphere in order to establish thermal coefficients of the materials. Softening and flowing characteristic of the vitreous materials were established by heating microscope measurements. The difference between thermal expansion coefficient (α) of the vitreous materials (10.2 × 10−6K−1 and 17.6 × 10−6K−1) and thermal expansion coefficient of the steel substrate OL 38 (10.8 × 10−6K−1) is under 37%. This value is fit for a good adherence between materials.
我们研究的目的包括SiO2-PbO-Na2O玻璃材料的热特性,以确定其主要用作密封剂的性能。为了评价玻璃材料-金属的粘附性,从实验和理论数据中确定了热膨胀系数(α)。所研究材料的差热分析提供了玻璃化转变、结晶和熔化的温度特征信息。为了确定材料的热系数,在空气气氛中进行了膨胀仪测量。通过加热显微镜测量,确定了玻璃材料的软化和流动特性。玻璃材料的热膨胀系数(α) (10.2 × 10−6K−1和17.6 × 10−6K−1)与钢基体ol38的热膨胀系数(10.8 × 10−6K−1)的差异小于37%。此值适用于材料之间良好的粘附性。
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引用次数: 1
Welding of magnesium and its alloys: an overview of methods and process parameters and their effects on mechanical behaviour and structural integrity of the welds 镁及其合金的焊接:方法和工艺参数的概述及其对焊接的机械行为和结构完整性的影响
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/mfreview/2021028
D. Klenam, Gabriel Seun Ogunwande, T. Omotosho, Blessing Ozah, N. Maledi, S. I. Hango, A. Fabuyide, Lesego Mohlala, J. W. van der Merwe, M. Bodunrin
An overview of welding methods and process parameters and its effects on mechanical behaviour and structural integrity of magnesium and its alloys are discussed. These alloys are less dense and beneficial structural alloys for improved energy efficiency, eco-friendliness and driver of circular economic model for sustainable design and innovative ecosystem. While the application of Mg-alloys is projected to increase, understanding the mechanical behaviour and structural integrity of welded joints are critical. Thus, fusion and solid-state welding processes of these alloys are discussed with emphasis on mechanical characterization. Laser welding is the most effective fusion welding technique for most Mg alloys whereas, the predominant solid-state method is friction stir welding. The importance of process variables such as heat inputs, welding velocity (speed) and post weld treatments on the microstructural evolution, on mechanical and physical properties of the distinct zones of the weld joints are described. The weldment is the most susceptible to failure due to phase transformation, defects such as microporosity and relatively coarse grain sizes after solidification. The implication of the design of quality weld joints of Mg alloys are explored with areas for future research directions briefly discussed.
综述了焊接方法、工艺参数及其对镁及其合金力学性能和结构完整性的影响。这些合金是低密度和有益的结构合金,可提高能源效率,生态友好和驱动可持续设计和创新生态系统的循环经济模式。虽然镁合金的应用预计会增加,但了解焊接接头的力学行为和结构完整性至关重要。因此,讨论了这些合金的熔合和固态焊接工艺,重点是力学特性。激光焊接是大多数镁合金最有效的熔焊技术,而主要的固态方法是搅拌摩擦焊。描述了热输入、焊接速度(速度)和焊后处理等工艺变量对焊接接头不同区域的显微组织演变、机械和物理性能的重要性。焊件在凝固后最容易因相变、微孔隙等缺陷和相对粗大的晶粒尺寸而失效。探讨了镁合金焊接接头质量设计的意义,并对今后的研究方向作了简要的讨论。
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引用次数: 1
A holistic End-of-Life (EoL) Index for the quantitative impact assessment of CFRP waste recycling techniques 一种用于碳纤维布废弃物回收技术定量影响评估的整体寿命终止(EoL)指数
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/mfreview/2021016
D. Markatos, C. Katsiropoulos, K. Tserpes, S. Pantelakis
In the present study, a holistic End-of-Life (EoL) Index is introduced to serve as a decision support tool for choosing the optimal recycling process among a number of alternative recycling techniques of CFRP waste. For the choice of the optimal recycling process, quality of the recycled fibers as well as cost and environmental impact of the recycling methods under consideration, are accounted for. Quality is interpreted as the reusability potential of the recycled fibers; that is quantified through the equivalent volume fraction of recycled fibers that balances the mechanical properties of a composite composed of a certain volume fraction of virgin fibers. The proposed Index is offering an estimated balanced score, quantifying a trade-off between the reusability potential of the recycled fibers as well as the cost and the environmental impact of the recycling methods considered.
在本研究中,引入了一个整体的寿命终止(EoL)指数,作为决策支持工具,在众多可选的碳纤维增强塑料废物回收技术中选择最佳回收工艺。为了选择最佳的回收工艺,考虑了回收纤维的质量以及所考虑的回收方法的成本和环境影响。质量被解释为再生纤维的再利用潜力;这是通过平衡由一定体积分数的原始纤维组成的复合材料的机械性能的再生纤维的等效体积分数来量化的。拟议的指数提供了一个估计的平衡分数,量化了回收纤维的再利用潜力以及所考虑的回收方法的成本和环境影响之间的权衡。
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引用次数: 3
A combination method for multi-criteria decision making problem in turning process 车削过程多准则决策问题的组合方法
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/mfreview/2021024
D. Duc Trung
This paper presents a multi-criteria decision making (MCDM) for a turning process. An experimental process was performed according to the sequence of a matrix using the Taguchi method with nine experiments. The parameters including workpiece speed, feed rate, depth of cut, and nose radius were selected as the input variables. At each experiment, three cutting force components that were measured in the three directions X, Y, and Z, were Fx, Fy, and Fz, respectively. The value of Material Removal Rate (MRR) was also calculated at each experiment. The main purpose of this study is determination of an experiment in total performed experiments simultaneously ensuring the minimum Fx, Fy, and Fz and the maximum MRR. The Entropy method was applied to determine the weights for parameters Fx, Fx, Fx, and MRR. Eight MCDM methods were applied for multi-criteria decision making, this has not been performed in any studies. The implementation steps of each method were also presented in this paper. Seven ones of these eight methods determined the best experiment in total nine performed experiments. A new multi-criteria decision-making method as well as orientation for the further works were also proposed in this study.
提出了车削加工的多准则决策方法。用田口法按照矩阵的顺序进行了一个实验过程,共有9个实验。选取工件速度、进给速度、切削深度和机头半径等参数作为输入变量。在每次实验中,分别在X、Y、Z三个方向上测量的三个切削力分量分别为Fx、Fy、Fz。同时计算每次实验的材料去除率(MRR)。本研究的主要目的是在同时进行的所有实验中确定一个实验,以确保最小的Fx, Fy和Fz以及最大的MRR。采用熵值法确定参数Fx、Fx、Fx和MRR的权重。八种MCDM方法被应用于多标准决策,这在任何研究中都没有进行过。文中还介绍了每种方法的实现步骤。在总共进行的9次实验中,这8种方法中有7种确定了最佳实验。提出了一种新的多准则决策方法,并对今后的研究工作提出了方向。
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引用次数: 27
Comparative investigation of the influence of kaolin and dolomite on the properties of polyurethane foam 高岭土和白云石对聚氨酯泡沫性能影响的对比研究
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/mfreview/2021025
J. Omotoyinbo, I. Oladele, J. M. Jabar, J. Borode, K. Alaneme, A. Akinwekomi, S. R. Oke, T. Omotosho, L. O. Saliu
This work investigates the influence of kaolin and dolomite on the properties of polyurethane foam. The selected fillers were pulverized and sieved to obtained < 90 μm that were used as reinforcements in the polyurethane matrix in a randomly dispersed mode. The matrix constituents were mixed in the same ratio while fillers were introduced via a one-shot system approach in predetermined proportions of 3–7 wt.%. The work was carried out to identify optimum fillers to be utilized in the production of polyurethane rigid foams given the effect of the fillers on the physical, mechanical, and chemical properties of the foam. FTIR, XRF, and SEM and mechanical property tests were carried out on the filled polyurethane foam. The presence of the fillers in the foam showed a rupture in the structure of the foams with the cells having similar arrangements. The addition of dolomite and Kaolin degrades the sulfonic acid groups and promoted the appearance of Si–O stretching vibration band. The density, hardness, flexural and compressive strengths of the polyurethane foam were enhanced with the the addition of dolomite and kaolin particles.
研究了高岭土和白云石对聚氨酯泡沫材料性能的影响。将所选择的填料粉碎、筛分,得到< 90 μm的填料,以随机分散的方式作为聚氨酯基体的增强材料。基体成分以相同的比例混合,而填料以预定比例3 - 7wt .%通过一次性系统方法引入。考虑到填料对泡沫的物理、机械和化学性能的影响,进行了这项工作,以确定用于生产聚氨酯硬质泡沫的最佳填料。对填充后的聚氨酯泡沫进行了FTIR、XRF、SEM和力学性能测试。泡沫中填充物的存在表明泡沫的结构破裂,细胞具有相似的排列。白云石和高岭土的加入降解了磺酸基团,促进了Si-O伸缩振动带的出现。白云石和高岭土颗粒的加入提高了聚氨酯泡沫的密度、硬度、抗折强度和抗压强度。
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引用次数: 2
Hot compression behaviour and microstructural evolution in aluminium based composites: an assessment of the role of reinforcements and deformation parameters 铝基复合材料的热压缩行为和微观结构演变:增强和变形参数作用的评估
IF 2.5 Q2 Engineering Pub Date : 2021-01-01 DOI: 10.1051/MFREVIEW/2021004
S. Babalola, K. Alaneme, S. R. Oke, L. Chown, N. Maledi, M. Bodunrin
The response of two different types of aluminium matrix composites (AMCs) reinforced with silicon carbide ceramic particulates or nickel metallic particulates to hot compression testing parameters was evaluated. The composites were produced via two-step stir-casting technique. Axisymmetric compression testing was performed on the samples at different deformation temperatures of 220 and 370 °Ϲ, 0.5 and 5 s−1 strain rates and total strains of 0.6 and 1.2. The initial and post-deformed microstructures were studied using optical and scanning electron microscopy. The results show that flow stress was significantly influenced by imposed deformation parameters and the type of reinforcements used in the AMCs. Nickel particulate reinforced aluminium matrix composite (AMC) showed superior resistance to deformation in comparison with silicon carbide reinforced AMC under the different testing conditions. In both AMCs, work hardening, dynamic recovery and dynamic recrystallisation influenced their response to imposed parameters. The signature of dynamic recrystallisation was very apparent in aluminium matrix composite reinforced with nickel particulates.
研究了碳化硅陶瓷颗粒增强铝基复合材料和金属镍颗粒增强铝基复合材料对热压缩试验参数的响应。采用两步搅拌铸造工艺制备复合材料。在220°和370°Ϲ、0.5和5 s−1应变速率、0.6和1.2总应变下对试样进行轴对称压缩试验。用光学显微镜和扫描电镜研究了变形前后的微观组织。结果表明,施加的变形参数和增强材料的种类对流变应力有显著影响。在不同的试验条件下,与碳化硅增强铝基复合材料相比,镍颗粒增强铝基复合材料表现出更强的抗变形能力。在这两种amc中,加工硬化、动态恢复和动态再结晶都会影响它们对施加参数的响应。镍颗粒增强铝基复合材料的动态再结晶特征非常明显。
{"title":"Hot compression behaviour and microstructural evolution in aluminium based composites: an assessment of the role of reinforcements and deformation parameters","authors":"S. Babalola, K. Alaneme, S. R. Oke, L. Chown, N. Maledi, M. Bodunrin","doi":"10.1051/MFREVIEW/2021004","DOIUrl":"https://doi.org/10.1051/MFREVIEW/2021004","url":null,"abstract":"The response of two different types of aluminium matrix composites (AMCs) reinforced with silicon carbide ceramic particulates or nickel metallic particulates to hot compression testing parameters was evaluated. The composites were produced via two-step stir-casting technique. Axisymmetric compression testing was performed on the samples at different deformation temperatures of 220 and 370 °Ϲ, 0.5 and 5 s−1 strain rates and total strains of 0.6 and 1.2. The initial and post-deformed microstructures were studied using optical and scanning electron microscopy. The results show that flow stress was significantly influenced by imposed deformation parameters and the type of reinforcements used in the AMCs. Nickel particulate reinforced aluminium matrix composite (AMC) showed superior resistance to deformation in comparison with silicon carbide reinforced AMC under the different testing conditions. In both AMCs, work hardening, dynamic recovery and dynamic recrystallisation influenced their response to imposed parameters. The signature of dynamic recrystallisation was very apparent in aluminium matrix composite reinforced with nickel particulates.","PeriodicalId":51873,"journal":{"name":"Manufacturing Review","volume":null,"pages":null},"PeriodicalIF":2.5,"publicationDate":"2021-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"57964535","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
Experimental and FE study of hybrid laminates aluminium carbon-fibre joints with different lay-up configurations 不同铺层构型混合层合板铝碳纤维接头的试验与有限元研究
IF 2.5 Q2 Engineering Pub Date : 2020-12-01 DOI: 10.1051/mfreview/2019027
R. Carbas, Miguel P. Palmares, L. D. da Silva
The use of composite materials in industry is growing due to various technological advances in composite materials accompanied by improvements in the structural adhesives used to bond them. Fibre metal laminates (FML's) are hybrid composite structures based on thin sheets of metal alloys and plies of fibre-reinforced polymeric materials. The fibre/metal composite technology combines the advantages of metallic materials and fibre-reinforced matrix systems. The aim of the present study is to use a concept similar to that used in FML to increase the peel strength of composite materials and increase the joint strength of hybrid laminates aluminium carbon-fibre adhesive joints. Carbon fibre-reinforced plastic (CFRP) composites were modified by including one or several aluminium sheets during the laminate manufacture to enhance the composite through the thickness properties. The objective was to identify the joint configuration that gives the best joint strength improvement in relation to the CFRP only reference joint. An adhesive developed for the aeronautical industry was used to manufacture single lap joints for tensile testing. Experimental and numerical studies were undertaken on modified CFRP joints to investigate the joint strength of different lay-up solutions to prevent delamination of adherends.
由于复合材料的各种技术进步以及用于粘合它们的结构粘合剂的改进,复合材料在工业中的使用正在增长。纤维-金属层压板(FML)是基于金属合金薄板和纤维增强聚合物材料层的混合复合材料结构。纤维/金属复合材料技术结合了金属材料和纤维增强基体系统的优点。本研究的目的是使用与FML中使用的概念类似的概念来提高复合材料的剥离强度,并提高混合层压板铝碳纤维粘合接头的接头强度。在层压板制造过程中,通过加入一块或几块铝板对碳纤维增强塑料(CFRP)复合材料进行改性,以增强复合材料的厚度性能。目的是确定与仅使用CFRP的参考接头相比,能够提供最佳接头强度改进的接头配置。一种为航空工业开发的粘合剂被用于制造用于拉伸测试的单搭接接头。对改性CFRP接头进行了实验和数值研究,以研究不同铺层方案的接头强度,以防止被粘物分层。
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引用次数: 10
Spot weld bonding − process behavior of three-sheet steel stack‑ups and analysis strategies with online measuring methods 三种叠层钢板点焊工艺行为及在线测量分析策略
IF 2.5 Q2 Engineering Pub Date : 2020-12-01 DOI: 10.1051/mfreview/2019029
S. Brechelt, P. Neef, H. Wiche, V. Wesling
Due to the increased demands for reducing CO2 emissions, improving fuel efficiency of modern vehicles has been continuously monitored. The body of a typical compact car design has a weight share of approx. 40%. In addition to increasing torsional stiffness and crash safety of the body, the aim is also to reduce the overall weight at the same time. In order to achieve these individual requirements, the use of three-sheet steel stack-ups with adhesive applications for car body construction is one of the current strategies used in automobile manufacturing. Adhesive applications lead to a change in process behavior of resistance spot welding. The effective weldability lobe is reduced and an adjusted preheat current is necessary to reconstitute the weldability of a component. Depending on squeeze time and electrode force the adhesive will be displaced. For an asymmetric sheet stack-up, the electrical resistance for every faying surface is highly differentiated. During welding, a specific characteristic of the electrical resistance is created for each individual material combination. These characteristics can be analyzed by using an online measurement device. In this manuscript, different sheet stack-ups are examined with regard to their weldability lobes and their process behavior. The individual three-sheet steel stack-ups used are made of low carbon steel (DX51), HSLA-steel (HX340) and UHS-steel (22MnB5). The corresponding characteristics of electrical resistance will be recorded by using an online measurement device. In addition, the process of adhesive displacement during the squeeze time and the initial welding current are discussed on the basis of the electrical energy generated in the component to be welded. The obtained results contribute to a direct verification of the welding process and an automatic detection of possible imperfect welds.
由于对减少二氧化碳排放的需求不断增加,现代汽车燃油效率的提高一直受到监测。典型紧凑型轿车的车身重量约占40%。除了增加车身的扭转刚度和碰撞安全性外,其目的还在于同时降低整体重量。为了实现这些单独的要求,在车身结构中使用带有粘合剂的三片钢叠层是当前汽车制造中使用的策略之一。粘合剂的应用导致电阻点焊过程行为的改变。有效的可焊性波瓣减少,并且需要调整预热电流来重建部件的可焊接性。根据挤压时间和电极力的不同,粘合剂会发生位移。对于非对称的薄片堆叠,每个接合表面的电阻是高度不同的。在焊接过程中,每个单独的材料组合都会产生特定的电阻特性。这些特性可以通过使用在线测量设备来分析。在这篇手稿中,对不同的叠片进行了可焊性凸起和工艺行为的检查。所使用的单个三片钢叠层由低碳钢(DX51)、HSLA钢(HX340)和UHS钢(22MnB5)制成。电阻的相应特性将通过使用在线测量设备进行记录。此外,基于待焊接部件中产生的电能,讨论了挤压时间内粘合剂位移的过程和初始焊接电流。所获得的结果有助于直接验证焊接过程和自动检测可能的不完美焊缝。
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引用次数: 1
Microstructural aspects of the protective ceramic coatings applied on the surfaces of refractory alloys produced by additive manufacturing 用增材制造法生产的耐火合金表面上的保护性陶瓷涂层的显微结构方面
IF 2.5 Q2 Engineering Pub Date : 2020-09-01 DOI: 10.1051/mfreview/2020031
A. Sobetkii, Laurentiu Mosinoiu, A. Paraschiv, Mircea Corban, R. Piticescu, G. Matache
The possibility of depositing multi layers made of metals/alloys and high temperature ceramics by electron beam physical evaporation process under high vacuum (EB-PVD) on the surface of a parallelepiped sample made by selective laser melting (SLM) from a Ni base refractory super alloy was experimentally tested. The SEM-EDAX micro structural analysis revealed the morphology and thickness of the coatings consisting of a NiCrAlY base alloy as bonding layer and three successive YSZ, LZO and GZO ceramic layers on the Ni-based super alloy substrate obtained by additive manufacturing. The adhesion of the layer deposited was evaluated by the scratch test method. The analysis highlighted the importance of pre-preparing the surface of the additive manufactured substrates, in order to control the adhesion and uniformity of the deposited layers.
实验研究了采用高真空电子束物理蒸发法制备镍基难熔高温合金平行六面体样品表面多层金属/合金和高温陶瓷的可能性。SEM-EDAX显微组织分析揭示了在镍基超级合金基体上由NiCrAlY基合金作为结合层和连续三个YSZ、LZO和GZO陶瓷层组成的涂层的形貌和厚度。采用划痕试验法对镀层的附着力进行了评价。分析强调了预先制备添加剂制造基板表面的重要性,以控制沉积层的附着力和均匀性。
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引用次数: 1
期刊
Manufacturing Review
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