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2011 International Symposium on Advanced Packaging Materials (APM)最新文献

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Study on thermal conductive adhesives for high-power LEDs packaging 大功率led封装用导热胶的研究
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105681
Mingxiang Chen, T. Xu, Sheng Liu, C. Wong
Direct bonded copper (DBC) as heat spreader and highly thermal conductive adhesives as thermal interface materials (TIMs), the light performances of packaged high-brightness light-emitting diodes (HB-LEDs) were tested. The results indicated that the light output power of LED modules increased with the thermal conductivities of TIMs. Apart from its low bulk thermal resistance, highly thermal conductive adhesive has high adhesion with adjacent substrates which resulted in low contact thermal resistance, then the optical performance and reliability of LED package can be improved.
采用直接键合铜(DBC)作为导热材料,高导热胶粘剂作为热界面材料(TIMs),测试了封装的高亮度发光二极管(hb - led)的光性能。结果表明,LED模组的光输出功率随TIMs热导率的增加而增加。高导热胶粘剂除了具有较低的体热阻外,还具有与邻近基板的高粘附性,从而降低了接触热阻,从而提高了LED封装的光学性能和可靠性。
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引用次数: 5
The popcorn effect of lead and lead-free mixed assembly process in high density plastic packages 高密度塑料包装中铅与无铅混合装配工艺的爆米花效应
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105694
Xiao Hong, P. Lai
The expansion of integrated circuit applications is driving chip costs down. To respond to the lower price the lower price expectations, manufacturers bring Plastic packages which is cost less expensive packaging solutions. Today although the electronic packaging industry there are still many enterprises were to have lead solder, but this does not preclude the “lead-free” has become the main topic of electronic materials and microelectronics. In this transitional period, lead and lead-free both assemble on the plastic package in the field of application is already unavoidable. Problem existed in lead or lead-free materials, technology, equipment, system compatibility and other issues. The reliability of the plastic package IC is becoming a key concern. The popcorn effect is caused when moisture inside a plastic package turns to steam and expands rapidly during infrared and vapor phase reflow solder process. Under certain conditions, the force from the expanding moisture can cause stresses inside the package. Solder ball inside with lead process and outside with lead-free may result in failure. It is prompted by the melting point of lead and lead-free material is different in the same BGA packaging chip. In most severe cases, the packaging defects and the stress may result in external package cracks. And in this paper, a sample is given that the BGA packaging chip exist void in the die/die attach interface. Capillary phenomenon is present in the package closest to the die attach, and lead to a short circuit between some pins. Pay more attention to the reliability of mixed assembly process is of great value.
集成电路应用的扩展正在推动芯片成本下降。为了响应价格越低,价格越低的期望,制造商带来了塑料包装,这是成本更低的包装解决方案。今天虽然电子封装行业仍有许多企业曾使用含铅焊料,但这并不排除“无铅”已成为电子材料和微电子的主要话题。在这一过渡时期,铅与无铅同时组装在塑料包装上的应用领域已经不可避免。存在有铅或无铅材料、工艺、设备、系统兼容性等问题。塑料封装集成电路的可靠性正成为一个关键问题。爆米花效应是在红外和气相回流焊接过程中,塑料包装内的水分变成蒸汽并迅速膨胀而产生的。在一定条件下,膨胀的湿气所产生的力会在包装内部造成压力。焊球内部带铅而外部无铅可能导致故障。这是由于同一块BGA封装芯片中含铅和无铅材料的熔点不同所致。在最严重的情况下,包装缺陷和应力可能导致外包装开裂。并给出了BGA封装芯片在模/模连接接口上存在空隙的实例。在封装中最靠近晶片连接处存在毛细现象,导致一些引脚之间短路。重视混合装配过程的可靠性是很有价值的。
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引用次数: 0
Investigation of accelerated surface oxidation of Sn-3.5Ag-0.5Cu solder particles by TEM and STEM 用TEM和STEM研究Sn-3.5Ag-0.5Cu钎料颗粒表面加速氧化
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105674
Xin Luo, Wenhui Du, Xiuzhen Lu, Toshikazu Yamaguchi, J. Gavin, L. Ye, Johan Liu
The composition and thickness of surface oxide of solder particles has a direct effect on adhesion and electrical resistance of soldering joint and resultant the quality of interconnect and the reliability of packaged system. Auger electron spectroscopy (AES), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM) and scanning transmission electron microscopy (STEM) were used to examine the oxide layer on solder powders in the present paper. However, for the surface oxide layer of a lead-free solder particle, the TEM sample for the oxide layer has never been done for studying its thickness or appearance before. And it is the first time in this work to use Focus Ion Beam (FIB) technology to prepare TEM specimen for solder particles and show TEM pictures of their surface oxide layer. High angle annular dark field (HAADF) pattern was applied to distinguish between the oxide layer and the solder matrix by the contrast of average atomic number. The solder powders were exposed in air (70% relative humidity) at 150°C for 0, 120 and 240 h to simulate the accelerated growth of oxide. The surface oxide thickness was 6 nm and 50 nm measured by TEM for 0 h and 120 h samples respectively. Confirming by AES measurement, the thickness of 5 nm and 50 nm were gotten using intersection analysis method for AES depth profiles. It is found that the increase of surface oxide thickness of solder particles is proportional to the rooting of time. The elemental distribution along the oxide was quantified by line scanning using STEM and the atomic ratio of Sn to O in the oxide layer nearer to the outer, the middle, and the inner (adjacent to the solder matrix) were found to be 1:2, 2:3 and 1:1, respectively. The result was validated using XPS which gave Sn to O ratio of 1:2 at 5 nm depth of surface oxide.
焊锡颗粒表面氧化物的组成和厚度直接影响到焊点的附着力和电阻,从而影响到互连质量和封装系统的可靠性。采用俄歇电子能谱(AES)、x射线光电子能谱(XPS)、透射电子显微镜(TEM)和扫描透射电子显微镜(STEM)对焊锡粉的氧化层进行了表征。然而,对于无铅焊料颗粒的表面氧化层,以前从未做过氧化层的TEM样品来研究其厚度或外观。本文首次利用聚焦离子束(FIB)技术制备了焊料颗粒的TEM试样,并展示了其表面氧化层的TEM图像。采用高角环形暗场(HAADF)模式,通过平均原子序数的对比来区分氧化层和焊料基体。将焊锡粉在空气中(相对湿度为70%)在150℃下暴露0、120和240 h,模拟氧化物的加速生长。透射电镜测定样品在0 h和120 h时的表面氧化厚度分别为6 nm和50 nm。通过AES深度剖面的交会分析,得到了5 nm和50 nm的厚度。结果表明,焊料颗粒表面氧化层厚度的增加与生根时间成正比。利用STEM对元素沿氧化物的分布进行了定量分析,发现靠近外侧、中部和内侧(靠近焊料基体)的氧化层中Sn与O的原子比分别为1:2、2:3和1:1。用XPS对结果进行了验证,在5 nm深度处,锡氧比为1:2。
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引用次数: 3
Investigation of BGA crack issue in normal production line 正常生产线BGA裂纹问题的调查
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105707
Y. Tao, Y. P. Wu, B. Wu, M. Cai
Recently, a serious crack issue for a commercial BGA has taken place frequently in the normal PCBA assembly line, which has lead to abnormal failure rate spikes in the first pass yield trend chart, and caused line down issue already. Both cross section and Dye & Pry has been carried out to find out the fracture mode in the suspected pin of the failed unit. The cross section result shows that both BGA solder separation and PCB prepreg separation occurs there. Dye & Pry reveals that the crack pins mainly gather at corner “D” of this BGA, and 100% dye is presented there. In order to find out the root cause of this case, a series of destructive experiments have been carried out. Firstly, shear test of the raw BGA solder joint are performed. It reveals that there is no obvious difference for the solder strength between the BGA balls at the four corners and those in the center area, which indicates that the BGA raw material is not related to the root cause of this case. Secondly, in order to identify the point at which the ball crack are starting in production line, samples including bare PCB and assembled PCBA have been collected at different work station in both SMT and product build line, which will all act as the experiment specimens for a series of cross section and Dye & Pry of next step. The results show that the FCT (Functional Circuit Test) after SMT line is one of the suspected stations where the solder crack initiation will take place. After that, Strain gauge has been performed to check in both these locations, and the results show that the strain value is out of spec. Finally, some idle probes under BGA in FCT is suggested to be the root cause to trigger solder crack initiation, and both cross section and Dye & Pry result proves that the BGA crack issue can be solved after removing those probes.
最近,在正常的PCBA装配线上,经常发生商用BGA的严重裂纹问题,导致一次合格率趋势图中不良率异常飙升,已经造成生产线停工问题。采用了截面法和Dye & Pry法来确定失效单元的疑似销的断裂模式。横截面结果表明,BGA焊料分离和PCB预浸料分离同时发生。Dye & Pry显示,裂纹针主要聚集在BGA的“D”角,此处呈现100%的染料。为了找出这种情况的根本原因,进行了一系列破坏性实验。首先,对BGA焊点进行了剪切试验。结果显示,四个角的BGA球与中心区域的BGA球的焊料强度没有明显差异,表明BGA原料与本案的根本原因无关。其次,为了确定生产线上球裂的起始点,我们在SMT和产品构建线的不同工位收集了裸PCB和组装好的PCBA样品,这些样品都将作为下一步一系列横截面和Dye &撬的实验样品。结果表明,SMT生产线后的功能电路测试(FCT)是可能产生焊点裂纹的工位之一。之后,在这两个位置进行应变片检查,结果表明应变值不符合规范。最后,FCT中BGA下的一些闲置探头是引发焊料裂纹的根本原因,截面和Dye & Pry结果都证明,移除这些探头后,可以解决BGA裂纹问题。
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引用次数: 1
A novel four layers package-on-package stacking technique 一种新颖的四层包对包堆叠技术
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105739
Shi Lingfeng, Xia Yuanming, Zhang Ke, Jia Jun, Liu Chen, Lai Xin-quan
Currently, the multilayer Package-on-Package (PoP) stacking technique as the mainstream 3D vertical packaging solution is extensively applied in the manufacture process of portable electronic instruments. While the warpages on the packages caused by the mismatch of the Coefficient of Thermal Expansion (CTE) and stiffness during the assembly and stacking processes are seriously threaten to the stability and reliability. In this paper, a novel four layers PoP stacking technique in which the number of memory die packaged are increased to twice of the traditional two layers PoP is presented. The metal cylinders with stable CTE are placed between the neighboring layers to reduce the warpages on the packages. The high memory density and excellent reliability could meet the requirements of the miniaturization and lightening of the portable instruments.
目前,作为主流3D垂直封装解决方案的多层PoP堆叠技术被广泛应用于便携式电子仪器的制造过程中。而在组装和堆叠过程中,由于热膨胀系数(CTE)和刚度的不匹配导致的封装翘曲严重威胁到封装的稳定性和可靠性。本文提出了一种新的四层PoP堆叠技术,将封装的存储芯片数量增加到传统两层PoP的两倍。在相邻层之间放置具有稳定CTE的金属圆柱体,以减少包装上的翘曲。存储密度高,可靠性好,能够满足便携式仪器小型化、轻量化的要求。
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引用次数: 6
Failure process of solder joint under mechanical vibration based on a real-time data acquisition method 基于实时数据采集方法的机械振动下焊点失效过程
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105715
Hongwu Zhang, F. Sun, Yang Liu, Zhenya Zhou, Y. Qin
Dynamic voltage signal across solder joints during mechanical vibration test was monitored and collected real-timely with a self-designed data acquisition system. Failure process of solder joint was studied by processing and analyzing data. In the paper, lifetime of solder joint was also compared by changing solder joint location, solder joint composition and vibration acceleration. Results indicated that voltage across solder joints kept at about 0.14v from 0s to 40s, which indicated that crack of solder joint did not form. Voltage of solder joint suddenly rose to 0.45v between 44.2s and 45.2s, which illustrated crack initiation and growth rapidly. In addition, lifetime of solder joint on the edge of test board was about 4.5 times longer than that of solder joint in the center of test board. It was found that with vibration acceleration from 20g to 25g increase of 25%, lifetime of solder joint decreased from 980s to 105s with 89%.
采用自行设计的数据采集系统,实时监测和采集机械振动试验过程中焊点间的动态电压信号。通过对数据的处理和分析,研究了焊点的失效过程。本文还通过改变焊点位置、焊点成分和振动加速度对焊点寿命进行了比较。结果表明:在0s ~ 40s期间,焊点间电压保持在0.14v左右,表明焊点未形成裂纹;在44.2s ~ 45.2s之间,焊点电压突然上升至0.45v,表明裂纹萌生和扩展迅速。此外,测试板边缘焊点的寿命约为测试板中心焊点的4.5倍。结果表明,当振动加速度从20g增加到25g,增加25%时,焊点的寿命从980s降低到105s,降低89%。
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引用次数: 2
Die backside stress modification by coating of Si3N4 or AlN layers 采用氮化硅或氮化铝涂层对模具背面应力进行改性
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105734
J. Liao, S. Liu, Y. T. Yu, Y. Lin, G. Jin, G. Huang, Z. Fu
The ability to improve the mechanical properties of a microelectronic package, including reducing the thermal-mechanical stress and increasing the die breaking strength is a long-sought goal in electrical assembly and packaging technology. Failure modes related with die backside stress caused by warpage or cosmetic defects may occur without a well control of die-backside stress. In this study, the modifications of die backside stress by coating of a thin layer of AlN or Si3N4 have been investigated. The simulation through the Finite Element Method (FEM) indicated that the stress distribution can be modified after coating and it is strongly related to the thickness of the coated layer, as the stress of die backside surface reduces. Die breaking strength has been measured by 3 point bending test and the measurement results are compared between samples with and without coatings. It is demonstrated that the die breaking strength is related with the thickness and the surface roughness of the coating layer of AlN or Si3N4. Improvement in the die breaking strength can be realized when the thickness and surface roughness are both optimized. The results suggested the additional coating of the die backside may be a feasible way to improve the mechanical properties of the electronic packages.
提高微电子封装的机械性能,包括降低热机械应力和提高模具断裂强度,是电气组装和封装技术长期追求的目标。由于翘曲或表面缺陷引起的与模具背面应力有关的失效模式可能在模具背面应力控制不好的情况下发生。在本研究中,研究了薄层AlN或Si3N4涂层对模具背面应力的影响。有限元模拟结果表明,涂层后的应力分布可以改变,且与涂层厚度密切相关,因为涂层后模具表面应力减小。采用三点弯曲试验法测定了模具的抗折强度,并对涂覆和未涂覆试样的测试结果进行了比较。结果表明,抗断模强度与氮化硅或氮化硅涂层的厚度和表面粗糙度有关。当厚度和表面粗糙度同时优化时,可实现模具断裂强度的提高。结果表明,在芯片背面进行附加涂层可能是改善电子封装力学性能的一种可行方法。
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引用次数: 1
Preparation of copper clad laminates with high performance bismaleimide-based copolymer matrix resins 高性能双马来酰亚胺基共聚物基树脂覆铜层压板的制备
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105742
Hongfu Zhou, Jianbin Wang
4,4′-Diphenyl Bismaleimide/Diallyl Bisphenol A/Bisphenol-A Cyanate Ester/Epoxy Resin copolymer matrix resins were developed by fusion prepolymerization and solution prepolymerization method, and use the bismaleimide (BMI)-based copolymer matrix resins/glass fabric prepared for copper clad laminates, which illustrate Tg at 230.7°C, dielectric constant at 3.57(1MHz) and dielectric loss constant at 0.0053(1MHz), volume resistivity at 2.3×1013Ω·cm and surface resistivity at 2.4×1015Ω, thermal expansion coefficient at 1.1×10–5/°C (x y-axis) and 5.7×10–5/°C (z-axis), dip soldering of resistance(288°C) is more than 62s, peel strength at 16.7N/cm, flexural strength at 458.3MP, moisture absorption at 0.19%, the test results explain that the performance is better than Japanese product copper clad laminates with bismaleimide/triazine-based resin(BT resin).
采用熔融预聚合和溶液预聚合的方法,制备了4,4′-二苯基双马来酰亚胺/二烯丙基双酚A/双酚A -氰酸酯/环氧树脂共聚物基体树脂,并采用双马来酰亚胺(BMI)基共聚物基体树脂/玻璃织物制备覆铜层合板,其Tg为230.7℃,介电常数为3.57(1MHz),介电损耗常数为0.0053(1MHz),体积电阻率为2.3×1013Ω·cm,表面电阻率为2.4×1015Ω。热膨胀系数为1.1×10-5 /°C (x y轴)和5.7×10-5 /°C (z轴),浸焊电阻(288°C)大于62s,剥离强度为16.7N/cm,抗折强度为458.3MP,吸湿率为0.19%,测试结果说明性能优于日本产品双马来酰亚胺/三嗪基树脂(BT树脂)覆铜板。
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引用次数: 1
The effect of thermal stress on high density packaging integrated circuits 热应力对高密度封装集成电路的影响
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105693
Bin Yao, P. Lai, J. Liu, Xiaosi Liang
The trend of electronics industry is toward advanced high density packaging technologies. The reliability of integrated circuits (ICs) which is significantly affected by thermal stress has become more essential as the packaging density increases. In this paper, an accelerated thermal reliability test method for evaluating the packaging reliability of ICs which includes hot step, cold step and rapid thermal cycling test is presented. The technology of FIMV (Force current measure voltage) was applied during the reliability test as an indicator of degradation of packaging property, which allowed the reliability performance of ICs to be assessed in real time. The experimental results showed that the thermal stress resulted in the degradation of interfacial adhesion of plastic packaging ICs. Because of the temperature changing during the rapid thermal test, the strain and stress due to the coefficient of thermal expansion (CTE) mismatch between the encapsulant and the adjacent materials could contribute to delamination or de-adhesion. In some cases it was directly linked to a failure if some severe defects occured because of delamination, such as wire bond lift-off or fracture. Crack in die attach adhesive based on the same failure mechanism was also found. Additionally, unwanted brittle Au-Al intermetallic compound was detected at the bond interface because of the effect of high temperature. The formation of the Au-Al intermetallic compound led to the increase of electrical resistance and the weakening of bond strength which resulted in bond lift-off finally. At last future research work in this field is suggested.
电子工业的发展趋势是采用先进的高密度封装技术。随着封装密度的增加,受热应力影响较大的集成电路的可靠性变得越来越重要。本文提出了一种集成电路封装可靠性的加速热可靠性测试方法,包括热步、冷步和快速热循环测试。在可靠性测试中,采用FIMV (Force current measure voltage)技术作为封装性能退化的指标,实时评估集成电路的可靠性性能。实验结果表明,热应力会导致塑料封装集成电路的界面附着力下降。在快速热测试过程中,由于温度的变化,由于封装剂与邻近材料之间的热膨胀系数(CTE)不匹配而产生的应变和应力可能导致分层或脱粘。在某些情况下,如果由于分层而发生严重缺陷,例如钢丝粘结脱落或断裂,则与故障直接相关。基于相同的失效机理,还发现了模具粘接胶的裂纹。此外,由于高温的影响,在键界面处发现了多余的脆性金铝金属间化合物。Au-Al金属间化合物的形成导致电阻增大,粘结强度减弱,最终导致粘结脱落。最后对该领域今后的研究工作提出了建议。
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引用次数: 0
Synthesis of agglomerate-free YAG: Ce3+ phosphors by co-precipitation and low temperature spray pyrolysis 共沉淀法和低温喷雾热解法制备无团块YAG: Ce3+荧光粉
Pub Date : 2011-12-19 DOI: 10.1109/ISAPM.2011.6105683
S. Gao, Yibin Chen, Renjie Zeng
Y3−xCexAl5O12 (YAG: Ce3+) phosphor particles were prepared by a new method called co-precipitation and low temperature spray pyrolysis (CP-LTSP) with oxalic acid and ammonia as precipitant. It corresponds to the first-step chemical liquid reaction, the second step dehydration and partial decomposition of precipitation droplets at 250°C and then heating at 1100°C or above. Spherical as-prepared particles and agglomerate-free YAG: Ce3+ phosphor particles were obtained respectively. Pure YAG phase could be formed after LTSP at 250°C and then annealing at 1100°C for 4 h. The emission spectra and XRD patterns of YAG: Ce3+ phosphor particles indicated that the optimum doping concentration of Ce3+ was 0.06. The emission intensity increased with the increase of annealing temperature. As a result, the YAG: Ce3+ phosphor particles without optimization annealed at 1550°C for 4 h had the similar emission intensity (96%) of the commercial phosphor by the solid-state method.
以草酸和氨为沉淀剂,采用共沉淀-低温喷雾热解(CP-LTSP)法制备了Y3−xCexAl5O12 (YAG: Ce3+)荧光粉颗粒。对应第一步化学液体反应,第二步250℃脱水部分分解沉淀液滴,然后1100℃以上加热。制备的YAG: Ce3+荧光粉颗粒分别为球形和无团聚体。经250℃LTSP, 1100℃退火4 h,可以形成纯净的YAG相。YAG: Ce3+荧光粒子的发射光谱和XRD分析表明,Ce3+的最佳掺杂浓度为0.06。发射强度随退火温度的升高而增大。结果表明,未经优化的YAG: Ce3+荧光粉颗粒在1550℃下退火4 h后,其发射强度(96%)与固态法制备的商用荧光粉相似。
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引用次数: 2
期刊
2011 International Symposium on Advanced Packaging Materials (APM)
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