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Engineered substrates for metasurface antennas 用于超表面天线的工程基底
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-04-01 DOI: 10.1016/j.addlet.2024.100212
Kelvin J. Nicholson , Ellen Gupta , Colin Bonner , Theodore Fessaras , Mark Mirotznik

This letter explores the advantages of additively manufactured substrates with spatially varying electromagnetic properties. These engineered substrates will be constructed using space filling curves (SFC) of various orders. New advanced manufacturing systems such as the nScrypt 3Dn-300, have enabled the rapid fabrication of these SFC substrates. This letter will apply the engineered SFC substrate to the design and fabrication of metasurface antennas. By utilising a SFC to vary the local substrate permittivity, along with the printed conductive patch dimensions, the range of achievable surface impedances can be greatly expanded. This enlarged design space will be leveraged to yield increased gain for a given metasurface antenna size. Methods to characterise the substrate permittivity and conductive ink are discussed along with a complete description of the metasurface antenna design, fabrication and validation process.

这封信探讨了具有空间变化电磁特性的快速制造基底的优势。这些工程基板将使用不同阶数的空间填充曲线(SFC)来制造。新的先进制造系统(如 nScrypt 3Dn-300 )能够快速制造这些 SFC 基底面。这封信将把工程 SFC 基底应用于元表面天线的设计和制造。通过利用 SFC 改变局部基底介电常数和印刷导电贴片尺寸,可以大大扩展可实现的表面阻抗范围。利用这一扩大的设计空间,可以在给定的元面天线尺寸下获得更高的增益。本文讨论了表征基底介电常数和导电油墨的方法,并完整描述了元表面天线的设计、制造和验证过程。
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引用次数: 0
Acoustic signal monitoring using audible cracking sounds for efficient in-situ crack detection in laser directed energy deposition of hard surfaces 利用可闻裂纹声进行声学信号监测,以便在硬表面激光定向能沉积过程中进行高效的原位裂纹检测
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-04-01 DOI: 10.1016/j.addlet.2024.100210
Hong-Seok Kim, Sang-Hu Park

Laser directed energy deposition (LDED) is a promising way for creating hard surfaces like ceramic-reinforced metal matrix composites (MMC), but it faces a significant challenge in identifying crack formation during the process. As an emerging solution, acoustic signal monitoring is easy to be integrated within the process, and significantly reduces the time needed to detect micro-cracks in as-built MMC surfaces. This study reports on cracking sounds produced while employing LDED with SiC particles on a stainless steel 316 L substrate, examining the sound characteristics across time and frequency domains. Different sound sources in LDED are analyzed in the frequency domain, specifying the suitable frequency range for crack monitoring. Interestingly, the in-process micro-cracking on the hard surfaces produces a distinct audible ‘ping’ sound typically ranging between 12000 and 16000 Hz. By recording this sound, an efficient approach is proposed to identify crack generation during the rapid cooling in the LDED process of hard materials.

激光定向能沉积(LDED)是制造陶瓷增强金属基复合材料(MMC)等硬质表面的一种很有前途的方法,但在工艺过程中识别裂纹的形成却面临着巨大的挑战。作为一种新兴的解决方案,声学信号监测很容易集成到工艺中,并大大缩短了检测竣工 MMC 表面微裂纹所需的时间。本研究报告了在不锈钢 316 L 基材上使用含碳化硅颗粒的 LDED 时产生的裂纹声,并检查了不同时域和频域的声音特征。在频域中分析了 LDED 中的不同声源,确定了适合裂纹监测的频率范围。有趣的是,硬表面上的过程中微裂纹会产生明显的 "乒 "声,频率通常在 12000 到 16000 Hz 之间。通过记录这种声音,提出了一种有效的方法来识别硬质材料在 LDED 过程中快速冷却时产生的裂纹。
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引用次数: 0
Material dependent influence of ring/spot beam profiles in laser powder bed fusion 激光粉末床熔融中环形/点状光束轮廓对材料的影响
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-04-01 DOI: 10.1016/j.addlet.2024.100211
Lova Chechik , Karen Schwarzkopf , Richard Rothfelder , Jonas Grünewald , Michael Schmidt

In recent years, the topic of beam shaping for improved laser material processing has rapidly grown influencing metal laser powder bed fusion (PBF-LB/M). Given the need to reduce the cost and improve control of the PBF-LB/M process to make it more competitive with traditional manufacturing methods, increasing productivity of PBF-LB/M is critical. When research reports a new beam profile (e.g. ring profile) to improve productivity on a specific material, it is often generalised, and assumed to have the capability to improve productivity in PBF-LB/M across the board. In this work, we use both low-fidelity simulations and experimental work to investigate the difference between Gaussian and ring/spot beam profiles on metals with very different thermal properties (a stainless steel and an aluminium alloy). We show that the two materials have opposite responses to the change in beam profile (both in terms of melt pool dimensions and thermal gradients); further, the most beneficial intensity distribution is dependent on the energy input to the material. This exemplifies yet another way in which the PBF-LB/M process is non-linear and contradicts the idea that a ring/spot laser profile is beneficial for all laser processing technologies. This highlights the need for further research into the non-linear effect of varying intensity distributions on laser processing before the benefits of dynamic beam shaping can be truly realised.

近年来,为改进激光材料加工而进行光束整形的课题迅速发展,对金属激光粉末床熔融(PBF-LB/M)产生了影响。鉴于需要降低 PBF-LB/M 工艺的成本并改善其控制,使其与传统制造方法相比更具竞争力,因此提高 PBF-LB/M 的生产率至关重要。当研究报告指出一种新的横梁轮廓(如环形轮廓)可提高特定材料的生产率时,通常会将其推广,并假定其具有全面提高 PBF-LB/M 生产率的能力。在这项工作中,我们利用低保真模拟和实验工作来研究高斯和环形/点状光束剖面在热性能截然不同的金属(不锈钢和铝合金)上的区别。我们发现,这两种材料对光束轮廓变化(熔池尺寸和热梯度)的反应截然相反;此外,最有利的强度分布取决于输入材料的能量。这再次证明了 PBF-LB/M 工艺的非线性,并与环形/点状激光轮廓有利于所有激光加工技术的观点相矛盾。这突出表明,在真正实现动态光束整形的优势之前,需要进一步研究不同强度分布对激光加工的非线性影响。
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引用次数: 0
On the potential of eddy current characterization of the ferritic content of recovered 316L powders after LaserPowder bed fusion fabrication 激光粉末床熔融制造后回收的 316L 粉末中铁素体含量的涡流表征潜力
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-04-01 DOI: 10.1016/j.addlet.2024.100207
R. Saddoud , K. Perlin , N. Sergeeva-Chollet , T. Delacroix , A. Skarlatos , J.P. Garandet

An original container was designed to measure the ferritic content of powder batches by the Eddy Current (EC) technique. As opposed to the standard X-Ray Diffraction (XRD) or Electronic BackScatter Diffraction (EBSD) methods, the EC measurements can be implemented on powder batches of significant sizes, say a hundred grams or so. Using a methodology based on the multiple recycling of an initially ferrite-free virgin powder, it was shown that the EC signals are sensitive to the ferritic content of the recovered powder. On the other hand, in the frequency range scanned by the sensor, the EC signals are virtually independent on the oxygen concentration within the tested powder.

设计了一个原始容器,用于通过涡流(EC)技术测量粉末批次中的铁素体含量。与标准的 X 射线衍射 (XRD) 或电子背散射衍射 (EBSD) 方法不同的是,EC 测量可在相当大的粉末批量(如一百克左右)上进行。使用一种基于对最初不含铁素体的原始粉末进行多次回收的方法,结果表明导电率信号对回收粉末中的铁素体含量非常敏感。另一方面,在传感器扫描的频率范围内,EC 信号几乎不受测试粉末中氧气浓度的影响。
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引用次数: 0
Additive manufacturing of high nitrogen austenitic steel using shell-core strategy 利用壳芯策略快速成型制造高氮奥氏体钢
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-03-20 DOI: 10.1016/j.addlet.2024.100205
L. Becker , F. Radtke , J. Lentz , S. Herzog , C. Broeckmann , S. Weber

Laser Powder Bed Fusion/Metal (PBF-LB/M) is a promising technology for industrial applications, but challenges such as long process times remain. Innovations such as the shell-core approach aim to address this by creating a dense shell around a minimally exposed powder core, significantly reducing processing times, with full densification and property adjustments achieved by subsequent hot isostatic pressing (HIP). This study focuses on the fabrication of shell-core samples using a powder mixture of austenitic steel and Si3N4 to produce high nitrogen steel PBF-LB/M components, which are otherwise difficult to produce due to the limited nitrogen solubility in the melt. PBF-LB/M induces Si3N4 decomposition, resulting in Si and N loss through laser-powder interaction. Si3N4 particles in the still powdered regions serve as a source of N enrichment during HIP, circumventing the limitations of nitrogen solubility in the melt and exploiting the higher solubility in the solid. After HIP, energy dispersive spectrometry and electron backscatter diffraction reveal a fully austenitic matrix with Si diffusion seams mainly in non-laser-exposed areas. The Si3N4 dissolution during HIP contributes to an interstitial dissolved N content of about 0.189 mass%, which, together with the higher Si content, increases hardness. Wavelength dispersive spectrometry (WDS) and nanoindentation line scans show decreasing Si and N concentrations from core to shell, resulting in reduced (nano)hardness in the shell. This innovative approach demonstrates the potential to produce AM components with enhanced properties by overcoming the limitations of nitrogen solubility in the steel melt during PBF-LB/M.

激光粉末床熔融/金属(PBF-LB/M)是一项很有前途的工业应用技术,但仍存在加工时间长等挑战。壳核方法等创新技术旨在解决这一问题,通过在微露的粉末核心周围形成致密外壳,大大缩短了加工时间,并通过随后的热等静压(HIP)实现完全致密化和性能调整。本研究的重点是使用奥氏体钢和 Si3N4 的粉末混合物制造壳芯样品,以生产高氮钢 PBF-LB/M 部件,由于氮在熔体中的溶解度有限,这种部件很难生产。PBF-LB/M 可诱导 Si3N4 分解,通过激光与粉末的相互作用造成硅和氮的损失。在 HIP 过程中,静止粉末区域的 Si3N4 颗粒可作为氮富集源,从而规避熔体中氮溶解度的限制,并利用固体中更高的溶解度。HIP 之后,能量色散光谱仪和电子反向散射衍射显示出完全奥氏体基体,硅扩散缝主要位于非激光暴露区域。在 HIP 过程中,Si3N4 的溶解导致间隙溶解 N 含量达到约 0.189 质量%,这与较高的 Si 含量一起提高了硬度。波长色散光谱法(WDS)和纳米压痕线扫描显示,从内核到外壳,硅和氮的浓度不断下降,导致外壳的(纳米)硬度降低。这种创新方法克服了 PBF-LB/M 过程中钢水中氮溶解度的限制,证明了生产具有更佳性能的 AM 部件的潜力。
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引用次数: 0
Additive friction stir deposition of super duplex stainless steel: Microstructure and mechanical properties 超级双相不锈钢的添加剂搅拌摩擦沉积:微观结构和机械性能
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-03-04 DOI: 10.1016/j.addlet.2024.100204
Meet Gor , Matthew Barnett , Daniel Fabijanic , Pinaki Prasad Bhattacharjee

Additive Friction Stir Deposition (AFSD) is an emerging solid-state metal additive manufacturing (AM) process that offers several key benefits, including high deposition rates and wrought-equivalent mechanical properties even in the as-deposited condition. The work presented is the first study to report on the development of microstructure and mechanical properties of AFSD-processed duplex stainless steel (DSS2507). The banded microstructure of the starting material was remarkably affected by AFSD processing; the austenite grains exhibited a refined and equiaxed morphology, while the ferrite grains appeared slightly larger and elongated. Microstructural observations revealed that the potential mechanism of microstructure evolution in austenite was discontinuous dynamic recrystallization (DDRX), while in ferrite, it was continuous dynamic recrystallization (CDRX). The occurrence of multiple thermal cycles during the AFSD process resulted in σ phase precipitation, which in turn led to considerable variation in mechanical properties with respect to the build direction. The top region of the as-built part with an insignificant σ phase fraction showed improved tensile strength and ductility combination compared to the as-received DSS2507 as well as other AM-processed DSS2507 alloys.

增材摩擦搅拌沉积(AFSD)是一种新兴的固态金属增材制造(AM)工艺,具有多种主要优点,包括沉积速率高,即使在沉积状态下也具有与锻造相当的机械性能。本研究首次报道了 AFSD 加工双相不锈钢 (DSS2507) 的微观结构和机械性能的发展。起始材料的带状微观结构受到 AFSD 加工的显著影响;奥氏体晶粒呈现出细化和等轴的形态,而铁素体晶粒则略微增大和拉长。微结构观察表明,奥氏体微结构演变的潜在机制是不连续动态再结晶(DDRX),而铁素体则是连续动态再结晶(CDRX)。在 AFSD 过程中发生的多次热循环导致了 σ 相析出,这反过来又导致了机械性能在构建方向上的显著变化。与收到的 DSS2507 和其他 AM 加工的 DSS2507 合金相比,σ 相析出不明显的坯件顶部区域显示出更好的拉伸强度和延展性组合。
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引用次数: 0
The role of process parameters and printing position on meltpool variations in LPBF Hastelloy X: Insights into laser-plume interaction 工艺参数和印刷位置对 LPBF 哈氏合金 X 熔池变化的影响:激光与熔池相互作用的启示
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-03-01 DOI: 10.1016/j.addlet.2024.100203
Jian Tang , Rafal Wróbel , Pooriya Scheel , Willy Gaechter , Christian Leinenbach , Ehsan Hosseini

Meltpool dimensions play a pivotal role in defining the defects and microstructure state of Laser Powder Bed Fusion (LPBF) builds. Therefore, it is crucial to investigate variations in meltpool geometries under different process conditions. In this work, we fabricated single tracks of LPBF Hastelloy X (HX) alloy under 36 printing conditions and examined the corresponding cross-section meltpool dimensions at two locations across the build platform. This investigation demonstrates the impacts of laser power, scan speed, powder layer thickness, and printing locations on resultant meltpool dimensions. As expected, we observed that meltpool dimensions increase as laser power increases or scan speed decreases. It was also concluded that thicker powder layers lead to wider and shallower meltpools due to reduced laser energy penetration into the solid beneath the powder layer. Additionally, the meltpool dimensions show variations dependent on deposition locations due to the different levels of interaction of the laser and its induced vapor plume, resulting in shallower and wider meltpools. These findings provide a systematic understanding of meltpool dimension variations across various process conditions for LPBF HX alloy, which ultimately offer insights into the formation of defects and microstructure features.

熔池尺寸在确定激光粉末床熔融(LPBF)构建的缺陷和微观结构状态方面起着关键作用。因此,研究不同工艺条件下熔池几何尺寸的变化至关重要。在这项工作中,我们在 36 种打印条件下制造了 LPBF 哈氏合金 X (HX) 的单轨,并在整个构建平台的两个位置检测了相应的横截面熔池尺寸。这项研究证明了激光功率、扫描速度、粉末层厚度和打印位置对熔池尺寸的影响。正如预期的那样,我们观察到熔池尺寸随着激光功率的增加或扫描速度的降低而增加。我们还得出结论,较厚的粉末层会导致较宽和较浅的熔池,原因是激光能量对粉末层下固体的穿透力降低。此外,由于激光与其诱导的蒸汽羽流的相互作用程度不同,熔池尺寸随沉积位置的不同而变化,从而导致熔池更浅、更宽。这些发现为我们系统地了解 LPBF HX 合金在不同工艺条件下的熔池尺寸变化提供了依据,最终有助于深入了解缺陷和微观结构特征的形成。
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引用次数: 0
Investigating the deformation and microstructural evolution of laser powder-bed fusion of Hastelloy X during high temperature fatigue loading 研究高温疲劳加载过程中激光粉末床融合哈氏合金 X 的变形和微观结构演变
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-02-09 DOI: 10.1016/j.addlet.2024.100201
Reza Esmaeilizadeh , Xiaolong Li , Mathias Kuhlow , Stuart Holdsworth , Ali Keshavarzkermani , Hamid Jahed , Ehsan Toyserkani , Ehsan Hosseini

This study investigates the fatigue behaviour of samples made by laser powder-bed fusion of Hastelloy X (LPBF-HX) with as-built and machined surface conditions at 700 °C under fully reversed strain-controlled cyclic loading. Samples with both surface conditions exhibited initially cyclic hardening followed by cyclic softening under large strain amplitude testing, where a slight continuous hardening was observed for tests with smaller strain amplitudes. The samples with machined surfaces showed longer endurance and higher stress ranges than those with as-built surfaces. Post-fatigue-test EBSD analysis showed the formation of the Goss texture and extensive local strain accumulation in the samples tested under high strain amplitude at 700 °C. Fractography investigations revealed that early crack initiation in the samples with as-built surfaces was from stress concentrations induced by valleys on the rough surface. No evidence of crack initiation induced by pre-existing defects was observed in the machined samples, and the excessive slip activity at the surface was found to be responsible for the crack initiation.

本研究探讨了通过激光粉末床熔融哈氏合金 X(LPBF-HX)制成的样品在 700 °C、完全反向应变控制循环加载条件下的疲劳行为。在大应变振幅试验中,两种表面条件的样品都表现出先循环硬化后循环软化的现象,而在较小应变振幅试验中,则观察到轻微的持续硬化现象。与表面原样相比,表面经过机加工的样品耐久性更长,应力范围更大。疲劳试验后的 EBSD 分析表明,在 700 °C 高应变幅值下进行试验的样品形成了 Goss 纹理和广泛的局部应变累积。断裂学研究表明,"原样表面 "样品的早期裂纹起因于粗糙表面上的凹谷所引起的应力集中。在加工过的样品中,没有观察到由预先存在的缺陷引起的裂纹萌生,而表面过度的滑移活动被认为是裂纹萌生的原因。
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引用次数: 0
Depowdering of an additively manufactured heat exchanger with narrow and turning channels 具有狭窄和转弯通道的添加式制造热交换器的除灰处理
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-02-09 DOI: 10.1016/j.addlet.2024.100202
Wenchao Du, Wenhua Yu, David M. France, Dileep Singh

The evolution of heat exchangers (HXs) manufactured by additive manufacturing techniques is significantly needed. The depowdering solution is a necessity, especially if flow channels are incorporated into the design. In this study, a one-piece HX with multiple layers of internal channels (printed by binder jetting additive manufacturing) was completely depowdered through a developed approach. Each HX channel has a semi-elliptical geometry, four perpendicular turnings along the approximately 200-mm length, and an approximately 80-mm center segment that is inaccessible due to the turnings. To depowder this component, two approaches including the compressed air and the vortex motion were tested first. It was found that the compressed air or vortex motion alone could partially depowder the internal unbound powder of the printed heat exchanger. Consequently, for complete depowdering, a combined approach of the vortex motion and compressed air blowing with multiple cycles was developed and tested. A study of the effect of the vortex duration in each depowdering cycle was conducted, and results showed that an increase from five minutes to ten minutes resulted in a reduced number of stages for a complete depowdering.

采用增材制造技术制造的热交换器(HX)亟待改进。去粉解决方案是必要的,尤其是在设计中加入了流道的情况下。在本研究中,通过开发的方法,对带有多层内部通道的一体式 HX(通过粘合剂喷射增材制造技术打印)进行了完全除粉。每个 HX 通道都具有半椭圆形的几何形状,在约 200 毫米的长度上有四个垂直的转角,中间约 80 毫米的部分由于转角而无法进入。为了对该部件进行除粉,首先测试了两种方法,包括压缩空气和涡流运动。结果发现,仅压缩空气或涡流运动就能对印刷热交换器内部未结合的粉末进行部分除粉。因此,为了实现完全除粉,我们开发并测试了一种涡流运动和压缩空气多次循环喷吹的组合方法。对每个除粉周期中涡流持续时间的影响进行了研究,结果表明,将持续时间从五分钟增加到十分钟,可减少完全除粉的阶段数。
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引用次数: 0
Understanding the role of geometry and interlayer cooling time on microstructure variations in LPBF Ti6Al4V through part-scale scan-resolved thermal modeling 通过部分尺度扫描分辨热建模了解几何形状和层间冷却时间对 LPBF Ti6Al4V 微观结构变化的作用
Q2 ENGINEERING, MANUFACTURING Pub Date : 2024-02-03 DOI: 10.1016/j.addlet.2024.100197
Alaa Olleak , Evan Adcock , Shawn Hinnebusch , Florian Dugast , Anthony D. Rollett , Albert C. To

In this study, we investigated the microstructural variation of Ti-6Al-4 V in inverted pyramid parts built using Laser Powder Bed Fusion (LPBF). Two parts were fabricated with and without ghost parts to study the effects of interlayer delay time on thermal history and microstructure. Finite Element Method (FEM) based process simulation was used to predict the thermal history and cooling rates during the LPBF process to understand the location-specific microstructure and mechanical properties variation. The thermal analysis findings revealed that the variations in the cooling rates and pre-deposition temperature were notably significant. Within the same part, the cooling rates exhibited significant variations, differing by up to three orders of magnitude in two scenarios: (1) within the same layer, influenced by the proximity to the edges, and (2) at different heights, attributable to the strongly varying cross-section. Comparing the two parts, the cooling rates of the part with ghost parts were approximately two orders of magnitude higher than in the part without the ghost parts. This significant difference can be attributed to the extended interlayer cooling time and lower pre-deposition temperature resulting from the presence of two ghost parts which introduced an effective delay time between laser scans. Experimental validation against microstructure images and hardness measurements showed similar trends with the predicted results. These findings provide valuable insights into controlling microstructure at specific locations during LPBF fabrication, which is essential for building complex geometries with controlled material properties.

在这项研究中,我们研究了使用激光粉末床熔融(LPBF)制造的倒金字塔部件中 Ti-6Al-4 V 的微观结构变化。为了研究层间延迟时间对热历史和微观结构的影响,我们分别制造了带幽灵部件和不带幽灵部件的两个零件。基于有限元法(FEM)的工艺模拟用于预测 LPBF 工艺过程中的热历史和冷却速率,以了解特定位置的微观结构和机械性能变化。热分析结果表明,冷却速率和沉积前温度的变化非常明显。在同一零件中,冷却速率变化显著,在两种情况下相差达三个数量级:(1)在同一层内,受靠近边缘的影响;(2)在不同高度,由于截面变化很大。比较两个部件,有幽灵部件的部件的冷却速率比没有幽灵部件的部件高出约两个数量级。这一显著差异可归因于两个幽灵部件的存在延长了层间冷却时间,降低了预沉积温度,从而引入了激光扫描之间的有效延迟时间。根据微观结构图像和硬度测量结果进行的实验验证显示了与预测结果相似的趋势。这些发现为在 LPBF 制作过程中控制特定位置的微观结构提供了有价值的见解,这对于制作具有可控材料特性的复杂几何形状至关重要。
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