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Influence of Lubricated Rolling/Sliding Tribotesting on Hydrogen Trapping in 100Cr6 Bearing Steel 润滑滚动/滑动摩擦试验对 100Cr6 轴承钢中氢捕集的影响
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-28 DOI: 10.1007/s11249-024-01871-3
Lisa-Marie Weniger, Birhan Sefer, Leonardo Pelcastre, Pia Åkerfeldt, Jens Hardell

As hydrogen reduces the fatigue life of 100Cr6 bearing steel significantly, extensive research on the interaction of hydrogen with 100Cr6 is necessary. This study investigated the influence of rolling/sliding tribotesting performed on a micro-pitting-rig on the hydrogen absorption and trapping behaviour of 100Cr6 bearing steel. Thermal desorption mass spectrometry was used to compare the hydrogen desorption spectra of 100Cr6 samples after tribological tests and static heated oil-immersion tests to untested reference samples. The approach was chosen to further understand the influence of both microstructural deformation as well as steel-oil contact on the hydrogen absorption and trapping behaviour of 100Cr6. The tribological test showed a stable friction behaviour and mild wear which was dominated by local plastic deformation of surface asperities. Despite the mild wear, a change in de-trapping temperatures was found for tribotested samples compared to oil-immersed and untested reference samples. This finding indicates that even mild tribotesting conditions alter the hydrogen trapping behaviour of 100Cr6 bearing steel.

由于氢会显著降低 100Cr6 轴承钢的疲劳寿命,因此有必要对氢与 100Cr6 的相互作用进行广泛研究。本研究调查了在微点蚀钻机上进行的滚动/滑动磨擦试验对 100Cr6 轴承钢吸氢和捕氢行为的影响。采用热解吸质谱法比较了 100Cr6 试样在摩擦学测试和静态加热油浸泡测试后与未测试参考试样的氢解吸光谱。选择这种方法是为了进一步了解微结构变形以及钢-油接触对 100Cr6 吸氢和捕氢行为的影响。摩擦学测试表明,摩擦行为稳定,磨损轻微,主要是表面尖角的局部塑性变形。尽管磨损轻微,但与浸油和未测试的参考样品相比,经过摩擦测试的样品的脱捕温度发生了变化。这一发现表明,即使是温和的摩擦试验条件也会改变 100Cr6 轴承钢的氢捕集行为。
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引用次数: 0
Effect of TiC/Bi on Self-Lubricating Properties of Al–Bi-TiC Alloy TiC/Bi 对 Al-Bi-TiC 合金自润滑性能的影响
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-25 DOI: 10.1007/s11249-024-01868-y
Jilin Miao, Yanguo Yin, Congmin Li, Ming Xu, Rongrong Li, Xiaoliang Fang, Shan Huang, Qi Chen

According to the comparative experiments on friction and wear of Al–TiC, Al–Bi (RC) and Al–Bi–TiC alloys, the friction-reduction and wear-resistance mechanisms of TiC/Bi were systematically investigated. The alloys were examined via the scanning electron microscope equipped with an energy dispersive spectrometer and a shape-measuring laser microscope (VK-X100). Basing the achievements, the Bi-phase accumulates on the friction surface with gradual enrichment, possessing anti-friction and self-lubrication on the friction surface. The stable TiC/Bi self-lubricating layer of Al–Bi–TiC alloy make the values of the wear measurements reduce from 82.2 mg to 26.7 mg in 2 h. Meanwhile, TiC particles have uniform load capacity and interfacial pinning properties, which solve the peeling off from the worn surface of Bi-phase.

根据 Al-TiC、Al-Bi(RC)和 Al-Bi-TiC 合金的摩擦和磨损对比实验,系统地研究了 TiC/Bi 的减摩和耐磨机理。通过配备了能量色散光谱仪和形状测量激光显微镜(VK-X100)的扫描电子显微镜对合金进行了检测。研究结果表明,双相在摩擦表面逐渐富集,在摩擦表面具有减摩和自润滑作用。稳定的 TiC/Bi 自润滑层使 Al-Bi-TiC 合金的磨损测量值在 2 h 内从 82.2 mg 降至 26.7 mg,同时 TiC 颗粒具有均匀的承载能力和界面针刺特性,解决了 Bi-phase 从磨损表面剥离的问题。
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引用次数: 0
Tribological and Wear Properties of Cu-Based Composite Reinforced by Core–Shell Structure in Multi-disk Clutch 核壳结构增强的铜基复合材料在多盘离合器中的摩擦学和磨损特性
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-21 DOI: 10.1007/s11249-024-01844-6
Yi Dong, Biao Ma, Cenbo Xiong, Qin Zhao, Hao Chen, Yi Zhang, GuoXin Xie

This work indicates that the core–shell structure is expected to meet the requirements of high friction and low wear for clutches. In the article, two types of core–shell particles are added to Cu-based friction materials for tribological testing. The results showed that as the concentration increased, the coefficient of friction showed a trend of first increasing (from 0.13 to 0.67) and then decreasing (from 0.67 to 0.57). At the same concentration, the COF of carbon coated copper (Cu@C) friction material is 0.4 higher than that of copper coated carbon (C@Cu) friction material, but the wear rate is 43.1% lower. Both materials exhibit high COF but their wear behavior are different due to the distinct components of the friction film.

这项工作表明,核壳结构有望满足离合器高摩擦和低磨损的要求。文章将两种核壳颗粒添加到铜基摩擦材料中进行摩擦学测试。结果表明,随着浓度的增加,摩擦系数呈现先增大(从 0.13 到 0.67)后减小(从 0.67 到 0.57)的趋势。在相同浓度下,碳包铜(Cu@C)摩擦材料的 COF 比碳包铜(C@Cu)摩擦材料高 0.4,但磨损率却低 43.1%。两种材料都表现出很高的 COF,但由于摩擦膜的成分不同,它们的磨损行为也不同。
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引用次数: 0
Quantitative Relationship Between Sliding-Generated Acoustic Emission and Friction Conditions at Bolted Joint Interfaces 滑动产生的声发射与螺栓连接界面摩擦条件之间的定量关系
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-17 DOI: 10.1007/s11249-024-01866-0
Jiaying Sun, Dongwu Li, Huiyi Yang, Chao Xu

Bolted joints are widely used in various engineering structures. The bolted joint may become loosening under long-term oscillating load, and cause reciprocating friction between the contact interfaces. Acoustic emission (AE) is a phenomenon of rapid release of transient elastic waves, which will be generated continuously during the reciprocating friction. The friction conditions will affect the characteristics of the contact interface and the related AE signals. Therefore, analyzing the quantitative relationship between friction conditions and AE signal is significant for applying AE technique in bolt loosening monitoring. However, researches on the relationship between AE Vrms and friction operating parameters are mostly focused on rotating machineries currently, whether the obtained conclusions are suitable for bolted joints is not clear. This paper finds that the commonly used quantitative relationship between the AE Vrms and friction operating parameters is not suitable for bolted joint structures by comparing the theoretical and experimental AE Vrms. The relationship is then modified through exponential parameter fitting and verified using the same experiments in this paper. The results show that the modified equation can accurately describe the quantitative relationship between the AE Vrms and the friction operating parameters, thus revealing the mechanism of acoustic emission signals generated during the gross-slip.

螺栓连接广泛应用于各种工程结构中。螺栓连接在长期振荡载荷作用下可能会出现松动,并导致接触界面之间产生往复摩擦。声发射(AE)是一种快速释放瞬态弹性波的现象,会在往复摩擦过程中持续产生。摩擦条件会影响接触界面的特性和相关的声发射信号。因此,分析摩擦条件与 AE 信号之间的定量关系对于将 AE 技术应用于螺栓松动监测具有重要意义。然而,目前有关 AE Vrms 与摩擦运行参数之间关系的研究大多集中在旋转机械上,所得出的结论是否适用于螺栓连接尚不明确。本文通过比较理论和实验 AE Vrms,发现常用的 AE Vrms 与摩擦运行参数之间的定量关系并不适用于螺栓连接结构。然后通过指数参数拟合修改了这一关系,并使用本文中的相同实验进行了验证。结果表明,修正后的方程能准确描述 AE Vrms 与摩擦运行参数之间的定量关系,从而揭示了毛滑动过程中产生声发射信号的机理。
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引用次数: 0
Insights into the Tribological Properties and Electrical Conductivity of Cu–C Coating Under Grease Lubrication 对油脂润滑下 Cu-C 涂层的摩擦学特性和导电性的深入研究
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-09 DOI: 10.1007/s11249-024-01855-3
Kuo Yang, Yanqiu Xia, Yi Zhang, Wenhao Chen, Xin Feng

In this paper, a Cu–C coating was prepared on a copper substrate through a magnetron sputtering coating process, and the effect of a composite grease containing WS2 and MoS2 on its tribological behavior and electrical conductivity was studied. Experimental results revealed that the Cu–C coating exhibited certain friction-reducing effects under dry sliding conditions with a 5 N load. In the lubricated state with polyurea-based grease, the Cu–C coating demonstrated lower friction coefficients and contact resistances at 2 N and 5 N loads, accompanied by reduced wear rates, indicating a synergistic effect between the lubricant and the coating, enhancing the friction-reducing performance. Furthermore, the incorporation of additives such as WS2 and MoS2 can effectively decrease both friction and contact resistance. Notably, 1% WS2 grease, in combination with Cu–C coating, exhibits superior compatibility, resulting in optimized tribological properties and electrical conductivity. Therefore, the results of this study suggest that the combination of Cu–C coatings with WS2 grease can effectively improve the electrical conductivity and friction-reducing and anti-wear capabilities of Cu–Cu sliding pairs, providing an effective solution for enhancing the electrical conductivity of electric vehicle connectors and improving the overall efficiency of the battery system.

本文通过磁控溅射镀膜工艺在铜基体上制备了 Cu-C 涂层,并研究了含有 WS2 和 MoS2 的复合油脂对其摩擦学行为和导电性能的影响。实验结果表明,Cu-C 涂层在 5 N 负载的干滑动条件下具有一定的减摩效果。在使用聚脲基润滑脂润滑的状态下,Cu-C 涂层在 2 N 和 5 N 负载下的摩擦系数和接触电阻较低,同时磨损率也有所降低,这表明润滑剂和涂层之间存在协同效应,从而提高了减摩性能。此外,添加 WS2 和 MoS2 等添加剂可有效降低摩擦和接触电阻。值得注意的是,1% WS2 润滑脂与 Cu-C 涂层的结合显示出卓越的兼容性,从而优化了摩擦学性能和导电性能。因此,本研究结果表明,Cu-C 涂层与 WS2 润滑脂的结合可有效提高 Cu-Cu 滑动副的导电性、减摩和抗磨损能力,为增强电动汽车连接器的导电性和提高电池系统的整体效率提供了有效的解决方案。
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引用次数: 0
The Effect of Temperature on the Current-Carrying Tribological Behaviour of C/Cu Contact Pairs in High Humidity Environments 温度对高湿度环境中铜/铜接触对载流摩擦学行为的影响
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-07 DOI: 10.1007/s11249-024-01856-2
De-Hui Ji, Li Xiao, Qiang Hu, Siyang Chen, Qiuping Li, Mingxue Shen

The environmental temperature alters the frictional behaviour by changing the state of the current-carrying contact interface, which makes the electrical contact invalid. In this work, the effects of three different temperatures (− 20, 0, 20 °C) on the current-carrying tribological behaviour of C–Cu tribo-pairs in high humidity environment (85%) were discussed. The evolution laws of friction coefficient, wear volume, contact surface properties, and contact resistance of tribo-pairs were studied, and the current-carrying wear mechanism of C–Cu at low temperature was analyzed in depth. The variation of friction coefficient with temperature shows a similar rule before and after current-carrying, that is, regardless of the current, the friction coefficient increases as temperature falls. However, the average friction coefficient at each temperature is lower than that without current. Although it will hasten the material surface's oxidation, a drop in temperature will effectively lessen the transfer behaviour of copper to carbon surface and reduce the wear volume of carbon materials. The amount of copper transferred increases as current rises. Compared with current, the change of temperature has a greater impact on the damage of tribo-pairs. At room temperature, the contact resistance under high current is greater than that of low current. However, the rule is just the opposite under low temperature (0 and − 20 °C). In addition, at 0 °C, although the contact resistance of low current (5 A) decreases significantly in the early stage of friction, its average resistance and fluctuation amplitude are the largest. As the temperature decreases, the current-carrying wear mechanism of C–Cu contact pairs gradually changes from adhesive wear to fatigue wear.

环境温度通过改变载流接触界面的状态来改变摩擦行为,从而使电接触失效。在这项工作中,讨论了三种不同温度(- 20、0、20 °C)对高湿度环境(85%)下 C-Cu 三元对载流摩擦学行为的影响。研究了摩擦系数、磨损量、接触表面性质和三元对接触电阻的演变规律,并深入分析了低温下 C-Cu 的载流磨损机理。摩擦系数随温度的变化在载流前后呈现出相似的规律,即无论电流大小,摩擦系数都随着温度的降低而增大。但是,每个温度下的平均摩擦系数都低于无电流时的摩擦系数。虽然会加速材料表面的氧化,但温度的降低会有效减少铜向碳表面的转移行为,减少碳材料的磨损量。铜的转移量随着电流的升高而增加。与电流相比,温度变化对三元对损坏的影响更大。在室温下,大电流下的接触电阻大于小电流下的接触电阻。但在低温条件下(0 和 -20 °C),情况正好相反。此外,在 0 °C 时,虽然小电流(5 A)的接触电阻在摩擦初期会显著下降,但其平均电阻和波动幅度最大。随着温度的降低,C-Cu 接触对的载流磨损机制逐渐从粘着磨损转变为疲劳磨损。
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引用次数: 0
The Effect of Lubricity of Calcium Sulfonate on ZnDTP and MoDTC 磺酸钙对 ZnDTP 和 MoDTC 润滑性的影响
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-06 DOI: 10.1007/s11249-024-01860-6
Yumi Hayashi, Kaisei Sato, Shinya Sasaki

Reduction of friction and wear by lubrication is necessary to improve the efficiency and prolong the lifespan of industrial machinery. However, several aspects regarding the lubrication effects in additive-combined oil are still unresolved. This study focuses on the effects of combining zinc dialkyldithiophosphate (ZnDTP), molybdenum dithiocarbamate (MoDTC), and Ca sulfonate on the frictional behavior of poly-α-olefin 4 (PAO4) lubricant oils. Ball-on-disk friction tests demonstrated that the exclusive addition of high-base Ca sulfonate solution reduced friction and wear of the lubricating oil. When combined with ZnDTP and MoDTC, the friction coefficients of PAO with high-base and low-base Ca sulfonate are affected by competitive reactions on the sliding surface. Quartz crystal microbalance with dissipation monitoring measurements suggests that high-base Ca sulfonate forms a stronger adsorption film than low-base Ca sulfonate. Atomic force microscope observations confirmed that the addition of low-base Ca sulfonate reduced friction and wear, whereas high-base Ca sulfonate induced competitive reactions with ZnDTP and MoDTC. This study provides valuable insights into the effects of the combination of additives on the lubricity of PAO and their impact on friction and wear characteristics, which are valuable for the design of suitable lubricants for industrial machinery.

要提高工业机械的效率并延长其使用寿命,就必须通过润滑来减少摩擦和磨损。然而,有关添加剂复合油润滑效果的几个方面仍未得到解决。本研究主要探讨了二烷基二硫代磷酸锌(ZnDTP)、二硫代氨基甲酸钼(MoDTC)和磺酸钙复合添加剂对聚-α-烯烃 4(PAO4)润滑油摩擦行为的影响。球盘摩擦试验表明,只添加高碱钙磺酸盐溶液可减少润滑油的摩擦和磨损。当与 ZnDTP 和 MoDTC 结合使用时,PAO 与高碱和低碱 Ca 磺酸盐的摩擦系数会受到滑动表面竞争反应的影响。石英晶体微天平与耗散监测测量表明,高碱磺酸钙形成的吸附膜比低碱磺酸钙更强。原子力显微镜观察证实,添加低碱钙磺酸盐可减少摩擦和磨损,而高碱钙磺酸盐则会诱发与 ZnDTP 和 MoDTC 的竞争反应。本研究就添加剂组合对聚酰胺氧化物润滑性的影响及其对摩擦和磨损特性的影响提供了宝贵的见解,这对设计适用于工业机械的润滑油非常有价值。
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引用次数: 0
Correction to: Roughness Evolution Induced by Third-Body Wear 更正:第三体磨损引起的粗糙度演变
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-03 DOI: 10.1007/s11249-024-01864-2
Joaquin Garcia-Suarez, Tobias Brink, Jean-François Molinari
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引用次数: 0
Numerical and Experimental Study of a Sector-Shaped Surface Texture in Friction Reduction 减摩过程中扇形表面纹理的数值和实验研究
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-03 DOI: 10.1007/s11249-024-01863-3
Yuan Wei, Haoming Yan, Shuang Li, Xuewen Wang

Reducing friction using lubricant is of great significance to reducing energy consumption and extending the life of machinery. Surface texturing is effective to enhance the lubrication condition, and it is crucial to properly design the texture’s morphology. In this study, a sector-shaped surface texture is designed and demonstrated using both numerical and experimental methods. A computational fluid dynamic method based on Navier–Stokes equations and a two-phase cavitation model is performed to evaluate the effect of the texture in the hydrodynamic lift and to optimize the geometrical parameters of the texture. The mechanism associated with the additional hydrodynamic pressure generation is also revealed according to the results of the simulation. Then, pin-on-disk rotary friction experiments are performed on steel disks textured by a femtosecond laser to verify the lubricant effect of the proposed texture. The results of the experiment suggest that the sector-shaped textures reduce friction more than conventional circle-shaped textures, which coincides well with the results of the simulation.

使用润滑剂减少摩擦对降低能耗和延长机械寿命具有重要意义。表面纹理可有效改善润滑条件,而正确设计纹理的形态至关重要。本研究采用数值和实验方法设计并演示了扇形表面纹理。基于纳维-斯托克斯方程和两相空化模型的计算流体动力学方法评估了纹理对流体动力升力的影响,并优化了纹理的几何参数。模拟结果还揭示了产生额外流体动力压力的相关机制。然后,在飞秒激光纹理钢盘上进行了针盘旋转摩擦实验,以验证拟议纹理的润滑效果。实验结果表明,扇形纹理比传统的圆形纹理更能减少摩擦,这与模拟结果非常吻合。
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引用次数: 0
Tribological Investigations on Additively Manufactured Inconel 718 Features with Silicon Carbide Ball: Role of the Tribo-Oxide Layer 碳化硅球对添加式制造 Inconel 718 特征的摩擦学研究:三氧化物层的作用
IF 2.9 3区 工程技术 Q2 ENGINEERING, CHEMICAL Pub Date : 2024-05-02 DOI: 10.1007/s11249-024-01858-0
M. M. Basha, M. R. Sankar, T. S. R. Ch. Murthy, A. K. Sahu, S. Majumdar

The current investigation delved into the friction and wear characteristics of abrasive-finished Inconel 718 alloys fabricated by additive manufacturing and casting methods. Silicon carbide balls were used as counter-body materials for all tribology tests. Variable loads of 10 N, 20 N, and 30 N were applied, along with frequencies of 5 Hz and 15 Hz, while maintaining a 1 mm stroke length for 30 min. Cast samples showed an increase in coefficient of friction (COF) when the load increased from 10 to 20 N at 5 Hz. COF value was decreased from 0.28 to 0.25 when the load was increased from 20 to 30 N while the frequency was maintained at 5 Hz. At the same frequency of 5 Hz, additively manufactured samples displayed a constant increase in COF from 0.19 to 0.35 as the load increased from 10 to 30 N. Consistent COF values were determined at 15 Hz for cast and additively manufactured samples. The COF for cast samples at a frequency of 15 Hz was 0.26, 0.25, and 0.25 for loads of 10 N, 20 N, and 30 N, respectively. For the same loads and frequencies, COF values of 0.23, 0.24, and 0.24 were reported in additively manufactured samples. At 15 Hz, both cast (7.25 × 10–6 mm3/N.m to 9.91 × 10–6 mm3/N.m) and additively manufactured (5.80 × 10–6 mm3/N.m to 6.18 × 10–6 mm3/N.m) samples exhibited constant increasing trends of specific wear rates when the loads increased from 10 to 30 N.

Graphical Abstract

目前的研究深入探讨了通过添加制造和铸造方法制造的磨料加工 Inconel 718 合金的摩擦和磨损特性。所有摩擦学测试均使用碳化硅球作为反体材料。测试中施加了 10 N、20 N 和 30 N 的不同载荷,频率分别为 5 Hz 和 15 Hz,同时在 30 分钟内保持 1 mm 的冲程长度。当负载从 10 牛顿增加到 20 牛顿,频率为 5 赫兹时,铸件样品的摩擦系数(COF)增加。当载荷从 20 牛增加到 30 牛,而频率保持在 5 赫兹时,COF 值从 0.28 降到 0.25。在相同的频率(5 赫兹)下,当载荷从 10 牛增加到 30 牛时,添加剂制造的样品的 COF 值从 0.19 持续增加到 0.35。在 15 Hz 频率下,铸造样品的 COF 值分别为 0.26、0.25 和 0.25,载荷分别为 10 N、20 N 和 30 N。在相同的载荷和频率下,加成型样品的 COF 值分别为 0.23、0.24 和 0.24。在 15 Hz 下,当载荷从 10 N 增加到 30 N 时,铸造样品(7.25 × 10-6 mm3/N.m 到 9.91 × 10-6 mm3/N.m)和添加制造样品(5.80 × 10-6 mm3/N.m 到 6.18 × 10-6 mm3/N.m)的特定磨损率都呈现出持续增长的趋势。
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引用次数: 0
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Tribology Letters
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