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Development of pre-molded internal thread on composite tubes 复合管预成型内螺纹的研制
Pub Date : 2021-01-01 DOI: 10.1177/26349833211000756
A. Takano, R. Kitamura, T. Masai, Sayaka Nishino
Premolded internal threads on composite tubes were developed. The composite tubes with threads on both ends were made using a mandrel with a male thread. The threads can be applied to struts with adjustable end fits and composite pressure vessels with threaded caps that enable disassembly for inspection and repair. Carbon fiber-reinforced plastic (CFRP) prepregs were laid up on a mandrel, wrapped with shrink tape, and cured in an oven. The threads were built-in, without using machine cutting, and the fibers on the thread were continuous through the thread and tubes for high strength. The thread was alternately rounded, convex, and concave in shape to enable CFRP prepregs to be laid up. Two types of specimen were made and tested. The layup sequence of specimen A was [0/h/90/h/0/h(1/2)]s, and that of specimen B was [0/h/90/h/90/h/0/h/90/h/90/h/90/h/90/h/0/h/90/90/0], where “h” denotes a helical layer along the concave part of the threads. The relation between load and strain is nonlinear because of the rounded shape of the threads; however, a simple and closed form analytical model was able to predict the strength of the threads and design of the threads. The model was compared with the experimental results. In addition, an application of threads for the pressure vessel of the hybrid rocket motor is also reported. The combustion test proceeded without failure. Visual inspection after the test indicated that the threads and tubes were not damaged, and thus, they can be applied to high-pressure and high-temperature rocket motors.
研制了复合材料管预成型内螺纹。两端有螺纹的复合管是用带公螺纹的芯轴制成的。螺纹可应用于具有可调末端配合的支柱和具有螺纹帽的复合压力容器,可以拆卸以进行检查和维修。碳纤维增强塑料(CFRP)预浸料铺在芯轴上,用收缩胶带包裹,然后在烤箱中固化。螺纹是内置的,不使用机器切割,螺纹上的纤维连续穿过螺纹和管,强度高。螺纹呈圆形、凸形和凹形交替,使CFRP预浸料得以铺层。制作并测试了两种类型的试样。标本的上篮序列是[0 / h / 90 / h / 0 / h(1/2)],和标本B是[0 / h / 90 /小时/ 90 / h / 0 / h / 90 /小时/ 90 /小时/ 90 /小时/ 90 / h / 0 / h / 90/90/0],“h”表示一个螺旋层沿着凹线程的一部分。由于螺纹呈圆形,载荷与应变之间呈非线性关系;然而,一个简单的和封闭形式的分析模型能够预测螺纹的强度和螺纹的设计。将模型与实验结果进行了比较。此外,还报道了螺纹在混合动力火箭发动机压力容器上的应用。燃烧试验进行得无故障。试验后的目视检查表明,螺纹和管没有损坏,可以应用于高压和高温火箭发动机。
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引用次数: 1
Facile growth of high transmittance ZnO micro-rod clusters on indium tin oxide by a wet-chemical synthesis method 湿化学合成法在氧化铟锡上生长高透射率ZnO微棒团簇
Pub Date : 2021-01-01 DOI: 10.1177/26349833211038954
S. Morkoç Karadeniz
A simple wet-chemical synthesis method was developed to fabricate Zinc oxide micro-rod clusters. The synthesis process involved the rapid dilution of a zinc-bearing alkaline solution at 150°C in a convection oven on indium tin oxide (ITO) substrates. The synthesis was carried out by immersing an unseeded ITO substrate in a mixture of zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and hexamethylenetetramine ((CH2)6N4) aqueous solution. The obtained sample was annealed at 400°C for 2 h. The structural, morphological and optical properties of the synthesized ZnO microstructures were investigated by X-ray diffraction, scanning electron microscopy and ultraviolet-visible spectroscopy, respectively. The ZnO rod clusters are hexagonal phase of the wurtzite structure. The crystal grain sizes of the films were found to be 72.6, 84.3 and 66.3 nm for the (100), (002) and (101) crystal planes, respectively. The optical bandgap of the ZnO was determined to be 3.147 eV.
提出了一种简单的湿化学合成法制备氧化锌微棒簇的方法。合成过程包括在对流烤箱中在氧化铟锡(ITO)衬底上在150°C下快速稀释含锌碱性溶液。将未播种的ITO底物浸入六水硝酸锌(Zn(NO3)2·6H2O)和六亚甲基四胺((CH2)6N4)水溶液的混合物中进行合成。将得到的样品在400℃下退火2 h,分别用x射线衍射、扫描电子显微镜和紫外可见光谱研究合成的ZnO微结构的结构、形态和光学性质。ZnO棒状团簇为六方相纤锌矿结构。在(100)、(002)和(101)晶面上,薄膜的晶粒尺寸分别为72.6、84.3和66.3 nm。ZnO的光学带隙为3.147 eV。
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引用次数: 0
Dynamic mechanical behaviors of epoxy resin/hollow polymeric microsphere composite foams under forced non-resonance and forced resonance 环氧树脂/中空聚合物微球复合泡沫在强制非共振和强制共振下的动态力学行为
Pub Date : 2021-01-01 DOI: 10.1177/26349833211008195
Rui Li, Guisen Fan, Ouyang Xiao, Guojun Wang, Hao Wei
Composite foams with 10–50 vol% hollow polymeric microspheres were prepared using bisphenol A epoxy resin and polyetheramine curing agent as the matrix. The results demonstrated that the density, hardness, and static mechanical properties of the epoxy resin/hollow polymer microsphere composite foams, as well as their dynamic mechanical properties under forced non-resonance, were similar to those of polymer/hollow glass microsphere composite foams. At 25°C and under 1–100 Hz forced resonance, the first-order and second-order resonance frequencies of the composite foams shifted to the low-frequency region as the volume fraction of hollow polymer microspheres increased. Meanwhile, the first-order and second-order loss factors of the as-prepared composite foams were improved by 41.7% and 103.3%, respectively, compared with the pure epoxy resin. Additionally, the first-order and second-order loss factors of the as-prepared composite foams reached a maximum at 40 vol% and 30 vol% hollow polymer microspheres, respectively. This research helps us to expand the application range of composite foam materials in damping research.
以双酚A型环氧树脂和聚醚胺固化剂为基体,制备了体积分数为10 ~ 50%的中空聚合物微球复合泡沫材料。结果表明:环氧树脂/中空聚合物微球复合泡沫的密度、硬度、静态力学性能以及在强制非共振条件下的动态力学性能与聚合物/中空玻璃微球复合泡沫相似;在25℃和1 ~ 100 Hz强制共振条件下,随着空心聚合物微球体积分数的增加,复合泡沫的一阶和二阶共振频率向低频区偏移。与纯环氧树脂相比,复合泡沫材料的一阶和二阶损失系数分别提高了41.7%和103.3%。此外,在所制备的复合泡沫材料的一阶和二阶损失因子分别达到40 vol%和30 vol%的中空聚合物微球的最大值。本研究有助于拓展复合泡沫材料在阻尼研究中的应用范围。
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引用次数: 1
Improving the mechanical properties of polypropylene composites with coconut shell particles 改善椰壳颗粒聚丙烯复合材料的力学性能
Pub Date : 2021-01-01 DOI: 10.1177/26349833211007497
H. C. Obasi, Uchechi C Mark, U. Mark
Conventional inorganic fillers are widely used as fillers for polymer-based composites. Though, their processing difficulties and cost have demanded the quest for credible alternatives of organic origin like coconut shell fillers. Dried shells of coconut were burnt, ground, and sifted to sizes of 63, 150, 300, and 425 µm. The ground coconut shell particles (CSP) were used as a filler to prepare polypropylene (PP) composites at filler contents of 0% to 40% via injection melt blending process to produce PP composite sheets. The effect of the filler particle size on the mechanical properties was investigated. The decrease in the size of filler (CSP) was found to improve the yield strength, tensile strength, tensile modulus, flexural strength, flexural modulus, and hardness of PP by 8.5 MPa, 15.75 MPa, 1.72 GPa, 7.5 MPa, 100 MPa, and 10.5 HR for 63 µm at 40%, respectively. However, the elongation at break and modulus of resilience of the PP composites were seen to increase with increase in the filler size. Scanning electron microscope analysis showed that fillers with 63 µm particle size had the best distribution and interaction with the PP matrix resulting in enhanced properties.
传统无机填料广泛用于聚合物基复合材料的填料。然而,它们的加工困难和成本要求人们寻找可靠的有机替代品,如椰子壳填料。晒干的椰子壳经过燃烧、研磨和筛选,尺寸分别为63、150、300和425微米。以椰壳颗粒(CSP)为填料,采用注射熔融共混法制备了填料含量为0% ~ 40%的聚丙烯(PP)复合材料。研究了填料粒径对复合材料力学性能的影响。填料(CSP)的减小可使PP的屈服强度、抗拉强度、抗拉模量、抗弯强度、抗弯模量和硬度分别提高8.5 MPa、15.75 MPa、1.72 GPa、7.5 MPa、100 MPa和10.5 HR(63µm),提高幅度为40%。而PP复合材料的断裂伸长率和回弹模量随填料尺寸的增大而增大。扫描电镜分析表明,粒径为63µm的填料分布最佳,与PP基体的相互作用也更好。
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引用次数: 6
Fabrication and microstructural analysis of 3A21/7075 aluminum alloy cladding material based on impact jet solid–liquid compound casting 冲击喷射固液复合铸造3A21/7075铝合金包层材料制备及显微组织分析
Pub Date : 2021-01-01 DOI: 10.1177/2633366X20934485
Hu Ming, Ren Xiaoxue, Sun Jian-bo, Z. Yunlong, Teng Chunfeng, Qiao Guang
To solve thickness problem for high-strength aluminum alloy used as plastic mold materials and eliminate oxide film on the surface of aluminum alloy, a new compound casting, namely impact jet solid–liquid compound casting, was developed to fabricate 3A21/7075 aluminum alloy cladding material. Then, optical microscope (OM), electron-backscattered diffraction (EBSD) technique, and transmission electron microscope (TEM) together with energy-dispersive spectrometer (EDS) were used to analyze microstructure of 3A21/7075 aluminum alloy cladding material. The OM and EBSD results showed that the 3A21/7075 aluminum alloy cladding material was composed of 3A21 cladding layer, fusion zone (FZ), heat-affected zone, and 7075 matrix. The grain morphology on both sides of FZ had great differences. Moreover, the TEM and EDS results showed that the 3A21 cladding layer showed a bulk phase and lots of fine and dispersed granular phases, while the 7075 matrix appeared undetermined strip phases and amounts of fine and dispersed rod-like phases. Moreover, FZ existed a great deal of fine and dispersed granular phases and rod-like phases. The 3A21/7075 aluminum alloy cladding material could effectively solve the problems mentioned above and the in-depth analysis of microstructures of 3A21/7075 aluminum alloy cladding material was of great importance in terms of engineering value and academic significance.
为解决高强铝合金作为塑料模具材料的厚度问题,消除铝合金表面氧化膜,研制了一种新型复合铸造方法,即冲击射流固液复合铸造,制备3A21/7075铝合金包层材料。利用光学显微镜(OM)、电子背散射衍射(EBSD)技术、透射电镜(TEM)和能谱仪(EDS)对3A21/7075铝合金包层材料的微观结构进行了分析。OM和EBSD结果表明,3A21/7075铝合金熔覆材料由3A21熔覆层、熔合区(FZ)、热影响区和7075基体组成。FZ两侧的晶粒形态差异较大。TEM和EDS结果表明,3A21熔覆层呈现出块状相和大量细小分散的颗粒相,而7075熔覆层呈现出未确定的条状相和大量细小分散的棒状相。FZ中存在大量细小分散的颗粒相和棒状相。3A21/7075铝合金包层材料可以有效地解决上述问题,深入分析3A21/7075铝合金包层材料的显微组织具有重要的工程价值和学术意义。
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引用次数: 0
Buckling and postbuckling of architectured materials: A review of methods for lattice structures and metal foams 建筑材料的屈曲和后屈曲:晶格结构和金属泡沫的研究方法综述
Pub Date : 2021-01-01 DOI: 10.1177/26349833211003904
C. Völlmecke, M. Todt, Stylianos Yiatros
Recent advances in manufacturing and material science have given rise to numerous architectured materials (archimats), which are tailored for multifunctionality and improved performance. Specifically, lattice structures and metal foams are usually lightweight optimized structural morphologies, which are prone to non-linear instability phenomena, leading to collapse or to a different stable state. This article offers an extensive review of analytical, numerical and experimental methods for investigating buckling and postbuckling in such materials. In terms of analytical modelling, linear elastic and geometrically non-linear models are presented. In numerical analysis, discrete and continuum models are presented, highlighting how numerical modelling can inform design of such materials and finally, experimental methods across different scales are reported, highlighting their merits, depending on the aim of the investigation.
制造业和材料科学的最新进展已经产生了许多建筑材料(archimats),这些材料是为多功能和改进的性能而量身定制的。具体来说,晶格结构和金属泡沫通常是轻量化的优化结构形态,容易出现非线性不稳定现象,导致崩溃或进入不同的稳定状态。本文提供了广泛的分析,数值和实验方法来研究屈曲和后屈曲在这类材料。在解析建模方面,提出了线性弹性模型和几何非线性模型。在数值分析中,提出了离散和连续模型,突出了数值建模如何为这些材料的设计提供信息,最后,根据调查的目的,报告了不同尺度的实验方法,突出了它们的优点。
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引用次数: 4
Vibration suppression analysis and experimental test of additional constrained damping layer in space science experiment cabinet 空间科学实验柜附加约束阻尼层的减振分析与实验试验
Pub Date : 2021-01-01 DOI: 10.1177/2633366X20978659
Haitao Luo, Siwei Guo, Changshuai Yu, Jia Fu, Haochen Wang, Guangming Liu, Zhong Luo
Aiming at the problem that the vibration of the space science experimental cabinet is too large during the launch phase of the rocket, the viscoelastic constrained damping layer is used to suppress the vibration. Firstly, to explore the vibration suppression mechanism of the constrained damping layer, the dynamic model of the constrained damping layer is established and the modal loss factor is calculated. Secondly, the influence of the modulus, material thickness, and the position and the area of the damping layer on the loss factor of the structure is analyzed. Finally, the simulation and experiment methods are used to calculate and verify the space science experiment cabinet with additional constrained damping layer. The results show that the viscoelastic constrained damping can effectively reduce the vibration level of the space science experiment cabinet, and the acceleration response in the resonance region is reduced by more than 56%. The viscoelastic constrained damping structure is simple and easy to realize, which can suppress the vibration of the space payload design is of great significance.
针对火箭发射阶段空间科学实验柜振动过大的问题,采用粘弹性约束阻尼层对其进行抑制。首先,为探索约束阻尼层的减振机理,建立了约束阻尼层的动力学模型,并计算了模态损失因子;其次,分析了模量、材料厚度、阻尼层位置和面积对结构损耗因子的影响;最后,采用仿真和实验相结合的方法对附加约束阻尼层的空间科学实验柜进行了计算和验证。结果表明,粘弹性约束阻尼能有效降低空间科学实验柜的振动水平,共振区加速度响应降低56%以上。粘弹性约束阻尼结构简单,易于实现,对空间有效载荷的振动抑制设计具有重要意义。
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引用次数: 2
Machining precision controlling method for plane surface assisted by SPDT SPDT辅助平面加工精度控制方法
Pub Date : 2021-01-01 DOI: 10.1177/2634983321995509
Jingjin Li, Shijun Ji, Ji Zhao, Fei Yuan, Handa Dai
In traditional processing mode, a given lathe and a set of fixed processing system can only produce a predetermined precision part. This article proposes a machining method that can control the surface precision of machining plane parts, and four gaskets with different accuracy requirements are processed on the same slow tool servo single-point diamond lathe for experimental verification. Then, the Peak Village (PV) value and surface topography of the processed parts were measured using the surface profiler Taylor Hobson PGI 1240 and Keyence VR-3200, respectively. Through the processing and analysis of the measured data, the maximum deviation between the PV value and the given PV value is 2.4 µm, the minimum deviation is 0.4 µm. And the PV value obtained by calculating the helical spacing measured by surface topography according to the method in this article is approximately equal to the measured PV value, so the correctness of the machining method is verified. Therefore, the machining method can control the surface accuracy of machining parts accurately according to the required accuracy.
在传统的加工方式中,给定的车床和一套固定的加工系统只能生产预定精度的零件。本文提出了一种能够控制加工平面零件表面精度的加工方法,并在同一台慢刀伺服单点金刚石车床上加工了4种不同精度要求的垫片进行实验验证。然后,分别使用Taylor Hobson PGI 1240和Keyence VR-3200表面轮廓仪测量加工零件的峰值村(PV)值和表面形貌。通过对实测数据的处理和分析,PV值与给定PV值的最大偏差为2.4µm,最小偏差为0.4µm。根据本文方法计算表面形貌测量的螺旋间距得到的PV值与实测PV值近似相等,从而验证了加工方法的正确性。因此,该加工方法可以根据所要求的精度精确地控制加工零件的表面精度。
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引用次数: 0
3D printing of a continuous fiber-reinforced composite based on a coaxial Kevlar/PLA filament 基于同轴凯夫拉/PLA长丝的连续纤维增强复合材料的3D打印
Pub Date : 2021-01-01 DOI: 10.1177/26349833211000058
Trenton Cersoli, B. Yelamanchi, E. MacDonald, J. G. Carrillo, P. Cortes
Additive manufacturing has allowed for the production of complex and mass customized geometries, but often at the expense of mechanical performance, a penalty which can be in part mitigated with the fabrication of composite parts. Thermoplastic structures fabricated with material extrusion additive manufacturing stand to be improved in terms of fracture toughness with the integration of continuous fibers. The present research program has investigated the production of a continuously reinforced filament to be used in open-source fused filament fabrication systems. Three different volume fractions of Kevlar fibers were incorporated into a polylactic acid (PLA) thermoplastic filament. It was observed that a 20% fiber volume fraction resulted in a doubling of the tensile strength relative to the unreinforced PLA parts. High-velocity impact tests were also performed on the reinforced printed thermoplastic material, and it was observed that the composite with the highest fiber volume fraction provided an impact energy resistance improved by a factor of four, relative to the plain PLA. The reinforced fibers have shown to restrain the penetration of the projectile at velocities similar to those that perforated the unreinforced PLA. The present work has demonstrated the production of printed composites without the need of modifying the extruding systems of a commercial 3D printer. This approach could represent an alternate and feasible process for producing continuously reinforced 3D-printed thermoplastic parts with utility for high-velocity impact applications.
增材制造允许生产复杂和大规模定制的几何形状,但通常以牺牲机械性能为代价,这种损失可以通过复合材料部件的制造部分减轻。材料挤压增材制造的热塑性结构在断裂韧性方面有待于与连续纤维的集成来提高。本研究计划研究了用于开源熔丝制造系统的连续增强长丝的生产。将三种不同体积分数的凯夫拉纤维掺入聚乳酸(PLA)热塑性长丝中。观察到,20%的纤维体积分数导致相对于未增强的PLA部件的抗拉强度增加一倍。对增强印刷热塑性材料也进行了高速冲击试验,观察到纤维体积分数最高的复合材料的抗冲击能量提高了四倍,相对于普通PLA。增强纤维已经显示出抑制弹丸的穿透速度类似于那些穿孔未增强PLA。目前的工作已经证明了生产印刷复合材料,而不需要修改商业3D打印机的挤出系统。这种方法可以代表一种替代和可行的工艺,用于生产连续增强的3d打印热塑性塑料部件,用于高速冲击应用。
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引用次数: 6
An investigation of the mechanical properties and bonding mechanism of Ti/Al-laminated composites fabricated by ultrasonic consolidation 超声固结制备Ti/ al层合复合材料的力学性能及结合机理研究
Pub Date : 2021-01-01 DOI: 10.1177/2633366X20969193
J. Bo, R. Xue-ping, Han Yujie, Hou Hongliang, Wang Yaoqi
Foils such as 1100 aluminum and TC4 titanium were used as matrix materials for ultrasonic consolidation test of dissimilar metal materials, and the samples of Ti/Al-laminated composites were prepared. The effect of amplitude and static pressure on the interfacial bonding strength of Ti/Al foil was studied by adhesion test. The mechanical properties of Ti/Al-laminated composites were tested by electronic universal testing machine. The microstructure of Ti/Al foil interface was observed by transmission electron microscope. The results show that ultrasonic consolidation can achieve a good bonding interface of Ti/Al foil, and the bonding strength of the interface increases first and then decreases with the increase of static pressure, and increases monotonously with the increase of amplitude. The optimum adhesion strength is 58.08 N cm−1. The high temperature deformation constitutive model of Ti/Al-laminated composites is established and verified. The Ti/Al interface has metallurgical bonding, and the inner microstructure of Ti/Al matrix is obviously refined. The surface of titanium foil has formed nanocrystalline.
以1100铝箔和TC4钛箔为基体材料,对异种金属材料进行超声固结试验,制备了Ti/ al层合复合材料样品。通过粘接试验,研究了振幅和静压对Ti/Al箔界面粘接强度的影响。采用电子万能试验机对Ti/ al复合材料的力学性能进行了测试。透射电镜观察了Ti/Al箔界面的微观结构。结果表明:超声固结能使Ti/Al箔形成良好的结合界面,界面结合强度随静压的增加先增大后减小,随振幅的增加而单调增加;最佳粘接强度为58.08 N cm−1。建立并验证了Ti/ al复合材料的高温变形本构模型。Ti/Al界面出现了冶金结合,Ti/Al基体内部组织明显细化。钛箔表面已形成纳米晶。
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引用次数: 1
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Composites and Advanced Materials
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