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Numerical investigation on orthogonal cutting and damage response of CFRP/Ti6Al4V stacks CFRP/Ti6Al4V 叠层的正交切削和损伤响应数值研究
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-02-19 DOI: 10.1177/08927057241234877
Chao Zhang, Keyi Liu, Fernando Cepero-Mejias, Jose L Curiel-Sosa, Chunjian Mao
CFRP/Ti6Al4V stacks are widely employed in aerospace, automotive and marine applications owing to their superior properties. However, machining these stacked structures pose challenges due to the intrinsic difference in the mechanical properties of CFRP and Ti6Al4V. Such difference can induce distinct failure mechanisms and chip formation processes compared to those observed in individual materials. This paper presents an explicit finite element (FE) modeling to predict the cutting forces and analyze the induced damage during the orthogonal cutting process. The proposed FE model is validated using available experimental data for separate CFRP and Ti6Al4V conditions before being applied to simulate the cutting behavior of CFRP/Ti6Al4V stacks. The effects of fiber angles, cutting sequences and cutting parameters on the cutting performance and damage mechanism of CFRP/Ti6Al4V stacks are investigated in detail. This work provides insights into the cutting behavior of CFRP/Ti6Al4V stacks and facilitates the optimization of machining process for such composite system.
CFRP/Ti6Al4V 叠层结构因其卓越的性能而被广泛应用于航空航天、汽车和船舶领域。然而,由于 CFRP 和 Ti6Al4V 的机械性能存在固有差异,加工这些堆叠结构面临着挑战。与单种材料相比,这种差异会导致不同的失效机制和切屑形成过程。本文提出了一种明确的有限元 (FE) 模型,用于预测正交切削过程中的切削力并分析诱发的损伤。在应用于模拟 CFRP/Ti6Al4V 复合材料的切割行为之前,利用现有的实验数据对所提出的 FE 模型进行了验证。详细研究了纤维角度、切割顺序和切割参数对 CFRP/Ti6Al4V 叠层切割性能和损伤机理的影响。这项研究有助于深入了解 CFRP/Ti6Al4V 复合材料的切削行为,并有助于优化此类复合材料系统的加工工艺。
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引用次数: 0
Nonlinear dynamical characteristics of carbon nanotube-reinforced composite beams with piezoelectric actuators and elastically restrained ends under thermo-electro-mechanical loads 带有压电致动器和弹性约束端部的碳纳米管增强复合梁在热-电-机械载荷下的非线性动力学特性
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-02-17 DOI: 10.1177/08927057241233187
Nguyen Van Thinh, Hoang Van Tung
Nonlinear free vibration and dynamical responses of carbon nanotube (CNT) reinforced composite beams with surface-bonded piezoelectric layers and tangentially restrained ends under thermo-electro-mechanical loads are investigated in this paper. The properties of constitutive materials are assumed to be temperature-dependent and effective properties of nanocomposite are estimated using an extended rule of mixture. Unlike previous studies, the present work considers the effects of tangentially elastic constraints of two ends on the nonlinear dynamic characteristics of hybrid beams. Motion equation is established within the framework of Euler-Bernoulli beam theory taking into account von Kármán nonlinearity. Analytical solution is assumed to satisfy simply supported boundary conditions and Galerkin procedure is employed to obtain a time ordinary differential equation including both quadratic and cubic nonlinear terms. This differential equation is numerically solved employing fourth-order Runge-Kutta scheme to determine the frequencies of nonlinear free vibration and nonlinear transient response. Parametric studies are executed to examine numerous influences on the nonlinear dynamical characteristics of hybrid nanocomposite beams. The study reveals that tangential constraints of ends substantially effect the frequencies and dynamic response of the beam, especially at elevated temperatures. The results also indicate that nonlinear dynamic responses can be controlled effectively by means of piezoelectric actuators and elasticity of tangential constraints of ends should be considered in design of piezo-CNTRC beams.
本文研究了碳纳米管(CNT)增强复合梁在热-电-机械载荷作用下的非线性自由振动和动态响应,碳纳米管(CNT)增强复合梁具有表面粘结压电层和切向约束端。假定构成材料的特性与温度有关,并使用扩展混合规则估算纳米复合材料的有效特性。与之前的研究不同,本文考虑了两端切向弹性约束对混合梁非线性动态特性的影响。在欧拉-伯努利梁理论框架内建立了运动方程,并考虑了 von Kármán 非线性因素。假定分析解满足简单支撑边界条件,并采用 Galerkin 程序获得包含二次和三次非线性项的时间常微分方程。该微分方程采用四阶 Runge-Kutta 方案进行数值求解,以确定非线性自由振动和非线性瞬态响应的频率。通过参数研究,考察了对混合纳米复合梁非线性动力学特性的诸多影响。研究发现,两端的切向约束对梁的频率和动态响应有很大影响,尤其是在高温条件下。研究结果还表明,通过压电致动器可以有效控制非线性动态响应,在设计压电-CNTRC 梁时应考虑两端切向约束的弹性。
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引用次数: 0
Tribological performance analysis of sustainable basalt micro-filler loaded bio-based polypropylene and high density polyethylene composites 负载生物基聚丙烯和高密度聚乙烯复合材料的可持续玄武岩微填料的摩擦学性能分析
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-01-29 DOI: 10.1177/08927057231223478
Praveenkumara Jagadeesh, Sanjay Mavinkere Rangappa, Suchart Siengchin
The current research work involves the fabrication and tribological properties analysis of constant basalt filler reinforced (30 wt %) bio-based polypropylene (PP) and high density polyethylene (HDPE) thermoplastic composites. Compression molding technique is used after an internal mixing process in order to produce composite samples. The physical and hardness properties have been evaluated for both neat polymers and composite samples. In order to study the coefficient of friction (COF) and specific wear rate (SWR) of PP and HDPE composite samples, the Taguchi and Analysis of Variance (ANOVA) methodologies were applied. For PP samples, the optimum parameters in response to COF are found to be 0 wt% basalt (rank 3), 9 N load (rank 1), 200 r/min speed (rank 4), and 100 m distance (rank 2); for the SWR output, the optimum parameters are 30 wt% basalt (rank 1), 6 N load (rank 4), 100 r/min speed (rank 2), and 200 m distance (rank 3). For HDPE samples, the optimum parameters in response to COF are 0 wt% basalt (rank 1), 6 N load (rank 3), 100 r/min speed (rank 4), and 100 m distance (rank 2); for the SWR output, the optimum parameters are 30 wt% basalt (rank 1), 6 N load (rank 3), 100 r/min speed (rank 4), and 150 m distance (rank 2). Consistently, it has been shown that incorporating basalt fillers to PP and HDPE composites has more dramatically decreased SWR than COF. The depth of wear constantly rises according to increasing load, irrespective of the processing variables, as shown in 2D depth profiles. It is discovered that the confirmation tests carried out for the optimum parameters are within statistically acceptable bounds. The depth profile plots revealed that the worn track edges are found with polymer bumps because of deep grooves and softened polymer debris, which commonly observed more with HDPE samples due to low softening temperature. Moreover, the worn surfaces of the composites have plowed lines and cracks that are brought about by the micro-cutting and micro-plowing activity of the erosive asperities counterface. In addition to surface characteristics, the transfer films created during sliding also significantly influenced the mode of sample wear.
目前的研究工作涉及恒定玄武岩填料增强(30 wt %)生物基聚丙烯(PP)和高密度聚乙烯(HDPE)热塑性复合材料的制造和摩擦学特性分析。在经过内部混合过程后,采用压缩成型技术生产复合材料样品。对纯净聚合物和复合材料样品的物理和硬度特性进行了评估。为了研究聚丙烯和高密度聚乙烯复合材料样品的摩擦系数(COF)和特定磨损率(SWR),采用了田口方法和方差分析(ANOVA)方法。对于聚丙烯样品,COF 的最佳参数为 0 wt%的玄武岩(排序 3)、9 N 的负载(排序 1)、200 r/min 的速度(排序 4)和 100 m 的距离(排序 2);对于 SWR 输出,最佳参数为 30 wt%的玄武岩(排序 1)、6 N 的负载(排序 4)、100 r/min 的速度(排序 2)和 200 m 的距离(排序 3)。对于高密度聚乙烯样品,响应 COF 的最佳参数为 0 wt%的玄武岩(排名 1)、6 N 的负载(排名 3)、100 r/min 的速度(排名 4)和 100 m 的距离(排名 2);对于 SWR 输出,最佳参数为 30 wt%的玄武岩(排名 1)、6 N 的负载(排名 3)、100 r/min 的速度(排名 4)和 150 m 的距离(排名 2)。一致表明,在 PP 和 HDPE 复合材料中加入玄武岩填料比 COF 更能显著降低 SWR。如二维磨损深度剖面图所示,无论加工变量如何,磨损深度随着载荷的增加而不断增加。我们发现,对最佳参数进行的确认测试在统计学上可接受的范围内。深度剖面图显示,由于凹槽较深和聚合物碎片软化,磨损的轨道边缘会出现聚合物凸起,而高密度聚乙烯样品由于软化温度较低,通常会出现这种情况。此外,复合材料的磨损表面还出现了犁纹和裂纹,这是由侵蚀性反面的微切割和微犁活动造成的。除表面特征外,滑动过程中产生的转移膜也对样品的磨损模式产生了重大影响。
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引用次数: 0
Dynamic characterization and damage analysis for the thermoplastic fiber-reinforced epoxy composites exposed to repeated low velocity impact 热塑性纤维增强环氧树脂复合材料在反复低速冲击下的动态特性和损伤分析
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-22 DOI: 10.1177/08927057231223927
Betul Sozen, T. Coskun, Omer Sinan Sahin
In the current study, contrary to conventional fiber-reinforced composites, polyamide fiber was used as reinforcement material, and the effects of thermoplastic fiber reinforcement on repeated low velocity impact (LVI) responses of composites were examined. In this regard, polyamide fiber-reinforced composites were fabricated using the vacuum-assisted hand lay-up method (VAHLM) and then exposed to repeated LVI loadings. Experimental tests were performed on the specimens for 100 impacts with a constant velocity of 3 m/s, which is equivalent to 25.2 J, and the impacts of repeated LVI loadings on the dynamic responses such as peak force, energy absorbing/rebounding, total impulse, bending stiffness and contact stiffness were examined. Moreover, the damage mechanisms resulting from the relative damage accumulation depending on the impact numbers were examined. According to the findings, the thermoplastic polyamide fibers absorbed more than 60% of the applied energy, and the absorbed energy increased with ascending impact number. Furthermore, the thermoplastic fiber-reinforced epoxy composites gained stiffness with increasing impact, which was linked to the thermoplastic chain structure. Despite quite a number of impact loadings, no serious damage mechanisms such as fiber breakage, perforation, or penetration were observed, and the specimens maintained their structural integrity. Due to the higher energy absorption of thermoplastics, the utilization of polyamide fibers in composites has been found to be well suited for applications subjected to repeated impacts.
与传统的纤维增强复合材料不同,本研究采用了聚酰胺纤维作为增强材料,并考察了热塑性纤维增强对复合材料重复低速冲击(LVI)响应的影响。为此,采用真空辅助手糊法(VAHLM)制造了聚酰胺纤维增强复合材料,然后将其暴露在重复低速冲击载荷下。对试样进行了 100 次恒速为 3 m/s(相当于 25.2 J)的冲击试验,并考察了重复 LVI 负载对峰值力、能量吸收/回弹、总冲量、弯曲刚度和接触刚度等动态响应的影响。此外,还研究了因冲击次数不同而产生的相对损伤累积所导致的损伤机制。研究结果表明,热塑性聚酰胺纤维吸收了 60% 以上的外加能量,且吸收的能量随着冲击次数的增加而增加。此外,热塑性纤维增强环氧树脂复合材料的刚度随着冲击力的增加而增加,这与热塑性链结构有关。尽管受到了多次冲击载荷,但没有观察到纤维断裂、穿孔或穿透等严重破坏机制,试样保持了结构的完整性。由于热塑性塑料具有较高的能量吸收能力,因此在复合材料中使用聚酰胺纤维非常适合反复受到冲击的应用。
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引用次数: 0
Revolutionizing transportation composite structures: Lightweight, sustainable, and multi-scale hybrid design through waste tire-driven graphene, hemp fiber, and bio-based overmoulding 革新交通复合结构:通过废轮胎驱动的石墨烯、麻纤维和生物基包覆成型实现轻质、可持续和多尺度混合设计
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-19 DOI: 10.1177/08927057231222821
Nargiz Aliyeva, Hatice S. Şaş, Burcu Saner Okan
The pursuit of lightweight, environmentally friendly composite structures in transportation is crucial for minimizing ecological footprints and promoting energy-efficient manufacturing techniques. This study presents a novel approach by replacing traditional long glass fiber reinforced homopolymer polypropylene (homoPP) compounds with short hemp fiber reinforced homoPP, incorporating graphene nanoplatelets (GNP) derived from recovered carbon black via waste tire pyrolysis, resulting in a remarkable 15% weight reduction. With new compound formulation by adjusting the amounts of compatibilizer and GNP, injection moulding process was integrated with overmoulding process by using bio-based UD prepregs to enhance the adhesion of injected part and interfacial interaction by decreasing the stress concentrations in the structure. This novel hybrid composite design having 40 wt% hemp fiber, 1.0 wt% GNP and 2.7 wt% compatibilizer provided to improve flexural modulus and strength by 169% and 67.9%, respectively, compared to neat homoPP. The overmolding process employed bio-based natural fibers reinforced UD tapes as inserts, leading to an impressive enhancement of 211% in tensile modulus and 93.6% in strength, further surpassing the performance of neat homoPP. This work not only achieves the conversion of conventional composite structures into recyclable, sustainable thermoplastic composites but also introduces multi-scale reinforcements with customizable functionality, demonstrating a significant step forward in the development of environmentally conscious materials and manufacturing methods by adopting Life-Cycle Assessment (LCA) methodology regarding the sustainability of the newly developed composites.
在交通运输领域追求轻质、环保的复合材料结构,对于最大限度地减少生态足迹和推广节能制造技术至关重要。本研究提出了一种新方法,即用短麻纤维增强均聚聚丙烯(HomoPP)取代传统的长玻璃纤维增强均聚聚丙烯(HomoPP)化合物,并在其中加入从废轮胎热解回收的炭黑中提取的石墨烯纳米颗粒(GNP),从而显著减轻 15%的重量。通过调整相容剂和 GNP 的用量,采用新的复合材料配方,使用生物基 UD 预浸料将注塑成型工艺与包覆成型工艺相结合,通过降低结构中的应力集中,增强注塑部件的粘附性和界面相互作用。这种新型混合复合材料设计含有 40 wt% 的麻纤维、1.0 wt% 的 GNP 和 2.7 wt% 的相容剂,与纯均聚丙烯相比,其弯曲模量和强度分别提高了 169% 和 67.9%。包覆成型工艺采用生物基天然纤维增强 UD 带作为插入物,使拉伸模量和强度分别提高了 211% 和 93.6%,进一步超越了纯均聚丙烯的性能。这项工作不仅实现了将传统复合材料结构转化为可回收、可持续的热塑性复合材料,还引入了具有可定制功能的多尺度增强材料,通过采用生命周期评估(LCA)方法对新开发的复合材料的可持续性进行评估,在开发具有环保意识的材料和制造方法方面迈出了重要一步。
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引用次数: 0
Fracture morphology and strength characteristics of poly-lactic acid and poly-ethylene terephthalate glycol composites combined with taguchi method and response surface methodology 结合塔口法和响应面法研究聚乳酸和聚对苯二甲酸乙二酯复合材料的断裂形态和强度特性
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-15 DOI: 10.1177/08927057231221749
Akash Jain, Ankit Sahai, R. Sharma
The emergence of additive manufacturing has enabled scientists to efficiently construct complex geometries, facilitating the development of novel, high-impact energy-absorbing structures suitable for a wide range of industrial applications. The present study conducted flexural and impact test to quantitatively assess the energy absorption capabilities of polymer composites fabricated through fused filament fabrication. Specifically, the polymer composites investigated were multi-walled carbon nanotubes reinforced poly-lactic acid, carbon fibre reinforced poly-ethylene terephthalate glycol, and carbon fibre reinforced poly-lactic acid. The investigation also examined the influence of different infill patterns and nozzle hole diameters on the polymer composites. The investigation depicts that by altering the process parameters, the flexural strength is improved from 21.079 MPa to 70.653 MPa by 235.18%. The experimental study of impact specimens utilising the Izod impact test demonstrates that the rectilinear infill pattern and a nozzle hole diameter of 0.6 mm result in the highest energy absorption of 37.76 kJ/m2 for carbon fibre reinforced poly-lactic acid. The study revealed that the energy absorption of the specimens was significantly influenced by both the independent and interaction effects of process variables. The application of the fused filament fabrication demonstrates an improved energy absorption, making it suitable for manufacturing of vehicle and aircraft components.
增材制造技术的出现使科学家们能够高效地构建复杂的几何形状,促进了新型、高冲击力吸能结构的开发,适合广泛的工业应用。本研究进行了弯曲和冲击测试,以定量评估通过熔融长丝制造技术制造的聚合物复合材料的能量吸收能力。具体而言,研究的聚合物复合材料包括多壁碳纳米管增强聚乳酸、碳纤维增强聚对苯二甲酸乙二醇和碳纤维增强聚乳酸。调查还研究了不同填充模式和喷嘴孔直径对聚合物复合材料的影响。调查显示,通过改变工艺参数,弯曲强度从 21.079 兆帕提高到 70.653 兆帕,提高了 235.18%。利用伊佐德冲击试验对冲击试样进行的实验研究表明,直线填充模式和 0.6 毫米的喷嘴孔直径使碳纤维增强聚乳酸的能量吸收率最高,达到 37.76 kJ/m2。研究表明,试样的能量吸收受到工艺变量的独立效应和交互效应的显著影响。熔融长丝制造技术的应用证明了其能量吸收能力的提高,使其适用于汽车和飞机部件的制造。
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引用次数: 0
A review on the influence of various metal oxide nanoparticles on structural, morphological, optical, thermal and electrical properties of PVA/PVP blends 综述各种金属氧化物纳米粒子对 PVA/PVP 共混物的结构、形态、光学、热学和电学特性的影响
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-15 DOI: 10.1177/08927057231222833
K. Meera, M. T. Ramesan
Biopolymer blend based nanocomposites have been interestingly investigated by researchers to achieve advanced composite functional materials that are environmentally amicable. Among the varieties of biopolymers, widespread attention has been given to polyvinyl alcohol (PVA) and polyvinyl pyrrolidone (PVP) owing to their interesting properties like water solubility, biodegradability, biocompatibility and non-toxicity. PVA and PVP form a completely miscible blend at all compositions as both the polymers are rich in a variety of functional groups that permit effective intermolecular interactions between the polymers as well as with filler. PVA/PVP blend exhibits excellent dopant sensitive properties also. Metal oxide nanoparticles (MONPs) have made a prominent place in the area of scientific and technological research due to their unique chemical and physical properties. Doping with MONPs enhances the properties of the PVA/PVP blend matrix and the resulting PVA/PVP/MONP polymer nanocomposites are suitable for multifunctional purposes. This review mainly focused on the influence of various MONPs such as ZnO, CuO, Al2O3, ZrO2, MnO, SnO, MgO, TiO2, etc. in the structural, morphological, thermal, optical and electrical properties of PVA/PVP blend as well as its applications in various fields.
研究人员对基于生物聚合物共混物的纳米复合材料进行了有趣的研究,以获得对环境无害的先进复合功能材料。在各种生物聚合物中,聚乙烯醇(PVA)和聚乙烯吡咯烷酮(PVP)因其水溶性、生物降解性、生物相容性和无毒性等有趣的特性而受到广泛关注。PVA 和 PVP 在所有成分中都能形成完全混溶的混合物,因为这两种聚合物都富含各种官能团,使聚合物之间以及与填料之间的分子间相互作用更为有效。PVA/PVP 共混物还具有出色的掺杂剂敏感特性。金属氧化物纳米粒子(MONPs)因其独特的化学和物理特性,在科技研究领域占据了重要地位。掺入 MONPs 可增强 PVA/PVP 共混基质的性能,由此制得的 PVA/PVP/MONP 聚合物纳米复合材料适用于多功能用途。本综述主要关注各种 MONPs(如 ZnO、CuO、Al2O3、ZrO2、MnO、SnO、MgO、TiO2 等)对 PVA/PVP 共混物结构、形态、热学、光学和电学性能的影响及其在各个领域的应用。
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引用次数: 0
Multi-scale analysis of styrene butadiene latex modified PVA fiber concrete 丁苯胶乳改性 PVA 纤维混凝土的多尺度分析
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-14 DOI: 10.1177/08927057231222285
Yong Feng, Jingjie Feng, Wang Chen, Chen Zhao, Zehua Li
Polyvinyl alcohol (PVA) concrete is a new green building material. In order to make it more widely used, this study used butylbenzene emulsion (SBL) to modify PVA fiber concrete. The enhancement mechanism of SBL on the PVA/cement interface was systematically investigated at multiple scales, including macroscopic mechanical properties, microstructural characteristics, nano-interface interactions. On a macro scale, the addition of SBL and PVA fibers can significantly improve the shear strength and flexural strength of composite concrete at 7 and 28 days, and SBL can make up for the decrease in compressive strength caused by PVA. On a micro scale, the corresponding polymer cement concrete was tested by scanning electron microscopy (SEM), X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FT-IR). It was observed that some gels and polymers filled the interfacial gap and effectively repaired the interfacial defects. The SBL brought the two interfaces closer together and described its bonding effect at the micro-interface. On the nano scale, SBL/PVA/C-S-H is modeled by molecular dynamics method. Binding energy, Relative concentrations, Radial distribution function, Mean-square displacement and Time correlation function were analyzed and calculated. The results show that SBL reduces the interfacial effect, enhances the interfacial hydrogen bond, van der Waals interaction, Ca-H coordination bond and stability, improves the interfacial adhesion, and further enhances the weak interfacial bond between organic polymer (PVA) and inorganic silicate (C-S-H).
聚乙烯醇(PVA)混凝土是一种新型绿色建筑材料。为了使其得到更广泛的应用,本研究采用丁苯乳液(SBL)对 PVA 纤维混凝土进行改性。本研究从宏观力学性能、微观结构特征、纳米界面相互作用等多个尺度系统研究了 SBL 对 PVA/水泥界面的增强机理。在宏观尺度上,添加 SBL 和 PVA 纤维能显著提高复合混凝土在 7 天和 28 天时的抗剪强度和抗折强度,SBL 还能弥补 PVA 导致的抗压强度下降。在微观尺度上,通过扫描电子显微镜(SEM)、X 射线衍射(XRD)和傅立叶变换红外光谱(FT-IR)对相应的聚合物水泥混凝土进行了测试。结果表明,一些凝胶和聚合物填充了界面间隙,有效修复了界面缺陷。SBL 使两个界面靠得更近,并描述了其在微界面上的粘合效果。在纳米尺度上,SBL/PVA/C-S-H 采用分子动力学方法建模。分析和计算了结合能、相对浓度、径向分布函数、均方位移和时间相关函数。结果表明,SBL 降低了界面效应,增强了界面氢键、范德华相互作用、Ca-H 配位键和稳定性,提高了界面粘附力,并进一步增强了有机聚合物(PVA)和无机硅酸盐(C-S-H)之间的弱界面键。
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引用次数: 0
Synthesis of polymethyl methacrylate/depolymerized polyethylene terephthalate blend reinforced by titanium dioxide nanoparticles for dental fillings applications 合成二氧化钛纳米粒子增强的聚甲基丙烯酸甲酯/聚对苯二甲酸乙二醇酯混合物,用于牙科填料应用
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-13 DOI: 10.1177/08927057231221737
Doaa S Jawad, Nassier A. Nassir, M. Alzuhairi
The aim of this study is to use recycled waste materials to modify the performance of composites used as dental fillings. For this purpose, depolymerized polyethylene terephthalate (DPET) polymers were prepared by recycling waste polyethylene terephthalate (PET) using the glycolysis process. DPET was then blended with polymethyl methacrylate (PMMA) at different weight percentages. Polymer blends were subjected to mechanical, physical, and biological tests. It is evident that PMMA blended with a 5 wt% of DPET exhibits the highest compressive strength which is approximately two times that obtained from neat PMMA, highlighting the suitability of these resins to replace amalgam and to be considered for dental restorations. It was also found that the water absorption of the blends investigated is relatively stable at 5 wt% DPET. The SEM images showed no distinguishable phases, highlighting the high compatibility between DPET and PMMA. The biological tests, including in vitro cytotoxicity, showed that the cell viability mean values of PMMA containing 5 wt% DPET is higher than that of control group. Interestingly, in dental practice, the reliable in vitro cytotoxic approach is considered as an important aid in clinical procedures in the use of dental filling systems. The microbiology study has shown that the inhibition zones against Streptococcus mutans of PMMA: 5 wt% DPET is higher than the control group. According to the obtained results, the blend of PMMA: 5 wt% DPET was selected as an optimum blend, which was then reinforced with various weight percentages of nano-sized titanium dioxide (TiO2). The composites were then tested under compression, microhardness, and impact tests. The results demonstrated the significant impact of TiO2 on enhancing the properties of the composites investigated. This can provide a new protocol for synthesizing nanocomposite materials for dentistry.
本研究的目的是利用回收的废料来改变用作牙科填充物的复合材料的性能。为此,利用乙二醇工艺回收聚对苯二甲酸乙二酯(PET)废料,制备了解聚聚对苯二甲酸乙二酯(DPET)聚合物。然后按不同的重量百分比将 DPET 与聚甲基丙烯酸甲酯(PMMA)混合。对聚合物混合物进行了机械、物理和生物测试。结果表明,含有 5 重量百分比 DPET 的聚甲基丙烯酸甲酯表现出最高的抗压强度,约为纯聚甲基丙烯酸甲酯的两倍,这突出表明这些树脂适合替代汞合金,并可考虑用于牙科修复。研究还发现,当 DPET 含量为 5 wt% 时,混合物的吸水性相对稳定。扫描电子显微镜图像显示,DPET 和 PMMA 之间没有可区分的相位,这突出表明了 DPET 和 PMMA 之间的高度相容性。包括体外细胞毒性在内的生物测试表明,含有 5 wt% DPET 的 PMMA 的细胞存活率平均值高于对照组。有趣的是,在牙科实践中,可靠的体外细胞毒性方法被认为是临床程序中使用牙科填充系统的重要辅助手段。微生物学研究表明,PMMA:5 wt% DPET 对变异链球菌的抑制区高于对照组。根据所得结果,PMMA:5 wt% DPET 的混合物被选为最佳混合物,然后用不同重量百分比的纳米二氧化钛(TiO2)对其进行增强。然后对复合材料进行了压缩、显微硬度和冲击测试。结果表明,二氧化钛对提高所研究复合材料的性能有显著影响。这为牙科用纳米复合材料的合成提供了新的方案。
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引用次数: 0
Eccentric ballistic impact of fiber-metal laminates and aluminum plates supported with different boundary conditions 以不同边界条件支撑的纤维-金属层压板和铝板的偏心弹道冲击力
IF 3.3 4区 材料科学 Q2 MATERIALS SCIENCE, COMPOSITES Pub Date : 2023-12-11 DOI: 10.1177/08927057231221775
C. Kalfountzos, G. Bikakis, E. Theotokoglou
This article investigates the eccentric ballistic impact response of square aluminum and fiber-metal laminated plates with the ANSYS AUTODYN hydrocode. The plates are impacted by a cylindrical projectile with normal high velocity. The validation of the numerical procedure is mainly carried out through comparisons with published experimental data. The modeling procedure and the verification of numerical results are described in detail so as to provide a useful reference. The effect of impact point eccentricity and different boundary conditions on the ballistic resistance of the targets is evaluated. It is found that the ballistic limits of the considered targets can be substantially affected by the boundary conditions and the eccentricity of impact. The targets are sorted in a descending order of ballistic resistance which is found invariant to the impact position.
本文利用 ANSYS AUTODYN 流体代码研究了方形铝板和纤维金属层压板的偏心弹道冲击响应。板材受到高速圆柱形弹丸的冲击。数值程序的验证主要通过与已公布的实验数据进行比较。本文详细介绍了建模过程和数值结果的验证,以便提供有用的参考。评估了撞击点偏心率和不同边界条件对目标弹道阻力的影响。结果发现,所考虑的目标的弹道极限会受到边界条件和撞击偏心的很大影响。按照弹道阻力从大到小的顺序对目标进行排序,发现目标的弹道阻力与撞击位置无关。
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引用次数: 0
期刊
Journal of Thermoplastic Composite Materials
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