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Characterization and mechanical performance of stone mastic asphalt mixtures modified with SBS and PE polymers SBS和PE改性石胶泥沥青混合料的表征及力学性能
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-27 DOI: 10.1007/s11043-025-09798-5
Amjad H. Albayati, Ahmed M. Mohammed, Mazen J. Al-Kheetan, Aliaa F. Al-ani, Mustafa M. Moudhafar, Yazeed S. Jweihan

This study investigates the characterization and mechanical performance of Stone Mastic Asphalt (SMA) mixtures modified with two types of polymers: styrene–butadiene–styrene (SBS) and high-molecular-weight polyethylene (PE). Neat asphalt cement PG 64-16 was modified using a higher content of SBS and PE at concentrations of 6%, 7%, and 8% by weight of asphalt through the dry blending method to produce Highly Modified Asphalts (HiMA). The physical and rheological properties of the modified binders were evaluated using penetration, softening point, rotational viscosity, and dynamic shear rheometer (DSR) tests. Also, their phase compatibility and morphological changes were evaluated using the storage stability testing and scanning electron microscopy (SEM) analysis. The mechanical performance of the corresponding SMA mixtures was assessed through Marshall stability and flow, moisture susceptibility, crack tolerance index (CT-index), resilient modulus, and rutting resistance tests. Also, a mechanistic durability analysis was conducted using the KENLAYER software. Results indicated that both polymers enhanced the binder’s stiffness and high-temperature performance, with SBS exhibiting greater overall improvements. SBS-modified binders displayed a relatively low softening point difference ((Delta )T) of 5.1 °C to 5.8 °C, indicating good thermal stability and uniform polymer dispersion. In contrast, PE-modified binders exhibited significantly higher (Delta )T values, reaching 13.5 °C with 8% PE content, indicating a greater tendency toward phase separation. Moreover, Marshall stability improved substantially, increasing by 43% for 8% SBS-modified mixes and 28% for 8% PE-modified mixes compared to the neat SMA mix. Flow number (FN) results indicated enhanced rutting resistance, with FN values increasing by 2.45 times for SBS mixes and 2.1 times for PE mixes at 8% polymer content. Additionally, moisture susceptibility was significantly improved, as evidenced by the tensile strength ratio (TSR) values of 97% with 8% SBS and 92% with 8% PE, compared to 81% for the neat mix. Resilient modules increased notably, with a 38% rise for 8% SBS mixes and a 24% rise for 8% PE mixes, reflecting enhanced stiffness and load-bearing capacity. Also, the CT-index significantly improved, reaching values of 154 for the 8% SBS mix and 127 for the 8% PE-modified mix, compared to 86 for the neat mix, indicating enhanced resistance to cracking. Finally, both polymer-modified mixes demonstrated improved durability, where the 8% SBS mix exhibited the longest design life (21.66 years) and the highest number of allowable load repetitions (5.42 × 106), followed by 8% PE (13.98 years and 3.50 × 106 repetitions).

本研究研究了用两种聚合物:苯乙烯-丁二烯-苯乙烯(SBS)和高分子量聚乙烯(PE)改性的石胶泥沥青(SMA)混合物的表征和力学性能。采用高含量的SBS和PE对纯沥青水泥PG 64-16进行了改性%, 7%, and 8% by weight of asphalt through the dry blending method to produce Highly Modified Asphalts (HiMA). The physical and rheological properties of the modified binders were evaluated using penetration, softening point, rotational viscosity, and dynamic shear rheometer (DSR) tests. Also, their phase compatibility and morphological changes were evaluated using the storage stability testing and scanning electron microscopy (SEM) analysis. The mechanical performance of the corresponding SMA mixtures was assessed through Marshall stability and flow, moisture susceptibility, crack tolerance index (CT-index), resilient modulus, and rutting resistance tests. Also, a mechanistic durability analysis was conducted using the KENLAYER software. Results indicated that both polymers enhanced the binder’s stiffness and high-temperature performance, with SBS exhibiting greater overall improvements. SBS-modified binders displayed a relatively low softening point difference ((Delta )T) of 5.1 °C to 5.8 °C, indicating good thermal stability and uniform polymer dispersion. In contrast, PE-modified binders exhibited significantly higher (Delta )T values, reaching 13.5 °C with 8% PE content, indicating a greater tendency toward phase separation. Moreover, Marshall stability improved substantially, increasing by 43% for 8% SBS-modified mixes and 28% for 8% PE-modified mixes compared to the neat SMA mix. Flow number (FN) results indicated enhanced rutting resistance, with FN values increasing by 2.45 times for SBS mixes and 2.1 times for PE mixes at 8% polymer content. Additionally, moisture susceptibility was significantly improved, as evidenced by the tensile strength ratio (TSR) values of 97% with 8% SBS and 92% with 8% PE, compared to 81% for the neat mix. Resilient modules increased notably, with a 38% rise for 8% SBS mixes and a 24% rise for 8% PE mixes, reflecting enhanced stiffness and load-bearing capacity. Also, the CT-index significantly improved, reaching values of 154 for the 8% SBS mix and 127 for the 8% PE-modified mix, compared to 86 for the neat mix, indicating enhanced resistance to cracking. Finally, both polymer-modified mixes demonstrated improved durability, where the 8% SBS mix exhibited the longest design life (21.66 years) and the highest number of allowable load repetitions (5.42 × 106), followed by 8% PE (13.98 years and 3.50 × 106 repetitions).
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引用次数: 0
Rapid performance grade assessment of virgin and recycled asphalt binders using a rheometer 使用流变仪快速评估原生和再生沥青粘合剂的性能等级
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-27 DOI: 10.1007/s11043-025-09797-6
Ankit Sharma, Gondaimei Ransinchung Rongmei Naga, Praveen Kumar

The Performance Grading (PG) criterion plays a pivotal role in grading bitumen for various applications, such as trading, road construction, and research and development works. The definition of high PG temperature hinges on the point where the Superpave rutting parameter, G*/sin(delta ), attains a value of 1 kPa. In this study, we present a novel mathematical model developed to accurately predict the high PG temperature of bitumen. To ascertain the PG temperature of the bitumen, we conducted the Original Binder Grading (OBG) test using a rheometer. Leveraging the data obtained from this test, our developed model forecasts the true high PG temperature based on the average value of G*/sin(delta ) measured at 64 °C. Notably, the model yields rapid results within approximately 15 minutes after initiating the OBG test, which effectively reduces test duration and empowers users to manage their work more efficiently. We anticipate that this model will be readily embraced by rheometer manufacturing industries, as it provides a direct and reliable means of determining the bitumen’s high PG temperature. This technological advancement promises to enhance testing procedures, streamline research, and support better decision-making processes across the bitumen industry. However, the model is not validated for polymer-modified binders and should be applied to unmodified binders only.

性能分级(PG)标准在各种应用的沥青分级中起着关键作用,例如贸易,道路建设和研究和开发工程。高PG温度的定义取决于Superpave车辙参数G*/sin (delta )达到1kpa的值。在这项研究中,我们提出了一个新的数学模型,以准确预测沥青的高PG温度。为了确定沥青的PG温度,我们使用流变仪进行了原始粘结剂分级(OBG)测试。利用从该测试中获得的数据,我们开发的模型基于在64°C下测量的G*/sin (delta )的平均值来预测真正的高温PG。值得注意的是,该模型在启动OBG测试后大约15分钟内产生快速结果,这有效地减少了测试持续时间,并使用户能够更有效地管理他们的工作。我们预计该模型将很容易被流变仪制造行业所接受,因为它提供了一种直接可靠的方法来确定沥青的高PG温度。这一技术进步有望加强测试程序,简化研究,并支持整个沥青行业更好的决策过程。然而,该模型并未对聚合物改性的粘合剂进行验证,而应仅应用于未改性的粘合剂。
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引用次数: 0
Energy evolution and fractional-order damage constitutive model of rock creep 岩石蠕变的能量演化与分数阶损伤本构模型
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-26 DOI: 10.1007/s11043-025-09796-7
Zhixi Liu, Dandan Ye

Rock is a fundamental material in mining engineering, and its creep behavior plays a critical role in determining the long-term stability of roadways. Consequently, investigating the creep constitutive models of rocks with varying brittleness holds significant practical importance. To investigate the evolution law of energy in uniaxial creep of rocks and establish a constitutive model, this study systematically examined the evolution of creep energy and energy distribution in four kinds of rocks—coal, mudstone, white sandstone, and red sandstone—through uniaxial creep-unloading tests. We constructed the fractional derivative damage constitutive models by introducing fractional derivative elements based on energy dissipation damage variables. The findings reveal the following: (1) The elastic strain energy density ((u^{mathrm{e}})) of rocks exhibits a linear decreasing trend with prolonged creep time, indicating a linear attenuation characteristic. (2) A method for calculating rock creep energy was proposed, leveraging the linear attenuation characteristics of (u^{mathrm{e}}). (3) The dissipated strain energy density ((u^{mathrm{d}})) and input strain energy density ((u)) of the four rocks with varying brittleness levels increase over time, and this growth can be partitioned into three stages: decay growth, steady growth, and accelerated growth. (4) As creep time increases, the proportion of (u^{mathrm{d}})/(u) gradually rises, reaching its maximum at the end of accelerated creep. Rocks with higher brittleness exhibit a greater proportion of (u^{mathrm{d}}) at these critical points. (5) A fractional derivative damage constitutive model was successfully developed, with the parameter (alpha ) of the fractional derivative element reflecting the degree of rock brittleness.

岩石是采矿工程的基础材料,其蠕变特性对巷道的长期稳定性起着至关重要的作用。因此,研究变脆性岩石的蠕变本构模型具有重要的实际意义。为研究岩石单轴蠕变过程中的能量演化规律,建立本构模型,通过单轴蠕变卸载试验,系统研究了煤、泥岩、白砂岩、红砂岩4种岩石的蠕变能量演化及能量分布。引入基于能量耗散损伤变量的分数阶导数单元,构建了分数阶导数损伤本构模型。结果表明:(1)岩石弹性应变能密度((u^{mathrm{e}}))随蠕变时间的延长呈线性下降趋势,呈现线性衰减特征;(2)利用(u^{mathrm{e}})的线性衰减特性,提出了一种计算岩石蠕变能量的方法。(3) 4种不同脆性程度岩石的耗散应变能密度((u^{mathrm{d}}))和输入应变能密度((u))随时间的推移均呈增加趋势,并可划分为衰减增长、稳定增长和加速增长3个阶段。(4)随着蠕变时间的增加,(u^{mathrm{d}}) / (u)的比例逐渐增大,在加速蠕变结束时达到最大值。脆性越高的岩石在这些临界点处的(u^{mathrm{d}})比例越大。(5)建立了分数阶导数损伤本构模型,分数阶导数单元参数(alpha )反映了岩石的脆性程度。
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引用次数: 0
Experimental study on shear mechanical properties and shear stress oscillation characteristics of regular tooth-shaped concrete joints 规则齿形混凝土节点剪切力学性能及剪应力振荡特性试验研究
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-25 DOI: 10.1007/s11043-025-09794-9
Mengtao Tian, Baohua Guo, Shengjin Cheng, Pengbo Zhong, Zhezhe Zhang, Chuangwei Zhu

As a weak link in engineering structures, the shear mechanical properties of rock joints are crucial for evaluating the stability of rock masses. To investigate the mechanism of shear stress oscillation in regular toothed joints and its relationship with specimen size and material parameters, this study conducted direct shear tests on five wave angles and six dimensions using RDS-200 under different normal stresses. The results show that (1) The peak shear strength of regular tooth-shaped rock-like joints shows a positive linear relationship with normal stress and undulating angle. For fixed-size specimens, increasing the undulating angle enhances both peak strength and pre-peak stiffness. When the sample size increases, the peak strength of the joints with the same undulating angle initially increases and then decreases, while the pre-peak stiffness generally decreases. (2) Shear stress oscillations predominantly occur under low normal stress or small undulating angles. Larger undulating angles reduce the oscillation climbing ratio, interval length, and frequency. (3) Increasing specimen size amplifies the oscillation climbing ratio, interval length, and average amplitude but lowers frequency, while higher normal stresses decrease both the oscillation climbing ratio and the number of oscillations but increase amplitude. The results provide a reference for optimizing the design and stability of rock structure.

岩体节理作为工程结构中的薄弱环节,其剪切力学特性是评价岩体稳定性的关键。为研究规则齿形接头剪应力振荡机理及其与试件尺寸、材料参数的关系,采用RDS-200进行了不同法向应力下5个波角、6个维度的直剪试验。结果表明:(1)规则齿状岩石节理的峰值抗剪强度与正应力和波动角呈线性正相关;对于固定尺寸的试样,增加波动角可以提高峰值强度和峰前刚度。当试样尺寸增大时,相同波动角节点的峰值强度先增大后减小,峰前刚度总体减小。(2)剪应力振荡主要发生在低正应力或小波动角下。较大的波动角减小了振荡爬升比、间隔长度和频率。(3)试样尺寸增大,振荡爬升比、段长和平均振幅增大,但频率降低;法向应力增大,振荡爬升比和振荡次数减小,但振幅增大。研究结果可为岩体结构的优化设计和稳定提供参考。
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引用次数: 0
Modeling of primary creep regeneration in engineering metallic alloys 工程金属合金初次蠕变再生的建模
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-19 DOI: 10.1007/s11043-025-09795-8
Andrew Rusinko

This paper aims to model the primary creep regeneration (PCR) phenomenon, which is observed at variable loadings applied during the creep of engineering alloys such as 316H stainless steel, 10% Cr martensitic steel, nickel-based alloy, etc. Since PCR is a multifactorial problem, this research addresses a partial case: deriving relationships between the extent of PCR and the value of plastic strain occurring on reversal loading. Model results are compared with the PCR phenomenon for 316H stainless steel in uniaxial tension/compression for various plastic strains on reversal stresses at equal creep dwell times and zero durations of reversal stress actions.

本文旨在模拟工程合金(如316H不锈钢、10% Cr马氏体钢、镍基合金等)在变载荷蠕变过程中观察到的一次蠕变再生(PCR)现象。由于聚合酶链反应是一个多因素问题,本研究解决了部分情况:推导了聚合酶链反应的程度与反向加载时发生的塑性应变值之间的关系。将模型结果与316H不锈钢在相同蠕变停留时间和零反转应力作用时间下,不同塑性应变在单轴拉伸/压缩条件下的PCR现象进行了比较。
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引用次数: 0
Dynamic response and damage evolution of freeze–thaw-fractured sandstone under SHPB impact: a coupled FDM–DEM approach SHPB冲击下冻融裂隙砂岩的动力响应与损伤演化:FDM-DEM耦合方法
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-16 DOI: 10.1007/s11043-025-09791-y
Huashuai Zhang, Huimei Zhang, Shiguan Chen

In this study, a three-dimensional split Hopkinson pressure bar (SHPB) impact numerical model was established through the FDM–DEM coupling method to explore the mesoscopic damage accumulation and dynamic mechanical response of fractured sandstone under freeze–thaw cycles. Based on the volume-expansion theory, a discrete-element model of the phase-change expansion of pore-water–ice was constructed. Combined with the parameter calibration optimized by the genetic algorithm, the damage evolution of the rock during the freeze–thaw process was simulated. The research results show that: (1) The discrete-element simulation results show high consistency with experimental data. Taking the 40-mm rock bridge as an example, the maximum relative errors of peak strength and elastic modulus under different freeze–thaw (FT) cycles are 8.54% and 3.49%, respectively, meeting accuracy requirements. This validates the reliability of the particle expansion model and FT damage analysis method. (2) Under uniaxial compression, rock-bridge length significantly influences the mechanical properties of FT sandstone. Specimens with 50-mm rock bridges exhibit the highest elastic modulus and peak strength. However, FT cycles induce nonlinear degradation in compressive strength. (3) Dynamic impact tests reveal that FT cycles exacerbate rock fragmentation. With increasing impact velocity and FT cycles, strain rate rises, leading to nonlinear attenuation of dynamic strength and decelerated growth of the dynamic increase factor (DIF). The presence of rock bridges further causes multistage evolution characteristics in dynamic stress–strain responses.

本研究通过FDM-DEM耦合方法,建立了三维劈裂霍普金森压杆(SHPB)冲击数值模型,探讨冻融循环作用下裂隙砂岩的细观损伤积累与动态力学响应。基于体积膨胀理论,建立了孔隙水冰相变膨胀的离散元模型。结合遗传算法优化的参数定标,模拟了冻融过程中岩石的损伤演化过程。研究结果表明:(1)离散元模拟结果与实验数据具有较高的一致性。以40-mm岩桥为例,不同冻融循环下峰值强度和弹性模量的最大相对误差分别为8.54%和3.49%,满足精度要求。验证了颗粒膨胀模型和FT损伤分析方法的可靠性。(2)单轴压缩条件下,岩桥长度对FT砂岩力学性能影响显著。50mm岩石桥的弹性模量和峰值强度最高。然而,FT循环引起抗压强度的非线性退化。(3)动力冲击试验表明,FT循环加剧了岩石破碎。随着冲击速度和FT循环次数的增加,应变率上升,导致动强度的非线性衰减和动态增加因子(DIF)的增长减速。岩桥的存在进一步导致了动应力-应变响应的多阶段演化特征。
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引用次数: 0
Modeling Joule heating in magnetized porous structures using statistical techniques 用统计技术模拟磁化多孔结构中的焦耳加热
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-12 DOI: 10.1007/s11043-025-09793-w
K. Nirisha, S. Sreedhar, V. Nagaradhika, S. Manjunatha, S. Ramesh, O. Anwar Beg

Hybrid nanofluids have been utilized in various thermal engineering applications, including heat exchangers, materials science research, and industrial domains like solar trough collectors, food processing, and aerospace engineering. This study’s ultimate objective is to examine a Casson hybrid nanofluid’s hydrodynamic and thermal behavior in a porous medium subjected to a bilinear stretching surface. The effects of thermal radiation, chemical reactions, volumetric heat source/sink, Joule heating, and viscous dissipation are all included in the mathematical model. When a magnetic field with inclination is present, the fluid is electrically conducting. By means of similarity transformations, the governing nonlinear coupled partial differential equations (PDEs) that characterize the flow phenomena are transformed into a system of coupled ordinary differential equations (ODEs). The MATLAB bvp4c solver in conjunction with a shooting technique yields numerical solutions. The outcomes, which show how different dimensionless parameters affect the flow field, temperature distribution, and concentration profiles, are displayed graphically and tabularly. The skin friction coefficient, Sherwood number, and Nusselt number at the stretching surface are among the derived quantities that are calculated and examined. As the Casson parameter rises, the momentum barrier layer becomes thinner. The Lorentz force causes the temperature to exhibit the inverse trend as the magnetic parameter increases, causing a drop in fluid velocity. The chemical reaction parameter and the Schmidt number tend to drop as the concentration profile rises, whereas the Soret effect demonstrates the exact reverse. According to statistical analysis using modified R-squared and R-squared metrics, this model matches the skin friction coefficient exceptionally well, with an average accuracy of 99.87%. The Nusselt number is noticeably more sensitive to thermal radiation and heat sources than the Dufour effect.

混合纳米流体已应用于各种热工程应用,包括热交换器、材料科学研究以及太阳能槽式集热器、食品加工和航空航天工程等工业领域。本研究的最终目的是研究卡森混合纳米流体在多孔介质中受到双线性拉伸表面的水动力和热行为。热辐射、化学反应、体积热源/热源、焦耳加热和粘性耗散的影响都包含在数学模型中。当有倾斜的磁场存在时,流体是导电的。通过相似变换,将描述流动现象的非线性耦合偏微分方程转化为耦合常微分方程。MATLAB bvp4c求解器结合射击技术产生数值解。结果显示了不同的无量纲参数如何影响流场、温度分布和浓度分布,并以图形和表格的形式显示。计算和检验了拉伸表面的表面摩擦系数、Sherwood数和Nusselt数等导出量。随着卡森参数的增大,动量势垒层变薄。洛伦兹力导致温度随着磁参数的增加而呈现相反的趋势,导致流体速度下降。随着浓度曲线的升高,化学反应参数和施密特数呈下降趋势,而索莱特效应则恰恰相反。利用改进的r平方和r平方度量进行统计分析,该模型与皮肤摩擦系数的匹配非常好,平均精度为99.87%。努塞尔数明显比杜福尔效应对热辐射和热源更为敏感。
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引用次数: 0
Compressive creep deformation and model of gangue backfill materials under the combined actions of seepage and stress 渗流与应力共同作用下矸石充填体压缩蠕变变形及模型
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-12 DOI: 10.1007/s11043-025-09788-7
Yang Zhao, Meng Li, Jixiong Zhang, Qiang Guo, Guohui Ren, Shihao Xing, Shuo Liu

The overburden stress and water environment for seepage in mines significantly affect the load-bearing capacity and deformation of gangue backfill materials (GBMs). A self-developed stress–seepage test system for backfill materials was used to conduct creep compression tests on GBMs during loading. Test results show that GBMs with a large particle size are significantly deformed, rotated, and broken, while those with a minute particle size appear to argillize under the combined action of axial stress and seepage pressure. The compressive creep deformation of GBM samples includes instantaneous deformation, attenuated creep deformation, and steady creep deformation. As the axial stress and seepage pressure increase, the instantaneous strain and creep strain of GBMs both enlarge. For instance, at a seepage pressure of 3 MPa, the instantaneous and creep strains of GBMs at axial stress of 10, 15, and 20 MPa are 1.18, 1.26, and 1.30 times as large as those at axial stress of 5 MPa, and 1.20, 1.39, and 1.56 times as large as those at axial stress of 5 MPa, respectively. The instantaneous strain and creep strain constantly increase, while the strain increments both decrease under increasing axial stress and seepage pressure. The seepage pressure degrades the mechanical properties of GBMs, which exhibit significant viscoelastic effects and nonlinear characteristics. Based on the theory of fractional-order calculus, a damaged Abel dashpot is constructed to optimize the conventional Burgers model, thus establishing a fractional-order creep constitutive model of GBMs under seepage and stress action to describe the creep properties. The model parameters were identified and verified using the creep compression test results during step-wise loading under the combined actions of seepage and stress. The parameter identification accuracy, as measured by (R^{2}), exceeded 0.997, indicating that the data were well-fitted.

矿山上覆岩应力和渗流水环境对矸石充填体的承载能力和变形有显著影响。采用自行研制的充填体应力-渗流试验系统,对充填体进行加载蠕变压缩试验。试验结果表明,在轴向应力和渗流压力的共同作用下,大粒径颗粒坝发生了明显的变形、旋转和破碎,而小粒径颗粒坝则发生了泥化。GBM试样的压缩蠕变包括瞬时变形、衰减蠕变和稳态蠕变。随着轴向应力和渗流压力的增大,基板的瞬时应变和蠕变应变均增大。例如,在渗流压力为3 MPa时,轴向应力为10、15、20 MPa时,GBMs的瞬时应变和蠕变应变分别是轴向应力为5 MPa时的1.18、1.26、1.30倍,是轴向应力为5 MPa时的1.20、1.39、1.56倍。随着轴向应力和渗流压力的增大,瞬时应变和蠕变应变不断增大,应变增量均减小。渗流压力使基板的力学性能下降,表现出明显的粘弹性效应和非线性特征。基于分数阶微积分理论,构建损伤Abel阻尼器,对传统Burgers模型进行优化,建立了渗流和应力作用下GBMs的分数阶蠕变本构模型,描述了GBMs的蠕变特性。利用渗流和应力共同作用下的阶梯加载蠕变压缩试验结果,对模型参数进行了识别和验证。通过(R^{2})测量的参数识别精度超过0.997,表明数据拟合良好。
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引用次数: 0
Experimental investigations on biochar immobilized bacteria based self-healing concrete 生物炭固定化菌基自愈混凝土的实验研究
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-10 DOI: 10.1007/s11043-025-09789-6
Chaturi B. Rajapur, Dinakar Pasla, Anush K. Chandrappa

Researchers have been studying self-healing in concrete for many years as a potential solution for self-repairing concrete structures. Bacterial concrete is one of the concrete types with self-healing characteristics. However, introducing and maintaining the required environment for bacteria is a challenging task. This study used biochar from the agricultural and food waste industries as an immobilizing agent for self-healing concrete containing Bacillus subtilis bacteria. As the self-healing due to bacteria is an alkaliphilic reaction, three cement types were used to investigate the self-healing characteristics. Three different methods, which included compressive strength recovery (M1), damage cycles using ultrasonic pulse velocity (M2), and the semicircular bending (SCB) test (M3), were used to quantify self-healing potential. In M1, control and bacterial concrete were loaded to a certain damage level, and self-healing was quantified based on strength recovery up to 84 days, while in M2, UPV was measured until the specimens were found to be intact. In M3, self-healing was quantified for concrete specimens subjected to tensile load. The M1 method indicated that ordinary Portland cement (OPC) exhibited on average 56.52% self-healing due to bacterial activity, while Portland Pozzolana and slag cement exhibited 20.82% and 49.67%, respectively. Further, the M2 method indicated that the degree of recovery in bacterial concrete was better than that of the control concrete. In addition, the M3 method, which is a first-of-its-kind test to quantify self-healing, showed that bacterial concrete was able to sustain a higher number of loading cycles compared to control specimens. The statistical analysis also indicated a significant effect of treatment and cement type on the self-healing potential.

多年来,研究人员一直在研究混凝土中的自修复,作为混凝土结构自修复的潜在解决方案。细菌混凝土是一种具有自愈特性的混凝土类型。然而,引入和维持细菌所需的环境是一项具有挑战性的任务。本研究使用来自农业和食物垃圾工业的生物炭作为含有枯草芽孢杆菌的自愈混凝土的固定化剂。由于细菌自愈是一种亲碱反应,因此采用三种类型的水泥来研究其自愈特性。三种不同的方法,包括抗压强度恢复(M1)、超声脉冲速度损伤循环(M2)和半圆弯曲(SCB)测试(M3),用于量化自愈潜力。在M1中,对照混凝土和细菌混凝土被加载到一定的损伤水平,并根据84天的强度恢复来量化自修复,而在M2中,UPV被测量,直到发现样本完好。M3中,混凝土试件在拉伸荷载作用下的自愈量化。M1法表明,普通硅酸盐水泥(OPC)的细菌活性自愈率平均为56.52%,硅酸盐水泥和矿渣水泥的细菌活性自愈率分别为20.82%和49.67%。此外,M2法还表明,细菌混凝土的回收率优于对照混凝土。此外,M3方法是首次量化自愈的测试,表明与对照样品相比,细菌混凝土能够承受更多的加载循环次数。统计分析还表明,治疗方法和水泥类型对自愈电位有显著影响。
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引用次数: 0
A coupled aging–viscoelastic–viscodamage model for predicting fatigue behavior in aged asphalt pavements 老化-粘弹-粘损伤耦合模型预测老化沥青路面疲劳行为
IF 2.3 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-06-09 DOI: 10.1007/s11043-025-09790-z
Masoud K. Darabi, Eisa Rahmani, Eyad A. Masad, Dallas N. Little

Oxidative aging increases the stiffness and brittleness of asphalt pavements, reducing resistance to fracture and fatigue cracking. This study introduces a coupled aging–viscoelastic–viscodamage constitutive model to capture the effects of oxidative aging on the mechanical behavior of asphalt pavements. The model integrates oxygen diffusion, aging time, and temperature into a state variable that modifies viscoelastic compliance, relaxation times, and damage properties. Using a continuum damage mechanics framework, the model effectively couples aging, fatigue damage, and viscoelastic behavior. The proposed model was implemented in a finite-element framework to simulate a 2D axisymmetric asphalt pavement subjected to mechanical pulse loading and oxygen diffusion over ten years. Results show that the simulated unaged pavement exhibits a bottom-to-top cracking pattern, while surface-down cracking dominates in the aged pavement due to oxygen-induced material degradation. Validation against laboratory data demonstrates the model’s ability to predict fatigue life, stiffness evolution, and damage density under various aging conditions. The findings highlight the importance of incorporating oxidative aging effects in pavement performance models to improve design and maintenance strategies for long-term durability.

氧化老化增加了沥青路面的刚度和脆性,降低了抗断裂和疲劳开裂的能力。本研究引入老化-粘弹性-粘损伤耦合本构模型,以捕捉氧化老化对沥青路面力学行为的影响。该模型将氧气扩散、老化时间和温度集成到一个状态变量中,该状态变量可以修改粘弹性顺应性、松弛时间和损伤特性。使用连续损伤力学框架,该模型有效地耦合了老化、疲劳损伤和粘弹性行为。在有限元框架中实现了所提出的模型,以模拟二维轴对称沥青路面在机械脉冲载荷和氧气扩散下的十年。结果表明:模拟未老化路面表现为自下而上的开裂模式,而老化路面主要由氧致材料降解引起的表面向下开裂;对实验室数据的验证表明,该模型能够预测各种老化条件下的疲劳寿命、刚度演变和损伤密度。研究结果强调了将氧化老化效应纳入路面性能模型以改进设计和维护策略以实现长期耐久性的重要性。
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Mechanics of Time-Dependent Materials
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