Pub Date : 2026-01-23DOI: 10.1016/j.jfca.2026.108911
Jiawei Su , Zhenke Yi , Yingxuan Zeng , He Wang , Ronghua Mo , Yuting Liang , Qiting Qiu , Kailin Xu , Kang Wang , Yingxia Wu , Xinyan Zhu , Tuerxun Subi , Zhifeng Zhou , Jufeng Ye
This study evaluated heavy metal contamination and health risks in tea consumed in Guangzhou. Fifty tea samples (green, black, oolong, and dark) from three districts were digested using an optimized microwave protocol with diluted nitric acid (∼42 % HNO₃), achieving complete matrix decomposition, stable recoveries (95–110 %), and reduced acid use. ICP-MS quantified As, Cd, Cr, Cu, and Pb, while Hg was measured using an automatic mercury analyzer. Metals were detected in 96–100 % of samples, with mean concentrations (mg/kg) following Cu > Cr > Pb > As > Cd > Hg. Dark tea accumulated the highest levels, and district differences reflected environmental contamination, with no significant tea variety × district interaction. Health risk assessment showed non-carcinogenic risks (HI) within acceptable limits for all groups, whereas total carcinogenic risk (TCR) exceeded 1 × 10⁻⁴ in several tea types, particularly among females (Green: 1.34 ×10⁻⁴; Black: 1.25 ×10⁻⁴; Dark: 2.10 ×10⁻⁴) compared with males (Green: 1.16 ×10⁻⁴; Black: 1.08 ×10⁻⁴; Dark: 1.82 ×10⁻⁴), highlighting potential long-term carcinogenic concerns. Arsenic was the main contributor. These findings provide region-specific evidence of Guangzhou tea contamination and demonstrate that the optimized microwave digestion method allows accurate, environmentally considerate heavy metal analysis.
{"title":"Heavy metal contamination and health risk assessment of tea in Guangzhou, China","authors":"Jiawei Su , Zhenke Yi , Yingxuan Zeng , He Wang , Ronghua Mo , Yuting Liang , Qiting Qiu , Kailin Xu , Kang Wang , Yingxia Wu , Xinyan Zhu , Tuerxun Subi , Zhifeng Zhou , Jufeng Ye","doi":"10.1016/j.jfca.2026.108911","DOIUrl":"10.1016/j.jfca.2026.108911","url":null,"abstract":"<div><div>This study evaluated heavy metal contamination and health risks in tea consumed in Guangzhou. Fifty tea samples (green, black, oolong, and dark) from three districts were digested using an optimized microwave protocol with diluted nitric acid (∼42 % HNO₃), achieving complete matrix decomposition, stable recoveries (95–110 %), and reduced acid use. ICP-MS quantified As, Cd, Cr, Cu, and Pb, while Hg was measured using an automatic mercury analyzer. Metals were detected in 96–100 % of samples, with mean concentrations (mg/kg) following Cu > Cr > Pb > As > Cd > Hg. Dark tea accumulated the highest levels, and district differences reflected environmental contamination, with no significant tea variety × district interaction. Health risk assessment showed non-carcinogenic risks (HI) within acceptable limits for all groups, whereas total carcinogenic risk (TCR) exceeded 1 × 10⁻⁴ in several tea types, particularly among females (Green: 1.34 ×10⁻⁴; Black: 1.25 ×10⁻⁴; Dark: 2.10 ×10⁻⁴) compared with males (Green: 1.16 ×10⁻⁴; Black: 1.08 ×10⁻⁴; Dark: 1.82 ×10⁻⁴), highlighting potential long-term carcinogenic concerns. Arsenic was the main contributor. These findings provide region-specific evidence of Guangzhou tea contamination and demonstrate that the optimized microwave digestion method allows accurate, environmentally considerate heavy metal analysis.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"151 ","pages":"Article 108911"},"PeriodicalIF":4.6,"publicationDate":"2026-01-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146076091","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.jfca.2026.108925
Martina Pes , Antonella Rotolo , Giancarla Alberti , Riccardo Magagnato , Leonardo Maria Zapelli , Daniele Merli
Honey, a widely consumed natural product, acts as a bioindicator of environmental contamination because it is produced by bees from nectar collected in polluted flowers. Among contaminants of concern, perfluoroalkyl and polyfluoroalkyl substances (PFAS) are particularly alarming for their persistence, bioaccumulation, and potential adverse health effects. This study presents the validation of a robust analytical UHPLC-MS/MS method designed to detect and quantify 28 PFAS in honey samples. The method demonstrated detection limits of 0,007 – 0,04 ng/mL with precision consistently > 90 % and accuracy ranging from 85 % to 110 %, depending on the specific PFAS and matrix. The analysis of both commercial and non-commercial honey samples revealed the widespread presence of PFAS indicating environmental exposure across diverse sources. Principal Component Analysis (PCA) was used to explore compositional differences between sample types. By providing a validated analytical approach and new data, this work supports improved monitoring of PFAS contamination in honey.
{"title":"Development and validation of an analytical method (UHPLC-MS/MS) for the determination of perfluoroalkyl and polyfluoroalkyl substances (PFAS) in honey.","authors":"Martina Pes , Antonella Rotolo , Giancarla Alberti , Riccardo Magagnato , Leonardo Maria Zapelli , Daniele Merli","doi":"10.1016/j.jfca.2026.108925","DOIUrl":"10.1016/j.jfca.2026.108925","url":null,"abstract":"<div><div>Honey, a widely consumed natural product, acts as a bioindicator of environmental contamination because it is produced by bees from nectar collected in polluted flowers. Among contaminants of concern, perfluoroalkyl and polyfluoroalkyl substances (PFAS) are particularly alarming for their persistence, bioaccumulation, and potential adverse health effects. This study presents the validation of a robust analytical UHPLC-MS/MS method designed to detect and quantify 28 PFAS in honey samples. The method demonstrated detection limits of 0,007 – 0,04 ng/mL with precision consistently > 90 % and accuracy ranging from 85 % to 110 %, depending on the specific PFAS and matrix. The analysis of both commercial and non-commercial honey samples revealed the widespread presence of PFAS indicating environmental exposure across diverse sources. Principal Component Analysis (PCA) was used to explore compositional differences between sample types. By providing a validated analytical approach and new data, this work supports improved monitoring of PFAS contamination in honey.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"150 ","pages":"Article 108925"},"PeriodicalIF":4.6,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146023618","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.jfca.2026.108928
Mohammad Shakil Khan , Saifuddin Rana , Abdullah Al Mamun , Shahida Arfine Shimul , Antar Sarkar , Sk. Ahmad Al Nahid
Heavy metal contamination in marine organisms threatens both ecosystem health and food safety. This study quantified six metals (Pb, Cd, Cr, Cu, Mn, and As) in muscle tissues of shrimp, crabs, and lobster collected from two landing sites along the Cox’s Bazar coast, Bangladesh. Concentrations were measured using atomic absorption spectrophotometry, and human health risks were evaluated through estimated daily intake (EDI), target hazard quotient (THQ), hazard index (HI), and target cancer risk (TCR). Significant species-specific differences (p < 0.05) were observed, with crabs showing higher accumulation of Cu, Cr, and As, whereas Pb remained consistently lowest across all species. Non-carcinogenic risks assessed by EDI, THQ, and HI values were within safe thresholds for consumers at current intake levels. In contrast, carcinogenic risk estimates for Cd and Cr slightly exceeded thresholds in several species, particularly Portunus pelagicus and P. sanguinolentus. These findings identify crabs as the most critical group requiring targeted monitoring in seafood safety programs. Although overall contamination levels complied with international food safety guidelines, some risk indices approached critical thresholds. This study provides the first integrated assessment of heavy metal contamination in shrimp, crabs, and lobster from Cox’s Bazar, establishing a baseline for seafood safety monitoring in Bangladesh.
{"title":"Seafood safety concerns: Human health risks from heavy metal bioaccumulation in crustaceans from Cox’s Bazar, Bangladesh","authors":"Mohammad Shakil Khan , Saifuddin Rana , Abdullah Al Mamun , Shahida Arfine Shimul , Antar Sarkar , Sk. Ahmad Al Nahid","doi":"10.1016/j.jfca.2026.108928","DOIUrl":"10.1016/j.jfca.2026.108928","url":null,"abstract":"<div><div>Heavy metal contamination in marine organisms threatens both ecosystem health and food safety. This study quantified six metals (Pb, Cd, Cr, Cu, Mn, and As) in muscle tissues of shrimp, crabs, and lobster collected from two landing sites along the Cox’s Bazar coast, Bangladesh. Concentrations were measured using atomic absorption spectrophotometry, and human health risks were evaluated through estimated daily intake (EDI), target hazard quotient (THQ), hazard index (HI), and target cancer risk (TCR). Significant species-specific differences (<em>p</em> < 0.05) were observed, with crabs showing higher accumulation of Cu, Cr, and As, whereas Pb remained consistently lowest across all species. Non-carcinogenic risks assessed by EDI, THQ, and HI values were within safe thresholds for consumers at current intake levels. In contrast, carcinogenic risk estimates for Cd and Cr slightly exceeded thresholds in several species, particularly <em>Portunus pelagicus</em> and <em>P. sanguinolentus</em>. These findings identify crabs as the most critical group requiring targeted monitoring in seafood safety programs. Although overall contamination levels complied with international food safety guidelines, some risk indices approached critical thresholds. This study provides the first integrated assessment of heavy metal contamination in shrimp, crabs, and lobster from Cox’s Bazar, establishing a baseline for seafood safety monitoring in Bangladesh.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"151 ","pages":"Article 108928"},"PeriodicalIF":4.6,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146076087","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.jfca.2026.108929
Anas Alshishani , Yousef Al-ebini , Maryam Shoai , Diya Alsafadi , Ghaid Hussein , Lena Shaghlil
This study evaluated the quality and safety of 176 different bottled water brands from markets across Jordanian governorates, assessing compliance with WHO/EPA/Jordanian standard (JS) guidelines. Both cupped and bottled packaging formats were evaluated for 10 regular parameters, 56 irregular elements (Li, B, Mg, Al, Si, K, Ca, V, Pd, Ag, Ru, Rh, Se, Mo, Zn, As, Ni, Cu, Mn, Co, Cr, Fe, Cd, Sn, Sb, Ba, Ir, Pt, Hg, Tl, Pb, Bi, Ce, Dy, Eu, Ga, Ge, In, Ir, La, Lu, Nd, Pr, Rb, Sm, Sc, Na, Ta, Te, Tb, Tm, W, Yb, Y, Zr, and bromate), 6 microbiological parameters (total coliforms, E. coli, Pseudomonas aeruginosa, total viable count, yeast and mold, and Salmonella), and 10 pesticides and organic pollutants. The standard Water Quality Index (WQI) may mask zero value. Bacterial override integrates microbiological and chemical risks. Most brands (≈74 %) were classified as “Excellent”, though some samples significantly exceeded guideline limits for contaminants (bromate, nitrite, nitrate, B, Ba, Al, Mg, Se, and Pb). Microbial hazard was significantly higher in cupped water than bottled, primarily due to packaging and handling practices. Spatial analysis revealed notable geographic disparities in water quality, underscoring the need for strengthened monitoring and regulatory oversight.
{"title":"Quality and safety assessment of bottled water in Jordan markets","authors":"Anas Alshishani , Yousef Al-ebini , Maryam Shoai , Diya Alsafadi , Ghaid Hussein , Lena Shaghlil","doi":"10.1016/j.jfca.2026.108929","DOIUrl":"10.1016/j.jfca.2026.108929","url":null,"abstract":"<div><div>This study evaluated the quality and safety of 176 different bottled water brands from markets across Jordanian governorates, assessing compliance with WHO/EPA/Jordanian standard (JS) guidelines. Both cupped and bottled packaging formats were evaluated for 10 regular parameters, 56 irregular elements (Li, B, Mg, Al, Si, K, Ca, V, Pd, Ag, Ru, Rh, Se, Mo, Zn, As, Ni, Cu, Mn, Co, Cr, Fe, Cd, Sn, Sb, Ba, Ir, Pt, Hg, Tl, Pb, Bi, Ce, Dy, Eu, Ga, Ge, In, Ir, La, Lu, Nd, Pr, Rb, Sm, Sc, Na, Ta, Te, Tb, Tm, W, Yb, Y, Zr, and bromate), 6 microbiological parameters (total coliforms, <em>E. coli</em>, <em>Pseudomonas aeruginosa</em>, total viable count, yeast and mold, and Salmonella), and 10 pesticides and organic pollutants. The standard Water Quality Index (WQI) may mask zero value. Bacterial override integrates microbiological and chemical risks. Most brands (≈74 %) were classified as “Excellent”, though some samples significantly exceeded guideline limits for contaminants (bromate, nitrite, nitrate, B, Ba, Al, Mg, Se, and Pb). Microbial hazard was significantly higher in cupped water than bottled, primarily due to packaging and handling practices. Spatial analysis revealed notable geographic disparities in water quality, underscoring the need for strengthened monitoring and regulatory oversight.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"151 ","pages":"Article 108929"},"PeriodicalIF":4.6,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146076080","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.jfca.2026.108927
Zhengtao Wu , Jiaxing Zeng , Yanhui Ye , Erhao Zhang , Zhendong Liu , Xiaozhong Lan , Liang Li
Turmeric is recognized worldwide both as a culinary spice and as an herbal remedy. Studies have reported significant variation in its chemical composition depending on its geographical source. Some suppliers falsely claim premium origins to pass off lower-quality products, driven by profit motives. To address this, there is a growing need for a rapid, practical method to verify the origin of turmeric. In this study, portable near-infrared spectroscopy (NIRS), combined with various chemometric methods, was used to identify turmeric from 9 different regions. The local outlier factor (LOF) method outperformed for detecting and removing outliers. Among preprocessing techniques, the first derivative (D1) method achieved the highest accuracy of 67.15% during testing. The k-nearest neighbor (KNN) algorithm delivered superior performance with a test accuracy of 86.35%. Competitive adaptive reweighted sampling (CARS) proved to be the most effective dimensionality reduction tool, maintaining a test accuracy of 96.77%. Among the optimization techniques, the Goose Optimization (GO) algorithm yielded the most robust results, achieving 100% accuracy across trainingand test metrics. The integration of portable NIRS with the LOF-D1-CARS-GO-KNN strategy presents a powerful, scientifically reliable approach for tracing the geographical origin of turmeric, thereby ensuring product authenticity and quality.
{"title":"Research on the identification of turmeric from different origins based on portable near-infrared spectroscopy combined with chemometrics","authors":"Zhengtao Wu , Jiaxing Zeng , Yanhui Ye , Erhao Zhang , Zhendong Liu , Xiaozhong Lan , Liang Li","doi":"10.1016/j.jfca.2026.108927","DOIUrl":"10.1016/j.jfca.2026.108927","url":null,"abstract":"<div><div>Turmeric is recognized worldwide both as a culinary spice and as an herbal remedy. Studies have reported significant variation in its chemical composition depending on its geographical source. Some suppliers falsely claim premium origins to pass off lower-quality products, driven by profit motives. To address this, there is a growing need for a rapid, practical method to verify the origin of turmeric. In this study, portable near-infrared spectroscopy (NIRS), combined with various chemometric methods, was used to identify turmeric from 9 different regions. The local outlier factor (LOF) method outperformed for detecting and removing outliers. Among preprocessing techniques, the first derivative (D1) method achieved the highest accuracy of 67.15% during testing. The k-nearest neighbor (KNN) algorithm delivered superior performance with a test accuracy of 86.35%. Competitive adaptive reweighted sampling (CARS) proved to be the most effective dimensionality reduction tool, maintaining a test accuracy of 96.77%. Among the optimization techniques, the Goose Optimization (GO) algorithm yielded the most robust results, achieving 100% accuracy across trainingand test metrics. The integration of portable NIRS with the LOF-D1-CARS-GO-KNN strategy presents a powerful, scientifically reliable approach for tracing the geographical origin of turmeric, thereby ensuring product authenticity and quality.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"150 ","pages":"Article 108927"},"PeriodicalIF":4.6,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146023620","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.jfca.2026.108926
Hang Long , Lidan Niu , Ying Li , Jingrong Chen , Fengqiong Chen , Yuhan He , Shihan Xu , Yixiang Liu , Xiao Xu , Jie Zheng
Chloropropanols and their fatty acid esters, particularly 3-monochloropropane-1,2-diol (3-MCPD), are contaminants produced by heating in high-fat foods, such as Chongqing hotpot base, and pose reproductive toxicity and carcinogenicity risks. Their quantitative analysis is challenging due to the complex composition of oils and spices. Here, we developed a sensitive isotope dilution gas chromatography-mass spectrometry (ID-GC-MS) method with an optimized pretreatment process, including modified melting and filtration, refined nitrogen evaporation, and centrifugation after derivatization. This method demonstrated excellent linearity (R² ≥ 0.999), high recoveries (97.27–118.20 %), precision (RSD ≤ 14.93 %), and extremely low limits of detection and quantification (LODs and LOQs) (0.04–2.25 μg/L and 0.13–7.50 μg/L), surpassing previous methods. This method was applied to 12 hotpot base samples, and analysis of different production steps confirmed that processing temperature, time, and ingredients significantly influence the formation of chloropropanol esters. This validated method helps to systematically monitor and improve food safety.
{"title":"Development and optimization of an effective method for the analysis of chloropropanols and their fatty acid esters in Chongqing hotpot base","authors":"Hang Long , Lidan Niu , Ying Li , Jingrong Chen , Fengqiong Chen , Yuhan He , Shihan Xu , Yixiang Liu , Xiao Xu , Jie Zheng","doi":"10.1016/j.jfca.2026.108926","DOIUrl":"10.1016/j.jfca.2026.108926","url":null,"abstract":"<div><div>Chloropropanols and their fatty acid esters, particularly 3-monochloropropane-1,2-diol (3-MCPD), are contaminants produced by heating in high-fat foods, such as Chongqing hotpot base, and pose reproductive toxicity and carcinogenicity risks. Their quantitative analysis is challenging due to the complex composition of oils and spices. Here, we developed a sensitive isotope dilution gas chromatography-mass spectrometry (ID-GC-MS) method with an optimized pretreatment process, including modified melting and filtration, refined nitrogen evaporation, and centrifugation after derivatization. This method demonstrated excellent linearity (R² ≥ 0.999), high recoveries (97.27–118.20 %), precision (RSD ≤ 14.93 %), and extremely low limits of detection and quantification (LODs and LOQs) (0.04–2.25 μg/L and 0.13–7.50 μg/L), surpassing previous methods. This method was applied to 12 hotpot base samples, and analysis of different production steps confirmed that processing temperature, time, and ingredients significantly influence the formation of chloropropanol esters. This validated method helps to systematically monitor and improve food safety.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"150 ","pages":"Article 108926"},"PeriodicalIF":4.6,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146023621","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.jfca.2026.108921
Maja Mikulic-Petkovsek , Saša Krošelj , Petra Povše , Gregor Osterc
This study evaluated the specific morphological and biochemical parameters of fruits from ten pear cultivars, including several traditional old cultivars, such as 'President Drouard', 'Hartilian', 'Clapp’s Favorite', 'Poire de Cure', 'False Pituralka', 'Risovka', 'Santa Maria', 'Starkrimson', 'Triomphe de Vienne' and 'Nordhäuser Winterflorelle'. Significant differences in fruit quality were observed among the evaluated pear cultivars. The cultivars 'Risovka' (32.62 g) and 'President Drouard' (47.31 g) exhibited the lowest fruit weight, whereas 'Triomphe de Vienne' produced very large fruits with an average weight of 254.4 g. The highest total sugar content was recorded in 'False Pituralka' (138.5 g/kg FW), followed by 'Hartilian', 'Poire de Cure' and 'Nordhäuser Winterflorelle'. In contrast, the lowest total acid content was observed in 'Triomphe de Vienne' and 'Nordhäuser Winterflorelle', resulting in a high sugar-to-acid ratio (S/A) and, consequently, a sweet perceived flavor. The more acidic cultivars, characterized by lower S/A ratios, included 'Starkrimson', 'Santa Maria', 'President Drouard', 'Poire de Cure' and 'Clapp’s Favorite'. The highest phenolic compound contents in the fruit flesh were detected in 'Hartilian', 'Risovka', 'President Drouard' and 'Poire de Cure' (58.77–82.12 mg/kg FW), whereas in the peel, the cultivars 'False Pituralka', 'President Drouard' and 'Poire de Cure' contained the highest phenolic levels (1291–2111 mg/kg FW). The characterization of old pear cultivars from a specific growing region is vital for assessing their quality, as they represent an excellent source of genetic diversity and are invaluable for breeding new cultivars.
本研究对10个梨品种果实的形态和生化指标进行了评价,其中包括“总统Drouard”、“Hartilian”、“Clapp’s Favorite”、“Poire de Cure”、“假Pituralka”、“Risovka”、“Santa Maria”、“Starkrimson”、“Triomphe de Vienne”和“Nordhäuser Winterflorelle”等传统老品种。各评价品种果实品质差异显著。品种‘Risovka’(32.62 g)和‘President Drouard’(47.31 g)的果实重量最低,而‘Triomphe de Vienne’的果实非常大,平均重量为254.4 g。总糖含量最高的是“假Pituralka”(138.5 g/kg FW),其次是“Hartilian”,“Poire de Cure”和“Nordhäuser Winterflorelle”。相比之下,在“凯旋门”和“Nordhäuser冬花”中观察到的总酸含量最低,导致糖酸比高(S/ a),因此,感知到的甜味。酸性较强的品种,其特征是较低的S/A比率,包括“Starkrimson”、“Santa Maria”、“President Drouard”、“Poire de Cure”和“Clapp’S Favorite”。果肉中酚类化合物含量最高的品种为‘Hartilian’、‘Risovka’、‘President Drouard’和‘Poire de Cure’(58.77 ~ 82.12 mg/kg FW),而果皮中酚类化合物含量最高的品种为‘False Pituralka’、‘President Drouard’和‘Poire de Cure’(1291 ~ 2111 mg/kg FW)。来自特定产区的老梨品种的特性对评估其质量至关重要,因为它们代表了遗传多样性的极好来源,对培育新品种具有不可估量的价值。
{"title":"Evaluation of fruit quality and chemical characterization of local and standard pear (Pyrus communis L.) cultivars grown in Slovenia","authors":"Maja Mikulic-Petkovsek , Saša Krošelj , Petra Povše , Gregor Osterc","doi":"10.1016/j.jfca.2026.108921","DOIUrl":"10.1016/j.jfca.2026.108921","url":null,"abstract":"<div><div>This study evaluated the specific morphological and biochemical parameters of fruits from ten pear cultivars, including several traditional old cultivars, such as 'President Drouard', 'Hartilian', 'Clapp’s Favorite', 'Poire de Cure', 'False Pituralka', 'Risovka', 'Santa Maria', 'Starkrimson', 'Triomphe de Vienne' and 'Nordhäuser Winterflorelle'. Significant differences in fruit quality were observed among the evaluated pear cultivars. The cultivars 'Risovka' (32.62 g) and 'President Drouard' (47.31 g) exhibited the lowest fruit weight, whereas 'Triomphe de Vienne' produced very large fruits with an average weight of 254.4 g. The highest total sugar content was recorded in 'False Pituralka' (138.5 g/kg FW), followed by 'Hartilian', 'Poire de Cure' and 'Nordhäuser Winterflorelle'. In contrast, the lowest total acid content was observed in 'Triomphe de Vienne' and 'Nordhäuser Winterflorelle', resulting in a high sugar-to-acid ratio (S/A) and, consequently, a sweet perceived flavor. The more acidic cultivars, characterized by lower S/A ratios, included 'Starkrimson', 'Santa Maria', 'President Drouard', 'Poire de Cure' and 'Clapp’s Favorite'. The highest phenolic compound contents in the fruit flesh were detected in 'Hartilian', 'Risovka', 'President Drouard' and 'Poire de Cure' (58.77–82.12 mg/kg FW), whereas in the peel, the cultivars 'False Pituralka', 'President Drouard' and 'Poire de Cure' contained the highest phenolic levels (1291–2111 mg/kg FW). The characterization of old pear cultivars from a specific growing region is vital for assessing their quality, as they represent an excellent source of genetic diversity and are invaluable for breeding new cultivars.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"151 ","pages":"Article 108921"},"PeriodicalIF":4.6,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146076079","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-20DOI: 10.1016/j.jfca.2026.108922
Esila BAYAR , Ayşe ÜNLÜ
Nutrient profiling (NP) is a method used to assess foods based on their nutrient composition, which holds relevance for public health interventions. Local cuisines are often evaluated for their gastronomic value, but their health impacts warrant equal attention. This study aimed to evaluate 52 local dishes from Afyonkarahisar in Türkiye using five different NP models. The selected NP models were NRF9.3, SAIN-LIM, and Choices Programme, alongside the FSA-Ofcom WXY and Nutri-Score. Scores generated from NP models were ranked for comparative assessment. Salads had the highest score of NRF9.3, while soups had the lowest. According to FSA-Ofcom WXY, 63.46 % of dishes were healthier. SAIN-LIM model classified 17.31 % of dishes as Class 1 (recommended), and 38.46 % as Class 4 (be limited). Nutri-Score results showed 26.92 % of dishes in Class A (best quality), with none in Class E (lowest quality). Meanwhile, 3.85 % of dishes complied with Choices Programme criteria. Strong, positive, and statistically significant correlation was observed between specific ranked scores (p < 0,05). The findings highlight the importance of evaluating local dishes based on portion size and content of saturated fat, sodium, and added sugars. It is recommended to use NP models as objective tools to guide nutrition policies and support healthier food choices.
{"title":"Afyonkarahisar province local dishes: Evaluation with five different nutrient profiling models","authors":"Esila BAYAR , Ayşe ÜNLÜ","doi":"10.1016/j.jfca.2026.108922","DOIUrl":"10.1016/j.jfca.2026.108922","url":null,"abstract":"<div><div>Nutrient profiling (NP) is a method used to assess foods based on their nutrient composition, which holds relevance for public health interventions. Local cuisines are often evaluated for their gastronomic value, but their health impacts warrant equal attention. This study aimed to evaluate 52 local dishes from Afyonkarahisar in Türkiye using five different NP models. The selected NP models were NRF9.3, SAIN-LIM, and Choices Programme, alongside the FSA-Ofcom WXY and Nutri-Score. Scores generated from NP models were ranked for comparative assessment. Salads had the highest score of NRF9.3, while soups had the lowest. According to FSA-Ofcom WXY, 63.46 % of dishes were healthier. SAIN-LIM model classified 17.31 % of dishes as Class 1 (recommended), and 38.46 % as Class 4 (be limited). Nutri-Score results showed 26.92 % of dishes in Class A (best quality), with none in Class E (lowest quality). Meanwhile, 3.85 % of dishes complied with Choices Programme criteria. Strong, positive, and statistically significant correlation was observed between specific ranked scores (p < 0,05). The findings highlight the importance of evaluating local dishes based on portion size and content of saturated fat, sodium, and added sugars. It is recommended to use NP models as objective tools to guide nutrition policies and support healthier food choices.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"150 ","pages":"Article 108922"},"PeriodicalIF":4.6,"publicationDate":"2026-01-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146023623","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-20DOI: 10.1016/j.jfca.2026.108918
Erin M. Goldberg , Amanda G.A. Sá , Adam J. Franczyk , Elaine S. Krul , Barbara Lyle , Mingyan Jing , Fiona Liu , Xin Wu , Nandika Bandara , Guillaume Brisson , Vicenta Garcia Campayo , Lingyun Chen , Sharon Hooper , Lamia L'Hocine , Mike Nickerson , Matthew Nosworthy , James D. House
The diversification of protein sources used in food formulation has increased the need to assess protein quality beyond traditional food forms. Protein digestibility is a key component of the Protein Digestibility Corrected Amino Acid Score (PDCAAS), the regulatory metric derived from rodent bioassays. Ethical concerns and the high cost of animal testing limit the ability of food formulators to screen protein ingredients and evaluate processing effects on digestibility. Findings from an international collaborative study are presented to position two in vitro methods, the pH-drop and pH-stat assays, as accredited approaches for determining protein digestibility. Nine laboratories participated in the study and analyzed 12 protein ingredients. Relative standard deviations for repeatability ranged from 0.8 to 2.1 % and 0.5–4.8 %, while reproducibility ranged from 1.2 to 3.6 % and 1.1–4.9 % for the pH-drop and pH-stat methods, respectively. Comparison between the two assays demonstrated strong correlation and moderate agreement, with the pH-stat assay yielding slightly lower digestibility values. In vitro protein digestibility coefficients aligned well with literature reported true faecal protein digestibility values for comparable, non-identical protein ingredients. Both methods received official AOCS Uniform Methods Committee approval, offering simple, affordable, reliable, and ethical tools to support informed decisions on protein digestibility during food formulation.
{"title":"A collaborative study to validate in vitro assays for protein digestibility assessment using pH-drop and pH-stat methods","authors":"Erin M. Goldberg , Amanda G.A. Sá , Adam J. Franczyk , Elaine S. Krul , Barbara Lyle , Mingyan Jing , Fiona Liu , Xin Wu , Nandika Bandara , Guillaume Brisson , Vicenta Garcia Campayo , Lingyun Chen , Sharon Hooper , Lamia L'Hocine , Mike Nickerson , Matthew Nosworthy , James D. House","doi":"10.1016/j.jfca.2026.108918","DOIUrl":"10.1016/j.jfca.2026.108918","url":null,"abstract":"<div><div>The diversification of protein sources used in food formulation has increased the need to assess protein quality beyond traditional food forms. Protein digestibility is a key component of the Protein Digestibility Corrected Amino Acid Score (PDCAAS), the regulatory metric derived from rodent bioassays. Ethical concerns and the high cost of animal testing limit the ability of food formulators to screen protein ingredients and evaluate processing effects on digestibility. Findings from an international collaborative study are presented to position two <em>in vitro</em> methods, the pH-drop and pH-stat assays, as accredited approaches for determining protein digestibility. Nine laboratories participated in the study and analyzed 12 protein ingredients. Relative standard deviations for repeatability ranged from 0.8 to 2.1 % and 0.5–4.8 %, while reproducibility ranged from 1.2 to 3.6 % and 1.1–4.9 % for the pH-drop and pH-stat methods, respectively. Comparison between the two assays demonstrated strong correlation and moderate agreement, with the pH-stat assay yielding slightly lower digestibility values. <em>In vitro</em> protein digestibility coefficients aligned well with literature reported true faecal protein digestibility values for comparable, non-identical protein ingredients. Both methods received official AOCS Uniform Methods Committee approval, offering simple, affordable, reliable, and ethical tools to support informed decisions on protein digestibility during food formulation.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"151 ","pages":"Article 108918"},"PeriodicalIF":4.6,"publicationDate":"2026-01-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146026251","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-20DOI: 10.1016/j.jfca.2026.108903
Uche O. Arunsi , Eziuche A. Ugbogu , Chollom L. Israel , Victor C. Nwankwo , Chinonye C. Arunsi , Daniel C. Ezirim , Ahmad Altayyar , Tuba Esatbeyoglu , Solomon Owumi
Termitomyces robustus is a seasonal edible mushroom with significant nutritional and therapeutic potential. This review summarizes its nutritional content, phytochemical profile, and health-promoting properties based on research from ScienceDirect, Wiley, Springer, and PubMed. T. robustus contains various bioactive compounds, including gallic acid, chlorogenic acid, caffeic acid, ellagic acid, catechin, epicatechin, rutin, isoquercitrin, quercitrin, quercetin, and kaempferol, which have antioxidant, anti-inflammatory, antidiabetic, antimicrobial, and antifungal effects. The mushroom also provides a rich source of B vitamins, essential for carbohydrate metabolism. Toxicological studies confirm it is safe for consumption. Mechanistic evidence indicates these compounds influence key biological pathways such as Nrf2/KEAP1, TBK1, PPAR-γ, and α-amylase, supporting their potential medical use. However, research gaps remain, including optimal doses and effects on protein expression, which should be explored with high-throughput techniques. Additionally, studying new bioactive compounds in T. robustus could lead to new therapeutic options. This review emphasizes the nutritional and medicinal importance of T. robustus and supports its wider study in functional foods and pharmaceuticals.
{"title":"Nutritional composition, phytochemistry, and mechanistic insights into the health-promoting properties of Termitomyces robustus: A comprehensive review","authors":"Uche O. Arunsi , Eziuche A. Ugbogu , Chollom L. Israel , Victor C. Nwankwo , Chinonye C. Arunsi , Daniel C. Ezirim , Ahmad Altayyar , Tuba Esatbeyoglu , Solomon Owumi","doi":"10.1016/j.jfca.2026.108903","DOIUrl":"10.1016/j.jfca.2026.108903","url":null,"abstract":"<div><div><em>Termitomyces robustus</em> is a seasonal edible mushroom with significant nutritional and therapeutic potential. This review summarizes its nutritional content, phytochemical profile, and health-promoting properties based on research from ScienceDirect, Wiley, Springer, and PubMed. <em>T. robustus</em> contains various bioactive compounds, including gallic acid, chlorogenic acid, caffeic acid, ellagic acid, catechin, epicatechin, rutin, isoquercitrin, quercitrin, quercetin, and kaempferol, which have antioxidant, anti-inflammatory, antidiabetic, antimicrobial, and antifungal effects. The mushroom also provides a rich source of B vitamins, essential for carbohydrate metabolism. Toxicological studies confirm it is safe for consumption. Mechanistic evidence indicates these compounds influence key biological pathways such as Nrf2/KEAP1, TBK1, PPAR-γ, and α-amylase, supporting their potential medical use. However, research gaps remain, including optimal doses and effects on protein expression, which should be explored with high-throughput techniques. Additionally, studying new bioactive compounds in <em>T. robustus</em> could lead to new therapeutic options. This review emphasizes the nutritional and medicinal importance of <em>T. robustus</em> and supports its wider study in functional foods and pharmaceuticals.</div></div>","PeriodicalId":15867,"journal":{"name":"Journal of Food Composition and Analysis","volume":"150 ","pages":"Article 108903"},"PeriodicalIF":4.6,"publicationDate":"2026-01-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146023615","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":2,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}