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Accelerated thermal-oxidative aging and degradation mechanism of high-density polyethylene butt-fusion welded joint 高密度聚乙烯对接熔焊接头的加速热氧化老化和降解机理
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-29 DOI: 10.1007/s11043-023-09655-3
Ying-Chun Chen, Yan-Feng Li, Jie Yang, Yan Xi, Qiang Li, Xiao-li Fan

High-density polyethylene (HDPE) pipelines are widely used for the transportation of natural gas. The butt-fusion welded joints melt and cool during the welding process, resulting in changes in mechanical properties, molecular chain spatial position microstructure, and functional groups. Herein, we investigate the aging behavior of an HDPE butt-fusion welded joint in accelerated thermal-oxidative aging tests under various temperature gradients. The Vicat softening temperature, oxidation induction time, and infrared spectrum were measured, and the microstructures were observed. The results indicated that the mechanical and chemical properties of the butt-fusion welded joint degraded with incresing aging temperature. Analysis was conducted to identify the molecular chain intersection mechanism in the heat-affected zone and the weld joining mechanism. The findings help understand the aging behavior of HDPE and provide guidelines to reduce the risk caused by butt-fusion welded joint degradation.

高密度聚乙烯(HDPE)管道广泛应用于天然气运输。对熔焊接接头在焊接过程中会熔化和冷却,从而导致机械性能、分子链空间位置微观结构和官能团发生变化。在此,我们通过各种温度梯度下的加速热氧化老化试验来研究高密度聚乙烯对熔焊接接头的老化行为。测量了维卡软化温度、氧化诱导时间和红外光谱,并观察了微观结构。结果表明,随着老化温度的升高,对接熔焊接头的机械和化学性能都有所下降。分析确定了热影响区的分子链交叉机制和焊接连接机制。研究结果有助于理解高密度聚乙烯的老化行为,并为降低对接熔接接头降解造成的风险提供指导。
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引用次数: 0
Thermoelectric interactions in Euler–Bernoulli microbeams under the influence of a thermal pulse via the size-dependent couple stress model 欧拉-伯努利微梁在热脉冲影响下通过尺寸相关耦合应力模型产生的热电相互作用
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-28 DOI: 10.1007/s11043-023-09661-5
Ahmed E. Abouelregal, Sami F. Megahid, Doaa Atta, Abdalah M. K. Al-Azmi

A novel comparative examination is conducted on homogeneous flexible microbeams to explore the impact of various electrical voltage sources on their thermomechanical properties. A mathematical model based on the modified couple stress theory has been established, allowing the prediction of size-dependent phenomena observed in microbeam resonators. In addition, the heat transfer inside the microbeam is characterized by the use of a non-Fourier law that involves thermal relaxation, implying an infinite speed of heat propagation. The developed theoretical framework is applied to investigate the thermoelastic response of an Euler–Bernoulli microbeam simply supported at both ends and subjected to a sinusoidal heat pulse. Moreover, a graphene strip, connected to an electrical voltage supply, acts as a heat source at a specific end of the microbeam. The Laplace transform method is used to solve the coupled heat transfer and motion equations. This gives closed formulas that describe the physical fields of thermoelastic microbeams. Numerical case studies are performed in a comparative analysis between the results obtained and those derived from conventional models using graphical representations. Additionally, an investigation is conducted to explore the influence of various factors, such as coupling stress, voltage, electrical resistance, and heat pulses, on the dynamic behavior of all the investigated fields.

对均质柔性微梁进行了一项新颖的比较研究,以探索各种电压源对其热机械特性的影响。基于修正的耦合应力理论建立的数学模型可以预测微梁谐振器中观察到的与尺寸有关的现象。此外,微梁内部传热的特点是使用非傅里叶定律,其中涉及热弛豫,这意味着热传播速度是无限的。所开发的理论框架被用于研究两端简单支撑的欧拉-伯努利微梁在正弦热脉冲作用下的热弹性响应。此外,与电压电源相连的石墨烯带在微梁的特定端部充当热源。拉普拉斯变换法用于求解热传递和运动耦合方程。这给出了描述热弹性微梁物理场的封闭公式。在对所获得的结果与使用图形表示的传统模型得出的结果进行比较分析时,进行了数值案例研究。此外,研究还探讨了耦合应力、电压、电阻和热脉冲等各种因素对所有研究领域动态行为的影响。
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引用次数: 0
Characterization of the thermal, water absorption, and viscoelastic behavior of short date palm fiber reinforced epoxy 短枣椰纤维增强环氧树脂的热性能、吸水性和粘弹性特征
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-28 DOI: 10.1007/s11043-023-09656-2
Khaled Abdessemed, Omar Allaoui, Belhi Guerira, Laala Ghelani

Two epoxy resins (flexible and rigid) with new formulations that are more respectful of the environment are used to make five blends of epoxy resins in different proportions reinforced by 30% date palm fibers (DPF). The purpose is to determine how the blend’s composition and the addition of DPF affect the material’s thermal, water absorption, and viscoelastic properties. It was found that water absorption increases with the increase of flexible epoxy content. The incorporation of DPF multiplies the water absorption by about 6. Thermogravimetric analysis (TGA) revealed that the maximum degradation temperature (Tmax) increases with increasing flexible epoxy content. The incorporation of DPF causes a slight decrease in Tmax. Dynamic mechanical analysis (DMA) showed that raising the amount of flexible epoxy reduces the storage modulus (E’) while expanding the size of the transition zone. Conversely, the incorporation of DPF increases E’ over the studied temperature range. Similarly, increasing the percentage of flexible resin decreases the glass transition temperature (Tg) from 65.15 °C (100% rigid) to 29.75 °C (100% flexible). On the other hand, the incorporation of DPF improves the Tg. Isochronous stress-strain curves revealed that, at room temperature, the R50S50 epoxy (50% flexible + 50% rigid) and the R50S50R composite (R50S50 + 30% DPF) have linear viscoelastic behavior for tensile stress of 0.5 MPa and nonlinear one for higher stresses. The Schapery model was successfully used to model the nonlinear viscoelastic behavior of R50S50 epoxy and R50S50R composite.

两种环氧树脂(柔性和刚性)采用了更环保的新配方,用于制造五种不同比例的环氧树脂混合物,并用 30% 的枣椰纤维(DPF)进行增强。目的是确定混合物的成分和 DPF 的添加如何影响材料的热性能、吸水性能和粘弹性能。研究发现,吸水性会随着柔性环氧树脂含量的增加而增加。热重分析(TGA)显示,最大降解温度(Tmax)随柔性环氧树脂含量的增加而升高。加入 DPF 后,Tmax 会略有下降。动态机械分析(DMA)显示,增加柔性环氧的含量会降低储存模量(E'),同时扩大过渡区的尺寸。相反,在研究的温度范围内,加入 DPF 会增加 E'。同样,增加柔性树脂的比例会降低玻璃化转变温度(Tg),从 65.15 °C(100% 刚性)降至 29.75 °C(100% 柔性)。另一方面,DPF 的加入提高了玻璃化转变温度(Tg)。等时应力-应变曲线显示,在室温下,R50S50 环氧树脂(50% 柔性 + 50% 刚性)和 R50S50R 复合材料(R50S50 + 30% DPF)在拉伸应力为 0.5 兆帕时具有线性粘弹性行为,而在更高应力下则具有非线性行为。Schapery 模型成功地用于模拟 R50S50 环氧树脂和 R50S50R 复合材料的非线性粘弹性行为。
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引用次数: 0
The effect of marine ageing on the mechanical properties of a structural adhesive 海洋老化对结构粘合剂机械性能的影响
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-22 DOI: 10.1007/s11043-023-09653-5

Abstract

The aim of this work is to study the behaviour of a structural adhesive in an aggressive setting such as the marine environment. For this purpose, an ageing procedure is carried out under marine environmental conditions and a comparison of the properties before and after the process is performed. This is especially important as the characteristics of an adhesive can be heavily affected by factors such as temperature and humidity. For the assessment of the mechanical properties of the material bulk tensile tests are conducted, digital image correlation (DIC) is also employed to obtain parameters such as Poisson’s ratio or Young’s modulus. A dynamic mechanical analysis (DMA) is also carried out, on which the time-temperature superposition principle (TTS) is applied to make a long-term prediction of the behaviour of the adhesive, constructing the master curves for dynamic loads by means of a frequency test and for sustained loads through a creep test. This ageing procedure has led to a reduction in the strength of the material, but has also made it more ductile and flexible, while the master curve obtained from the frequency sweeps shows a smaller dependence of frequency in the aged material and the master curve obtained from the creep tests shows a similar behaviour for both the aged and unaged material.

摘要 这项工作的目的是研究结构粘合剂在海洋环境等侵蚀性环境中的行为。为此,在海洋环境条件下进行了老化程序,并对老化前后的特性进行了比较。这一点尤为重要,因为粘合剂的特性会受到温度和湿度等因素的严重影响。为了评估材料的机械性能,我们进行了大量拉伸试验,还采用了数字图像相关技术(DIC)来获取泊松比或杨氏模量等参数。此外,还进行了动态机械分析(DMA),在此基础上应用时间-温度叠加原理(TTS)对粘合剂的行为进行长期预测,通过频率测试构建动态载荷的主曲线,通过蠕变测试构建持续载荷的主曲线。老化过程导致材料强度降低,但也使其更具延展性和柔韧性,而通过频率扫描获得的主曲线显示,老化材料对频率的依赖性较小,通过蠕变试验获得的主曲线显示,老化材料和未老化材料的行为相似。
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引用次数: 0
Magneto-photo-thermoelastic interaction in a slim strip characterized by hereditary features with two relaxation times 细长带中的磁-光-热弹性相互作用,其特点是具有两个弛豫时间的遗传特征
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-21 DOI: 10.1007/s11043-023-09658-0
A. Sur
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引用次数: 0
Modified Moore–Gibson–Thompson Pennes’ bioheat transfer model for a finite biological tissue subjected to harmonic thermal loading 受谐波热负荷影响的有限生物组织的修正摩尔-吉布森-汤普森-潘尼斯生物传热模型
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-19 DOI: 10.1007/s11043-023-09647-3
Sami F. Megahid, Ahmed E. Abouelregal, Hamid M. Sedighi

Medical scientists frequently employ the Pennes bioheat equation as a computational tool to comprehend the intricate dynamics of thermal energy dispersion within living tissues. This equation, endowed with pronounced utility, finds paramount significance in the realm of therapeutic interventions, notably hyperthermia, wherein regulated elevation of tissue temperatures is administered for multifarious medical objectives. The utilization of this technology significantly enhances the optimization of treatment protocols and the preservation of temperature levels within crucial anatomical regions of the human body. To ensure the effectiveness of therapies and to uphold the utmost welfare of patients, meticulous monitoring of the thermal response of tissues subjected to thermal stimuli becomes imperative. This study introduces a mathematical formulation of the Pennes equation, specifically tailored for capturing the biothermal conduction phenomena transpiring in the intricate structure of skin tissue by employing the Moore–Gibson–Thompson (MGT) equation. This model enables accurate predictions of the thermal response of human skin to temperature variations. The key differentiating factor of this model is the incorporation of the concept of time delay. This inclusion serves the purpose of minimizing the rapid propagation of thermal energy within biological tissues, ultimately restricting its diffusion at limited rates. The proposed model is employed to characterize the intricacies of heat transfer in a slender, constrained stratum of skin tissue that is subject to a harmonic thermal stimulus. The computational outcomes are presented with the aid of illustrative figures, effectively highlighting the impact of model parameters on the temperature and deformation distributions within the material.

医学家经常使用彭氏生物热方程作为计算工具,以理解热能在活体组织内分散的复杂动态。该方程具有显著的实用性,在治疗干预领域,尤其是热疗领域,具有极其重要的意义。这项技术的应用极大地促进了治疗方案的优化和人体重要解剖区域温度水平的保持。为了确保治疗的有效性,维护患者的最大福祉,必须对受到热刺激的组织的热反应进行细致的监测。本研究采用摩尔-吉布森-汤普森(MGT)方程,介绍了彭斯方程的数学公式,专门用于捕捉皮肤组织复杂结构中发生的生物热传导现象。该模型能够准确预测人体皮肤对温度变化的热反应。该模型的关键区别在于加入了时间延迟的概念。加入这一概念的目的是尽量减少热能在生物组织内的快速传播,最终限制热能以有限的速度扩散。所提出的模型用于描述受到谐波热刺激的细长、受约束的皮肤组织层中热传递的复杂性。计算结果借助示意图展示,有效地突出了模型参数对材料内部温度和变形分布的影响。
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引用次数: 0
Characterization of the creep behavior and modeling considering viscoelastic-plastic damage of quartz sandstone under thermo-hydro-mechanical conditions 石英砂岩在热-水-机械条件下的蠕变行为特征及粘弹-塑性损伤模型研究
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-14 DOI: 10.1007/s11043-023-09652-6
Haopeng Jiang, Annan Jiang, Tengfei Jiang

Deep underground civil works such as surrounding rocks of oil, gas pipelines and geothermal wellbore that pass through groundwater are often affected by the combined influences of thermal, hydraulic, and mechanical factors. In order to investigate the long-term stability of rock masses of this environment, creep experimental of quartz sandstone under the coupling effect of thermo-hydro-mechanical conditions. The study involved analyzing the long-term creep deformation, isochronous stress-strain curves, and long-term strength variations. Additionally, a fractional-order viscoelastic-plastic creep damage model was developed by integrating statistical damage analysis, Biot’s coefficient, and fractional-order integration theory. This model aimed to characterize the three-stage creep properties of different temperatures and water pressures. The experimental results indicate that the creep strain of quartz sandstone gradually increases with temperature and pore water pressure, while the long-term strength decreases. The axial creep strains of quartz sandstone are 0.330% at 20 °C, 0.381% at 50 °C, 0.448% at 70 °C, and 0.473% at 90 °C, respectively. This observation suggests that the coupled effect of temperature and pore water pressure has caused a certain level of damage to the rock. Furthermore, the proposed creep model effectively captured characteristics subjected to coupling effects of thermo-hydro-mechanical factors. The results provide a relevant reference value for the theoretical study of the creep mechanical behavior of rocks in multi-field environments.

穿越地下水的石油、天然气管道和地热井井筒等深层地下土木工程的围岩通常会受到热力、水力和机械因素的共同影响。为了研究这种环境下岩体的长期稳定性,我们对石英砂岩进行了热-水-机械耦合作用下的蠕变实验。研究包括分析长期蠕变变形、等时应力-应变曲线和长期强度变化。此外,通过综合统计损伤分析、Biot 系数和分数阶积分理论,建立了分数阶粘弹塑性蠕变损伤模型。该模型旨在描述不同温度和水压下的三阶段蠕变特性。实验结果表明,石英砂岩的蠕变应变随温度和孔隙水压力逐渐增大,而长期强度则逐渐减小。石英砂岩的轴向蠕变应变在 20 °C 时分别为 0.330%、50 °C 时为 0.381%、70 °C 时为 0.448%、90 °C 时为 0.473%。这一观测结果表明,温度和孔隙水压力的耦合效应对岩石造成了一定程度的破坏。此外,所提出的蠕变模型有效地捕捉到了热-水-机械因素耦合效应下的特征。研究结果为多场环境下岩石蠕变力学行为的理论研究提供了相关参考价值。
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引用次数: 0
A semi-physical thermodynamic transient rolling resistance model with nonlinear viscoelasticity 具有非线性粘弹性的半物理热力瞬态滚动阻力模型
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-06 DOI: 10.1007/s11043-023-09650-8
Jukka Hyttinen, Rickard Österlöf, Jenny Jerrelind, Lars Drugge

Rolling resistance dictates a large part of the energy consumption of trucks. Therefore, it is necessary to have a sound understanding of the parameters affecting rolling resistance. This article proposes a semi-physical thermodynamic tyre rolling resistance model, which captures the essential properties of rolling resistance, such as transient changes due to temperature effects and the strain-amplitude dependency of the viscous properties. In addition, the model includes cooling effects from the surroundings. Both tyre temperature and rolling resistance are obtained simultaneously in the simulation model for each time step. The nonlinear viscoelasticity in rubber is modelled using the Bergström–Boyce model, where the viscous creep function is scaled with temperature changes. The cooling of the tyre is considered with both convective and radiative cooling. Moreover, the article explains different material parameters and their physical meaning. Additionally, examples of how the model could be used in parameter studies are presented.

滚动阻力决定了卡车能耗的很大一部分。因此,有必要对影响滚动阻力的参数有一个良好的了解。本文提出了一个半物理热力学轮胎滚动阻力模型,该模型捕捉了滚动阻力的基本特性,如温度效应引起的瞬态变化和粘性特性的应变-振幅依赖性。此外,该模型还包括来自周围环境的冷却效应。仿真模型在每个时间步长同时得到轮胎温度和滚动阻力。采用Bergström-Boyce模型对橡胶的非线性粘弹性进行了建模,其中黏性蠕变函数随温度变化而缩放。轮胎的冷却采用对流冷却和辐射冷却两种方式。并对不同的材料参数及其物理意义进行了说明。此外,还举例说明了该模型在参数研究中的应用。
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引用次数: 0
A study of Ni–Ti shape memory alloy-steel fiber hybrid reinforcement in GGBS mortar for corrosion resistance Ni-Ti形状记忆合金-钢纤维复合增强GGBS砂浆耐腐蚀性能的研究
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-12-04 DOI: 10.1007/s11043-023-09651-7
Geethu Elsa Thomas, A. S. Sajith, P. V. Indira

Fiber-reinforced concrete (FRC) has become popular due to its ability to enhance mechanical properties. However, FRC has limitations regarding aging, durability, and corrosion. A superelastic shape memory alloy (SMA) is an alternate reinforcement material that can enhance a structure’s lifespan. This study evaluates the mechanical, durability, and corrosion resistance characteristics of hybrid combinations of nickel–titanium (Ni–Ti) SMA fibers and steel fibers in mortar. Three hybrid fiber combinations (GH1-75% steel fiber+ 25% SMA fiber, GH2-50% steel fiber+50% SMA fiber, and GH3-25% steel fiber+75% SMA fiber) were investigated in this study, with a total of 0.50% fiber volume ratio. To enhance the durability properties of the mortar, ground granulated blast furnace slag (GGBS) was used as a partial replacement for cement. The engineering properties of these hybrid fiber combinations in GGBS mortar were evaluated through compressive strength, flexural strength, and split tensile strength. Durability features were assessed based on acid, sulfate, chloride, and marine water resistance. The results showed that the hybrid mix with a greater quantity of steel fiber (GH1) had superior mechanical properties due to the steel fiber’s greater modulus of elasticity. However, when exposed to an aggressive environment, the hybrid combination with a greater quantity of Ni–Ti SMA fibers (GH3) in mortar showed higher durability and corrosion resistance. The samples from durability studies were further tested for Scanning Electron Microscopy, Energy Dispersive X-ray Spectroscopy, X-Ray Diffraction Analysis, and Fourier Transform Infrared Spectroscopy. The microstructural studies revealed the factors contributing to the enhanced durability and corrosion resistance of Ni–Ti SMA fibers in the composite.

纤维增强混凝土(FRC)因其提高力学性能的能力而受到欢迎。然而,FRC在老化、耐久性和腐蚀方面有局限性。超弹性形状记忆合金(SMA)是一种可以提高结构寿命的替代增强材料。本研究评估了镍钛(Ni-Ti) SMA纤维和钢纤维混合组合砂浆的机械性能、耐久性和耐腐蚀性。本研究研究了三种混合纤维组合(GH1-75%钢纤维+ 25% SMA纤维,GH2-50%钢纤维+50% SMA纤维,GH3-25%钢纤维+75% SMA纤维),纤维体积比为0.50%。为了提高砂浆的耐久性,采用磨碎的矿渣颗粒代替水泥。通过抗压强度、抗折强度和劈裂抗拉强度来评价这些混杂纤维组合在GGBS砂浆中的工程性能。耐久性是根据耐酸、硫酸盐、氯化物和耐海水性能来评估的。结果表明:钢纤维(GH1)用量越大,钢纤维的弹性模量越大,复合材料的力学性能越好;然而,当暴露在恶劣环境中时,在砂浆中加入更多Ni-Ti SMA纤维(GH3)的混合组合具有更高的耐久性和耐腐蚀性。对耐久性研究的样品进行了进一步的扫描电子显微镜、能量色散x射线光谱、x射线衍射分析和傅里叶变换红外光谱测试。显微组织研究揭示了复合材料中Ni-Ti SMA纤维耐久性和耐腐蚀性增强的因素。
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引用次数: 0
Free vibration analysis of bio-inspired helicoid laminated composite plates resting on elastic foundation using isogeometric analysis and artificial neural network 基于等几何分析和人工神经网络的弹性基础仿生螺旋面复合材料层合板自由振动分析
IF 2.5 4区 材料科学 Q2 Engineering Pub Date : 2023-11-27 DOI: 10.1007/s11043-023-09649-1
Ngoc-Tu Do, Truong Thanh Nguyen, Trung Thanh Tran, Pham Binh Le, Quoc-Hoa Pham

The main aim of this study is to further extend isogeometric analysis (IGA) based on higher-order shear deformation theory (HSDT) with Soldatos’s continuous function (f(z)) for examining the free vibration characteristics of bio-inspired helicoid laminated composite (BiHLC) plates resting on elastic foundation (EF). The foundation follows Pasternak’s model with springer stiffness ((k_{1})) and shear stiffness ((k_{2})). The governing equation is derived by using Hamilton’s principle. The performance of the proposed formula is confirmed by comparing the obtained results with those of previous publications. In addition, an artificial neural network (ANN) model is set up by using Matlab software to accurately predict the natural frequencies of BiHLC plates without running code. Finally, some examples are conducted to provide novel results in the free vibration of BiHLC plates with different values of geometrical dimensions, material properties, boundary conditions (BCs), and foundation stiffness.

本研究的主要目的是利用Soldatos的连续函数(f(z))进一步扩展基于高阶剪切变形理论(HSDT)的等几何分析(IGA),以研究基于弹性基础(EF)的仿生螺旋面层合复合材料(BiHLC)板的自由振动特性。基础遵循帕斯捷尔纳克的弹簧刚度((k_{1}))和剪切刚度((k_{2}))模型。利用汉密尔顿原理推导了控制方程。通过将所得结果与已有文献的结果进行比较,证实了所提公式的有效性。此外,利用Matlab软件建立人工神经网络(ANN)模型,无需运行代码即可准确预测bihplc板的固有频率。最后,通过算例对具有不同几何尺寸、材料特性、边界条件和基础刚度值的BiHLC板的自由振动进行了分析,得到了新的结果。
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引用次数: 0
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Mechanics of Time-Dependent Materials
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