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Investigating Temperature-Dependent Mechanical Properties of PLA in FDM: Experimental and Simulation Approaches FDM中PLA的温度相关力学性能研究:实验和仿真方法
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-25 DOI: 10.1007/s11665-025-11754-w
Farbod Bijari, Nahal Barzegar Bagheri

Fused Deposition Modeling (FDM) is a common additive manufacturing method used to produce intricate three-dimensional structures from thermoplastics. Its affordability and adaptability have contributed to its widespread use in fields such as medicine, electronics, and aerospace. This research focused on analyzing the mechanical properties of PLA (Polylactic Acid) samples produced via FDM. Since polymers display viscoelastic behavior above their glass transition temperature, this effect was disregarded due to the complexity of computations. Instead, key material properties, including Young’s modulus, thermal expansion, and conductivity, were considered temperature-dependent. To support the simulations, Differential Scanning Calorimetry (DSC) and Thermomechanical Analysis (TMA) were conducted to determine the PLA’s glass transition temperature and thermal expansion coefficients. Tensile tests were carried out at four different temperatures (25, 55, 85, and 115 °C), with results compared to finite element simulations in Abaqus. The findings showed that at 25 °C, PLA samples were rigid and glassy, but as they approached the glass transition temperature, they became softer and more rubber-like, leading to a significant reduction in tensile strength. The highest tensile strength was observed in the horizontally printed sample (H1) at 25 °C (31.66 MPa), while the lowest tensile strength was recorded in the vertically printed sample (V1) at 115 °C (3.41 MPa). All samples were fabricated using 100% infill density to ensure structural integrity and accurate comparison. The greatest elongation was measured at 55 °C. Experimental stress–strain curves closely matched simulation results, with an error margin of less than 5%. An analysis of distortion revealed that vertically printed samples deformed more due to layer accumulation, weaker interlayer adhesion, and extended cooling times. In contrast, horizontally printed samples experienced minimal distortion, benefiting from stronger platform contact and a lower number of layers.

熔融沉积建模(FDM)是一种常用的增材制造方法,用于从热塑性塑料中生产复杂的三维结构。它的可负担性和适应性使其在医学、电子和航空航天等领域得到广泛应用。本研究重点分析了FDM法制备的聚乳酸(PLA)样品的力学性能。由于聚合物在其玻璃化转变温度以上表现出粘弹性行为,由于计算的复杂性,这种影响被忽略。相反,关键的材料特性,包括杨氏模量、热膨胀和导电性,被认为是温度相关的。为了支持模拟,采用差示扫描量热法(DSC)和热力学分析(TMA)测定PLA的玻璃化转变温度和热膨胀系数。在四种不同温度(25、55、85和115°C)下进行拉伸试验,并将结果与Abaqus中的有限元模拟结果进行比较。研究结果表明,在25°C时,PLA样品是刚性和玻璃状的,但当它们接近玻璃化转变温度时,它们变得更软,更像橡胶,导致抗拉强度显著降低。水平印刷样品(H1)在25°C (31.66 MPa)时抗拉强度最高,垂直印刷样品(V1)在115°C (3.41 MPa)时抗拉强度最低。所有样品均采用100%填充密度制作,以确保结构完整性和准确比较。在55℃时测得最大伸长率。实验应力-应变曲线与仿真结果吻合较好,误差小于5%。变形分析表明,垂直印刷的样品由于层堆积、层间粘附较弱和冷却时间延长而变形更多。相比之下,水平印刷样品经历最小的扭曲,受益于更强的平台接触和更少的层数。
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引用次数: 0
Performance of Ceramic/Ultra-high Molecular Weight Polyethylene Composite Body Armor Panel Against Multiple Hardened Steel Core Projectile Impacts 陶瓷/超高分子量聚乙烯复合防弹衣面板抗多次硬化钢芯弹丸冲击的性能
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-25 DOI: 10.1007/s11665-025-11724-2
Ankush Thakur, Mohit Gupta, Nitin Thakur, Puneet Mahajan

Ballistic standards require body armor to withstand multiple projectiles without getting penetrated. The response of a ceramic/composite armor, in terms of its back face signature (BFS) when eight hardened steel cores (HSC) at 715 m/s are fired on it, is studied numerically using finite element (FE) method. The armor consists of ceramic, hard and soft ultra-high molecular weight polyethylene (UHMWPE) layers and foam. The FE model of the projectile and armor was developed in LS-Dyna and different material models were employed to constitute their behaviors. Initially, the influence of contact conditions between ceramic tiles forming the strike face of the armor panel was studied in terms of damage propagation in adjacent tiles. Further, the deformation of the various layers and penetration of ceramic tiles and hard UHMWPE along with the reduction in length of projectiles were investigated. The developed FE model was validated by comparing the average BFS and bullet length reduction values against experimental data. It was found that although significant bullet impact energy was absorbed in damaging ceramic tiles, it still influenced the displacement response of hard armor panel (HAP) layers. The delamination lengths between composite layers are also discussed. The presented modeling techniques and developed FE model may help in improving the design of bulletproof armor panels capable of withstanding multiple bullet impacts.

弹道标准要求防弹衣能承受多重射弹而不被击穿。采用有限元法研究了8个淬硬钢芯(HSC)以715 m/s的速度对陶瓷/复合装甲的后表面特征(BFS)响应。装甲由陶瓷、硬、软超高分子量聚乙烯(UHMWPE)层和泡沫组成。在LS-Dyna中建立了弹丸和装甲的有限元模型,采用不同的材料模型来构成弹丸和装甲的行为。首先,从损伤在相邻瓷砖间传播的角度,研究了形成装甲面板打击面的瓷砖之间接触条件的影响。此外,还研究了随着弹丸长度的减小,瓷砖和硬质超高分子量聚乙烯的各层变形和侵彻情况。通过将平均BFS和子弹长度压缩值与实验数据进行比较,验证了所建立的有限元模型。研究发现,尽管子弹冲击能在陶瓷损伤中被大量吸收,但仍会影响硬装甲板层的位移响应。本文还讨论了复合材料层间的分层长度。所提出的建模技术和所建立的有限元模型可为改进耐多弹冲击防弹装甲板的设计提供参考。
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引用次数: 0
Microstructure Evaluation and Mechanical Properties of 3D-Printed Maraging Steel-300 Samples: Joined by GTAW Process 3d打印马氏体时效钢-300试样的组织评价与力学性能:GTAW工艺
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-25 DOI: 10.1007/s11665-025-11818-x
Manoj Kumar, Santosh Kumar, Pankaj Kumar Singh, Bipin Kumar Srivastava

Maraging steel is extensively utilized in industrial applications owing to its superior mechanical properties, including high strength, toughness, and dimensional stability. This study evaluates the feasibility of gas tungsten arc welding (GTAW) for repairing maraging steel components fabricated via laser-powder bed fusion (L-PBF). Specimens (100 × 50 × 2 mm) were produced in three build orientations (0°, 45°, and 90°) using maraging steel powder, followed by solution treatment and age hardening. Autogenous GTAW was employed to join both additively manufactured (AM) and conventionally processed samples. Microstructural and mechanical properties of the weldments were analyzed through optical and scanning electron microscopy, microhardness, and tensile testing. Results indicate orientation-dependent hardness in AM samples: 45° samples exhibited 16% lower, while 90° samples showed 4% higher hardness compared to conventional counterparts. Additionally, the ultimate tensile strength of 90° AM samples was 5% higher than that of conventional weldments. The findings demonstrate the potential of GTAW as a cost-effective repair strategy for L-PBF-fabricated maraging steel (grade 300) components.

马氏体时效钢由于其优异的机械性能,包括高强度、高韧性和尺寸稳定性,在工业应用中得到了广泛的应用。研究了钨极气体保护焊(GTAW)修复激光-粉末床熔合(L-PBF)制备的马氏体时效钢构件的可行性。采用马氏体时效钢粉在0°、45°和90°三个构建方向制作100 × 50 × 2mm的试样,然后进行固溶处理和时效硬化。采用自生GTAW连接增材制造(AM)和常规加工样品。通过光学显微镜、扫描电镜、显微硬度和拉伸试验分析了焊接件的组织和力学性能。结果表明,AM样品的硬度与取向有关:与常规样品相比,45°样品的硬度降低16%,而90°样品的硬度提高4%。此外,90°AM试样的极限抗拉强度比常规焊缝高5%。研究结果表明,对于l - pbf制造的马氏体时效钢(300级)部件,GTAW是一种具有成本效益的修复策略。
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引用次数: 0
Effect of Surfactants and Hybrid Filler on Microstructural and Mechanical Properties of Al7075/TiC/Graphene Alloy Composite via Additive Manufacturing 表面活性剂和杂化填料对增材制造Al7075/TiC/石墨烯合金复合材料显微组织和力学性能的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-25 DOI: 10.1007/s11665-025-11873-4
M. Anandh Babu, R. Mohan, R. Latha, P. Prabhu, R. Venkatesh, S. Prabagaran, Vinayagam Mohanavel, Manzoore Elahi M. Soudagar, A. H. Seikh

The aluminum alloy composite processed with additive manufacturing technology (laser powder bed melting—LPBM) has better microstructural and mechanical properties and is familiar with making design freedom geometry. However, the combinations of composite powder found agglomeration, porosity due to high laser energy, and micro hot cracks, leading to a reduction in the functional properties of the composite. This research intends to overcome the above challenges and enrich the microstructural and mechanical properties of aluminum alloy (Al7075) powder blended with 0.5 wt.% graphene and 2.5-7.5 wt.% of titanium carbide (TiC) nanoparticles via a high-energy ball milling process, associated with 1% polyvinyl alcohol surfactants prevents the agglomeration. With the support of the laser powder bed melting process (LPBM), the Al7075/graphene/TiC composite is prepared with a 70 µm hatching distance with 60% overlap under argon build atmosphere, which helps to reduce the oxide formation. The LPBM-developed samples are involved in the aging process to limit the residual stress, which assists in determining the hot cracks. Effects of LPBM processing and filler on microstructural, physical, and mechanical properties are studied. The transmission electron microscope (TEM) analyzed image shows homogenous particle dispersion with improved interfacial bonding strength, with a grain size from 6 to 18 µm. The LPBM processed Al7075/1 wt.% graphene/7.5 wt.% TiC sample is 0.47% of porosity, optimum tensile strength (598 MPa), reduced elongation (7.2%), optimum impact strength (15.3 J/mm2), and improved microhardness of 228HV, respectively.

采用增材制造技术(激光粉末床熔化- lpbm)加工的铝合金复合材料具有较好的显微组织和力学性能,且易于制作设计自由几何形状。然而,复合粉末的组合存在结块、高激光能量导致的孔隙和微热裂纹,导致复合材料的功能性能降低。本研究旨在克服上述挑战,通过高能球磨工艺,将0.5 wt.%的石墨烯和2.5-7.5 wt.%的碳化钛(TiC)纳米颗粒混合在铝合金(Al7075)粉末中,并添加1%的聚乙烯醇表面活性剂防止团聚,从而丰富其显微组织和力学性能。在激光粉末床熔融工艺(LPBM)的支持下,在氩气气氛下制备了Al7075/石墨烯/TiC复合材料,其孵化距离为70 μ m,重叠度为60%,有助于减少氧化物的形成。lpbm开发的样品参与时效过程,以限制残余应力,这有助于确定热裂纹。研究了LPBM加工工艺和填料对材料显微组织、物理性能和力学性能的影响。透射电子显微镜(TEM)分析图像显示,颗粒分散均匀,界面结合强度提高,粒径在6 ~ 18µm之间。LPBM处理的Al7075/1 wt.%石墨烯/7.5 wt.% TiC样品孔隙率为0.47%,抗拉强度为598 MPa,伸长率为7.2%,冲击强度为15.3 J/mm2,显微硬度为228HV。
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引用次数: 0
Microstructure, Mechanical Properties and Degradation Behavior of Extruded Mg-Y-Cu (Ni) Alloys for Fracturing Degradation Tools 挤压Mg-Y-Cu (Ni)合金的显微组织、力学性能及降解行为
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-25 DOI: 10.1007/s11665-025-11841-y
Wenjuan Tan, Jing Jiang, Guangli Bi, Yuandong Li, Tijun Chen

The microstructure, mechanical properties and degradation behavior of the extruded Mg-2Y-1Cu (MYC, at.%) and Mg-2Y-0.5Cu-0.5Ni (MYCN, at.%) alloys were investigated in this study. The experimental results revealed that the addition of Ni effectively refined the grain size and modified the distribution and precipitation behavior of second phase in the extruded MYC alloy. The volume fraction of the long-period stacking ordered (LPSO) phases increased from 26.8% in the extruded MYC alloy to 39.9% in the extruded MYCN alloy. Tensile testing results indicated that the Ni addition enhanced the compressive strength from 332 MPa for the extruded MYC alloy to 351 MPa for the extruded MYCN alloy. Moreover, the immersion experiments and electrochemical tests indicated that the addition of Ni significantly increased the degradation rate, hydrogen evolution and weight loss rate of the extruded MYC alloy. The hydrogen evolution rate and weight loss rate of the extruded MYCN alloy were 21.985 ml/cm2·h and 23 mg/cm2·h, increased by 174% and 170% compared to those of the extruded MYC alloy, respectively. The enhanced degradation rate of the extruded MYCN alloy was mainly due to the significant galvanic corrosion between second phase and α-Mg matrix. Additionally, the high compressive strengths of the extruded MYCN alloy were mainly attributed to grain refinement and second phase strengthening resulting from LPSO phase.

研究了挤压Mg-2Y-1Cu (MYC)的显微组织、力学性能和降解行为。%)和Mg-2Y-0.5Cu-0.5Ni (MYCN, at。本研究对%)合金进行了研究。实验结果表明,Ni的加入有效地细化了MYC合金的晶粒尺寸,改变了第二相的分布和析出行为。长周期有序堆积相(LPSO)的体积分数从挤压MYC合金的26.8%增加到挤压MYCN合金的39.9%。拉伸试验结果表明,Ni的加入使挤压态MYC合金的抗压强度由332 MPa提高到351 MPa。此外,浸渍实验和电化学测试表明,Ni的加入显著提高了挤压MYC合金的降解速率、析氢速率和失重速率。挤压后的MYCN合金的析氢率和失重率分别为21.985 ml/cm2·h和23 mg/cm2·h,分别比挤压后的MYC合金提高了174%和170%。挤压后的MYCN合金降解速率的提高主要是由于第二相与α-Mg基体之间存在明显的电偶腐蚀。拉伸后的MYCN合金具有较高的抗压强度,主要是由于LPSO相产生的晶粒细化和第二相强化。
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引用次数: 0
Investigating the Effects of Plasma-Sintered WC-17Co Morphology and Content Changes on the Properties of Laser-Melted Fe-Based Coatings 等离子体烧结WC-17Co形貌及含量变化对激光熔铁基涂层性能影响的研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-22 DOI: 10.1007/s11665-025-11890-3
Meng Ying, Ming Yu Lu, Yun Li, Yong Ming Shao, Yan Sun

In order to investigate the influence of the shape of the powder raw material on the coating properties, this paper investigates the plasma-sintered WC particles added to Fe-based powder to prepare coatings, and characterization methods such as coating microstructure, microhardness, and friction and wear are examined. The results show that with the increase of the mass fraction of added WC-17Co, the physical phases of the coatings appeared Fe3W3C3 and Co3W3C3, and at the same time, the microstructure of the coatings had a dense and homogeneous grain structure without obvious defects, and irregular aggregation of WC particles was clearly observed, and fine WC precipitates dispersed in the coatings were also observed. The hardness of the coating increases with the increase of WC-17Co content, and the spherical shape of the powder has a better improvement effect. With the addition of 30% WC-17Co, the hardness of the coating reaches 800HV0.2, which is 60% higher than that of the unadded coating. Spherical WC particles with 30% addition showed a more significant improvement, with a wear rate of 10-8, which was significantly better than that of non-spherical particles. Spherical particles have a smoother particle surface, which facilitates inter-particle movement and provides better spatial accumulation of powders, and at the same volume, the WC content of the spherical form of the powder is higher.

为了研究粉末原料形状对涂层性能的影响,本文研究了将等离子烧结WC颗粒添加到铁基粉末中制备涂层,并对涂层微观结构、显微硬度、摩擦磨损等表征方法进行了研究。结果表明:随着WC- 17co质量分数的增加,涂层的物相出现Fe3W3C3和Co3W3C3,同时涂层的显微组织具有致密均匀的晶粒结构,无明显缺陷,WC颗粒不规则聚集明显,并有细小的WC析出物分散在涂层中。涂层硬度随WC-17Co含量的增加而增加,粉末呈球形有较好的改善效果。WC-17Co添加量为30%时,涂层硬度达到800HV0.2,比未添加涂层硬度提高60%。添加30%的球形WC颗粒改善效果更为显著,磨损率为10-8,明显优于非球形WC颗粒。球形颗粒颗粒表面光滑,有利于颗粒间的运动,粉末的空间堆积更好,在相同体积下,球形粉末的WC含量更高。
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引用次数: 0
Enhanced Mechanostructure, Corrosion, and Tribological Properties of Incoloy-925 by Warm-Rolling Process 热轧工艺对incoly -925的力学组织、腐蚀和摩擦学性能的改善
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-22 DOI: 10.1007/s11665-025-11835-w
Seda Bayram, Sinan Sezek, Bünyamin Aksakal

In this study, the effects of warm rolling at 520 °C on the microstructure, mechanical, tribological, corrosion, and thermal oxidation behaviors of Incoloy-925 alloy were investigated. Plastic deformation applied at rates of 30, 50, and 70% led to a significant grain size reduction from 150 to 8 µm, resulting in improved hardness (up to 339 HV) and yield strength (up to 1480 MPa). Wear tests showed that the coefficient of friction decreased from 0.653 (untreated) to 0.548 (70% deformation), and the total mass loss dropped from 7 to 1 mg. Corrosion analysis revealed that the corrosion rate declined from 6.94 to 1.02 mpy with the increase in deformation, attributing to enhanced passive film formation and a more homogeneous surface structure. TGA/DTA analyses confirmed that warm rolling improved thermal oxidation resistance. The mass loss decreased from 0.91% (untreated) to 0.49% (70% deformation). Exothermic reactions between 400 and 950 °C observed in DTA curves indicated phase transformations, which were consistent with XRD findings revealing γ, δ, and MC-type carbide phases. Overall, the results demonstrate that warm rolling significantly enhances the surface integrity, thermal stability, and corrosion and wear resistance of Incoloy-925 alloy, making it a strong candidate for demanding industrial and biomedical applications.

在本研究中,研究了520℃温轧对incoly -925合金显微组织、力学、摩擦学、腐蚀和热氧化行为的影响。在30%、50%和70%的塑性变形率下,晶粒尺寸从150µm显著减小到8µm,从而提高了硬度(高达339 HV)和屈服强度(高达1480 MPa)。磨损试验表明,摩擦系数从0.653(未处理)下降到0.548(70%变形),总质量损失从7 mg下降到1 mg。腐蚀分析表明,随着变形量的增加,腐蚀速率从6.94 mpy下降到1.02 mpy,这是由于钝化膜的形成增强,表面结构更加均匀。TGA/DTA分析证实,热轧提高了耐热氧化性能。质量损失从0.91%(未处理)下降到0.49%(变形70%)。在400 ~ 950℃的放热反应中,DTA曲线显示出相变,这与XRD结果一致,显示出γ、δ和mc型碳化物相。总体而言,结果表明,热轧显著提高了incoly -925合金的表面完整性、热稳定性、耐腐蚀和耐磨性,使其成为要求苛刻的工业和生物医学应用的有力候选者。
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引用次数: 0
Microstructure and Performances of Ni-ZrO2-CeO2 Nanocomposites via Ultrasonic Pulse Electrodeposition 超声脉冲电沉积Ni-ZrO2-CeO2纳米复合材料的微观结构与性能
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-22 DOI: 10.1007/s11665-025-11845-8
Yunwei Zhu, Lixin Wei

The current study investigated the synthesis of pure Ni, Ni-ZrO2, and Ni-ZrO2-CeO2 nanocomposites using ultrasonic pulse electrodeposition. The study focused on evaluating their mechanical properties, surface characteristics, wear performance, and corrosion resistance. The findings revealed that pure Ni composites demonstrated coarse particles with an irregular structure. However, the Ni-ZrO2-CeO2 nanocomposites revealed the most compact, uniform, and refined microstructure among the three, with average grain sizes of 67.9 nm for Ni and 20.8 nm for ZrO2/CeO2 nanoparticles. The microhardness measurements revealed high values for all composites, with pure Ni, Ni-ZrO2, and Ni-ZrO2-CeO2 nanocomposites respectively averaging 375.4, 430.1, and 525.9 Hv. Moreover, the Ni-ZrO2-CeO2 nanocomposites demonstrated improved tribological performance, maintaining a low friction coefficient of approximately 0.31. The worn mass loss comparison showed that pure Ni composites had the 34.55 mg/m2 highest average mass loss, whereas Ni-ZrO2-CeO2 nanocomposites demonstrated the minimal average mass loss, at 14.87 mg/m2. In a 3.5 wt.% solution of NaCl, the Ni-ZrO2-CeO2 nanocomposites revealed outstanding corrosion resistance, sustaining minimal damage and achieving the 0.06 mm/year lowest corrosion rate among the composites. The addition of ZrO2 and CeO2 nanoparticles in the Ni-ZrO2-CeO2 composite refined the grain structure and promoted a uniform, densely packed microstructure, significantly improving corrosion resistance upon comparison with pure Ni and Ni-ZrO2 composites. These results underline the potential of UPE for fabricating high-performance nanocomposites with advanced properties for various technological applications.

本研究采用超声脉冲电沉积法制备了纯Ni、Ni- zro2和Ni- zro2 - ceo2纳米复合材料。研究的重点是评估它们的机械性能、表面特性、磨损性能和耐腐蚀性。结果表明,纯Ni复合材料具有不规则结构的粗颗粒。而Ni-ZrO2-CeO2纳米复合材料的微观结构最为致密、均匀、精细,Ni纳米颗粒的平均晶粒尺寸为67.9 nm, ZrO2/CeO2纳米颗粒的平均晶粒尺寸为20.8 nm。显微硬度测量显示,所有复合材料的显微硬度值都很高,纯Ni、Ni- zro2和Ni- zro2 - ceo2纳米复合材料的平均硬度分别为375.4、430.1和525.9 Hv。此外,Ni-ZrO2-CeO2纳米复合材料的摩擦学性能得到了改善,摩擦系数保持在0.31左右。磨损质量损失比较表明,纯Ni复合材料的平均质量损失最高,为34.55 mg/m2,而Ni- zro2 - ceo2纳米复合材料的平均质量损失最小,为14.87 mg/m2。在3.5 wt.%的NaCl溶液中,Ni-ZrO2-CeO2纳米复合材料表现出优异的耐腐蚀性能,损伤最小,腐蚀速率最低,为0.06 mm/年。在Ni-ZrO2-CeO2复合材料中加入ZrO2和CeO2纳米颗粒细化了晶粒结构,促进了均匀致密的微观组织,与纯Ni和Ni-ZrO2复合材料相比,显著提高了耐腐蚀性。这些结果强调了UPE在各种技术应用中制造具有先进性能的高性能纳米复合材料的潜力。
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引用次数: 0
Effects of Chromium Content, Temperature and Strain Rate on Microstructure and Mechanical Properties of As-Cast AlCoCrxFeNi2.2 High-Entropy Alloys 铬含量、温度和应变速率对铸态AlCoCrxFeNi2.2高熵合金组织和力学性能的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-21 DOI: 10.1007/s11665-025-11853-8
Mingyun Yu, Tingjun Song, Jingan Chen, Peipei Sun, Shijing Yan, Jinming Zhu, Cailiu Yin

A series of AlCoCrxFeNi2.2 (x = 0, 0.3, 0.7, 1.1, 1.5, 1.9, 2.3) high-entropy alloys were designed and prepared. The effects of the Cr content on the microstructures and mechanical properties of the AlCoCrxFeNi2.2 alloys were studied. All the alloys consisted of face-centered cubic (FCC) and body-centered cubic (BCC) phases. The Cr-free AlCoFeNi2.2 alloy exhibited a fine alternating lamellar eutectic structure, which became coarser with increasing Cr content. When x = 2.3, the lamellar eutectic structure disappears. Room temperature uniaxial tensile tests revealed significant changes in the mechanical properties with increasing Cr content. For 0 ≤ x ≤ 1.1, with increasing Cr content, the yield strength and hardness of the alloy decrease, whereas the ductility increases. Conversely, for 1.1 ≤ x ≤ 2.3, increasing the Cr content resulted in a higher yield strength and hardness of the alloy, accompanied by a decrease in ductility. The AlCoCr0.7FeNi2.2 alloy exhibited superior overall mechanical properties at room temperature. The tensile yield strength, hardness, and elongation were 472.9 MPa, 294.8 HV, and 26.3%, respectively. Uniaxial tensile tests on the AlCoCr0.7FeNi2.2 alloy at various temperatures and strain rates revealed that the strength increased with increasing temperature and decreasing strain rate. A mathematical description of the effects of temperature and strain rate on the strength of an alloy can be given by the Arrhenius-type equation. These results demonstrate that the AlCoCr0.7FeNi2.2 alloy maintains excellent properties even at elevated temperatures.

设计并制备了一系列AlCoCrxFeNi2.2 (x = 0,0.3, 0.7, 1.1, 1.5, 1.9, 2.3)高熵合金。研究了Cr含量对AlCoCrxFeNi2.2合金组织和力学性能的影响。所有合金均由面心立方相(FCC)和体心立方相(BCC)组成。无Cr的AlCoFeNi2.2合金呈现出良好的交变片层共晶结构,随着Cr含量的增加,其结构逐渐变粗。当x = 2.3时,片层共晶结构消失。室温单轴拉伸试验表明,随着Cr含量的增加,材料的力学性能发生了显著变化。当0≤x≤1.1时,随着Cr含量的增加,合金的屈服强度和硬度降低,而塑性提高。相反,当1.1≤x≤2.3时,Cr含量的增加导致合金的屈服强度和硬度升高,但塑性降低。在室温下,AlCoCr0.7FeNi2.2合金表现出优异的综合力学性能。拉伸屈服强度为472.9 MPa,硬度为294.8 HV,延伸率为26.3%。对AlCoCr0.7FeNi2.2合金在不同温度和应变速率下的单轴拉伸试验表明,强度随温度升高和应变速率降低而升高。温度和应变速率对合金强度影响的数学描述可以用arrhenius型方程给出。这些结果表明,即使在高温下,AlCoCr0.7FeNi2.2合金也能保持优异的性能。
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引用次数: 0
Microstructural and Mechanical Characterization of Heat-Treated and Laser Shock-Peened SS316L Fabricated by Selective Laser Melting 选择性激光熔化热处理和冲击强化SS316L的显微组织和力学性能
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-08-21 DOI: 10.1007/s11665-025-11811-4
M. Veluchamy, Somasundaram Kumanan

This work investigates the effects of heat treatment and laser shock peening (LSP) on the nanomechanical behavior of SS316L fabricated by selective laser melting (SLM). The nanoindentation, microstructural studies, phase analysis, and microhardness testing were performed under different conditions. Microstructural analysis revealed columnar structure in the as-built sample and annealing twins in the heat-treated sample. The LSP induced a high-pressure shock wave, causing severe plastic deformation and grain refinement. Phase analysis confirmed the presence of the face-centered cubic (FCC) austenite (γ) phase with no new crystalline phases. The LSP impacts increased FWHM values due to enhanced microstrain and grain refinement in LSP samples. The surface microhardness, reduced modulus, nanohardness, plastic deformation, elastic modulus, and contact stiffness of the AB + LSP sample improved by 25.81, 7.25, 24.70, 63.63, 8.97, and 9.91% as compared to the AB sample. Similarly, the HT + LSP sample showed improvements by 18.18, 6.78, 28.46, 81.27, 8.14, and 16.06% in these properties compared to the HT sample. The indentation depth and creep of AB + LSP reduced by 49.05 and 30.76%, while for HT + LSP, they reduced by 25.27 and 26.92%, respectively. These findings confirm that LSP effectively enhances the surface strength and durability of SS316L.

Graphical Abstract

研究了热处理和激光冲击强化(LSP)对选择性激光熔化(SLM)制备的SS316L纳米力学行为的影响。在不同的条件下进行了纳米压痕、显微组织研究、物相分析和显微硬度测试。显微组织分析表明,试样为柱状结构,热处理试样为退火孪晶。LSP诱发了高压激波,造成了严重的塑性变形和晶粒细化。相分析证实了面心立方(FCC)奥氏体(γ)相的存在,没有新的晶相。LSP的影响增加了FWHM值,这是由于LSP样品的微应变增强和晶粒细化。与AB试样相比,AB + LSP试样的表面显微硬度、还原模量、纳米硬度、塑性变形、弹性模量和接触刚度分别提高了25.81%、7.25、24.70、63.63、8.97和9.91%。同样,与HT样品相比,HT + LSP样品的这些性能分别提高了18.18%、6.78%、28.46%、81.27%、8.14%和16.06%。AB + LSP的压痕深度和蠕变分别降低了49.5%和30.76%,HT + LSP的压痕深度和蠕变分别降低了25.27%和26.92%。这些结果证实了LSP有效地提高了SS316L的表面强度和耐久性。图形抽象
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引用次数: 0
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Journal of Materials Engineering and Performance
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