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Residual Stress Measurements in Tensile Armours of Flexible Pipes by the Contour and X-Ray Diffraction Methods 用等高线法和 X 射线衍射法测量柔性管拉伸铠装中的残余应力
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-12 DOI: 10.1007/s11340-024-01045-1
I.L. Diehl, C.A. Theis Soares Diehl, T.R. Schifelbain de Lima, T.G. Rosauro Clarke, M. Torres Piza Paes

Background

Excessive levels of residual stresses (RS) in metallic components of flexible pipes can lead to failure by fatigue or stress-corrosion cracking (SCC) mechanisms. Accurate measurements of residual stresses are essential in order to support comprehensive integrity assessments of these structures.

Objective

This paper aims at proposing a methodology for in-field evaluation of the residual stresses in the tensile armour of flexible pipes. This methodology is evaluated by comparing results from the contour method (CM), a portable (PXRD) and a benchtop (BXRD) X-ray diffractometer.

Methods

A set of samples with a controlled RS state was used to evaluate PXRD depth-profiles by comparison with BXRD measurements. CM was used to investigate stress values elsewhere in the cross-section of the samples. PXRD was then used to measure the total stress on a full-scale flexible riser.

Results

Strong texture was seen in XRD measurements due to the preferential orientation in the samples, but a method to overcome this is proposed. RS measurements with PXRD were in close agreement with BXRD values in all samples. Total stress profiles obtained by PXRD on a tensile armour of flexible pipe are given. CM did not provide reliable results in the near-surface region of shot-peened samples, but reasonable agreement was found with BXRD after manual adjustment of a smoothing parameter when depths from 0.3 mm to 1.5 mm were analyzed.

Conclusion

A methodology has been established for non-destructive in-loco profiling of the total stress state in tensile armours of flexible pipes with PXRD; in a real application scenario it could provide valuable information that could help to understand damage initiation mechanisms.

摘要 背景 柔性管道金属部件中残余应力 (RS) 水平过高会导致疲劳或应力腐蚀开裂 (SCC) 机制失效。为了支持对这些结构进行全面的完整性评估,必须对残余应力进行精确测量。 本文旨在提出一种现场评估柔性管道拉伸铠装残余应力的方法。通过比较等值线法 (CM)、便携式 (PXRD) 和台式 (BXRD) X 射线衍射仪的结果,对该方法进行评估。 方法 使用一组具有受控 RS 状态的样品,通过与 BXRD 测量结果进行比较来评估 PXRD 深度剖面图。CM 用于调查样品横截面其他地方的应力值。然后使用 PXRD 测量全尺寸柔性隔水管的总应力。 结果 由于样品的优先取向,XRD 测量中出现了强烈的纹理,但提出了克服这一问题的方法。用 PXRD 测量的 RS 值与所有样品的 BXRD 值非常接近。给出了通过 PXRD 获得的软管拉伸铠装的总应力曲线。在分析深度为 0.3 毫米至 1.5 毫米的喷丸强化样品时,CM 无法在近表面区域提供可靠的结果,但在手动调整平滑参数后,发现与 BXRD 的结果基本一致。 结论 已经建立了一种利用 PXRD 对柔性管道拉伸铠装中的总应力状态进行非破坏性室内剖面分析的方法;在实际应用场景中,该方法可以提供有价值的信息,有助于了解损坏的引发机制。
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引用次数: 0
Improving Deep Learning-Based Digital Image Correlation with Domain Decomposition Method 用领域分解法改进基于深度学习的数字图像相关性
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-12 DOI: 10.1007/s11340-024-01040-6
Y. Chi, Y. Liu, B. Pan

Background

Deep learning-based digital image correlation (DL-based DIC) has gained increasing attention in the last two years. However, existing DL-based DIC algorithms are impractical because their application scenarios are mostly limited to small deformations.

Objective

To enable the use of DL-based DIC in real-world general experimental mechanics scenarios that would involve large deformations and rotations, we propose to improve DL-based DIC with the domain decomposition method (DDM).

Methods

In the improved method, the region of interest is divided into subimages, and subimages are pre-aligned using the preregistered control points to effectively eliminate the large deformation components. The residual deformations in each subimage are small and limited, which can be well extracted using existing DL-based DIC methods.

Results

Through synthesized and real-world experiments, the improved DL-based DIC method can achieve high-accuracy pixelwise matching in practical applications with strong robustness and high computational efficiency.

Conclusions

The improved DL-based DIC combines the advantages of traditional and DL-based DIC methods but overcomes the limitations, greatly improving the robustness and applicability of existing DL-based methods.

背景基于深度学习的数字图像相关性(DL-based DIC)在过去两年中受到越来越多的关注。为了将基于深度学习的数字图像关联技术应用于涉及大变形和大旋转的真实世界一般力学实验场景,我们建议使用域分解方法(DDM)对基于深度学习的数字图像关联技术进行改进。结果通过综合和实际实验,改进的基于 DL 的 DIC 方法可以在实际应用中实现高精度的像素匹配,具有较强的鲁棒性和较高的计算效率。结论改进的基于 DL 的 DIC 方法结合了传统 DIC 方法和基于 DL 的 DIC 方法的优点,克服了其局限性,大大提高了现有基于 DL 方法的鲁棒性和适用性。
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引用次数: 0
Digital Image Correlation at Extreme Temperatures Using Shortwave Ultraviolet (UV-C) Lights and Filters 使用短波紫外线 (UV-C) 灯和滤光片进行极端温度下的数字图像相关性分析
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-08 DOI: 10.1007/s11340-024-01044-2
P. Dewanjee, M. A. Lea, L. J. Rowley, M. W. Estrada, R. K. Singh, S. Sarker, R. B. Berke

Background

DIC is a widely used optical method that uses cameras to track the motion of an applied random surface pattern to measure the full-field deformation. Due to its non-contacting nature, DIC is very preferable to be used in the areas of high temperature experimental mechanics. One of the biggest challenges of DIC at extreme temperatures is the blackbody radiation emitted from the glowing surface of the specimen. This glow from the blackbody radiation of the specimen is relatively higher at longer wavelengths and lower at shorter wavelengths.    

Objective

Previously, studies have shown the usefulness of using shorter wavelength of lights such as blue filtered light (450 nm) and UV-A filtered light (365 nm) for high temperature measurements. By contrast, this study uses UV-C filtered technique which utilizes even shorter wavelength of filtered light (UV-C, 254 nm) to demonstrate its effectiveness at elevated temperatures.

Methods

Four different DIC techniques using an unfiltered blue light (200–1000 nm), a blue filtered light (450 nm), a UV-A filtered light (365 nm), and a UV-C (254 nm) filtered light have been performed at extreme temperatures in this study. 

Results

It was found that the techniques using unfiltered blue, blue filtered, and UV-A filtered lights could only go up to a temperature of 900 °C, 1200 °C, and 1600 °C respectively before showing significant saturations in the images.

Conclusions

The new UV-C DIC showed no sign of saturation even up to a temperature of 1600 °C while providing comparable axial displacement and coefficient of thermal expansion (CTE) data and therefore demonstrating the usefulness of this method in higher temperatures. We also include helpful recommendations for how to produce speckle patterns having sufficient contrast at UV-C wavelengths.

背景DIC 是一种广泛使用的光学方法,它使用照相机跟踪外加随机表面图案的运动,以测量全场变形。由于其非接触性质,DIC 非常适合用于高温实验力学领域。DIC 在极端温度下面临的最大挑战之一是试样发光表面发出的黑体辐射。这种来自试样黑体辐射的辉光在波长较长时相对较高,而在波长较短时较低。目的以前的研究表明,使用较短波长的光,如蓝色滤波光(450 纳米)和紫外线-A 滤波光(365 纳米)进行高温测量非常有用。方法本研究在极端温度下使用未经过滤的蓝光(200-1000 nm)、蓝光过滤光(450 nm)、UV-A 过滤光(365 nm)和 UV-C 过滤光(254 nm)等四种不同的 DIC 技术。结果发现,使用未经过滤的蓝光、蓝光过滤光和 UV-A 过滤光的技术只能分别达到 900 ℃、1200 ℃ 和 1600 ℃ 的温度,然后才会在图像中显示出明显的饱和。我们还就如何在 UV-C 波长下生成具有足够对比度的斑点图提出了有用的建议。
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引用次数: 0
Biaxial Extension of Cruciform Specimens: Embedding Equilibrium Into Design and Constitutive Characterization 十字形试样的双轴延伸:将平衡嵌入设计和构造表征中
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-08 DOI: 10.1007/s11340-024-01052-2
G. Vitucci

Background

Main desired features of biaxial tests are: uniformity of stresses and strains; high strain levels in gauge areas; reliable constitutive parameters identification. Despite cruciform specimen suitability to modern tensile devices, standard testing techniques are still debated because of difficulties in matching these demands.

Objective

This work aims at providing rational performance objectives and efficient cruciform specimens shapes in view of constitutive characterization.

Methods

Objective performance is evaluated along particular lines lying on principal directions in equibiaxial tensile tests. A rich specimen profile geometry is purposely optimized via finite elements analysis by varying cost function and material compressibility. Experimental tests, monitored via digital image correlation, are carried out for validation.

Results

New shapes are designed and tested in a biaxial tensile apparatus and show to perform better than existing ones. Elastic parameter identification is efficiently performed by only exploiting full field strain measurements along statically significant lines.

Conclusions

Small gauge areas and small fillet radii cruciform specimens approach the ideal deformation behaviour. For the constitutive parameters identification in planar tensile experiments, it suffices to monitor strains along the gauge lines.

背景双轴测试所需的主要特征是:应力和应变的均匀性;量规区域的高应变水平;可靠的构成参数识别。尽管十字形试样适用于现代拉伸设备,但由于难以满足这些要求,标准测试技术仍存在争议。方法在等轴拉伸试验中,沿着主要方向上的特定线评估目标性能。通过有限元分析,改变成本函数和材料可压缩性,有目的地优化了丰富的试样轮廓几何形状。结果设计出了新的形状,并在双轴拉伸设备中进行了测试,结果表明其性能优于现有形状。仅利用沿静态重要线的全场应变测量,就能有效地进行弹性参数识别。结论小测量区域和小圆角半径十字形试样接近理想的变形行为。对于平面拉伸实验中的构成参数识别,只需监测沿量规线的应变即可。
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引用次数: 0
On the Cover: Unique Identification of Stiffness Parameters in Hyperelastic Models for Anisotropic, Deformable, Thin Materials Based on a Single Experiment - A Feasibility Study Based on Virtual Full-Field Data 封面:基于单一实验的各向异性、可变形薄材料超弹性模型中刚度参数的独特识别--基于虚拟全场数据的可行性研究
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-07 DOI: 10.1007/s11340-024-01051-3
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引用次数: 0
An Improved Strain Field Reconstruction Method Based on Digital Twin for Test Monitoring 基于数字孪生的改进型应变场重建方法用于测试监控
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-06 DOI: 10.1007/s11340-024-01035-3
B. Wang, X. Ke, Z. Song, K. Du, X. Bi, P. Hao, C. Zhou

Background

For the static loading test in the aerospace field, conventional strain field reconstruction methods relying on finite element analysis (FEA) or test data are difficult to meet the accuracy requirements of test monitoring.

Objective

This study aims to construct a high-accuracy strain field for real-time test monitoring.

Methods

An improved strain field reconstruction method based on digital twin (DT) named as DT-SFRM is proposed. The DT is built by data fusion of FEA results and test data, which combines the benefits of these data. The FEA conducted before formal test provides approximate strain field distribution, and the strain gauges data with high accuracy are used to modify FEA strain fields in real time. After that, the real-time DT is used to determine the possible risk regions of test articles. Finally, a large opening cylindrical shell (LOCS) buckling test is conducted to validate the advantages of DT-SFRM.

Results

Results show that the accuracy of DT-SFRM is much higher and less affected by the nonlinearity of test data than that of conventional methods. Compared with the time cost by conventional real-time FEA (about 50 min), the DT method only takes 9s to reconstruct strain field, and the possible risk regions predicted by DT-SFRM are more consistent with test buckling regions of LOCS than conventional methods.

Conclusions

The DT-SFRM is validated to have a higher accuracy and better monitoring effect, and it is more suitable for test monitoring of complex structures.

背景对于航空航天领域的静态加载测试,传统的应变场重建方法依赖于有限元分析(FEA)或测试数据,难以满足测试监控的精度要求。方法提出了一种基于数字孪生(DT)的改进应变场重建方法,命名为 DT-SFRM。DT 由有限元分析结果和测试数据融合而成,综合了这些数据的优点。在正式测试前进行的有限元分析可提供近似的应变场分布,而高精度的应变片数据可用于实时修改有限元分析应变场。然后,利用实时 DT 确定试验品可能存在的风险区域。结果结果表明,与传统方法相比,DT-SFRM 的精度更高,受试验数据非线性的影响更小。与传统的实时有限元分析所耗费的时间(约 50 分钟)相比,DT 方法重建应变场仅需 9 秒钟,而且与传统方法相比,DT-SFRM 预测的可能风险区域与 LOCS 试验屈曲区域更为一致。
{"title":"An Improved Strain Field Reconstruction Method Based on Digital Twin for Test Monitoring","authors":"B. Wang,&nbsp;X. Ke,&nbsp;Z. Song,&nbsp;K. Du,&nbsp;X. Bi,&nbsp;P. Hao,&nbsp;C. Zhou","doi":"10.1007/s11340-024-01035-3","DOIUrl":"10.1007/s11340-024-01035-3","url":null,"abstract":"<div><h3>Background</h3><p>For the static loading test in the aerospace field, conventional strain field reconstruction methods relying on finite element analysis (FEA) or test data are difficult to meet the accuracy requirements of test monitoring.</p><h3>Objective</h3><p>This study aims to construct a high-accuracy strain field for real-time test monitoring.</p><h3>Methods</h3><p>An improved strain field reconstruction method based on digital twin (DT) named as DT-SFRM is proposed. The DT is built by data fusion of FEA results and test data, which combines the benefits of these data. The FEA conducted before formal test provides approximate strain field distribution, and the strain gauges data with high accuracy are used to modify FEA strain fields in real time. After that, the real-time DT is used to determine the possible risk regions of test articles. Finally, a large opening cylindrical shell (LOCS) buckling test is conducted to validate the advantages of DT-SFRM.</p><h3>Results</h3><p>Results show that the accuracy of DT-SFRM is much higher and less affected by the nonlinearity of test data than that of conventional methods. Compared with the time cost by conventional real-time FEA (about 50 min), the DT method only takes 9s to reconstruct strain field, and the possible risk regions predicted by DT-SFRM are more consistent with test buckling regions of LOCS than conventional methods.</p><h3>Conclusions</h3><p>The DT-SFRM is validated to have a higher accuracy and better monitoring effect, and it is more suitable for test monitoring of complex structures.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":"64 4","pages":"519 - 537"},"PeriodicalIF":2.0,"publicationDate":"2024-03-06","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140056415","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Near Edge Residual Stress Measurement Using Incremental Hole Drilling 利用增量式钻孔测量近边缘残余应力
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-05 DOI: 10.1007/s11340-024-01041-5
M. D. Olson, A. T. DeWald, B. T. Watanabe

Background

Hole drilling is a measurement technique used to determine near surface residual stresses and has been codified in ASTM E837-20. In ASTM E837-20, the minimum allowable distance to a free edge is prescribed as 1.5 times the gauge circle diameter.

Objective

This work examines the effect arising from the distance from a free edge on a hole drilling measurement and provides an approach to determine residual stress for measurements where the edge distance is closer than that currently permitted by ASTM E837-20.

Methods

Numerical experiments were performed to understand how the compliance matrices change when the distance from a hole drilling measurement to a free edge varies. In addition, a series of hole drilling measurements were performed at various distances from a free edge using a shot peened aluminum plate with a nominally equibiaxial stress state to demonstrate the approach.

Results

The numerical experiments determined that the use of corrected compliance matrices is appropriate when the edge distance is as small as 0.35 times the gauge circle diameter. Physical measurements supported the use of custom compliance matrices for a given free edge distance and specimen thicknesses.

摘要 背景 钻孔是一种用于确定近表面残余应力的测量技术,已编入 ASTM E837-20 标准。在 ASTM E837-20 中,到自由边缘的最小允许距离被规定为测量圆直径的 1.5 倍。 目的 本文研究了自由边缘距离对钻孔测量的影响,并提供了一种方法,用于确定边缘距离比 ASTM E837-20 目前允许的距离更近时的残余应力。 方法 进行了数值实验,以了解当钻孔测量到自由边缘的距离发生变化时,顺应性矩阵如何变化。此外,还使用名义上处于等轴应力状态的喷丸强化铝板,在距自由边缘不同距离处进行了一系列钻孔测量,以演示该方法。 结果 数值实验确定,当边缘距离小到 0.35 倍测量圆直径时,使用校正顺应性矩阵是合适的。物理测量支持在给定自由边缘距离和试样厚度的情况下使用自定义顺应性矩阵。
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引用次数: 0
Stress Evaluation Through the Layers of a Fibre-Metal Hybrid Composite by IHD: An Experimental Study 通过 IHD 评估纤维-金属混合复合材料层间的应力:一项实验研究
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-05 DOI: 10.1007/s11340-024-01047-z
J. P. Nobre, T. C. Smit, R. Reid, Q. Qhola, T. Wu, T. Niendorf

Background

Incremental hole-drilling (IHD) has shown its importance in the measurement of the residual stress distribution within the layers of composite laminates. However, validation of these results is still an open issue, especially near the interfaces between plies.

Objectives

In this context, this study is focused on experimentally verifying its applicability to fibre metal laminates.

Methods

Tensile loads are applied to cross-ply GFRP-steel [0/90/steel]s samples. Due to the difference in the mechanical properties of each ply, Classical Lamination Theory (CLT) predicts a distribution of the uniform stress within each layer, with pulse gradients between them. The interfaces act as discontinuous regions between the plies. The experimental determination of such stress variation is challenging and is the focus of this research. A horizontal tensile test device was designed and built for this purpose. A differential method is used to eliminate the effect of the existing residual stresses in the samples, providing a procedure to evaluate the ability of the IHD technique to determine the distribution of stress due to the applied tensile loads only. The experimentally measured strain-depth relaxation curves are compared with those determined numerically using the finite element method (FEM) to simulate the hole-drilling. Both are used as input for the IHD stress calculation method (unit pulse integral method). The distribution of stress through the composite laminate, determined by classical lamination theory (CLT), is used as a reference.

Results

Unit pulse integral method results, using the experimental and numerical strain-depth relaxation curves, compare reasonably well with those predicted by CLT, provided that there is no material damage due to high applied loads.

Conclusions

IHD seems to be an important measurement technique to determine the distribution of residual stresses in fibre metal laminates and should be further developed for a better assessment of the residual stresses at the interfaces between plies.

摘要 背景 增量式钻孔(IHD)在测量复合材料层压板层内残余应力分布方面具有重要作用。然而,这些结果的验证仍是一个未决问题,尤其是在层间界面附近。 在这种情况下,本研究的重点是通过实验验证其对金属纤维层压板的适用性。 方法 在交叉层 GFRP-钢 [0/90/steel] 样品上施加拉伸载荷。由于各层的机械性能不同,经典层压理论(CLT)预测了各层内部的均匀应力分布,以及各层之间的脉冲梯度。界面是层间的不连续区域。这种应力变化的实验测定具有挑战性,也是本研究的重点。为此,我们设计并制造了一个水平拉伸试验装置。采用差分法消除样品中现有残余应力的影响,提供了一种程序来评估 IHD 技术仅确定外加拉伸载荷引起的应力分布的能力。实验测得的应变-深度松弛曲线与使用有限元法(FEM)模拟钻孔时数值确定的应变-深度松弛曲线进行了比较。两者都被用作 IHD 应力计算方法(单位脉冲积分法)的输入。通过经典层压理论(CLT)确定的复合材料层压板应力分布用作参考。 结果 使用实验和数值应变-深度松弛曲线得出的单位脉冲积分法结果与 CLT 预测的结果比较合理,前提是施加的高载荷不会导致材料损坏。 结论 IHD 似乎是确定金属纤维层压板残余应力分布的一种重要测量技术,应进一步开发,以更好地评估层间界面的残余应力。
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引用次数: 0
Ballistic and Blast-Relevant, High-Rate Material Properties of Physically and Chemically Crosslinked Hydrogels 物理和化学交联水凝胶的弹道和爆炸相关高速材料特性
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-04 DOI: 10.1007/s11340-024-01043-3
E. C. Bremer-Sai, J. Yang, A. McGhee, C. Franck

Background

Hydrogels are one of the most ubiquitous polymeric materials. Among them gelatin, agarose and polyacrylamide-based formulations have been effectively utilized in a variety of biomedical and defense-related applications including ultrasound-based therapies and soft tissue injury investigations stemming from ballistic and blast exposures. Interestingly, while in most cases accurate prediction of the mechanical response of these surrogate gels requires knowledge of the underlying finite deformation, high-strain rate material properties, it is these properties that have remained scarce in the literature.

Objective

Building on our prior works using Inertial Microcavitation Rheometry (IMR), here we present a comprehensive list of the high-strain rate (> 10(^3) 1/s) mechanical properties of these three popular classes of hydrogel materials characterized via laser-based IMR, further showing that the choice in finite-deformation, rate-dependent constitutive model can be informed directly by the type of crosslinking mechanism and resultant network structure of the hydrogel, thus providing a chemophysical basis of the the choice of phenomenological constitutive model.

Methods

We analyze existing experimental gelatin IMR datasets and compare the results with prior data on polyacrylamide.

Results

We show that a Neo-Hookean Kelvin-Voigt (NHKV) model can suitably simulate the high-rate material response of dynamic, physically crosslinked hydrogels like gelatin, while the introduction of a strain-stiffening parameter through the use of the quadratic Kelvin-Voigt (qKV) model was necessary to appropriately model chemically crosslinked hydrogels such as polyacrylamide due to the nature of the static,covalent bonds that comprise their structure.

Conclusions

In this brief we show that knowledge of the type of underlying polymer structure, including its bond mobility, can directly inform the appropriate finite deformation, time-dependent viscoelastic material model for commonly employed tissue surrogate hydrogels undergoing high strain rate loading within the ballistic and blast regimes.

背景水凝胶是最普遍的聚合物材料之一。其中以明胶、琼脂糖和聚丙烯酰胺为基础的配方已被有效地应用于各种生物医学和国防相关领域,包括基于超声波的治疗以及弹道和爆炸引起的软组织损伤研究。有趣的是,在大多数情况下,要准确预测这些代用凝胶的机械响应,需要了解其基本的有限变形、高应变率材料特性,而这些特性在文献中仍然很少见。目标在我们之前使用惯性微空化流变仪(IMR)所做工作的基础上,我们在此列出了通过基于激光的 IMR 表征的这三类常用水凝胶材料的高应变速率(> 10(^3) 1/s)力学性能的综合清单,进一步表明有限变形、速率依赖性构效模型的选择可以直接参考水凝胶的交联机制类型和由此产生的网络结构,从而为现象学构效模型的选择提供化学物理基础。方法我们分析了现有的明胶 IMR 实验数据集,并将结果与之前的聚丙烯酰胺数据进行了比较。结果我们发现,Neo-Hookean Kelvin-Voigt(NHKV)模型可以适当地模拟动态物理交联水凝胶(如明胶)的高速材料响应,而通过使用二次开尔文-Voigt(qKV)模型引入应变加固参数对于适当模拟化学交联水凝胶(如聚丙烯酰胺)是必要的,这是因为构成聚丙烯酰胺结构的静态共价键的性质决定的。结论在本简介中,我们展示了基本聚合物结构类型的知识,包括其键的流动性,可直接为在弹道和爆炸环境中承受高应变率加载的常用组织代用水凝胶提供适当的有限变形、随时间变化的粘弹性材料模型。
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引用次数: 0
Improvement in Calibration Procedure in Nanoindentation: An Indenter Bluntness Indicator 纳米压痕校准程序的改进:压头钝度指示器
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-03-01 DOI: 10.1007/s11340-024-01048-y
D. Chicot, A. Montagne, A. Mejias, F. Roudet, T. Coorevits

Background

Nanoindentation experiments require the calibration of the tip area function, which involves up to 9 fitting coefficients following classical method. These coefficients are determined from indentation tests on a reference material. However, their values may vary from one test batch to another. Consequently, these coefficients cannot describe the amplitude of the indenter tip defect.

Objective

The main objective of this study is to propose a contact area function that uses only one fitting coefficient to represent the indenter tip defect. This coefficient corresponds to the distance between the blunt and ideal indenter tip.

Methodology

To demonstrate the efficiency of the proposed contact area function, we reanalyzed nearly 40 calibration procedures, while keeping the same experimental protocol, performed between 2014 and today. A novel two-step calibration methodology is advanced. We compared the results of the proposed method to those obtained with the classic methodology.

Results

This two-step methodology was applied to a fused silica calibration sample. The values of the Young's modulus and instrumented hardness are equals to 71 and 10 GPa, respectively. The length of the indenter tip defect increases gradually from 5 to 30 nm accordingly to the frequency of use of the indenter. The values of the mechanical properties calculated by this methodology are in good agreement with those obtained using the classical contact area function.

Conclusion

The methodology presented in this paper demonstrates its ability to accurately calibrate the tip area function. This new calibration procedure considers both the Young’s modulus and the tip defect parameter as free parameters. Furthermore, the calibration parameters have a clear physical meaning and their values remain stables from one batch to another.

背景纳米压痕实验需要校准针尖面积函数,按照经典方法,这涉及多达 9 个拟合系数。这些系数是根据参考材料的压痕测试确定的。然而,它们的值可能会因测试批次的不同而不同。本研究的主要目的是提出一种接触面积函数,该函数只使用一个拟合系数来表示压头尖端缺陷。为了证明所提出的接触面积函数的效率,我们重新分析了 2014 年至今进行的近 40 次校准过程,同时保持相同的实验方案。我们提出了一种新颖的两步校准方法。我们将所提方法的结果与经典方法的结果进行了比较。杨氏模量和仪器硬度值分别等于 71 和 10 GPa。随着压头使用频率的增加,压头尖端缺陷的长度从 5 纳米逐渐增加到 30 纳米。本文提出的方法证明了其精确校准顶端面积函数的能力。这种新的校准程序将杨氏模量和针尖缺陷参数都视为自由参数。此外,校准参数具有明确的物理意义,其值在不同批次之间保持稳定。
{"title":"Improvement in Calibration Procedure in Nanoindentation: An Indenter Bluntness Indicator","authors":"D. Chicot,&nbsp;A. Montagne,&nbsp;A. Mejias,&nbsp;F. Roudet,&nbsp;T. Coorevits","doi":"10.1007/s11340-024-01048-y","DOIUrl":"10.1007/s11340-024-01048-y","url":null,"abstract":"<div><h3>Background</h3><p>Nanoindentation experiments require the calibration of the tip area function, which involves up to 9 fitting coefficients following classical method. These coefficients are determined from indentation tests on a reference material. However, their values may vary from one test batch to another. Consequently, these coefficients cannot describe the amplitude of the indenter tip defect.</p><h3>Objective</h3><p>The main objective of this study is to propose a contact area function that uses only one fitting coefficient to represent the indenter tip defect. This coefficient corresponds to the distance between the blunt and ideal indenter tip.</p><h3>Methodology</h3><p>To demonstrate the efficiency of the proposed contact area function, we reanalyzed nearly 40 calibration procedures, while keeping the same experimental protocol, performed between 2014 and today. A novel two-step calibration methodology is advanced. We compared the results of the proposed method to those obtained with the classic methodology.</p><h3>Results</h3><p>This two-step methodology was applied to a fused silica calibration sample. The values of the Young's modulus and instrumented hardness are equals to 71 and 10 GPa, respectively. The length of the indenter tip defect increases gradually from 5 to 30 nm accordingly to the frequency of use of the indenter. The values of the mechanical properties calculated by this methodology are in good agreement with those obtained using the classical contact area function.</p><h3>Conclusion</h3><p>The methodology presented in this paper demonstrates its ability to accurately calibrate the tip area function. This new calibration procedure considers both the Young’s modulus and the tip defect parameter as free parameters. Furthermore, the calibration parameters have a clear physical meaning and their values remain stables from one batch to another.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":"64 4","pages":"467 - 485"},"PeriodicalIF":2.0,"publicationDate":"2024-03-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140018544","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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Experimental Mechanics
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