首页 > 最新文献

Journal of Micromanufacturing最新文献

英文 中文
Micro-texturing on flat and cylindrical surfaces using electric discharge micromachining 利用电火花微加工技术在平面和圆柱表面上进行微纹理加工
Pub Date : 2020-12-21 DOI: 10.1177/2516598420980404
Mahavir Singh, V. Jain, J. Ramkumar
The present work discusses micro-texturing on flat and cylindrical surfaces using the electric-discharge micromachining (EDMM) process. The arrays of micro-dimples are generated on flat Ti-6Al-4V surfaces using a block–electric discharge grinding (block-EDG)–fabricated microtools of an average diameter of 148 µm and 105 µm. Large-area surface texturing on flat Ti-6Al-4V and aluminium surfaces are performed to analyse the variation in water contact angle with varying depths of dimples. Adopting the electric discharge–milling (ED-milling) strategy, micro-pillars of dimensions 242 µm × 166 µm × 50 µm are machined on flat Ti-6Al-4V surfaces. The EDMM process for non-flat surfaces, such as curved (internal and external), spherical and freeform surfaces, is receiving attention in various applications. Machining of the aforementioned surfaces using the EDMM process appears to be problematic, due to the continuous change in curvature, which results in the subsequent spark gap variation. In the present work, processing of cylindrical surfaces for micro-features generation, such as micro-dimple arrays, has been attempted. Arrays of micro-dimples are machined on copper and Ti-6Al-4V cylindrical surfaces. A precise indexing setup is fabricated to hold and index the workpiece at the desired angular positions. Unlike machining on flat surfaces, the relative dimensions of the tool and the workpiece’s curvature result in non-uniform wear at the tool’s end cross-section. Owing to this non-uniform wear of tool electrode caused by the curvature effect of the workpiece, the formation of a microscopic bump/spike is observed on the dimple’s bottom. The depth of the dimple up to which the entire bottom surface of the tool is not exposed to the sparks is defined as its critical depth. For a combination of a tool and a workpiece of diameters 500 µm and 5 mm, respectively, the critical depth of the dimple is found to be 12.53 µm. However, the critical depth increases with a decrease in workpiece diameter, provided the diameter of the tool is constant.
本工作讨论了利用电火花微加工(EDMM)工艺在平面和圆柱表面上的微织构。在Ti-6Al-4V平面上,采用平均直径为148µm和105µm的块放电磨削(block-EDG)制造的微工具产生微凹窝阵列。在平面Ti-6Al-4V和铝表面进行大面积表面织构,分析了水接触角随韧窝深度的变化。采用电火花铣削(ED-milling)策略,在Ti-6Al-4V平面上加工尺寸为242µm × 166µm × 50µm的微柱。非平面的电火花加工,如曲面(内部和外部),球面和自由曲面,在各种应用中受到关注。由于曲率的连续变化,使用EDMM加工上述表面似乎是有问题的,这导致随后的火花间隙变化。在目前的工作中,已尝试处理圆柱表面的微特征生成,如微窝阵列。在铜和Ti-6Al-4V圆柱表面加工微凹窝阵列。制造一个精确的分度装置来保持和分度工件在所需的角度位置。与在平面上加工不同,刀具的相对尺寸和工件的曲率导致刀具末端截面的非均匀磨损。由于工件的曲率效应引起的工具电极的不均匀磨损,在凹窝的底部观察到微观凹凸/尖峰的形成。刀具的整个底面不暴露在火花下的凹痕深度被定义为其临界深度。对于直径分别为500 μ m和5mm的工具和工件的组合,发现韧窝的临界深度为12.53 μ m。然而,在刀具直径一定的情况下,临界深度随着工件直径的减小而增大。
{"title":"Micro-texturing on flat and cylindrical surfaces using electric discharge micromachining","authors":"Mahavir Singh, V. Jain, J. Ramkumar","doi":"10.1177/2516598420980404","DOIUrl":"https://doi.org/10.1177/2516598420980404","url":null,"abstract":"The present work discusses micro-texturing on flat and cylindrical surfaces using the electric-discharge micromachining (EDMM) process. The arrays of micro-dimples are generated on flat Ti-6Al-4V surfaces using a block–electric discharge grinding (block-EDG)–fabricated microtools of an average diameter of 148 µm and 105 µm. Large-area surface texturing on flat Ti-6Al-4V and aluminium surfaces are performed to analyse the variation in water contact angle with varying depths of dimples. Adopting the electric discharge–milling (ED-milling) strategy, micro-pillars of dimensions 242 µm × 166 µm × 50 µm are machined on flat Ti-6Al-4V surfaces. The EDMM process for non-flat surfaces, such as curved (internal and external), spherical and freeform surfaces, is receiving attention in various applications. Machining of the aforementioned surfaces using the EDMM process appears to be problematic, due to the continuous change in curvature, which results in the subsequent spark gap variation. In the present work, processing of cylindrical surfaces for micro-features generation, such as micro-dimple arrays, has been attempted. Arrays of micro-dimples are machined on copper and Ti-6Al-4V cylindrical surfaces. A precise indexing setup is fabricated to hold and index the workpiece at the desired angular positions. Unlike machining on flat surfaces, the relative dimensions of the tool and the workpiece’s curvature result in non-uniform wear at the tool’s end cross-section. Owing to this non-uniform wear of tool electrode caused by the curvature effect of the workpiece, the formation of a microscopic bump/spike is observed on the dimple’s bottom. The depth of the dimple up to which the entire bottom surface of the tool is not exposed to the sparks is defined as its critical depth. For a combination of a tool and a workpiece of diameters 500 µm and 5 mm, respectively, the critical depth of the dimple is found to be 12.53 µm. However, the critical depth increases with a decrease in workpiece diameter, provided the diameter of the tool is constant.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"68 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-12-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"127704810","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 12
Study, analysis, and characterization of ultra-precision diamond tools for single-point diamond turning 单点金刚石车削超精密金刚石刀具的研究、分析与表征
Pub Date : 2020-11-11 DOI: 10.1177/2516598420965338
RamaGopal V. Sarepaka, Sivasakthi Balan, Somaiah Doodala, R. Panwar, D. R. Kotaria
In multiple applications of advanced instrumentation, single-point diamond turning (SPDT) is a popular and effective process to generate novel surfaces with nanometric surface roughness and sub-micron surface irregularities, albeit at a high cost. In SPDT, precision diamond tooling contributes significantly to the process cost escalation. Hence, for SPDT, it is vital to have an optimal precision diamond tool deployment. In this article, details of comprehensive precision diamond tool selection and tool characterization are discussed. Three makes of selected ultra-precision diamond (UPD) tools and standard diamond tools (of a global make), designated as CFT, are considered for this study. In this tool bench-marking exercise, the fabrication of Cu–Be alloy predesigned precision components (PDPCs) of a critical geometry is selected. UPD and CFT tools are deployed to fabricate (under similar machining-metrology conditions) the PDPCs. These diamond tools are evaluated in terms of the quality parameters (variation in radius of curvature, form error, and surface roughness) of the workpieces. Further, to explore the progressive wear of these tools, multiple machining cycles are conducted on these workpieces, and their quality parameters are analyzed. Thus, the precision diamond tools of three makes are benchmarked against the CFT tool. Based on the final outcome of this analysis, suitable recommendations are provided to precision diamond tool manufacturers to improve their product in terms of performance and optimized costs to meet the ever-growing tooling demands of the SPDT community.
在先进仪器的多种应用中,单点金刚石车削(SPDT)是一种流行且有效的工艺,可以产生具有纳米级表面粗糙度和亚微米级表面不规则性的新表面,尽管成本很高。在SPDT中,精密金刚石工具对工艺成本的上升有很大的贡献。因此,对于SPDT来说,拥有最佳精度的金刚石工具部署至关重要。本文详细讨论了综合精密金刚石刀具的选择和刀具特性。本研究考虑了三种选定的超精密金刚石(UPD)工具和标准金刚石工具(全球制造),称为CFT。在这个工具基准测试练习中,选择了临界几何形状的Cu-Be合金预先设计的精密部件(pdpc)的制造。UPD和CFT工具被用于制造pdpc(在类似的加工计量条件下)。这些金刚石工具是根据工件的质量参数(曲率半径的变化、形状误差和表面粗糙度)来评估的。进一步,为了探究这些刀具的渐进磨损,对这些工件进行了多次加工循环,并对其质量参数进行了分析。因此,三个品牌的精密金刚石工具以CFT工具为基准。根据分析的最终结果,为精密金刚石工具制造商提供了合适的建议,以提高其产品的性能和优化成本,以满足SPDT社区不断增长的工具需求。
{"title":"Study, analysis, and characterization of ultra-precision diamond tools for single-point diamond turning","authors":"RamaGopal V. Sarepaka, Sivasakthi Balan, Somaiah Doodala, R. Panwar, D. R. Kotaria","doi":"10.1177/2516598420965338","DOIUrl":"https://doi.org/10.1177/2516598420965338","url":null,"abstract":"In multiple applications of advanced instrumentation, single-point diamond turning (SPDT) is a popular and effective process to generate novel surfaces with nanometric surface roughness and sub-micron surface irregularities, albeit at a high cost. In SPDT, precision diamond tooling contributes significantly to the process cost escalation. Hence, for SPDT, it is vital to have an optimal precision diamond tool deployment. In this article, details of comprehensive precision diamond tool selection and tool characterization are discussed. Three makes of selected ultra-precision diamond (UPD) tools and standard diamond tools (of a global make), designated as CFT, are considered for this study. In this tool bench-marking exercise, the fabrication of Cu–Be alloy predesigned precision components (PDPCs) of a critical geometry is selected. UPD and CFT tools are deployed to fabricate (under similar machining-metrology conditions) the PDPCs. These diamond tools are evaluated in terms of the quality parameters (variation in radius of curvature, form error, and surface roughness) of the workpieces. Further, to explore the progressive wear of these tools, multiple machining cycles are conducted on these workpieces, and their quality parameters are analyzed. Thus, the precision diamond tools of three makes are benchmarked against the CFT tool. Based on the final outcome of this analysis, suitable recommendations are provided to precision diamond tool manufacturers to improve their product in terms of performance and optimized costs to meet the ever-growing tooling demands of the SPDT community.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"84 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-11-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128171392","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Improvement in surface quality of diamond-turned aluminium substrate by using hydrogen peroxide: a molecular dynamics simulation study 过氧化氢改善金刚石转铝基板表面质量的分子动力学模拟研究
Pub Date : 2020-11-05 DOI: 10.1177/2516598420963996
Prabhat Ranjan, Anuj Sharma, R. Balasubramaniam
In this work, the atomic mechanism of chemical treatment on diamond-turned aluminium surface due to aqueous H2O2 is investigated using a reactive molecular dynamics simulation (R-MDS). This study is carried out to understand the mechanism of surface quality improvement of a diamond-turned aluminium workpiece due to chemical treatment. Surface quality improvement is focused to analyse the effect of chemical treatment process for improving surface finish, reflectance and chemical stability of the workpiece. It is observed that the diamond-turned surface contains a higher cohesive energy as compared to atomically smooth surfaces. Chemical treatment does more material removal on nano-peaks with respect to the smooth surface, and this helps to reduce the cohesive energy as low as naturally possible. By applying this treatment, the optical quality of the workpiece gets enhanced drastically. R-MDS also reveals that the nano-peaks of diamond turn machining (DTM) surface can further improve surface finish by using the chemical treatment process, and the same is validated by experiments. Experimental data also support that due to the reduction of surface roughness, reflectance increases in a broad band of wavelength. The present work shows that material removal from the nano-peaks of workpiece occurs due to the oxygen radicals generated from H2O2, which raise the local temperature, followed by temperature-assisted chemical reaction. When most of the nano-peak atoms are removed, further material removal stops. Experimental results also support the mechanism of such process of chemical treatment. Hence, the diamond turned surface can be further improved beyond the capability of the diamond turning process to cater the need for optics and astronomical mirror at-least one step ahead in the domain of ultra-precision manufacturing.
本文采用反应分子动力学模拟(R-MDS)研究了H2O2对金刚石转铝表面化学处理的原子机理。本研究旨在了解化学处理对金刚石车削铝工件表面质量改善的机理。重点分析了化学处理工艺对提高工件表面光洁度、反射率和化学稳定性的效果。与原子光滑表面相比,金刚石表面具有更高的内聚能。相对于光滑的表面,化学处理可以在纳米峰上去除更多的材料,这有助于尽可能自然地降低内聚能。通过这种处理,工件的光学质量得到了极大的提高。R-MDS还揭示了金刚石车削加工(DTM)表面的纳米峰可以通过化学处理工艺进一步提高表面光洁度,并通过实验验证了这一点。实验数据也支持,由于表面粗糙度的降低,反射率在较宽的波长范围内增加。本研究表明,由于H2O2产生的氧自由基提高了局部温度,随后发生了温度辅助化学反应,材料从工件的纳米峰上去除。当大多数纳米峰原子被去除时,进一步的材料去除就停止了。实验结果也支持了这一化学处理过程的机理。因此,金刚石车削表面可以进一步改进,超越金刚石车削工艺的能力,以满足光学和天文反射镜在超精密制造领域至少领先一步的需求。
{"title":"Improvement in surface quality of diamond-turned aluminium substrate by using hydrogen peroxide: a molecular dynamics simulation study","authors":"Prabhat Ranjan, Anuj Sharma, R. Balasubramaniam","doi":"10.1177/2516598420963996","DOIUrl":"https://doi.org/10.1177/2516598420963996","url":null,"abstract":"In this work, the atomic mechanism of chemical treatment on diamond-turned aluminium surface due to aqueous H2O2 is investigated using a reactive molecular dynamics simulation (R-MDS). This study is carried out to understand the mechanism of surface quality improvement of a diamond-turned aluminium workpiece due to chemical treatment. Surface quality improvement is focused to analyse the effect of chemical treatment process for improving surface finish, reflectance and chemical stability of the workpiece. It is observed that the diamond-turned surface contains a higher cohesive energy as compared to atomically smooth surfaces. Chemical treatment does more material removal on nano-peaks with respect to the smooth surface, and this helps to reduce the cohesive energy as low as naturally possible. By applying this treatment, the optical quality of the workpiece gets enhanced drastically. R-MDS also reveals that the nano-peaks of diamond turn machining (DTM) surface can further improve surface finish by using the chemical treatment process, and the same is validated by experiments. Experimental data also support that due to the reduction of surface roughness, reflectance increases in a broad band of wavelength. The present work shows that material removal from the nano-peaks of workpiece occurs due to the oxygen radicals generated from H2O2, which raise the local temperature, followed by temperature-assisted chemical reaction. When most of the nano-peak atoms are removed, further material removal stops. Experimental results also support the mechanism of such process of chemical treatment. Hence, the diamond turned surface can be further improved beyond the capability of the diamond turning process to cater the need for optics and astronomical mirror at-least one step ahead in the domain of ultra-precision manufacturing.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"4 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-11-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"129975890","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Feasibility analysis for granulation of silver using Granshot method 颗粒法制粒银的可行性分析
Pub Date : 2020-11-01 DOI: 10.1177/2516598420931013
Ankit Bairwa, A. Reddy, Gurmeet Singh
Metal granshot is a process that is used to convert metal lumps or scraps into metal grains of uniform sizes and shapes. The concept of metal granulation is based on the heat difference between melting and pouring medium. The commercial uses of metal granules are jewelry making and spray coating of costly metals such as silver, gold, and platinum. The basic aim of the silver granshot process is to get uniform size, shape, and maximum yield of silver metal granules. During processing, the metal gets superheated within vacuum up to viscosity more than 2.2 cP flow out of the minimum diameter orifice and allow to drop in the coolant with high pressurized argon gas. The present study focuses on the granulation of silver and tries to achieve the maximum yield of metal. The shape and size of the granules produced were observed using scanning electron microscopy and the results show that the average diameters of granules are between 1.2 mm and 3.8 mm. Yield is also considered as an important factor for granulation of valuable metals like silver, and after experimentation successfully achieved the 99.9 percent yield. The granulation process of silver will help to ease the trading of metal in the jewelry industry.
金属弹丸是一种将金属块或废料转化为均匀大小和形状的金属颗粒的过程。金属造粒的概念是基于熔化介质和浇注介质之间的热差。金属颗粒的商业用途是珠宝制作和昂贵金属(如银、金和铂)的喷涂。银颗粒工艺的基本目标是获得均匀的尺寸、形状和最大产量的银金属颗粒。在加工过程中,金属在真空中被过热,粘度超过2.2 cP,从最小直径孔流出,并允许用高压氩气滴入冷却剂。本文的研究重点是银的造粒,并试图达到最大的金属产量。用扫描电镜对所制颗粒的形状和大小进行了观察,结果表明,所制颗粒的平均直径在1.2 ~ 3.8 mm之间。产率也被认为是制粒银等贵重金属的重要因素,经过实验成功达到99.9%的产率。白银的造粒过程将有助于缓解珠宝行业的金属交易。
{"title":"Feasibility analysis for granulation of silver using Granshot method","authors":"Ankit Bairwa, A. Reddy, Gurmeet Singh","doi":"10.1177/2516598420931013","DOIUrl":"https://doi.org/10.1177/2516598420931013","url":null,"abstract":"Metal granshot is a process that is used to convert metal lumps or scraps into metal grains of uniform sizes and shapes. The concept of metal granulation is based on the heat difference between melting and pouring medium. The commercial uses of metal granules are jewelry making and spray coating of costly metals such as silver, gold, and platinum. The basic aim of the silver granshot process is to get uniform size, shape, and maximum yield of silver metal granules. During processing, the metal gets superheated within vacuum up to viscosity more than 2.2 cP flow out of the minimum diameter orifice and allow to drop in the coolant with high pressurized argon gas. The present study focuses on the granulation of silver and tries to achieve the maximum yield of metal. The shape and size of the granules produced were observed using scanning electron microscopy and the results show that the average diameters of granules are between 1.2 mm and 3.8 mm. Yield is also considered as an important factor for granulation of valuable metals like silver, and after experimentation successfully achieved the 99.9 percent yield. The granulation process of silver will help to ease the trading of metal in the jewelry industry.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"210 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125358747","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Nanoparticles containing boron and its compounds—synthesis and applications: A review 含硼纳米颗粒及其化合物的合成与应用综述
Pub Date : 2020-11-01 DOI: 10.1177/2516598420965319
Shreyansh Tatiya, Mohit Pandey, S. Bhattacharya
Nanomaterials have already contributed to many innovative products in the consumer markets. Constant efforts are directed at attaining unique morphologies and reduction in size. Exponential growth in research is thus involved in the synthesis of the novel nanomaterials. Boron and its compounds with distinct functional and structural properties find extensive usage in a variety of fields ranging from nuclear technology to electronics, ceramics, etc. Also, due to their non-toxicity, they are considered an attractive intermediate in the healthcare and cosmetic industry. The majority of reviews on boron and its compounds are focused on morphologies and the structure of the boron compound obtained. Here, we offer a comprehensive review of the unique properties of the major boron compounds: boron carbide (B4C), boron nitride (BN), and heterostructures with metals and organic compounds. In each section, we also describe the subsequent synthesis routes and the challenges associated with them. We have also summarized the various morphologies and shapes reported to be associated with boron and its compounds. In recent years, however, primary research on boron nanoparticle (BNP) has focused on non-toxic/greener and energy-efficient synthesis routes. The usage and production of pure BNPs in the industry are very scarce and are often associated with nanoclusters of boron and other elements. The intricate structural design and low purity of the nanoproducts formed make BNP synthesis challenging. Thus, in the last section, we summarize the challenges and outlook of the current research with future prospects in the area of BNP research.
纳米材料已经为消费市场上的许多创新产品做出了贡献。不断的努力是为了获得独特的形态和缩小尺寸。因此,新型纳米材料的合成涉及到指数增长的研究。硼及其化合物具有独特的功能和结构特性,广泛应用于从核技术到电子、陶瓷等各个领域。此外,由于它们的无毒性,它们被认为是医疗保健和化妆品行业有吸引力的中间体。大多数关于硼及其化合物的评论都集中在硼化合物的形态和结构上。本文综述了主要的硼化合物的独特性质:碳化硼(B4C)、氮化硼(BN)以及与金属和有机化合物的异质结构。在每个部分中,我们还描述了随后的合成路线以及与之相关的挑战。我们还总结了与硼及其化合物有关的各种形态和形状。然而,近年来对纳米硼颗粒(BNP)的研究主要集中在无毒/绿色和节能的合成路线上。在工业中,纯BNPs的使用和生产非常稀少,通常与硼和其他元素的纳米团簇有关。复杂的结构设计和形成的纳米产品的低纯度使BNP合成具有挑战性。因此,在最后一节中,我们总结了当前研究的挑战和展望,并展望了BNP研究领域的未来前景。
{"title":"Nanoparticles containing boron and its compounds—synthesis and applications: A review","authors":"Shreyansh Tatiya, Mohit Pandey, S. Bhattacharya","doi":"10.1177/2516598420965319","DOIUrl":"https://doi.org/10.1177/2516598420965319","url":null,"abstract":"Nanomaterials have already contributed to many innovative products in the consumer markets. Constant efforts are directed at attaining unique morphologies and reduction in size. Exponential growth in research is thus involved in the synthesis of the novel nanomaterials. Boron and its compounds with distinct functional and structural properties find extensive usage in a variety of fields ranging from nuclear technology to electronics, ceramics, etc. Also, due to their non-toxicity, they are considered an attractive intermediate in the healthcare and cosmetic industry. The majority of reviews on boron and its compounds are focused on morphologies and the structure of the boron compound obtained. Here, we offer a comprehensive review of the unique properties of the major boron compounds: boron carbide (B4C), boron nitride (BN), and heterostructures with metals and organic compounds. In each section, we also describe the subsequent synthesis routes and the challenges associated with them. We have also summarized the various morphologies and shapes reported to be associated with boron and its compounds. In recent years, however, primary research on boron nanoparticle (BNP) has focused on non-toxic/greener and energy-efficient synthesis routes. The usage and production of pure BNPs in the industry are very scarce and are often associated with nanoclusters of boron and other elements. The intricate structural design and low purity of the nanoproducts formed make BNP synthesis challenging. Thus, in the last section, we summarize the challenges and outlook of the current research with future prospects in the area of BNP research.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"6 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"114091371","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 7
Experimental and numerical investigation of difference in diameter enlargement and circularity of micro-holes drilled by flexural spindle head 弯曲主轴头钻孔微孔扩径和圆度差异的实验与数值研究
Pub Date : 2020-11-01 DOI: 10.1177/2516598420964049
S. Shinde, R. Lekurwale
The flexural bearing or the flexural cartridge allows very nano-meter axial displacement movement, which is frictionless and noiseless. The repeatability of the mechanism obtained is achieved by bending of the load element. The bearing can operate under stringent conditions such as vacuum, elevated temperatures (0–40 °C), and moist conditions. Hence, due to these indigenous properties, these bearings are observed in applications such as linear bearing of linear compressor, flexural bearing electromagnetic linear actuator, and parasitic error-free mechanism. The endorsed capability of obtaining high-level positional accuracy along with repeatability leads to design and development of low-cost flexural cartridge for micro-drilling spindle head. This flexural cartridge provides a linear guideway while feeding inside the test specimen (in micro-drilling operation). The designed head dampens and nullifies the force, acting on the shaft carrying the micro-tool. The designed spindle head carrying the three-leg spiral flexural stack is assembled on the designed machine tool. The run out measured on the spindle shaft is 50 µm. Four test specimens, namely aluminum, brass, acrylic and mild steel, are drilled by three drills of diameter 1 mm, 0.8 mm, and 0.5 mm each. The main objective of the article is to understand the differential analysis of diameter enlargement and circularity between the experimental method and the numerical method. The answers predicted by the experimental method may have second possible value as it depends upon judgment of inscribing the circle/points in the computer-aided design (CAD) environment. This ambiguity is excluded by the MATLAB code, which gives one specific answer. The maximum difference in diameter enlargement for aluminum, brass, acrylic, and mild steel specimens are 3.8 µm, 11 µm, 24.6 µm, and 16.1 µm, respectively, whereas the maximum difference in circularity for the same specimens is 11.8 µm, 1.3 µm, 8.2 µm, and 16.8 µm, respectively. This difference is termed as the |error|.
弯曲轴承或弯曲弹匣允许非常纳米的轴向位移运动,这是无摩擦和无噪音的。所获得的机构的重复性是通过加载元件的弯曲来实现的。轴承可以在真空,高温(0-40°C)和潮湿条件等严格条件下运行。因此,由于这些固有特性,这些轴承在线性压缩机的线性轴承,弯曲轴承电磁线性执行器和寄生无误差机构等应用中被观察到。由于具有较高的定位精度和可重复性,微钻主轴头用低成本弯曲装盒的设计和开发成为可能。这种弯曲药筒提供了一个线性导轨,同时在试样内部喂入(在微钻孔操作中)。设计的头部阻尼和抵消力,作用在承载微工具的轴上。所设计的主轴头携带三脚螺旋弯曲堆装配在所设计的机床上。在主轴轴上测量的偏差为50µm。用直径分别为1mm、0.8 mm、0.5 mm的三把钻头钻取铝、黄铜、亚克力、低碳钢四种试件。本文的主要目的是了解实验方法和数值方法对直径扩大和圆度的差异分析。实验方法预测的答案可能具有第二种可能的价值,因为它取决于在计算机辅助设计(CAD)环境中对圆/点的刻划判断。这种模糊性被MATLAB代码排除,它给出了一个具体的答案。铝、黄铜、亚克力和低碳钢试件的最大直径增大差异分别为3.8µm、11µm、24.6µm和16.1µm,而相同试件的最大圆度差异分别为11.8µm、1.3µm、8.2µm和16.8µm。这种差异被称为“错误”。
{"title":"Experimental and numerical investigation of difference in diameter enlargement and circularity of micro-holes drilled by flexural spindle head","authors":"S. Shinde, R. Lekurwale","doi":"10.1177/2516598420964049","DOIUrl":"https://doi.org/10.1177/2516598420964049","url":null,"abstract":"The flexural bearing or the flexural cartridge allows very nano-meter axial displacement movement, which is frictionless and noiseless. The repeatability of the mechanism obtained is achieved by bending of the load element. The bearing can operate under stringent conditions such as vacuum, elevated temperatures (0–40 °C), and moist conditions. Hence, due to these indigenous properties, these bearings are observed in applications such as linear bearing of linear compressor, flexural bearing electromagnetic linear actuator, and parasitic error-free mechanism. The endorsed capability of obtaining high-level positional accuracy along with repeatability leads to design and development of low-cost flexural cartridge for micro-drilling spindle head. This flexural cartridge provides a linear guideway while feeding inside the test specimen (in micro-drilling operation). The designed head dampens and nullifies the force, acting on the shaft carrying the micro-tool. The designed spindle head carrying the three-leg spiral flexural stack is assembled on the designed machine tool. The run out measured on the spindle shaft is 50 µm. Four test specimens, namely aluminum, brass, acrylic and mild steel, are drilled by three drills of diameter 1 mm, 0.8 mm, and 0.5 mm each. The main objective of the article is to understand the differential analysis of diameter enlargement and circularity between the experimental method and the numerical method. The answers predicted by the experimental method may have second possible value as it depends upon judgment of inscribing the circle/points in the computer-aided design (CAD) environment. This ambiguity is excluded by the MATLAB code, which gives one specific answer. The maximum difference in diameter enlargement for aluminum, brass, acrylic, and mild steel specimens are 3.8 µm, 11 µm, 24.6 µm, and 16.1 µm, respectively, whereas the maximum difference in circularity for the same specimens is 11.8 µm, 1.3 µm, 8.2 µm, and 16.8 µm, respectively. This difference is termed as the |error|.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"5 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-11-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"131040213","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 3
Freeform machining of ophthalmic toric lens mould using fast tool servo-assisted ultra-precision diamond turning process 用快速刀具伺服辅助超精密金刚石车削工艺加工眼晶状体模具
Pub Date : 2020-10-12 DOI: 10.1177/2516598420939745
I. Singh, G. S, T. N. Reddy, P. Vinod
This research aims to establish a methodology for machining of toric lenses, using fast tool servo-assisted single point diamond turning and to assess the generated surface for its characteristics. Using the established mathematical model, toric surface is explained to understand the geometry and to generate the parameters required for fast tool servo machining. A toric surface with a major diameter of 18.93 mm and a minor diameter of 15.12 mm has been cut on the intelligent ultra-precision turning machine (iUPTM). The surface profile and surface roughness were measured. After analysing the measurement data of the machined surface, on two perpendicular axes of the toric lens, form accuracy of 0.49 µm peak-to-valley (PV), and surface roughness of 12 nm in Ra, 4–8 nm in Sa are obtained. From the experimental results obtained, it can be concluded that the proposed method is a reasonable alternative for manufacturing toric lens mould.
本研究旨在建立一种利用快速刀具伺服辅助单点金刚石车削加工环面透镜的方法,并评估其生成表面的特性。利用建立的数学模型,对环形曲面进行了解释,以理解几何形状并生成快速刀具伺服加工所需的参数。在智能超精密车床(iUPTM)上加工了一个长径18.93 mm、小径15.12 mm的环形表面。测量了表面轮廓和表面粗糙度。通过对加工表面的测量数据进行分析,在环面透镜的两个垂直轴上,获得了0.49µm的峰谷(PV)精度,Ra的表面粗糙度为12 nm, Sa的表面粗糙度为4 ~ 8 nm。实验结果表明,该方法是制造环面透镜模具的一种合理选择。
{"title":"Freeform machining of ophthalmic toric lens mould using fast tool servo-assisted ultra-precision diamond turning process","authors":"I. Singh, G. S, T. N. Reddy, P. Vinod","doi":"10.1177/2516598420939745","DOIUrl":"https://doi.org/10.1177/2516598420939745","url":null,"abstract":"This research aims to establish a methodology for machining of toric lenses, using fast tool servo-assisted single point diamond turning and to assess the generated surface for its characteristics. Using the established mathematical model, toric surface is explained to understand the geometry and to generate the parameters required for fast tool servo machining. A toric surface with a major diameter of 18.93 mm and a minor diameter of 15.12 mm has been cut on the intelligent ultra-precision turning machine (iUPTM). The surface profile and surface roughness were measured. After analysing the measurement data of the machined surface, on two perpendicular axes of the toric lens, form accuracy of 0.49 µm peak-to-valley (PV), and surface roughness of 12 nm in Ra, 4–8 nm in Sa are obtained. From the experimental results obtained, it can be concluded that the proposed method is a reasonable alternative for manufacturing toric lens mould.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"4 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-10-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"128775688","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 2
An analytical modelling of cutting forces in orthogonal elliptical vibration cutting 正交椭圆振动切削的切削力解析模型
Pub Date : 2020-10-12 DOI: 10.1177/2516598420936131
Arvind Shivaji Shirale, S. Sahu, S. Patel, J. Ramkumar, S. Shekhar
In the present work, an analytical model is proposed to predict the cutting forces in elliptical vibration cutting (EVC). In general, cutting force in metal cutting is a function of the shear angle (φ) and shear strength (τ) of the material. However, these parameters vary dynamically over a cutting cycle of EVC. In this work, the shear angle has been modelled based on the plasticity theory of maximum shear stress criteria. For transient shear strength prediction, the Johnson–Cook model is used. This model predicts shear strength for time-varying strain and strain rate in EVC. The obtained analytical results of cutting forces were compared with experimental results published in the literature and found to be in good agreement (within 12% error) with them. Based on the proposed model, the cutting forces can be modelled as a function of cutting process parameters (depth of cut, cutting velocity), tool parameter (rake angle), physical and thermo-mechanical properties for different materials, without any experimental inputs from EVC.
本文提出了椭圆振动切削中切削力的解析模型。一般来说,金属切削中的切削力是材料剪切角(φ)和剪切强度(τ)的函数。然而,这些参数在EVC的切割周期内是动态变化的。在这项工作中,剪切角是基于最大剪应力准则的塑性理论建模的。暂态抗剪强度预测采用Johnson-Cook模型。该模型预测了随时间变化的应变和应变速率下EVC的抗剪强度。将得到的切削力分析结果与文献中发表的实验结果进行比较,发现两者吻合较好(误差在12%以内)。基于所提出的模型,切削力可以建模为切削工艺参数(切削深度、切削速度)、刀具参数(前倾角)、不同材料的物理和热机械性能的函数,而无需任何EVC的实验输入。
{"title":"An analytical modelling of cutting forces in orthogonal elliptical vibration cutting","authors":"Arvind Shivaji Shirale, S. Sahu, S. Patel, J. Ramkumar, S. Shekhar","doi":"10.1177/2516598420936131","DOIUrl":"https://doi.org/10.1177/2516598420936131","url":null,"abstract":"In the present work, an analytical model is proposed to predict the cutting forces in elliptical vibration cutting (EVC). In general, cutting force in metal cutting is a function of the shear angle (φ) and shear strength (τ) of the material. However, these parameters vary dynamically over a cutting cycle of EVC. In this work, the shear angle has been modelled based on the plasticity theory of maximum shear stress criteria. For transient shear strength prediction, the Johnson–Cook model is used. This model predicts shear strength for time-varying strain and strain rate in EVC. The obtained analytical results of cutting forces were compared with experimental results published in the literature and found to be in good agreement (within 12% error) with them. Based on the proposed model, the cutting forces can be modelled as a function of cutting process parameters (depth of cut, cutting velocity), tool parameter (rake angle), physical and thermo-mechanical properties for different materials, without any experimental inputs from EVC.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"10 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-10-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"130054373","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Effect of machining parameters and vibration on polymethylmethacrylate curved surface in single-point diamond turning 单点金刚石车削加工参数和振动对聚甲基丙烯酸甲酯曲面的影响
Pub Date : 2020-10-12 DOI: 10.1177/2516598420941728
K. Mahajan, R. Pawade
Single-point diamond turning (SPDT) is an emerging process for achieving nanometric surface finish, required in various optical devices made from metals like aluminum, copper, and nonmetals like polymers. The optical devices are manufactured in different shapes and profiles, preferably flat and curved surfaces. During the manufacturing of optical devices, controllable and noncontrollable parameters affect the desired surface finish. In this article, controllable machining parameters such as the incremental distance of X slide, feed rate, spindle speed, and depth of cut are selected to study their effect on surface finish and vibration generation of the curved surface. The chosen workpiece material is polymethylmethacrylate (PMMA). Design of experiment (DoE) is used to find out the optimum parameters of surface finish and infeed vibration responses. According to the Taguchi and analysis of Variance (ANOVA) analysis, the feed rate is the most influencing parameter for surface roughness, and incremental distance is for infeed vibration. A confirmation test is carried out to verify the experimental responses with a mathematical regression model, and it shows a close difference within 2.7 percent. Further, minimum surface roughness is perceived as 12.4 nm, corresponding to an infeed vibration amplitude of 4.9 µm/s2, which is signified at a lower frequency.
单点金刚石车削(SPDT)是一种用于实现纳米级表面光加工的新兴工艺,用于由铝、铜等金属和聚合物等非金属制成的各种光学器件。所述光学器件以不同的形状和轮廓制造,优选为平面和曲面。在光学器件的制造过程中,可控和不可控制的参数会影响期望的表面光洁度。本文选取X滑块增量距离、进给速度、主轴转速、切削深度等可控加工参数,研究其对曲面光洁度和曲面振动产生的影响。所选择的工件材料是聚甲基丙烯酸甲酯(PMMA)。采用试验设计法(DoE)确定了表面光洁度和进给振动响应的最佳参数。根据田口和方差分析(ANOVA)分析,进给速度是影响表面粗糙度的最大参数,增量距离是影响进给振动的最大参数。用数学回归模型对实验响应进行了验证试验,结果表明,两者之间的差异在2.7%以内。此外,最小表面粗糙度为12.4 nm,对应于4.9 μ m/s2的进给振动幅值,这是在较低的频率下表示的。
{"title":"Effect of machining parameters and vibration on polymethylmethacrylate curved surface in single-point diamond turning","authors":"K. Mahajan, R. Pawade","doi":"10.1177/2516598420941728","DOIUrl":"https://doi.org/10.1177/2516598420941728","url":null,"abstract":"Single-point diamond turning (SPDT) is an emerging process for achieving nanometric surface finish, required in various optical devices made from metals like aluminum, copper, and nonmetals like polymers. The optical devices are manufactured in different shapes and profiles, preferably flat and curved surfaces. During the manufacturing of optical devices, controllable and noncontrollable parameters affect the desired surface finish. In this article, controllable machining parameters such as the incremental distance of X slide, feed rate, spindle speed, and depth of cut are selected to study their effect on surface finish and vibration generation of the curved surface. The chosen workpiece material is polymethylmethacrylate (PMMA). Design of experiment (DoE) is used to find out the optimum parameters of surface finish and infeed vibration responses. According to the Taguchi and analysis of Variance (ANOVA) analysis, the feed rate is the most influencing parameter for surface roughness, and incremental distance is for infeed vibration. A confirmation test is carried out to verify the experimental responses with a mathematical regression model, and it shows a close difference within 2.7 percent. Further, minimum surface roughness is perceived as 12.4 nm, corresponding to an infeed vibration amplitude of 4.9 µm/s2, which is signified at a lower frequency.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"126 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-10-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"125580617","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Experimental investigations on ultra-precision machining of polycarbonate and related issues 聚碳酸酯超精密加工及相关问题的实验研究
Pub Date : 2020-10-05 DOI: 10.1177/2516598420938495
V. Mishra, Rohit Sharma, K. Mahajan, J. Kumar, Neha Khatri, Anikate Gupta, H. Garg, V. Karar, R. Pawade, RamaGopal V. Sarepaka
Optical plastic lenses are progressively substituting glass optics due to their lightweight and low costs. Polycarbonate (PC) is considered as one of the leading optical materials due to its good mechanical and optical properties. Ultra-precision machining is the most suited process to develop PC optical components. Nevertheless, ultra-precision machining is considered as one of the deterministic processes to ensure the surface quality required for optical components. However, it is important to understand the behavior of the material during each stage of manufacturing. PC offers many challenges during its processing to achieve the nanometric finish and sub-micron form accuracies. In this article, the various issues of PC machining are discussed through experimental investigations. The effect of machining variables, that is, machining parameters, cutting temperature, and vacuum clamping on surface quality is studied. The results show the importance of the selection of optimum conditions for machining PC with good surface quality. The PC optical component is developed with surface finish (Ra) 18.1 nm and profile accuracies (Pv) of 0.116 µm. The study is helpful to understand the various issues involved in PC machining and hence to minimize their effects on surface quality.
光学塑料透镜由于其轻量化和低成本正逐渐取代玻璃光学。聚碳酸酯(PC)由于其良好的机械性能和光学性能而被认为是光学材料的主导之一。超精密加工是最适合开发PC光学元件的工艺。然而,超精密加工被认为是保证光学元件表面质量的决定性工艺之一。然而,了解材料在制造的每个阶段的行为是很重要的。PC在实现纳米光洁度和亚微米形状精度的加工过程中提出了许多挑战。本文通过实验研究,讨论了PC机加工中的各种问题。研究了加工参数、切削温度、真空夹紧等加工变量对表面质量的影响。结果表明,选择最佳加工条件对加工具有良好表面质量的PC至关重要。PC光学元件的表面光洁度(Ra)为18.1 nm,轮廓精度(Pv)为0.116µm。该研究有助于理解PC加工中涉及的各种问题,从而最大限度地减少它们对表面质量的影响。
{"title":"Experimental investigations on ultra-precision machining of polycarbonate and related issues","authors":"V. Mishra, Rohit Sharma, K. Mahajan, J. Kumar, Neha Khatri, Anikate Gupta, H. Garg, V. Karar, R. Pawade, RamaGopal V. Sarepaka","doi":"10.1177/2516598420938495","DOIUrl":"https://doi.org/10.1177/2516598420938495","url":null,"abstract":"Optical plastic lenses are progressively substituting glass optics due to their lightweight and low costs. Polycarbonate (PC) is considered as one of the leading optical materials due to its good mechanical and optical properties. Ultra-precision machining is the most suited process to develop PC optical components. Nevertheless, ultra-precision machining is considered as one of the deterministic processes to ensure the surface quality required for optical components. However, it is important to understand the behavior of the material during each stage of manufacturing. PC offers many challenges during its processing to achieve the nanometric finish and sub-micron form accuracies. In this article, the various issues of PC machining are discussed through experimental investigations. The effect of machining variables, that is, machining parameters, cutting temperature, and vacuum clamping on surface quality is studied. The results show the importance of the selection of optimum conditions for machining PC with good surface quality. The PC optical component is developed with surface finish (Ra) 18.1 nm and profile accuracies (Pv) of 0.116 µm. The study is helpful to understand the various issues involved in PC machining and hence to minimize their effects on surface quality.","PeriodicalId":129806,"journal":{"name":"Journal of Micromanufacturing","volume":"42 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2020-10-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"114970336","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
期刊
Journal of Micromanufacturing
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1