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Operando Characterizations of Lithium Penetration-Induced Fracture in Solid Electrolytes 固体电解质中锂离子穿透诱发断裂的操作特性分析
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-06-26 DOI: 10.1007/s11340-024-01085-7
M. Lu, S. Xia

Background

Lithium penetration-induced fracture within solid electrolytes (SEs) is a major issue hindering the commercialization of solid-state lithium-ion batteries (SS-LIBs). Such fracture has been frequently observed during electrochemical plating of lithium (Li)-metal anodes, but its mechanistic origin is still largely unclear.

Objective

We present the first quantitative operando analysis of the fracture characteristics of a model SE material under battery-relevant electrochemical cycling conditions.

Methods

Full-field deformation during Li deposition-induced cracking of garnet-type LLZTO was measured using the digital image correlation (DIC) method. The obtained displacement data were denoised via equilibrium smoothing, and then fitted to the linear elastic asymptotic crack-tip field to extract the electrochemical fracture toughness values under different current densities.

Results

The physics-based equilibrium smoothing method demonstrated effectiveness in enhancing the accuracy of DIC measurements. The electrochemical fracture toughness obtained was substantially lower than the mechanical fracture toughness of the same material determined through indentation, attributed to combined effects of electrochemical embrittlement and a transition in fracture mode from intergranular to transgranular.

Conclusion

The discrepancy between the two types of fracture toughness suggests that electrochemical cycling could have a significant impact on the fracture mode and resistance of a solid electrolyte.

背景固态电解质(SE)中锂渗透引起的断裂是阻碍固态锂离子电池(SS-LIB)商业化的一个主要问题。在锂(Li)金属阳极的电化学电镀过程中,经常会观察到这种断裂,但其机理起源在很大程度上仍不清楚。通过平衡平滑法对获得的位移数据进行去噪处理,然后与线性弹性渐近裂纹尖端场进行拟合,以提取不同电流密度下的电化学断裂韧性值。获得的电化学断裂韧性大大低于通过压痕法测定的同种材料的机械断裂韧性,这归因于电化学脆化和断裂模式从晶间过渡到晶间的综合影响。
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引用次数: 0
Effect of Speckle Edge Characteristics on DIC Calculation Error 斑点边缘特性对 DIC 计算误差的影响
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-06-07 DOI: 10.1007/s11340-024-01078-6
H. Cui, Z. Zeng, H. Zhang, F. Yang

Background

In DIC studies, positional parameters and speckle size are commonly used to characterise speckle images. The influence of edge parameters is ignored. This leads to a great difference between the DIC calculation results of simulated and real images. And some contradictory results are also produced.

Objective

The main objective of this paper is to investigate the effect of edge parameters. As well as to give more reasonable parameters to describe the speckle characteristics.

Methods

Firstly, this paper proposes a series of more reasonable parameters to describe the speckle features based on the mathematical expression of the speckle image. Subsequently, the effect of different edge functions on the computational error of DIC is investigated. The effect of different edge functions on pre-filtering is also investigated. Finally, real speckle images are produced using Gaussian and step functions to study the difference between the simulated and real speckle images.

Results

Generally, it is believed that prefiltering can reduce the computational error of DIC, but for Gaussian edges, prefiltering hardly reduces the error, whereas hybrid edges correctly exhibit this phenomenon. Although the Gaussian edge perform well in the simulation, the actual speckle images taken show that the DIC error corresponding to the camera-acquired Gaussian speckle is much larger than that of the step speckle.

Conclusions

The introduction of edge parameters to describe speckle images is necessary for DIC studies. Pre-filtering always reduces the DIC error, but for Gaussian edges this property cannot be demonstrated. The most suitable edges in reality are step edges, not Gaussian edges.

背景在 DIC 研究中,位置参数和斑点大小通常用于描述斑点图像的特征。而边缘参数的影响却被忽略了。这就导致了模拟图像和真实图像的 DIC 计算结果之间存在很大差异,并产生了一些相互矛盾的结果。本文的主要目的是研究边缘参数的影响。方法首先,本文根据斑点图像的数学表达式,提出了一系列更合理的参数来描述斑点特征。随后,研究了不同边缘函数对 DIC 计算误差的影响。还研究了不同边缘函数对预滤波的影响。结果一般认为,预过滤可以减少 DIC 的计算误差,但对于高斯边缘,预过滤几乎不能减少误差,而混合边缘却能正确显示这一现象。虽然高斯边缘在模拟中表现良好,但实际拍摄的斑点图像显示,相机获取的高斯斑点对应的 DIC 误差远远大于阶跃斑点。预滤波总能减少 DIC 误差,但对于高斯边缘,这一特性却无法体现。现实中最合适的边缘是阶梯边缘,而不是高斯边缘。
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引用次数: 0
Stereo-DIC Challenge 1.0 – Rigid Body Motion of a Complex Shape Stereo-DIC Challenge 1.0 - 复杂形状的刚体运动
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-31 DOI: 10.1007/s11340-024-01077-7
W. Ahmad, J. Helm, S. Bossuyt, P. Reu, D. Turner, L.K. Luan, P. Lava, T. Siebert, M. Simonsen

Background

Stereo-DIC is a widely used optical measurement technique that provides a dense full-field 3D measurement of the shape, displacement, and strain of a solid sample. When compared with 2D-DIC, Stereo-DIC provides greater flexibility and expands its use beyond flat, planar specimens. Furthermore, the widespread availability of commercial systems has led to the adoption of the technique throughout industry, academia, and government research labs.

Objective

Even though some research has been done to understand the effects of different experimental and stereo-DIC parameters, no reference is available to benchmark and compare the performance of current stereo-DIC algorithms to each other.

Methods

This paper provides the description and analysis of a carefully controlled 3D experiment and associated images used to compare the results from five subset based DIC software packages. Both the images and analysis codes used in this paper to compare the results are described here and are available for download and use for continued research.

Results

We show that over a very large range of motion, the 3D errors are very small, less than 80(mu)m over a travel of ±20 mm out-of-plane and ±20 mm in-plane. While all codes performed similarly, there are important differences noted in the paper.

Conclusion

The image sets and results comparison software are hosted by the International DIC Society (www.iDICs.org) and are freely available for download and analysis for comparison with results in this paper. Furthermore, it is hoped that this set of images can be used for future research in improving stereo-DIC by future authors.

背景立体-DIC 是一种广泛使用的光学测量技术,可对固体样品的形状、位移和应变进行密集的全场三维测量。与 2D-DIC 相比,立体-DIC 提供了更大的灵活性,并将其应用扩展到平面试样之外。此外,商业系统的普及也促使该技术在工业界、学术界和政府研究实验室得到广泛应用。方法本文描述并分析了一个精心控制的三维实验和相关图像,用于比较基于子集的五个 DIC 软件包的结果。结果我们发现,在很大的运动范围内,三维误差非常小,在平面外±20 毫米和平面内±20 毫米的行程中,误差小于 80 (mu)米。虽然所有代码的性能相似,但本文中指出了一些重要的差异。结论图像集和结果比较软件由国际 DIC 协会 (www.iDICs.org) 托管,可免费下载和分析,以便与本文中的结果进行比较。此外,我们还希望这组图像可用于未来作者改进立体 DIC 的研究。
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引用次数: 0
Optimizing Pure Shear Experiment to Properly Characterize the Shear Properties of Thin-Walled Aluminum Alloy Tubes 优化纯剪切实验,正确表征薄壁铝合金管的剪切特性
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-30 DOI: 10.1007/s11340-024-01080-y
S. Zhang, X. Wang, W. Hu, G. Liu

Background

For an anisotropic thin-walled tube without changing its circular geometry, only the experimental data of initial yield and subsequent plastic deformation along the axial and circumferential directions can be obtained till now. These experimental data are not sufficient to construct an anisotropic constitutive relation for simulations of tube deformation processes.

Objective

A novel shear test of tubular materials is proposed to achieve the state of shearing plastic deformation along the axial direction of thin-walled tubes.

Methods

Two semi-circle mandrels and one specially designed tubular specimen are used in the shear experiment. Optimizations of the specimen shape and mandrel structure were carried out by using FE simulation. The influence of the specimen shape, such as the length of the shear zone and the length of the axial slot, on the stress state of the shear zone was discussed. A thin-walled 5052 aluminum tube was used in the shear experiment using the optimized specimen shape. To understand the corresponding relationship between the tensile properties and the shear properties of an anisotropic tube, the uniaxial tension stress-strain relationship was equivalently transformed to the shear stress-stain relationship using the Mises, Tresca, Hill48, and Barlat-lian constitutive functions.

Results

After optimizing the specimen shape, the shearing condition of the tested tube is closer to the pure shear stress state. Based on the tests, the pure shear stress state can be maintained to a large deformation extent. The experimental shear stress-strain relationship was compared with the converted stress-strain relationship based on the uniaxial tension tests using the Mises, Tresca, Hill48, and Barlat-lian constitutive functions. The results show a large difference between the transformed stress-strain relationship and the shear stress-strain relationship.

Conclusions

This testing method can provide necessary empirical data with the principal stress directions along the direction at an angle of 45° to the tube axis. The shear plastic deformation properties of some anisotropic materials cannot be equivalently described by the experimental data of the tensile test. The shearing characteristics obtained by this novel experimental method can be applied to the characterizations of anisotropic constitutive relations for simulations of tube deformation processes.

背景对于不改变圆形几何形状的各向异性薄壁管材,目前只能获得初始屈服和随后沿轴向和圆周方向塑性变形的实验数据。这些实验数据不足以构建用于模拟管材变形过程的各向异性构成关系。方法在剪切实验中使用了两个半圆心轴和一个特殊设计的管状试样。通过有限元模拟对试样形状和心轴结构进行了优化。讨论了剪切区长度和轴向槽长度等试样形状对剪切区应力状态的影响。在剪切实验中使用了薄壁 5052 铝管,并使用了优化后的试样形状。为了了解各向异性管材的拉伸性能和剪切性能之间的对应关系,使用 Mises、Tresca、Hill48 和 Barlat-lian 构成函数将单轴拉伸应力-应变关系等效转换为剪切应力-应变关系。根据试验结果,纯剪应力状态可以维持到较大的变形程度。使用 Mises、Tresca、Hill48 和 Barlat-lian 构成函数,将实验剪应力-应变关系与基于单轴拉伸试验的换算应力-应变关系进行了比较。结果表明,转换后的应力-应变关系与剪切应力-应变关系之间存在很大差异。结论 这种测试方法可以提供必要的经验数据,即主应力方向沿与管轴线成 45° 角的方向。某些各向异性材料的剪切塑性变形特性无法用拉伸试验的实验数据等效描述。通过这种新型实验方法获得的剪切特性可用于各向异性构成关系的表征,以模拟管材的变形过程。
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引用次数: 0
Cryogenic Fracture Characterisation of High-Grade Pipeline Steels Using the Dynamic Tensile Tear Test Equipped with a Large-Surface Spray Cooling System 利用配备大型表面喷雾冷却系统的动态拉伸撕裂试验对高等级管道钢进行低温断裂表征
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-30 DOI: 10.1007/s11340-024-01082-w
B. Paermentier, S. Cooreman, S. Coppieters, R. Talemi

Background

In contrast to traditional impact-based testing, the Dynamic Tensile Tear Test (DT3) has shown great potential to characterise high-grade pipeline steels as it mimics the in-field pipeline conditions. However, material characterisation using the DT3 method has only been performed at room temperature and lower-shelf characterisation has not yet been investigated.

Objective

This study investigates a solution to perform low-temperature characterisation and analyse dynamic brittle fracture behaviour using the DT3 setup.

Methods

A large-surface spray cooling system using liquid nitrogen was constructed and implemented onto the DT3 system. Cooling performance and temperature uniformity were assessed using thermocouples across a large surface area up to 412 cm2 (2 × 206 cm2). Numerical validation was performed through Finite Element (FE) analysis using the Modified Bai-Wierzbicki (MBW) material model. A combined stress–strain criterion was used to take into account cleavage failure.

Results

Temperatures down to -125 °C were reached using the spray cooling system and a fracture tests was performed at -80 °C. The obtained data and resulting fracture surface indicated clear brittle fracture behaviour. An average crack velocity of 152 m/s was measured, which is in the same order of magnitude associated with crack velocities observed in large-scale testing.

Conclusions

The constructed spray cooling system proved to be capable of cooling a large volume down to cryogenic temperatures while achieving acceptable temperature uniformity. Lower-shelf characterisation of X70 grade pipeline steel was achieved using the DT3 method and a good correlation was obtained between numerical data and experimental observations.

背景与传统的冲击试验相比,动态拉伸撕裂试验(DT3)模拟了现场管道条件,因此在表征高等级管道钢方面显示出巨大的潜力。然而,使用 DT3 方法进行的材料表征仅在室温下进行,尚未对低温表征进行研究。本研究调查了使用 DT3 设置进行低温表征和分析动态脆性断裂行为的解决方案。使用热电偶对高达 412 平方厘米(2 × 206 平方厘米)的大表面区域的冷却性能和温度均匀性进行了评估。通过使用改良 Bai-Wierzbicki (MBW) 材料模型进行有限元 (FE) 分析,进行了数值验证。结果使用喷雾冷却系统将温度降至 -125 °C,并在 -80 °C下进行了断裂测试。获得的数据和断裂面显示了明显的脆性断裂行为。测得的平均裂纹速度为 152 米/秒,与大规模测试中观察到的裂纹速度处于同一数量级。使用 DT3 方法实现了 X70 级管线钢的下层表征,并在数值数据和实验观察之间获得了良好的相关性。
{"title":"Cryogenic Fracture Characterisation of High-Grade Pipeline Steels Using the Dynamic Tensile Tear Test Equipped with a Large-Surface Spray Cooling System","authors":"B. Paermentier,&nbsp;S. Cooreman,&nbsp;S. Coppieters,&nbsp;R. Talemi","doi":"10.1007/s11340-024-01082-w","DOIUrl":"10.1007/s11340-024-01082-w","url":null,"abstract":"<div><h3>Background</h3><p>In contrast to traditional impact-based testing, the Dynamic Tensile Tear Test (DT3) has shown great potential to characterise high-grade pipeline steels as it mimics the in-field pipeline conditions. However, material characterisation using the DT3 method has only been performed at room temperature and lower-shelf characterisation has not yet been investigated.</p><h3>Objective</h3><p>This study investigates a solution to perform low-temperature characterisation and analyse dynamic brittle fracture behaviour using the DT3 setup.</p><h3>Methods</h3><p>A large-surface spray cooling system using liquid nitrogen was constructed and implemented onto the DT3 system. Cooling performance and temperature uniformity were assessed using thermocouples across a large surface area up to 412 cm<sup>2</sup> (2 × 206 cm<sup>2</sup>). Numerical validation was performed through Finite Element (FE) analysis using the Modified Bai-Wierzbicki (MBW) material model. A combined stress–strain criterion was used to take into account cleavage failure.</p><h3>Results</h3><p>Temperatures down to -125 °C were reached using the spray cooling system and a fracture tests was performed at -80 °C. The obtained data and resulting fracture surface indicated clear brittle fracture behaviour. An average crack velocity of 152 m/s was measured, which is in the same order of magnitude associated with crack velocities observed in large-scale testing.</p><h3>Conclusions</h3><p>The constructed spray cooling system proved to be capable of cooling a large volume down to cryogenic temperatures while achieving acceptable temperature uniformity. Lower-shelf characterisation of X70 grade pipeline steel was achieved using the DT3 method and a good correlation was obtained between numerical data and experimental observations.</p></div>","PeriodicalId":552,"journal":{"name":"Experimental Mechanics","volume":"64 7","pages":"1123 - 1142"},"PeriodicalIF":2.0,"publicationDate":"2024-05-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141191317","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
A Deep Learning-Driven Fast Scanning Method for Micro-Computed Tomography Experiments on CMCs 用于 CMC 显微计算机断层扫描实验的深度学习驱动型快速扫描方法
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-24 DOI: 10.1007/s11340-024-01081-x
R.Q. Zhu, G.H. Niu, Z.L. Qu, P.D. Wang, D.N. Fang

Background

In-situ micro-computed tomography (µCT) technology is an attractive approach to investigate the evolution process of damage inside ceramic matrix composites (CMCs) during high-temperature service. The evolution process is highly time-sensitive under temperature-induced loads, and fast scanning is very necessary for in-situ µCT tests.

Objective

The objective of this work is to provide a fast scanning method for in situ µCT tests on CMCs with complex microstructures by the innovation of a reconstruction algorithm.

Method

To overcome the severe degradation of the reconstructed image quality resulting from sparse CT scans, a deep-learning-based multi-domain sparse reconstruction method was proposed. Three sub-networks including the projection-domain, image-domain, and fusion network were constructed in the multi-domain method to make full use of the information from the projection and image domain.

Results

The proposed deep-learning-based sparse reconstruction method provided satisfactory µCT images on C/SiC composites with acceptable quality. The scanning time was reduced by 6 times. All selected evaluation metrics of the proposed method are higher than those of other single-domain methods and traditional iterative method. The segmentation accuracy of the µCT images obtained by the proposed method can meet the subsequent quantitative analysis. An in-situ tensile test of CMCs is conducted to further evaluate the performance in the practical application of in-situ experiments. The results indicate that the weak and thin micro-cracks can still be effectively retained and recovered. A detailed workflow to implement the method generally is also provided.

Conclusions

Based on the deep-learning-based multi-domain sparse reconstruction method, the process of in-situ µCT tests can be greatly accelerated with little loss of the reconstructed image quality.

背景原位微计算机断层扫描(µCT)技术是研究高温服役期间陶瓷基复合材料(CMC)内部损伤演变过程的一种极具吸引力的方法。为了克服稀疏 CT 扫描导致的重建图像质量严重下降的问题,提出了一种基于深度学习的多域稀疏重建方法。结果基于深度学习的稀疏重建方法为 C/SiC 复合材料提供了令人满意的 µCT 图像,图像质量可以接受。扫描时间缩短了 6 倍。与其他单域方法和传统迭代法相比,所提方法的所有选定评价指标都更高。该方法获得的 µCT 图像的分割精度可以满足后续定量分析的需要。对 CMC 进行了原位拉伸试验,以进一步评估其在原位实验实际应用中的性能。结果表明,薄弱的微裂纹仍能有效保留和恢复。结论基于深度学习的多域稀疏重建方法可以大大加快原位 µCT 试验的进程,而重建图像的质量几乎没有损失。
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引用次数: 0
Characterization on Fracture Toughness of Cermet Coating Coupling Instrumented Indentation and X‑Ray Computed Tomography 将仪器压痕法和 X 射线计算机断层扫描法相结合,表征金属陶瓷涂层的断裂韧性
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-23 DOI: 10.1007/s11340-024-01075-9
R. Huang, Y. Zheng, S. Luo, H. Bai, P. Wang, Y. Chen, Z. Qu

Background

The surface brittle fracture of cermet coating seriously restricts its application. Accurate evaluation of the fracture toughness of cermet coating is a prerequisite for improving its life.

Objective

This paper aims to propose an accurate characterization method for fracture toughness of cermet coating.

Methods

By coupling instrumented indentation and X‑ray computed tomography (XCT), the indentation-induced fracture behaviors under various loads within WC-12%Co coatings were studied. The three-dimensional subsurface crack morphologies and the damage evolution within the coating were nondestructively observed by XCT. The indentation response was correlated with the damage evolution. The impact of substrate effects on indentation-induced fracture behaviors was further studied using finite element analysis (FEA).

Results

The Palmqvist shape of the indentation crack under low loads was successfully identified. The first pop-in event in the load-displacement (P-h) curve was determined to be triggered by bottom cracking, marking the onset of the multiple fracture mode. Laugier’s equation offered a stable and reliable estimation of fracture toughness for the coating in the radial cracking mode.

Conclusions

XCT plays a crucial role in selecting the appropriate equation for indentation toughness calculation. The critical indentation depth for the first pop-in was suggested as the threshold for reliably extracting intrinsic fracture toughness of cermet coatings. Numerical results revealed a constant linear relationship between the critical depth and coating thickness, and a high sensitivity of the critical depth to yield stress of the substrate. The proposed analytical procedure holds potential for generalization to diverse cermet coatings on metal substrates.

背景金属陶瓷涂层的表面脆性断裂严重限制了其应用。本文旨在提出一种精确表征金属陶瓷涂层断裂韧性的方法。方法通过仪器压痕法和 X 射线计算机断层扫描(XCT),研究了 WC-12%Co 涂层在各种载荷下的压痕诱导断裂行为。XCT 对涂层内的三维次表层裂纹形态和损伤演变进行了非破坏性观察。压痕响应与损伤演变相关。利用有限元分析 (FEA) 进一步研究了基底效应对压痕诱导断裂行为的影响。载荷-位移(P-h)曲线中的第一个弹入事件被确定为由底部开裂引发,标志着多重断裂模式的开始。结论 XCT 在选择适当的压痕韧性计算公式方面起着至关重要的作用。建议将首次弹入的临界压痕深度作为可靠提取金属陶瓷涂层内在断裂韧性的临界值。数值结果表明,临界深度与涂层厚度之间存在恒定的线性关系,临界深度对基体屈服应力的敏感性很高。所提出的分析程序有望推广到金属基底上的各种金属陶瓷涂层。
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引用次数: 0
An Experimental Method for Stereo-DIC Measurement of Large-Scale Thin-Film Structures 大尺度薄膜结构的立体 DIC 测量实验方法
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-21 DOI: 10.1007/s11340-024-01079-5
K. Wei, G. Wei, X.X. Shao, D.P. Jin, X.Y. He

Background

Due to their flexible configuration and lightweight characteristics, film structures have gained significant attention in the field of aerospace engineering. The scales of film structures typically range from several meters to over ten meters. Stereo-digital image correlation (stereo-DIC) methods offer distinct advantages for obtaining full-field measurement results. However, challenges persist in fabricating high-quality speckle patterns and addressing the problem of imaging reflections, particularly for large-scale transparent or semi-transparent film structures.

Objective

This paper presents an experimental measurement method for large-scale, transparent thin-film structures. The method focuses on fabricating high-quality digital speckle patterns without altering the vibration characteristics of thin film, as well as addressing the problem of imaging reflections.

Methods

A combined large-scale backlighting system and transmission imaging are introduced to solve the problem of reflections. To avoid altering the characteristics of the thin film, a single-particle transfer printing technique is developed. A large umbrella thin-film structure with a diameter of 6 meters is selected to validate the effectiveness of the proposed method. The structure is composed of multiple steel trusses and fan-shaped films.

Results

With high-quality speckle patterns and solving the problem of reflections, the full-field displacement results of the umbrella thin-film structure are measured. The first-order and second-order natural frequencies along with corresponding mode shapes are further obtained.

Conclusion

The effectiveness of the experimental method is demonstrated through rotational and vibration tests conducted on the large umbrella thin-film structure. This method provides a powerful means for studying the mechanical behavior and vibration characteristics of large-scale thin-film structures.

背景由于其灵活的构造和轻质的特点,薄膜结构在航空航天工程领域备受关注。薄膜结构的尺度通常从几米到十几米不等。立体数字图像相关(stereo-DIC)方法在获得全场测量结果方面具有明显优势。然而,在制作高质量斑点图案和解决成像反射问题方面仍然存在挑战,尤其是在大型透明或半透明薄膜结构方面。该方法的重点是在不改变薄膜振动特性的情况下制作高质量的数字斑点图,并解决成像反射问题。方法采用大型背光系统和透射成像相结合的方法来解决反射问题。为了避免改变薄膜的特性,开发了一种单颗粒转移印刷技术。选择了一个直径为 6 米的大型伞状薄膜结构来验证所提方法的有效性。结果利用高质量斑点模式并解决反射问题,测量了伞状薄膜结构的全场位移结果。结论通过对大型伞状薄膜结构进行旋转和振动测试,证明了该实验方法的有效性。该方法为研究大型薄膜结构的机械行为和振动特性提供了有力的手段。
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引用次数: 0
Experimental Examination of Additively Manufactured Patterns on Structural Nuclear Materials for Digital Image Correlation Strain Measurements 用于数字图像相关应变测量的核结构材料上添加式制造图案的实验检验
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-20 DOI: 10.1007/s11340-024-01076-8
K.A. Novich, T.L. Phero, S.E. Cole, C.M. Greseth, M.D. McMurtrey, D. Estrada, B.J. Jaques

Background

There are a limited number of commercially available sensors for monitoring the deformation of materials in-situ during harsh environment applications, such as those found in the nuclear and aerospace industries. Such sensing devices, including weldable strain gauges, extensometers, and linear variable differential transformers, can be destructive to material surfaces being investigated and typically require relatively large surface areas to attach (> 10 mm in length). Digital image correlation (DIC) is a viable, non-contact alternative to in-situ strain deformation. However, it often requires implementing artificial patterns using splattering techniques, which are difficult to reproduce.

Objective

Additive manufacturing capabilities offer consistent patterns using programmable fabrication methods.

Methods

In this work, a variety of small-scale periodic patterns with different geometries were printed directly on structural nuclear materials (i.e., stainless steel and aluminum tensile specimens) using an aerosol jet printer (AJP). Unlike other additive manufacturing techniques, AJP offers the advantage of materials selection. DIC was used to track and correlate strain to alternative measurement methods during cyclic loading, and tensile tests (up to 1100 µɛ) at room temperature.

Results

The results confirmed AJP has better control of pattern parameters for small fields of view and facilitate the ability of DIC algorithms to adequately process patterns with periodicity. More specifically, the printed 100 μm spaced dot and 150 μm spaced line patterns provided accurate measurements with a maximum error of less than 2% and 4% on aluminum samples when compared to an extensometer and commercially available strain gauges.

Conclusion

Our results highlight a new pattern fabrication technique that is form factor friendly for digital image correlation in nuclear applications.

背景在恶劣环境应用(如核工业和航空航天工业)中,用于现场监测材料变形的商用传感器数量有限。此类传感设备,包括可焊接应变计、拉伸计和线性可变差分变压器,可能会对被测材料表面造成破坏,而且通常需要相对较大的表面积才能安装(长度为 10 毫米)。数字图像相关(DIC)是原位应变变形的一种可行的非接触式替代方法。方法在这项工作中,使用气溶胶喷射打印机(AJP)在核结构材料(即不锈钢和铝拉伸试样)上直接打印了各种具有不同几何形状的小尺寸周期性图案。与其他增材制造技术不同,AJP 具有材料选择的优势。在室温下进行循环加载和拉伸试验(最大 1100 µɛ)时,使用 DIC 跟踪应变并将其与其他测量方法相关联。结果结果证实 AJP 能够更好地控制小视场的图案参数,并促进 DIC 算法充分处理具有周期性的图案的能力。更具体地说,与拉伸计和市场上销售的应变计相比,打印出的 100 μm 间距点和 150 μm 间距线图案提供了精确的测量,对铝样品的最大误差分别小于 2% 和 4%。
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引用次数: 0
Experiments on Low–Cycle Ductile Damage and Failure Under Biaxial Loading Conditions 双轴加载条件下的低循环韧性损伤和破坏实验
IF 2 3区 工程技术 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2024-05-20 DOI: 10.1007/s11340-024-01074-w
S. Gerke, Z. Wei, M. Brünig

Background

The damage and failure behavior of ductile metals depends on the stress state as well as on the loading history. Biaxial experiments with suitable specimens can be used to targeted generate different loading conditions, thus allowing the investigation of a wide variety of load cycles with different stress states.

Objective

In the biaxial experiments with the newly presented HC-specimen cyclic shear loads are superimposed by various constant compressive and tensile loads. Buckling during compressive loading in both axes is avoided by an additional newly introduced downholder.

Methods

The strain fields at the surfaces of the biaxial specimens are evaluated by digital image correlation (DIC), and after failure the corresponding fracture surfaces are analyzed by scanning electron microscopy (SEM). Associated numerical simulations employing the presented material model provide information on the current stress states.

Results

The introduced downholder successfully prevents buckling during compressive loading. The strain fields detect a clear influence of the shear direction and a tensile superposition of the cyclic shear load leads to more brittle and a compressive superposition to more ductile behavior. The accompanying numerical calculations reveal the associated, different stress states.

Conclusions

The new experimental program with biaxially loaded specimens for the investigation of damage and failure behavior under cyclic loading enables the targeted examination of a wide variety of load cycles and is thus suitable for the comprehensive analysis of these phenomena.

背景韧性金属的破坏和失效行为取决于应力状态和加载历史。使用合适的试样进行双轴实验可以有针对性地生成不同的加载条件,从而可以研究具有不同应力状态的各种加载循环。方法通过数字图像相关技术(DIC)评估双轴试样表面的应变场,并通过扫描电子显微镜(SEM)分析失效后的相应断裂面。采用所介绍的材料模型进行的相关数值模拟提供了有关当前应力状态的信息。应变场检测到剪切方向的明显影响,循环剪切载荷的拉伸叠加导致脆性增加,而压缩叠加导致韧性增加。伴随的数值计算揭示了相关的不同应力状态。结论使用双轴加载试样研究循环加载下的破坏和失效行为的新实验程序能够有针对性地检查各种加载循环,因此适合对这些现象进行全面分析。
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引用次数: 0
期刊
Experimental Mechanics
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