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Through-thickness particle distribution, microstructure evolution and tribological performance of B4C/BN-AA6061 composite via friction stir processing 搅拌摩擦加工 B4C/BN-AA6061 复合材料的通厚颗粒分布、微结构演变和摩擦学性能
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-28 DOI: 10.1016/j.wear.2024.205555

In this study, we investigated the interactions between BN and B4C particles in particle reinforced Al matrix composites (PRAMCs) during friction stir processing (FSP), focusing on particle distribution, microstructure evolution, hardness, and wear resistance. PRAMCs were fabricated with BN accounting for 0 wt%, 10 wt%, 20 wt%, 30 wt% and 100 wt% of the reinforcement particles. Optical microscopy (OM) and scanning electron microscopy (SEM) revealed that particle distribution varied through thickness, becoming more inhomogeneous with increasing BN mass ratio. The most uniform distribution was noted 3 mm beneath the surface, particularly in the BN-30%-3 mm sample. This sample also showed improved homogeneity in B4C distribution, as confirmed by the box-counting (BC) method. The refined grain structure due to particle stimulated nucleation (PSN) and Zener pinning contributed to an average hardness of 96.67 HV in the BN-30%-3 mm sample, significantly enhancing wear resistance. The wear rate in this sample was reduced by 97.2 % compared to the FSP-3 mm sample, likely due to finer grains, higher hardness, and increased reinforcement, which collectively reduced adhesion and fatigue wear.

在本研究中,我们研究了颗粒增强铝基复合材料(PRAMCs)中的 BN 和 B4C 颗粒在搅拌摩擦加工(FSP)过程中的相互作用,重点关注颗粒分布、微观结构演变、硬度和耐磨性。在制造 PRAMC 时,BN 分别占增强粒子的 0 wt%、10 wt%、20 wt%、30 wt% 和 100 wt%。光学显微镜(OM)和扫描电子显微镜(SEM)显示,颗粒分布随厚度而变化,随着 BN 质量比的增加而变得更加不均匀。表面下 3 毫米处的分布最为均匀,尤其是在 BN-30%-3 毫米的样品中。盒式计数法(BC)证实,该样品的 B4C 分布的均匀性也有所改善。颗粒刺激成核(PSN)和齐纳引脚使晶粒结构更加细化,从而使 BN-30%-3 mm 样品的平均硬度达到 96.67 HV,显著提高了耐磨性。与 FSP-3 mm 样品相比,该样品的磨损率降低了 97.2%,这可能是由于更细的晶粒、更高的硬度和更强的加固作用共同降低了附着力和疲劳磨损。
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引用次数: 0
Comparative analysis of pin-on-disc and inertia-dynamometer sliding tests on a friction material 摩擦材料上的盘上销和惯性动力计滑动试验对比分析
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-22 DOI: 10.1016/j.wear.2024.205552

The development of modern brake systems requires the assessment of multiple aspects. Among these, parameters related to the tribological behaviour, vibration, and particulate matter emission are typically evaluated using inertia dynamometers and tribometers. While these two testing systems have been previously compared regarding emissions and tribological behaviours, vibrations were not compared, nor have all these aspects been examined simultaneously. This study investigates the scale effects between a pin-on-disc tribometer and a reduced-scale dynamometer operating under dragging conditions with two levels of pressure and velocity, and a disc temperature not exceeding 260 °C. Regarding the vibration, the pin-on-disc exhibited higher and broader values in the normal direction, 1.3–15.5 m/s2, than the reduced-scale dynamometer, 0.37–0.42 m/s2, while the tangential vibrations exceeded those in the normal direction in both systems. The wear rates in the two systems were overall similar, in the range of 1–4 e−14 m2/N. During the tests the disc temperature in the dynamometer increased at a higher rate compared to the pin-on-disc, affecting the tribological and emission behaviours: steady state values were obtained only in the pin-on-disc tests. The particulate concentration values observed during dynamometer tests better correlated with the peak values from pin-on-disc tests rather than with the steady-state values. This study highlights the importance of including transient values in the evaluation of pin-on-disc testing.

现代制动系统的开发需要对多个方面进行评估。其中,与摩擦学行为、振动和微粒物质排放相关的参数通常使用惯性功率计和摩擦计进行评估。虽然这两种测试系统以前在排放和摩擦学行为方面进行过比较,但没有对振动进行过比较,也没有同时对所有这些方面进行过检查。本研究调查了针盘摩擦磨损试验机和缩小比例测功机在拖曳条件下的比例效应,拖曳条件包括两级压力和速度以及不超过 260 °C 的圆盘温度。在振动方面,针盘式摩擦磨损试验机在法线方向的振动值(1.3-15.5 m/s2)比缩小比例测功机的振动值(0.37-0.42 m/s2)更高、更宽,而两个系统的切向振动都超过了法线方向的振动值。两个系统的磨损率总体上相似,都在 1-4 e-14 m2/N 之间。在测试过程中,测功机中的圆盘温度比针盘上的温度上升得更快,从而影响了摩擦学和排放行为:只有在针盘上的测试中才能获得稳定状态值。在测功机测试中观察到的颗粒浓度值与盘上销钉测试的峰值相关性更好,而不是与稳态值相关。这项研究强调了将瞬态值纳入针盘测试评估的重要性。
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引用次数: 0
Influence of structure parameters on the tribological properties of MoB/Cu laminated composites 结构参数对 MoB/Cu 层状复合材料摩擦学特性的影响
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-16 DOI: 10.1016/j.wear.2024.205549

Strong-bonding MoB/Cu laminated (MCL) composites are fabricated by the hot-press method at 1030 °C for 1 h under 20 MPa pressure. The microstructure, tribological properties, and elemental microanalysis are systematically investigated. The structure parameters of laminated composites play a key role in the properties of friction and wear resistance. The average friction coefficient is below 0.3 and the wear rate is almost one order of magnitude lower when the measured ratio of copper thickness to MoB thickness is below 4, compared with the sample whose λ equals 13. The primary phases of MCL are Al2O3, Cu(Al), and MoB. They helped the lubricating film to form on the worn surface during the wear process. These tribo-films effectively moderate the wear while safeguarding the metal matrix.

在 20 兆帕压力下,采用热压法在 1030 °C、1 小时内制成了强键合 MoB/Cu 层状 (MCL) 复合材料。系统地研究了复合材料的微观结构、摩擦学性能和元素显微分析。层压复合材料的结构参数对摩擦和耐磨性能起着关键作用。与 λ 等于 13 的样品相比,当测得的铜厚度与 MoB 厚度之比低于 4 时,平均摩擦系数低于 0.3,磨损率几乎降低了一个数量级。MCL 的主要相为 Al2O3、Cu(Al) 和 MoB。它们有助于在磨损过程中在磨损表面形成润滑膜。这些三重膜在保护金属基体的同时,有效地减缓了磨损。
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引用次数: 0
Effect of surface microstructure spacing on the cavitation erosion process of stainless steel 表面微观结构间距对不锈钢气蚀过程的影响
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-15 DOI: 10.1016/j.wear.2024.205542

Fabricating microstructures on the surface is an innovative method to mitigate cavitation erosion (CE), but there are few studies focus on the effects and mechanisms of microstructure spacing on CE performance. This study has prepared a regular dot array-shaped microstructure with different spacings on the surface of samples. The CE experiments were carried out on both the microstructured samples and smooth samples through a magnetostrictive-vibration cavitation facility. Mass loss measurement and microscopic morphology were utilized to reveal CE characteristics. Numerical simulation was used to study the parameters of the flow field. The results clearly show that the microstructure spacing of 0.25 mm, 0.50 mm, and 1.00 mm samples can improve CE resistance. On these microstructured surfaces, the volume fraction of vapor is reduced and the bubbles move away from it. However, when the microstructure spacing enlarges to 1.50 mm, the damage inside the microstructure groove increases, which will reduce the CE resistance of the materials. As the spacing increases, the volume fraction of vapor on the sample surfaces will increase, and the bubbles in the microstructure groove will congregate, resulting in increasing damage. The research provides the dimensional basis for designing cavitation-resistant surface microstructures.

在样品表面制备微结构是减轻空化侵蚀(CE)的一种创新方法,但很少有研究关注微结构间距对 CE 性能的影响和机制。本研究在样品表面制备了不同间距的规则点阵状微结构。通过磁致伸缩振动空化设备对微结构样品和光滑样品进行了 CE 实验。质量损失测量和显微形态学被用来揭示 CE 特性。数值模拟用于研究流场参数。结果清楚地表明,微结构间距为 0.25 毫米、0.50 毫米和 1.00 毫米的样品可以提高抗 CE 能力。在这些微结构表面上,水蒸气的体积分数降低,气泡会远离它。然而,当微结构间距增大到 1.50 毫米时,微结构凹槽内的损伤会增加,从而降低材料的抗 CE 能力。随着间距的增大,样品表面水蒸气的体积分数会增加,微结构凹槽中的气泡会聚集,导致损伤加剧。该研究为设计抗气蚀表面微结构提供了尺寸依据。
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引用次数: 0
Effects of excitation parameters on fretting wear and corrosion of 316L stainless steel under random impact-sliding condition 激励参数对随机冲击-滑动条件下 316L 不锈钢摩擦磨损和腐蚀的影响
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.wear.2024.205541

In heat exchanger applications, the random vibration due to fluid excitation can cause mechanical wear between tubes and supports. In corrosive environments, the synergy between wear and corrosion can make wear more severe. Therefore, this paper focused on the effects of excitation amplitude and excitation force ratio (drag force/lift force) on fretting wear and corrosion of 316L stainless steel under random impact-sliding conditions. The results showed that as the excitation parameters increased, the friction coefficient and total wear amount would increase, the open circuit potential (OCP) decreased and the polarization curve self-corrosion potential shifted negatively. All synergistic coefficients in this paper were greater than 1, indicating that there was an obvious positive synergy between wear and corrosion. In the fretting wear and corrosion process, pure wear always played a dominant role. Under impact-sliding conditions, as the excitation force increased, the rate of wear-promoted corrosion increased from 3.0 × 10−7 to 2.0 × 10−6 g/h, an increase of 6.67 times. However, the rate of corrosion-promoted wear decreased from 1.1 × 10−6 to 2.0 × 10−7 g/h, a decrease of 5.5 times, showing a certain self-limiting property. The total synergy rose slowly with the increase of excitation parameters. The wear mechanism of materials under impact is characterized by adhesive wear, while under impact-sliding conditions, the wear mechanism involves abrasive wear and corrosion wear.

在热交换器应用中,流体激振引起的随机振动会造成管子和支架之间的机械磨损。在腐蚀环境中,磨损和腐蚀之间的协同作用会使磨损更加严重。因此,本文重点研究了在随机冲击滑动条件下,激振振幅和激振力比(阻力/提升力)对 316L 不锈钢的摩擦磨损和腐蚀的影响。结果表明,随着激振参数的增加,摩擦系数和总磨损量增加,开路电位(OCP)降低,极化曲线自腐蚀电位负移。本文中所有的协同系数都大于 1,表明磨损和腐蚀之间存在明显的正协同作用。在摩擦磨损和腐蚀过程中,纯磨损始终起主导作用。在冲击滑动条件下,随着激振力的增加,磨损促进腐蚀的速率从 3.0 × 10-7 g/h 增加到 2.0 × 10-6 g/h,增加了 6.67 倍。然而,腐蚀促进磨损的速率却从 1.1 × 10-6 g/h 降至 2.0 × 10-7 g/h,下降了 5.5 倍,显示出一定的自限制特性。随着激励参数的增加,总协同效应缓慢上升。材料在冲击条件下的磨损机理以粘着磨损为特征,而在冲击-滑动条件下,磨损机理涉及磨料磨损和腐蚀磨损。
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引用次数: 0
The effect of grits interference on materials removal mechanism during scratching process of silicon carbide 碳化硅划痕过程中砂粒干涉对材料去除机理的影响
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.wear.2024.205527

Silicon carbide (SiC) as a difficult-to-process material is hard to achieve ductile grinding completely, and is likely to occur brittle breakage with low processing efficiency, leading to its low performance, therefore, it is necessary to study its removal mechanism to improve the processing quality. The removal mechanism of single grit cutting is well understood. In the real processing of SiC, there are multiple grits at different positions to remove the materials simultaneously, but the phenomenon of materials removal by multiple grits cannot be observed separately. In order to clarify the interference behavior of neighbored grits, current study conducted a neighbored scratch experiment under varied force in sequence. The experiment evidently revealed the deformation, pits, fracture morphology and removal modes under different interference conditions. Since in-situ monitor of materials removal is unable to be realized, a numerical model with different scratch intervals by coupling the smoothed particle hydrodynamics (SPH) and finite element method (FEM) was used to understand the material damage and stress distribution. Based on the observation from experimental and SPH-FEM results, a theoretical model of neighbored scratch stress field is established to explain the mechanism from plastic and fracture mechanics. From the model, the size of the plastic zone and the interval between the neighbored plastic zone are critical to control the interference mode. The interference mode affects the distribution of stress field and realizes the enhancement effect of material removal. Therefore, the materials removal model could be adopted to control the grinding efficiency and quality in industry.

碳化硅(SiC)作为一种难加工材料,很难完全实现韧性磨削,容易发生脆性断裂,加工效率低,导致其性能低下,因此有必要对其去除机理进行研究,以提高加工质量。单砂粒切削的去除机理已为人们所熟知。在 SiC 的实际加工过程中,不同位置有多个磨粒同时去除材料,但无法分别观察多个磨粒去除材料的现象。为了弄清相邻磨粒的干涉行为,本研究依次进行了不同作用力下的相邻划痕实验。实验明显揭示了不同干涉条件下的变形、凹坑、断口形态和去除模式。由于无法实现材料去除的原位监测,因此采用平滑粒子流体力学(SPH)和有限元法(FEM)耦合建立了不同划痕间隔的数值模型,以了解材料的损伤和应力分布。根据实验和 SPH-FEM 的观察结果,建立了邻近划痕应力场的理论模型,从塑性力学和断裂力学的角度解释了其机理。根据该模型,塑性区的大小和相邻塑性区之间的间隔是控制干涉模式的关键。干涉模式影响应力场的分布,实现材料去除的增强效应。因此,该材料去除模型可用于控制工业中的研磨效率和质量。
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引用次数: 0
Investigation of the tribological behaviors for 4H–SiC substrate under different lubrication conditions 不同润滑条件下 4H-SiC 衬底的摩擦学行为研究
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.wear.2024.205537

Lubrication conditions are an important factor affecting both the machining efficiency and quality of 4H–SiC. To investigate the tribological behaviors under different lubrication conditions, a series of scratching experiments are conducted under different loads and environments. The X-ray photoelectron spectroscopy (XPS) surveys and atomistic simulations are used to explain the different tribological behaviors. Both experimental and simulation results show that liquid lubrication can significantly reduce the coefficient of friction (COF) and minimize structural damage. Compared to pure water, the H2O2 solution is more conducive to the oxidation of SiC atoms and the modification of tribological behaviors. However, the difference in tribological behaviors between H2O2 solution and pure water diminishes as the load increases. The XPS surveys show that the liquids lead to higher-order oxidized species of SiC atoms, such as Si4C4-xO2 and Si-Ox-Cy, which are also observed in the simulation results. It is shown that the oxidized species can reduce the direct bonding between SiC and diamond indenter, which is an important reason for the lower COFs in the liquids. Since the liquids can reduce the direct bonding and mechanical interaction between 4H–SiC and diamond, the material removal rate is much lower under lubrication conditions.

润滑条件是影响 4H-SiC 加工效率和质量的重要因素。为了研究不同润滑条件下的摩擦学行为,我们在不同载荷和环境下进行了一系列划痕实验。X 射线光电子能谱(XPS)调查和原子模拟用于解释不同的摩擦学行为。实验和模拟结果都表明,液体润滑能显著降低摩擦系数(COF),并将结构损伤降至最低。与纯水相比,H2O2 溶液更有利于 SiC 原子的氧化和摩擦学行为的改变。然而,随着载荷的增加,H2O2 溶液与纯水在摩擦学行为上的差异会逐渐减小。XPS 勘测表明,液体会导致 SiC 原子的高阶氧化物种,如 Si4C4-xO2 和 Si-Ox-Cy,模拟结果中也观察到了这些氧化物种。结果表明,氧化物会减少 SiC 与金刚石压头之间的直接结合,这是液体中 COF 值较低的一个重要原因。由于液体可以减少 4H-SiC 与金刚石之间的直接结合和机械相互作用,因此在润滑条件下材料去除率会大大降低。
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引用次数: 0
A comprehensive sliding wear prediction method for planetary roller screw mechanism 行星滚柱丝杠机构的综合滑动磨损预测方法
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.wear.2024.205536

The thread-pairs wear has a significant role in the transmission accuracy, operational stability and service life of planetary roller screw mechanism (PRSM). Nevertheless, the previous literatures still lack the investigation on the wear evolution of roller, nut and screw. Hence, an accumulative wear depth (AWD) prediction model is proposed for PRSM with reciprocating motion. The presented model is validated by the measured wear phenomena of thread pairs and the experimental results in the literature. The equivalent sliding wear experiment of PRSM is designed and the sliding wear coefficient of PRSM material is obtained by the equivalent sliding wear experiment. Considering the thread profile error caused by AWD of roller, nut and screw, the load distribution (LD) and sliding velocities on screw-roller (SR) and nut-roller (NR) sides are calculated. More importantly, the interactions between the AWD, LD and sliding velocity are investigated. Furthermore, the effects of axial load on the AWD, sliding velocities in contact regions and load distribution coefficient are analyzed.

螺纹对磨损对行星滚柱丝杠机构(PRSM)的传动精度、运行稳定性和使用寿命具有重要影响。然而,以往的文献仍缺乏对滚子、螺母和螺杆磨损演变的研究。因此,本文针对往复运动的行星滚柱丝杠机构提出了累积磨损深度(AWD)预测模型。通过测量螺纹对的磨损现象和文献中的实验结果,对所提出的模型进行了验证。设计了 PRSM 的等效滑动磨损实验,并通过等效滑动磨损实验获得了 PRSM 材料的滑动磨损系数。考虑到滚子、螺母和螺杆的 AWD 导致的螺纹轮廓误差,计算了螺杆-滚子(SR)和螺母-滚子(NR)两侧的载荷分布(LD)和滑动速度。更重要的是,研究了 AWD、LD 和滑动速度之间的相互作用。此外,还分析了轴向载荷对 AWD、接触区域滑动速度和载荷分布系数的影响。
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引用次数: 0
The braking performance and failure mechanism of copper-based brake pads during repeated emergency braking at 400 km/h 时速 400 公里反复紧急制动时铜基刹车片的制动性能和失效机理
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.wear.2024.205532
Copper-based brake pads have played a pivotal role in the braking systems of commercial high-speed trains travelling at speeds ranging from 200 to 350 km/h. In this study, the braking performance and friction and wear mechanism of copper-based brake pads at 400 km/h were further evaluated using a full-scale dynamometer. The results show that under repeated emergency braking conditions at 400 km/h, the mean friction coefficient can be maintained at about 0.3 and remains stable within six braking cycles. Subsequently, a fade phenomenon in the mean friction coefficient emerges accompanied by a significant increase in braking distance, while the mean wear loss is relatively high throughout the entire testing process. Microstructural characteristics of the friction film and matrix indicate that strong oxidation plays an important role in the failure process of the brake pads. The friction film primarily composed of oxides exhibits numerous defects, which are susceptible to peeling off during braking, thereby compromising wear resistance. Additionally, as the braking cycles accumulate, oxidation gradually invades and weakens the matrix, leading to violent migration of the copper-rich friction film across the friction interfaces and resulting in the deterioration of friction performance. This work provides valuable insights into the failure behavior of copper-based brake pads at higher braking speeds and can provide potential direction for further improving their performance.
铜基制动片在时速 200 至 350 公里的商用高速列车制动系统中发挥着举足轻重的作用。在这项研究中,使用全尺寸测功机进一步评估了铜基刹车片在 400 km/h 下的制动性能和摩擦磨损机理。结果表明,在时速 400 公里的反复紧急制动条件下,平均摩擦系数可保持在 0.3 左右,并在六个制动周期内保持稳定。随后,伴随着制动距离的显著增加,平均摩擦系数出现衰减现象,而在整个测试过程中,平均磨损损耗相对较高。摩擦膜和基体的微观结构特征表明,强氧化在刹车片的失效过程中起着重要作用。主要由氧化物组成的摩擦膜存在大量缺陷,在制动过程中容易剥落,从而影响耐磨性。此外,随着制动周期的累积,氧化物会逐渐侵入并削弱基体,导致富铜摩擦膜在摩擦界面上剧烈迁移,从而导致摩擦性能下降。这项研究对铜基刹车片在较高制动速度下的失效行为提供了宝贵的见解,并为进一步提高其性能提供了潜在的方向。
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引用次数: 0
Wear performance of ZrO2 reinforced stellite 6 matrix coatings prepared by laser cladding at elevated temperature 高温下激光熔覆制备的 ZrO2 增强人造卫星 6 基体涂层的磨损性能
IF 5.3 1区 工程技术 Q1 ENGINEERING, MECHANICAL Pub Date : 2024-08-10 DOI: 10.1016/j.wear.2024.205539

In order to modify the wear resistance of Stellite 6 superalloy as wear resistant coating at room temperature-1000 °C, the different contents (1.0, 2.5 and 4.0 wt%) of ZrO2 reinforced Stellite 6 matrix coatings were fabricated over the Inconel 718 nickel alloy substrate by laser cladding technology. The microstructure, hardness and high-temperature wear behavior of Stellite 6 matrix coatings with ZrO2 was systematically studied. The sliding wear test were done using a ball-on-disk tribometer against Si3N4 at room temperature-1000 °C. The results showed that the ZrO2 showed obvious fine-grain strengthening and dispersion strengthening effect. The hardness of coatings reinforced by ZrO2 were 470–540 Hv. A critical valve of ZrO2 content was existed for the wear performance of Stellite 6 matrix coatings. The coating with 2.5 wt% ZrO2 had the desirable wear resistance, and the wear rate was in the order of 10−5 mm3/N.m. This was attributed to the high microhardness and the formation of solid lubricants, as well as the friction film on the sliding surfaces.

为了改变Stellite 6超合金作为耐磨涂层在室温-1000 °C条件下的耐磨性,采用激光熔覆技术在Inconel 718镍合金基体上制作了不同含量(1.0、2.5和4.0 wt%)的ZrO2增强Stellite 6基体涂层。对含有 ZrO2 的 Stellite 6 基体涂层的微观结构、硬度和高温磨损行为进行了系统研究。在室温-1000 °C条件下,使用盘上球摩擦磨损测试仪对Si3N4进行了滑动磨损测试。结果表明,ZrO2 具有明显的细晶粒强化和分散强化效果。ZrO2 增强涂层的硬度为 470-540 Hv。ZrO2 含量对 Stellite 6 基体涂层的磨损性能存在临界值。ZrO2 含量为 2.5 wt% 的涂层具有理想的耐磨性,磨损率约为 10-5 mm3/N.m,这归因于高微硬度、固体润滑剂的形成以及滑动表面摩擦膜的形成。
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引用次数: 0
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